#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2010998.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010998_Fobs loop_ _publ_author_name 'Marcus, Sebastian T.' 'Gahan, Lawrence R.' 'Bernhardt, Paul V.' _publ_section_title ; The Ni^II^, Hg^II^ and Cu^II^ complexes of 12-membered-ring mixed-donor macrocycles ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 655 _journal_page_last 658 _journal_volume 56 _journal_year 2000 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 95.627 _cell_angle_beta 112.107 _cell_angle_gamma 99.509 _cell_length_a 8.6167 _cell_length_b 9.3975 _cell_length_c 10.1180 _exptl_crystal_F_000 394.00 _reflns_d_resolution_high 0.8419 _[local]_cod_data_source_file fg1589IIIsup4.hkl _[local]_cod_data_source_block III #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1238LG34 (C8 H21 Cu N3 O2).(NO3)2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 134.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 400.04 400.71 3.47 o 2 0 0 33.78 23.01 0.85 o 3 0 0 3518.11 3399.06 18.67 o 4 0 0 562.99 555.56 5.41 o 5 0 0 2132.21 2088.71 18.79 o 6 0 0 20.08 18.85 1.41 o 7 0 0 125.89 128.64 3.28 o 8 0 0 5.97 8.09 1.34 o 9 0 0 85.73 89.24 3.61 o -9 1 0 207.15 208.88 5.08 o -8 1 0 68.86 68.72 2.81 o -7 1 0 7.20 6.52 1.15 o -6 1 0 659.14 635.58 6.17 o -5 1 0 774.24 794.64 7.91 o -4 1 0 2165.57 2120.37 16.56 o -3 1 0 34.98 42.16 1.15 o -2 1 0 1976.03 2020.38 11.96 o -1 1 0 5195.50 5177.29 50.94 o 0 1 0 2442.04 2712.82 79.80 o 1 1 0 6950.94 7557.67 71.92 o 2 1 0 1223.54 1305.83 9.78 o 3 1 0 6966.93 7348.73 30.86 o 4 1 0 2.94 -1.44 1.53 o 5 1 0 658.43 673.76 7.10 o 6 1 0 793.21 792.71 8.08 o 7 1 0 344.58 334.74 5.20 o 8 1 0 322.56 328.46 5.61 o 9 1 0 25.68 25.31 2.26 o -9 2 0 50.50 48.58 2.80 o -8 2 0 163.88 155.89 3.87 o -7 2 0 248.47 252.84 4.40 o -6 2 0 56.73 52.74 2.04 o -5 2 0 260.76 240.27 3.55 o -4 2 0 76.78 82.85 1.97 o -3 2 0 1632.57 1609.53 13.88 o -2 2 0 6015.61 6110.01 28.33 o -1 2 0 108.00 98.62 1.47 o 0 2 0 7152.26 7757.59 96.88 o 1 2 0 4077.28 4613.76 19.58 o 2 2 0 208.70 181.64 2.15 o 3 2 0 723.62 793.61 8.40 o 4 2 0 1960.04 2045.33 18.05 o 5 2 0 20.99 17.58 1.40 o 6 2 0 726.50 741.24 7.63 o 7 2 0 340.45 349.61 5.52 o 8 2 0 10.30 9.00 1.68 o -9 3 0 444.95 433.28 7.36 o -8 3 0 34.56 28.98 2.16 o -7 3 0 258.91 243.78 4.41 o -6 3 0 705.46 682.97 6.81 o -5 3 0 1490.00 1509.92 15.01 o -4 3 0 759.64 827.10 8.40 o -3 3 0 17.50 29.40 1.43 o -2 3 0 1045.84 1112.24 10.00 o -1 3 0 3.23 3.80 0.70 o 0 3 0 1038.31 1050.70 19.13 o 1 3 0 176.56 197.91 2.28 o 2 3 0 128.71 178.85 2.52 o 3 3 0 1456.30 1468.74 12.68 o 4 3 0 335.96 337.05 4.25 o 5 3 0 380.57 379.60 4.94 o 6 3 0 21.32 18.11 1.61 o 7 3 0 164.11 170.38 4.12 o 8 3 0 116.75 114.24 4.02 o -9 4 0 96.79 98.82 3.77 o -8 4 0 275.71 263.52 5.41 o -7 4 0 56.93 50.63 2.38 o -6 4 0 1170.20 1220.77 11.89 o -5 4 0 56.81 68.82 2.40 o -4 4 0 2296.49 2350.23 22.74 o -3 4 0 3774.40 3900.66 27.53 o -2 4 0 930.21 958.59 10.04 o -1 4 0 3117.80 3306.66 21.00 o 0 4 0 89.37 95.19 2.34 o 1 4 0 1172.42 1173.20 10.59 o 2 4 0 93.53 81.71 1.98 o 3 4 0 6.84 10.79 1.14 o 4 4 0 631.09 608.25 6.11 o 5 4 0 277.04 293.61 4.63 o 6 4 0 403.68 413.92 6.02 o 7 4 0 134.67 131.01 3.86 o -9 5 0 0.70 1.44 3.02 o -8 5 0 248.79 269.00 5.68 o -7 5 0 127.75 138.52 3.96 o -6 5 0 182.75 182.96 4.28 o -5 5 0 2735.62 2881.92 28.79 o -4 5 0 17.70 23.27 1.68 o -3 5 0 851.21 818.27 8.30 o -2 5 0 1997.80 2079.69 19.06 o -1 5 0 510.17 489.32 4.94 o 0 5 0 1221.59 1234.20 8.45 o 1 5 0 1297.91 1387.53 13.02 o 2 5 0 451.59 432.72 4.85 o 3 5 0 135.88 133.29 2.98 o 4 5 0 562.86 587.73 6.45 o 5 5 0 255.52 251.19 4.58 o 6 5 0 147.50 138.74 3.81 o 7 5 0 218.76 231.70 5.40 o -8 6 0 14.60 23.73 2.36 o -7 6 0 102.82 109.15 3.76 o -6 6 0 148.49 155.58 4.09 o -5 6 0 402.89 427.00 6.23 o -4 6 0 169.31 176.49 3.84 o -3 6 0 0.66 3.60 2.13 o -2 6 0 1046.26 1033.32 10.24 o -1 6 0 247.58 271.11 3.94 o 0 6 0 518.92 500.70 6.07 o 1 6 0 722.72 720.92 7.02 o 2 6 0 1128.22 1125.93 11.19 o 3 6 0 574.27 551.92 6.33 o 4 6 0 101.50 107.11 3.14 o 5 6 0 514.28 504.45 6.92 o 6 6 0 124.20 124.95 4.03 o -8 7 0 96.26 104.89 4.40 o -7 7 0 0.54 0.00 3.50 o -6 7 0 152.35 156.53 4.38 o -5 7 0 100.68 110.50 3.54 o -4 7 0 246.51 256.52 4.88 o -3 7 0 158.13 151.37 3.64 o -2 7 0 365.22 402.41 5.37 o -1 7 0 234.76 237.85 4.11 o 0 7 0 10.20 10.01 0.92 o 1 7 0 734.85 767.71 7.53 o 2 7 0 702.95 699.17 7.44 o 3 7 0 1.45 2.96 2.34 o 4 7 0 110.41 120.16 3.46 o 5 7 0 65.99 65.49 3.17 o -7 8 0 224.71 245.40 6.21 o -6 8 0 15.39 13.07 1.96 o -5 8 0 385.77 387.41 6.56 o -4 8 0 10.06 12.98 1.72 o -3 8 0 44.96 52.07 2.52 o -2 8 0 972.16 994.35 9.69 o -1 8 0 1.12 1.42 2.32 o 0 8 0 125.52 118.38 3.93 o 1 8 0 224.18 245.20 4.69 o 2 8 0 540.69 560.19 7.25 o 3 8 0 214.39 207.51 4.62 o 4 8 0 39.29 43.01 2.65 o -7 9 0 33.63 34.94 3.28 o -6 9 0 335.02 344.05 7.16 o -5 9 0 0.02 1.73 2.79 o -4 9 0 572.36 565.46 7.99 o -3 9 0 41.07 35.42 2.19 o -2 9 0 87.72 83.37 3.08 o -1 9 0 339.07 335.71 5.72 o 0 9 0 240.61 239.67 6.16 o 1 9 0 508.65 522.76 7.45 o 2 9 0 75.23 63.46 2.94 o 3 9 0 137.68 130.11 4.49 o -5 10 0 184.93 184.35 5.47 o -4 10 0 82.70 84.82 3.78 o -3 10 0 116.53 115.55 4.02 o -2 10 0 2.03 6.80 1.56 o -1 10 0 910.22 923.86 10.34 o 0 10 0 35.28 33.57 1.82 o 1 10 0 145.86 147.51 4.61 o 2 10 0 413.78 406.65 7.76 o -3 11 0 93.43 88.21 3.99 o -2 11 0 241.87 225.69 5.88 o -1 11 0 0.03 -2.62 2.88 o 1 -11 1 214.41 195.19 5.59 o 2 -11 1 9.51 2.30 3.76 o 3 -11 1 189.67 204.02 5.92 o -2 -10 1 0.05 -3.59 3.59 o -1 -10 1 225.56 231.38 5.85 o 0 -10 1 207.50 201.27 4.79 o 1 -10 1 166.88 162.18 4.54 o 2 -10 1 131.15 138.05 4.26 o 3 -10 1 30.21 30.56 2.50 o 4 -10 1 256.00 239.34 6.03 o 5 -10 1 46.56 48.00 3.26 o -4 -9 1 69.98 68.61 3.43 o -3 -9 1 72.95 81.59 3.65 o -2 -9 1 24.93 24.94 2.05 o -1 -9 1 23.28 24.71 2.05 o 0 -9 1 383.55 400.65 9.86 o 1 -9 1 52.53 48.68 2.52 o 2 -9 1 111.70 120.50 3.67 o 3 -9 1 52.51 60.05 2.90 o 4 -9 1 51.84 53.78 2.77 o 5 -9 1 383.90 388.04 7.13 o 6 -9 1 36.88 33.03 2.90 o -5 -8 1 175.87 167.93 4.84 o -4 -8 1 109.62 115.65 3.70 o -3 -8 1 25.10 30.21 2.11 o -2 -8 1 38.12 39.46 2.19 o -1 -8 1 11.13 13.73 1.59 o 0 -8 1 126.48 107.31 2.85 o 1 -8 1 219.05 217.43 4.38 o 2 -8 1 121.10 104.42 3.32 o 3 -8 1 486.49 521.45 7.09 o 4 -8 1 348.03 347.51 6.01 o 5 -8 1 2.59 0.64 2.74 o 6 -8 1 366.87 385.15 6.87 o 7 -8 1 3.44 0.00 4.00 o -6 -7 1 21.33 23.23 2.21 o -5 -7 1 518.08 485.64 7.23 o -4 -7 1 85.74 93.84 3.10 o -3 -7 1 592.34 598.37 7.12 o -2 -7 1 50.64 47.85 2.13 o -1 -7 1 48.82 48.69 2.05 o 0 -7 1 458.31 446.57 9.23 o 1 -7 1 13.39 12.61 1.45 o 2 -7 1 557.05 586.91 6.77 o 3 -7 1 18.65 22.26 1.79 o 4 -7 1 263.26 266.70 5.09 o 5 -7 1 181.17 190.49 4.57 o 6 -7 1 3.88 6.19 1.62 o 7 -7 1 269.31 264.63 5.92 o 8 -7 1 29.25 34.01 3.08 o -7 -6 1 310.51 320.36 6.49 o -6 -6 1 143.84 145.01 4.08 o -5 -6 1 30.07 31.65 1.97 o -4 -6 1 1079.13 1107.65 11.22 o -3 -6 1 48.81 49.14 2.08 o -2 -6 1 1256.66 1216.16 11.59 o -1 -6 1 150.13 163.26 3.25 o 0 -6 1 165.76 156.65 5.77 o 1 -6 1 1289.04 1332.78 12.82 o 2 -6 1 183.57 190.60 3.63 o 3 -6 1 341.67 348.72 5.10 o 4 -6 1 4.42 5.22 2.71 o 5 -6 1 301.71 313.41 5.42 o 6 -6 1 17.29 15.56 1.89 o 7 -6 1 140.97 138.58 4.26 o 8 -6 1 89.02 91.51 3.99 o -7 -5 1 20.43 21.79 2.19 o -6 -5 1 162.21 172.37 4.08 o -5 -5 1 190.90 182.06 3.82 o -4 -5 1 437.28 455.21 5.59 o -3 -5 1 886.19 884.22 8.74 o -2 -5 1 190.84 210.13 3.38 o -1 -5 1 1436.51 1329.91 12.96 o 0 -5 1 108.98 95.10 2.88 o 1 -5 1 3853.25 4184.17 27.89 o 2 -5 1 466.99 516.21 5.38 o 3 -5 1 2.19 2.64 2.18 o 4 -5 1 1396.91 1371.66 14.35 o 5 -5 1 87.17 87.87 2.88 o 6 -5 1 201.79 225.97 4.67 o 7 -5 1 4.12 0.00 2.90 o 8 -5 1 56.48 57.40 2.91 o -8 -4 1 22.16 26.18 2.32 o -7 -4 1 293.23 297.09 5.44 o -6 -4 1 13.58 13.12 1.49 o -5 -4 1 360.35 348.12 5.01 o -4 -4 1 125.90 121.25 2.82 o -3 -4 1 12.36 19.28 1.23 o -2 -4 1 532.29 493.88 4.84 o -1 -4 1 431.08 409.62 4.01 o 0 -4 1 4913.04 4940.72 83.82 o 1 -4 1 930.67 991.66 10.24 o 2 -4 1 2653.99 2949.09 22.45 o 3 -4 1 163.76 166.17 3.11 o 4 -4 1 138.87 149.22 3.15 o 5 -4 1 925.36 917.79 9.08 o 6 -4 1 143.82 148.13 3.54 o 7 -4 1 163.14 167.65 4.04 o 8 -4 1 30.61 33.95 2.33 o 9 -4 1 108.44 112.60 4.14 o -8 -3 1 152.77 148.95 4.30 o -7 -3 1 37.00 39.30 2.07 o -6 -3 1 262.94 266.62 4.49 o -5 -3 1 12.48 9.86 1.25 o -4 -3 1 1883.26 1852.08 17.83 o -3 -3 1 83.83 95.12 2.04 o -2 -3 1 272.76 229.87 2.70 o -1 -3 1 790.58 803.57 7.76 o 0 -3 1 247.47 260.98 10.82 o 1 -3 1 18080.44 18110.51 188.51 o 2 -3 1 436.46 435.18 4.39 o 3 -3 1 12.78 9.02 1.05 o 4 -3 1 1130.75 1131.35 10.91 o 5 -3 1 725.60 679.94 6.75 o 6 -3 1 265.35 266.01 4.41 o 7 -3 1 116.32 119.33 3.35 o 8 -3 1 74.82 74.35 2.91 o 9 -3 1 28.22 27.72 2.63 o -9 -2 1 20.27 18.21 2.13 o -8 -2 1 406.32 400.82 6.32 o -7 -2 1 661.93 662.76 7.30 o -6 -2 1 75.87 73.18 2.44 o -5 -2 1 1375.80 1408.40 13.98 o -4 -2 1 2146.98 2322.32 18.73 o -3 -2 1 3026.80 3194.01 19.97 o -2 -2 1 688.34 724.43 6.93 o -1 -2 1 1679.57 1731.52 11.61 o 0 -2 1 1429.33 1523.47 7.70 o 1 -2 1 504.49 642.83 6.45 o 2 -2 1 1623.11 1608.33 12.76 o 3 -2 1 40.57 25.85 1.09 o 4 -2 1 299.31 256.09 3.38 o 5 -2 1 95.45 98.89 2.49 o 6 -2 1 757.45 747.78 7.44 o 7 -2 1 276.84 274.20 4.75 o 8 -2 1 107.87 112.11 3.50 o 9 -2 1 119.42 119.36 4.20 o -9 -1 1 161.04 161.18 4.48 o -8 -1 1 0.23 -0.26 2.23 o -7 -1 1 474.99 470.18 5.94 o -6 -1 1 298.75 297.03 4.34 o -5 -1 1 906.58 920.19 9.48 o -4 -1 1 1548.93 1609.11 14.48 o -3 -1 1 1881.22 2006.83 14.23 o -2 -1 1 1307.59 1317.32 9.67 o -1 -1 1 4678.61 4553.85 46.40 o 0 -1 1 5027.06 5183.28 48.77 o 1 -1 1 2237.99 2284.00 11.65 o 2 -1 1 4359.03 4468.59 20.14 o 3 -1 1 14.21 22.03 0.95 o 4 -1 1 92.18 100.06 2.14 o 5 -1 1 871.57 832.50 8.58 o 6 -1 1 19.81 20.51 1.50 o 7 -1 1 69.84 71.74 2.57 o 8 -1 1 55.33 55.42 2.55 o 9 -1 1 50.09 52.69 3.04 o -9 0 1 375.28 384.30 6.69 o -8 0 1 318.41 287.62 5.03 o -7 0 1 91.36 86.27 2.71 o -6 0 1 24.06 17.77 1.34 o -5 0 1 4.93 1.87 1.40 o -4 0 1 6457.42 6614.93 30.53 o -3 0 1 381.89 374.53 3.68 o -2 0 1 44.28 44.96 0.98 o -1 0 1 3927.04 3229.89 13.40 o 0 0 1 662.90 699.03 30.04 o 1 0 1 3153.71 2922.43 28.53 o 2 0 1 222.20 228.36 2.25 o 3 0 1 10.48 4.95 0.67 o 4 0 1 146.79 156.55 2.57 o 5 0 1 778.85 792.30 7.79 o 6 0 1 254.28 261.23 4.30 o 7 0 1 10.66 7.42 1.44 o 8 0 1 45.10 49.02 2.57 o -9 1 1 49.02 44.46 2.73 o -8 1 1 168.25 165.13 3.81 o -7 1 1 108.24 111.47 2.98 o -6 1 1 10.91 10.96 1.13 o -5 1 1 956.59 916.45 9.10 o -4 1 1 29.96 24.08 1.14 o -3 1 1 485.57 482.94 4.63 o -2 1 1 404.34 448.91 4.66 o -1 1 1 1753.60 1694.07 8.64 o 0 1 1 3553.93 3659.68 111.58 o 1 1 1 85.19 72.89 1.17 o 2 1 1 867.20 860.32 8.55 o 3 1 1 80.29 84.44 1.79 o 4 1 1 733.23 714.00 7.34 o 5 1 1 236.20 230.56 3.66 o 6 1 1 294.99 315.97 4.73 o 7 1 1 220.15 224.99 4.42 o 8 1 1 17.14 20.93 2.03 o -9 2 1 428.12 433.79 6.98 o -8 2 1 1.34 1.68 2.22 o -7 2 1 502.80 504.37 5.96 o -6 2 1 308.61 277.20 4.12 o -5 2 1 761.36 737.04 7.19 o -4 2 1 2181.96 2260.43 18.50 o -3 2 1 131.64 128.69 2.24 o -2 2 1 493.30 470.41 4.83 o -1 2 1 7105.56 7231.03 70.68 o 0 2 1 1446.30 1518.16 10.85 o 1 2 1 123.84 134.48 1.74 o 2 2 1 1627.83 1741.98 13.65 o 3 2 1 1072.64 1035.29 10.19 o 4 2 1 22.19 27.82 1.40 o 5 2 1 838.38 848.09 8.17 o 6 2 1 63.71 65.72 2.46 o 7 2 1 370.16 394.44 6.04 o 8 2 1 128.76 140.71 4.26 o -9 3 1 68.09 75.73 3.31 o -8 3 1 355.89 363.45 5.72 o -7 3 1 0.17 -1.77 2.53 o -6 3 1 1105.50 1064.74 10.33 o -5 3 1 351.93 345.92 4.75 o -4 3 1 1163.66 1202.92 11.57 o -3 3 1 60.79 39.05 1.45 o -2 3 1 146.98 162.19 2.17 o -1 3 1 1160.28 1183.60 10.21 o 0 3 1 117.21 101.25 1.16 o 1 3 1 1024.13 1085.99 10.73 o 2 3 1 769.37 791.04 7.74 o 3 3 1 177.29 173.00 2.86 o 4 3 1 555.77 551.89 5.60 o 5 3 1 3.71 1.99 2.05 o 6 3 1 553.81 535.13 6.70 o 7 3 1 44.99 44.83 2.37 o -9 4 1 7.57 3.81 3.47 o -8 4 1 193.73 188.42 4.51 o -7 4 1 112.06 118.70 3.49 o -6 4 1 5.42 10.57 1.56 o -5 4 1 2868.43 2937.47 27.56 o -4 4 1 9.28 10.50 1.29 o -3 4 1 1797.98 1866.22 17.19 o -2 4 1 1888.19 1943.81 15.98 o -1 4 1 1042.82 1186.52 10.24 o 0 4 1 941.78 933.09 13.37 o 1 4 1 95.16 107.32 2.14 o 2 4 1 618.13 628.30 6.44 o 3 4 1 907.76 918.17 9.21 o 4 4 1 9.61 6.82 1.15 o 5 4 1 45.23 49.29 2.17 o 6 4 1 22.39 21.88 1.89 o 7 4 1 142.22 141.93 4.32 o -9 5 1 34.78 44.41 2.98 o -8 5 1 10.59 17.17 2.10 o -7 5 1 36.47 44.78 2.50 o -6 5 1 745.28 804.42 8.64 o -5 5 1 0.69 0.23 2.72 o -4 5 1 870.32 870.39 8.41 o -3 5 1 17.00 16.23 1.27 o -2 5 1 1052.52 1034.60 9.91 o -1 5 1 1192.79 1197.36 11.61 o 0 5 1 364.14 368.46 10.66 o 1 5 1 886.76 878.52 8.60 o 2 5 1 0.23 0.10 0.97 o 3 5 1 1112.75 1062.67 10.84 o 4 5 1 122.76 128.21 3.27 o 5 5 1 55.27 55.59 2.50 o 6 5 1 138.28 143.30 3.93 o -9 6 1 2.57 6.00 3.17 o -8 6 1 79.22 84.67 3.56 o -7 6 1 0.88 2.59 3.83 o -6 6 1 45.14 53.46 2.74 o -5 6 1 1019.00 1049.74 10.66 o -4 6 1 16.27 9.02 1.60 o -3 6 1 841.00 861.50 8.83 o -2 6 1 1.42 1.01 1.55 o -1 6 1 542.37 522.85 5.43 o 0 6 1 451.52 454.69 5.37 o 1 6 1 1435.93 1482.92 15.14 o 2 6 1 1136.39 1131.49 11.35 o 3 6 1 9.39 12.87 1.44 o 4 6 1 531.47 515.82 6.65 o 5 6 1 15.47 16.74 1.90 o 6 6 1 71.18 78.48 3.38 o -8 7 1 0.09 -0.39 3.24 o -7 7 1 199.27 208.74 5.21 o -6 7 1 340.11 355.07 6.30 o -5 7 1 2.66 2.46 2.63 o -4 7 1 5.51 9.55 1.37 o -3 7 1 227.72 232.94 4.19 o -2 7 1 951.29 939.13 9.69 o -1 7 1 0.96 0.59 1.97 o 0 7 1 1437.73 1451.12 10.66 o 1 7 1 1.18 3.89 2.24 o 2 7 1 552.52 537.65 6.62 o 3 7 1 852.80 813.26 8.49 o 4 7 1 181.32 186.88 4.42 o 5 7 1 142.78 143.32 4.51 o -8 8 1 132.43 136.71 4.94 o -7 8 1 24.02 26.01 2.49 o -6 8 1 487.34 518.68 7.90 o -5 8 1 5.99 3.31 2.84 o -4 8 1 133.06 131.66 3.70 o -3 8 1 250.02 252.42 4.74 o -2 8 1 141.95 138.00 3.60 o -1 8 1 346.64 315.52 5.10 o 0 8 1 61.45 64.68 1.85 o 1 8 1 445.75 409.28 6.10 o 2 8 1 72.99 76.80 2.89 o 3 8 1 134.08 136.08 3.96 o 4 8 1 8.51 7.65 1.64 o -7 9 1 254.76 270.59 6.81 o -6 9 1 7.62 10.17 1.92 o -5 9 1 352.87 360.19 6.57 o -4 9 1 31.67 27.39 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152.75 4.77 o -7 0 9 221.85 225.21 4.92 o -6 0 9 602.65 561.98 7.33 o -5 0 9 64.88 65.31 2.56 o -4 0 9 2.36 -0.72 2.10 o -3 0 9 275.57 272.14 4.80 o -2 0 9 68.96 75.55 2.67 o -1 0 9 273.94 272.82 4.87 o 0 0 9 31.69 34.41 1.47 o 1 0 9 2.40 1.60 2.44 o 2 0 9 269.63 257.66 5.48 o 3 0 9 0.96 1.62 2.49 o -9 1 9 71.81 77.27 3.61 o -8 1 9 16.79 15.62 2.19 o -7 1 9 215.70 222.23 4.79 o -6 1 9 37.98 39.76 2.12 o -5 1 9 76.59 76.81 2.75 o -4 1 9 90.60 85.66 2.88 o -3 1 9 757.37 766.52 7.92 o -2 1 9 155.37 158.46 3.72 o -1 1 9 101.29 104.80 3.12 o 0 1 9 207.87 219.28 3.20 o 1 1 9 9.87 8.87 1.60 o 2 1 9 43.84 45.16 2.60 o -9 2 9 0.94 -3.28 3.28 o -8 2 9 16.99 20.11 2.26 o -7 2 9 0.16 0.56 2.18 o -6 2 9 209.17 202.01 4.34 o -5 2 9 26.33 27.73 1.87 o -4 2 9 66.34 67.86 2.57 o -3 2 9 19.80 15.68 1.66 o -2 2 9 17.93 21.13 1.76 o -1 2 9 157.05 162.95 3.99 o 0 2 9 30.15 28.16 2.43 o 1 2 9 13.23 16.56 1.89 o 2 2 9 8.72 8.70 1.66 o -8 3 9 6.69 2.42 3.00 o -7 3 9 181.89 177.70 4.34 o -6 3 9 49.52 46.53 2.46 o -5 3 9 23.25 27.36 1.86 o -4 3 9 569.11 538.55 6.93 o -3 3 9 320.89 321.83 5.40 o -2 3 9 52.64 46.89 2.38 o -1 3 9 4.60 4.37 2.73 o 0 3 9 51.86 61.66 2.75 o 1 3 9 12.97 16.06 2.03 o -8 4 9 32.53 34.36 2.52 o -7 4 9 229.17 224.15 5.11 o -6 4 9 448.95 452.19 6.78 o -5 4 9 82.86 86.68 3.07 o -4 4 9 184.39 189.38 4.41 o -3 4 9 53.05 61.11 2.62 o -2 4 9 78.66 75.64 2.94 o -1 4 9 183.90 194.31 4.68 o 0 4 9 101.35 99.60 3.56 o -7 5 9 23.23 21.52 2.07 o -6 5 9 399.95 399.72 6.78 o -5 5 9 14.88 18.20 1.86 o -4 5 9 16.70 14.89 1.74 o -3 5 9 433.79 464.49 7.26 o -2 5 9 9.62 7.98 1.86 o -1 5 9 123.31 126.95 4.16 o -6 6 9 0.07 -2.36 2.36 o -5 6 9 173.69 183.85 4.83 o -4 6 9 60.87 67.58 2.95 o -3 6 9 70.25 69.64 3.17 o -2 6 9 18.44 24.26 2.13 o -2 -7 10 0.06 2.88 2.88 o -5 -6 10 109.52 115.37 4.56 o -4 -6 10 52.61 60.74 3.49 o -3 -6 10 100.27 104.85 4.32 o -2 -6 10 114.16 124.44 4.69 o -1 -6 10 24.45 15.43 2.60 o 0 -6 10 206.64 215.44 4.18 o -6 -5 10 322.45 328.81 7.50 o -5 -5 10 94.60 80.82 4.04 o -4 -5 10 65.33 69.95 3.72 o -3 -5 10 17.07 16.68 2.06 o -2 -5 10 328.69 351.75 6.83 o -1 -5 10 161.73 169.45 5.22 o 0 -5 10 10.97 10.67 1.58 o 1 -5 10 88.32 89.17 3.91 o -7 -4 10 100.45 101.75 4.54 o -6 -4 10 288.38 303.03 7.06 o -5 -4 10 71.49 74.88 3.49 o -4 -4 10 164.17 180.81 4.94 o -3 -4 10 324.97 349.33 6.63 o -2 -4 10 1.54 -2.95 2.95 o -1 -4 10 186.49 192.27 4.88 o 0 -4 10 101.30 107.22 2.85 o 1 -4 10 56.82 53.63 3.08 o -7 -3 10 150.31 164.80 5.41 o -6 -3 10 63.95 67.96 3.49 o -5 -3 10 410.09 417.04 7.20 o -4 -3 10 17.97 16.62 1.94 o -3 -3 10 70.45 78.43 3.19 o -2 -3 10 351.82 369.51 6.37 o -1 -3 10 22.71 21.60 2.05 o 0 -3 10 233.50 221.55 5.13 o 1 -3 10 37.61 37.75 2.66 o 2 -3 10 35.49 37.03 2.65 o -8 -2 10 182.96 204.35 6.08 o -7 -2 10 0.51 -1.15 2.73 o -6 -2 10 84.43 90.32 3.56 o -5 -2 10 2.89 4.69 1.50 o -4 -2 10 193.53 185.07 4.61 o -3 -2 10 119.13 125.40 3.69 o -2 -2 10 454.70 463.69 6.95 o -1 -2 10 149.74 147.77 4.08 o 0 -2 10 3.16 3.49 1.64 o 1 -2 10 325.53 321.11 6.36 o 2 -2 10 0.85 2.35 2.21 o -8 -1 10 27.54 27.66 2.81 o -7 -1 10 10.83 13.73 2.05 o -6 -1 10 85.22 78.90 3.21 o -5 -1 10 450.14 425.38 6.64 o -4 -1 10 14.43 14.89 1.69 o -3 -1 10 76.33 81.99 3.04 o -2 -1 10 150.68 144.33 3.97 o -1 -1 10 78.61 78.87 3.04 o 0 -1 10 117.51 119.82 4.09 o 1 -1 10 8.48 12.38 1.53 o -8 0 10 47.13 43.27 2.90 o -7 0 10 283.01 281.36 5.98 o -6 0 10 104.70 110.10 3.57 o -5 0 10 70.66 80.09 3.00 o -4 0 10 46.33 44.62 2.35 o -3 0 10 88.72 85.72 3.06 o -2 0 10 381.14 390.48 6.30 o -1 0 10 13.07 11.71 1.68 o 0 0 10 8.24 7.43 1.43 o 1 0 10 113.92 118.77 3.93 o -8 1 10 201.77 199.46 5.36 o -7 1 10 7.80 5.42 1.73 o -6 1 10 330.95 323.29 5.84 o -5 1 10 234.02 225.93 4.81 o -4 1 10 142.46 146.57 3.84 o -3 1 10 200.74 199.99 4.44 o -2 1 10 6.35 4.40 2.75 o -1 1 10 89.57 92.18 3.24 o 0 1 10 39.91 43.13 1.88 o 1 1 10 137.57 130.95 4.32 o -8 2 10 5.51 9.62 1.79 o -7 2 10 200.83 187.55 5.02 o -6 2 10 2.22 1.72 2.72 o -5 2 10 649.21 627.54 7.77 o -4 2 10 15.57 15.98 1.65 o -3 2 10 149.20 148.15 3.92 o -2 2 10 206.68 197.29 4.53 o -1 2 10 82.50 79.74 3.36 o 0 2 10 172.87 181.82 4.55 o -7 3 10 222.71 213.94 5.24 o -6 3 10 300.93 296.51 6.00 o -5 3 10 0.13 2.08 1.22 o -4 3 10 475.85 473.80 6.93 o -3 3 10 38.00 43.20 2.46 o -2 3 10 164.85 173.44 4.54 o -1 3 10 6.16 8.89 1.54 o 0 3 10 54.53 54.26 2.11 o -7 4 10 61.47 58.54 2.99 o -6 4 10 56.69 60.89 3.02 o -5 4 10 145.35 156.47 4.52 o -4 4 10 29.16 28.16 2.31 o -3 4 10 162.27 169.65 4.67 o -2 4 10 2.03 1.59 2.90 o -5 5 10 66.12 71.61 3.29 o -4 5 10 55.33 60.50 3.04 o -3 5 10 43.78 49.00 2.94 o -4 -5 11 14.58 16.38 2.28 o -3 -5 11 141.36 145.95 5.21 o -2 -5 11 81.51 83.67 4.00 o -5 -4 11 169.71 182.38 5.58 o -4 -4 11 113.81 107.82 4.33 o -3 -4 11 12.22 8.76 2.29 o -2 -4 11 133.59 153.07 4.84 o -1 -4 11 18.27 21.19 2.24 o -6 -3 11 114.05 109.68 4.46 o -5 -3 11 9.17 6.69 2.03 o -4 -3 11 206.23 215.11 5.76 o -3 -3 11 76.39 76.04 3.55 o -2 -3 11 0.57 -2.11 2.87 o -1 -3 11 59.79 70.05 3.48 o 0 -3 11 25.67 25.42 2.00 o -6 -2 11 0.14 -3.43 3.43 o -5 -2 11 203.80 213.77 5.58 o -4 -2 11 170.04 162.00 4.81 o -3 -2 11 97.30 98.59 3.82 o -2 -2 11 46.10 42.37 2.77 o -1 -2 11 31.01 33.12 2.55 o 0 -2 11 57.51 57.65 2.31 o -7 -1 11 53.81 63.75 3.40 o -6 -1 11 187.91 165.73 4.87 o -5 -1 11 0.94 -1.32 2.72 o -4 -1 11 569.86 587.73 8.25 o -3 -1 11 96.13 95.71 3.44 o -2 -1 11 43.56 44.71 2.73 o -1 -1 11 109.06 105.68 3.99 o 0 -1 11 36.18 35.40 1.85 o -7 0 11 24.73 24.91 2.34 o -6 0 11 429.03 427.94 7.46 o -5 0 11 292.78 292.41 6.18 o -4 0 11 3.92 5.95 2.98 o -3 0 11 333.59 349.50 6.60 o -2 0 11 26.57 22.39 2.31 o -1 0 11 201.66 212.60 5.25 o -7 1 11 320.66 323.12 6.71 o -6 1 11 0.08 0.98 2.59 o -5 1 11 123.63 119.03 4.12 o -4 1 11 61.11 65.28 3.16 o -3 1 11 215.33 210.05 5.14 o -2 1 11 47.87 50.26 2.92 o -1 1 11 10.44 9.65 2.00 o -6 2 11 87.39 87.71 3.68 o -5 2 11 10.60 5.33 3.05 o -4 2 11 285.49 298.96 6.09 o -3 2 11 2.02 1.90 2.45 o -2 2 11 76.17 90.06 3.59 o -5 3 11 62.13 73.80 3.28 o -4 3 11 0.13 -2.28 2.62 o -3 3 11 140.27 142.31 4.56 o -4 -1 12 5.67 4.85 1.64 o