#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:21:17 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180779 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/10/2011009.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011009_Fobs loop_ _publ_author_name 'Chiaroni, Ang\`ele' 'Riche, Claude' 'Khuong-Huu, Qui' 'Nguyen-Ngoc, Hanh' 'Nguyen-Viet, Kinh' 'Khuong-Huu, Fran\,coise' _publ_section_title ; New limonoids from Harrisonia perforata (Blanco) Merr. ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 711 _journal_page_last 713 _journal_volume 56 _journal_year 2000 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _exptl_crystal_F_000 552.00 _cod_data_source_file gs1076Dsup3.hkl _cod_data_source_block D #BEGIN Tags that were not found in dictionaries: _shelx_title ' Haperforine D* C27 H34 O10 *P21 ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 101.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 133.65 152.46 1.77 o 2 0 0 255.04 326.98 3.69 o 3 0 0 1499.42 1682.09 62.43 o 4 0 0 575.70 581.08 13.76 o 5 0 0 892.00 1130.64 43.92 o 6 0 0 420.91 596.84 26.42 o 7 0 0 80.68 81.68 5.09 o 8 0 0 122.77 127.91 9.14 o 9 0 0 10.40 10.63 0.95 o 10 0 0 175.63 171.86 18.53 o 11 0 0 0.33 0.21 0.08 o 1 1 0 3535.87 3475.29 123.74 o 2 1 0 2675.29 2864.16 40.80 o 3 1 0 178.95 246.34 3.78 o 4 1 0 290.06 390.07 9.33 o 5 1 0 375.09 481.69 11.45 o 6 1 0 37.62 43.04 1.18 o 7 1 0 292.27 300.36 9.93 o 8 1 0 100.23 101.30 3.87 o 9 1 0 91.83 89.76 9.46 o 10 1 0 32.18 30.23 3.30 o 11 1 0 5.77 6.14 0.83 o 0 2 0 5280.28 4827.30 515.52 o 1 2 0 140.63 197.66 6.74 o 2 2 0 348.03 461.68 24.80 o 3 2 0 340.07 420.30 9.87 o 4 2 0 1166.19 1423.00 28.35 o 5 2 0 27.98 23.03 0.84 o 6 2 0 75.46 78.77 2.32 o 7 2 0 67.01 60.43 2.06 o 8 2 0 182.47 196.73 8.57 o 9 2 0 157.44 164.93 16.06 o 10 2 0 8.96 7.97 1.09 o 11 2 0 38.18 31.31 4.43 o 1 3 0 519.03 631.99 15.28 o 2 3 0 1144.18 1429.64 60.28 o 3 3 0 818.18 1002.19 56.57 o 4 3 0 764.92 996.42 13.48 o 5 3 0 293.67 227.50 6.96 o 6 3 0 209.56 177.97 6.03 o 7 3 0 7.49 9.78 0.37 o 8 3 0 129.73 129.31 5.77 o 9 3 0 14.41 15.79 2.20 o 10 3 0 1.34 2.46 0.12 o 11 3 0 17.93 16.04 1.92 o 0 4 0 160.24 257.41 6.93 o 1 4 0 496.83 654.71 9.45 o 2 4 0 57.33 79.06 2.71 o 3 4 0 40.65 47.32 1.88 o 4 4 0 156.39 215.41 12.27 o 5 4 0 74.69 72.88 1.66 o 6 4 0 43.66 41.40 1.02 o 7 4 0 55.53 53.26 2.26 o 8 4 0 27.38 31.20 1.76 o 9 4 0 90.94 96.85 8.55 o 10 4 0 126.33 121.53 15.29 o 11 4 0 6.76 7.93 0.93 o 1 5 0 143.27 108.46 2.38 o 2 5 0 202.98 248.80 24.12 o 3 5 0 0.87 1.58 0.13 o 4 5 0 334.16 416.94 56.74 o 5 5 0 121.10 163.50 9.65 o 6 5 0 66.94 61.95 2.36 o 7 5 0 361.77 350.95 12.38 o 8 5 0 119.41 113.68 15.09 o 9 5 0 4.69 3.41 0.56 o 10 5 0 7.24 6.38 0.78 o 11 5 0 3.29 3.50 0.37 o 0 6 0 31.27 47.33 0.42 o 1 6 0 21.98 20.20 0.34 o 2 6 0 447.57 576.91 10.41 o 3 6 0 5.68 9.36 0.24 o 4 6 0 32.83 35.89 1.80 o 5 6 0 58.25 61.51 3.18 o 6 6 0 8.44 10.55 0.44 o 7 6 0 7.59 8.30 0.73 o 8 6 0 124.89 121.29 13.61 o 9 6 0 29.78 27.02 4.16 o 10 6 0 24.88 24.03 3.89 o 1 7 0 23.25 28.18 0.34 o 2 7 0 147.59 190.19 6.07 o 3 7 0 34.56 39.38 0.61 o 4 7 0 0.74 1.27 0.18 o 5 7 0 98.43 96.42 3.54 o 6 7 0 113.42 115.89 7.85 o 7 7 0 95.32 100.84 14.46 o 8 7 0 25.27 26.36 3.65 o 9 7 0 0.72 0.70 0.09 o 10 7 0 2.14 2.19 0.46 o 0 8 0 457.23 531.35 106.14 o 1 8 0 15.44 22.07 3.33 o 2 8 0 243.60 231.03 4.59 o 3 8 0 15.33 18.74 0.31 o 4 8 0 140.23 160.52 4.93 o 5 8 0 9.11 9.74 0.34 o 6 8 0 146.29 146.80 16.40 o 7 8 0 25.25 25.45 1.84 o 8 8 0 4.66 4.77 0.81 o 9 8 0 2.67 3.16 0.37 o 1 9 0 168.76 157.27 1.91 o 2 9 0 38.08 32.64 0.91 o 3 9 0 97.36 89.34 1.84 o 4 9 0 19.88 18.66 0.68 o 5 9 0 62.88 61.21 4.86 o 6 9 0 14.47 16.29 1.69 o 7 9 0 13.02 14.57 1.93 o 8 9 0 0.24 0.13 0.08 o 0 10 0 275.46 290.82 3.22 o 1 10 0 34.54 38.70 0.55 o 2 10 0 10.92 13.18 0.56 o 3 10 0 5.46 6.55 0.52 o 4 10 0 128.04 139.01 9.79 o 5 10 0 17.19 14.43 1.44 o 6 10 0 23.08 25.30 2.29 o 7 10 0 10.40 10.62 1.39 o 1 11 0 21.73 24.04 0.59 o 2 11 0 47.11 51.67 1.55 o 3 11 0 1.63 2.11 0.27 o 4 11 0 37.45 40.03 2.38 o 5 11 0 11.82 11.75 1.15 o 6 11 0 11.99 10.59 0.64 o 0 12 0 107.09 112.74 1.39 o 1 12 0 15.05 13.70 0.23 o 2 12 0 15.42 15.62 0.71 o 3 12 0 9.61 11.69 0.20 o 4 12 0 0.94 1.36 0.09 o 5 12 0 4.61 4.88 0.42 o 1 13 0 10.59 9.59 0.16 o 2 13 0 2.02 2.15 0.09 o -11 0 1 140.55 135.29 1.60 o -10 0 1 14.10 21.00 0.45 o -9 0 1 5.71 5.78 0.23 o -8 0 1 101.02 100.26 1.24 o -7 0 1 101.65 110.00 1.30 o -6 0 1 31.60 32.64 0.47 o -5 0 1 7.19 2.28 0.09 o -4 0 1 123.57 82.19 0.91 o -3 0 1 57.31 34.84 0.41 o -2 0 1 131.84 180.63 2.37 o -1 0 1 4477.17 3233.20 32.84 o 1 0 1 7969.48 3865.34 39.32 x 2 0 1 5436.92 5331.22 54.23 o 3 0 1 545.51 573.07 6.76 o 4 0 1 42.41 29.70 0.39 o 5 0 1 10.01 6.48 0.17 o 6 0 1 138.32 146.63 1.64 o 7 0 1 0.37 0.30 0.10 o 8 0 1 1.39 1.67 0.17 o 9 0 1 87.35 78.75 1.05 o 10 0 1 15.73 12.58 0.33 o 11 0 1 0.35 0.46 0.11 o -11 1 1 0.40 0.55 0.14 o -10 1 1 199.59 219.56 2.49 o -9 1 1 27.65 30.81 0.54 o -8 1 1 29.16 33.56 2.43 o -7 1 1 424.92 485.89 70.49 o -6 1 1 62.05 55.25 1.52 o -5 1 1 397.74 483.50 4.60 o -4 1 1 361.32 393.80 6.90 o -3 1 1 992.16 1308.86 31.36 o -2 1 1 1316.22 1455.75 76.36 o -1 1 1 1383.31 1277.68 147.21 o 0 1 1 3310.79 2891.82 77.71 o 1 1 1 4600.49 3641.02 445.46 o 2 1 1 1340.46 1288.89 39.90 o 3 1 1 1367.96 1440.58 11.00 o 4 1 1 143.71 134.83 2.75 o 5 1 1 284.57 275.32 4.29 o 6 1 1 204.68 166.88 1.30 o 7 1 1 8.15 8.27 0.57 o 8 1 1 15.81 12.87 0.39 o 9 1 1 9.08 9.06 0.29 o 10 1 1 23.34 21.60 0.42 o 11 1 1 22.23 19.88 0.36 o -11 2 1 6.00 5.60 0.21 o -10 2 1 48.96 55.86 0.81 o -9 2 1 118.57 131.45 1.60 o -8 2 1 245.99 250.90 6.59 o -7 2 1 193.91 222.51 1.73 o -6 2 1 233.09 242.04 5.29 o -5 2 1 343.32 458.34 4.49 o -4 2 1 97.40 108.40 2.12 o -3 2 1 1277.55 1704.93 88.96 o -2 2 1 642.44 738.07 15.42 o -1 2 1 6003.45 5675.76 536.11 o 0 2 1 10253.62 7384.04 1146.54 o 1 2 1 292.97 296.29 32.32 o 2 2 1 3750.23 4208.01 187.27 o 3 2 1 25.78 21.69 1.42 o 4 2 1 586.34 690.11 14.39 o 5 2 1 463.65 633.39 5.88 o 6 2 1 117.59 109.98 2.54 o 7 2 1 82.37 76.44 1.08 o 8 2 1 55.95 52.55 0.74 o 9 2 1 21.97 19.12 0.41 o 10 2 1 16.94 13.96 0.33 o 11 2 1 12.87 12.10 0.27 o -11 3 1 5.59 5.82 0.20 o -10 3 1 0.49 0.56 0.15 o -9 3 1 189.98 210.91 2.41 o -8 3 1 28.05 26.49 0.84 o -7 3 1 24.48 26.95 0.52 o -6 3 1 48.24 36.55 0.83 o -5 3 1 663.49 917.92 21.48 o -4 3 1 111.14 80.43 2.60 o -3 3 1 241.00 324.25 21.22 o -2 3 1 503.40 638.26 10.60 o -1 3 1 1704.98 2006.33 14.90 o 0 3 1 1287.29 1485.02 46.10 o 1 3 1 140.86 154.47 43.12 o 2 3 1 4570.75 5408.22 550.07 o 3 3 1 314.54 260.65 72.32 o 4 3 1 297.50 298.91 71.88 o 5 3 1 254.90 239.59 11.03 o 6 3 1 239.70 235.05 9.28 o 7 3 1 15.32 15.92 0.50 o 8 3 1 90.39 79.93 1.94 o 9 3 1 33.60 28.78 0.52 o 10 3 1 14.71 14.82 0.34 o 11 3 1 6.07 4.07 0.17 o -11 4 1 5.59 6.54 0.20 o -10 4 1 9.46 11.25 0.30 o -9 4 1 19.09 25.21 0.48 o -8 4 1 338.32 355.22 9.27 o -7 4 1 11.40 15.08 1.06 o -6 4 1 181.26 186.47 6.97 o -5 4 1 369.48 410.81 37.98 o -4 4 1 1213.27 1598.08 60.79 o -3 4 1 14.74 18.35 0.41 o -2 4 1 3013.18 3448.85 25.50 o -1 4 1 668.86 754.19 6.21 o 0 4 1 701.49 891.40 37.13 o 1 4 1 1423.64 1900.06 128.03 o 2 4 1 960.99 1262.62 125.77 o 3 4 1 598.70 995.07 119.43 o 4 4 1 372.05 533.90 50.87 o 5 4 1 111.95 111.26 11.67 o 6 4 1 111.48 113.53 10.76 o 7 4 1 232.20 215.65 17.18 o 8 4 1 15.97 14.29 0.35 o 9 4 1 103.43 94.02 1.20 o 10 4 1 32.36 28.89 0.49 o 11 4 1 6.37 5.73 0.18 o -11 5 1 6.01 6.59 0.18 o -10 5 1 4.87 5.72 0.21 o -9 5 1 34.91 39.87 0.64 o -8 5 1 82.68 87.87 1.15 o -7 5 1 70.75 82.75 4.82 o -6 5 1 269.23 297.50 17.65 o -5 5 1 3.53 4.09 0.21 o -4 5 1 65.93 51.46 1.70 o -3 5 1 777.89 1069.89 11.39 o -2 5 1 127.66 159.04 1.21 o -1 5 1 298.31 422.54 4.04 o 0 5 1 228.82 250.34 52.00 o 1 5 1 394.21 530.65 32.31 o 2 5 1 1.30 24.75 20.00 o 3 5 1 111.04 115.14 6.59 o 4 5 1 445.88 477.06 153.84 o 5 5 1 126.72 133.60 16.76 o 6 5 1 99.99 112.28 10.11 o 7 5 1 58.73 67.08 8.47 o 8 5 1 70.08 63.74 0.90 o 9 5 1 33.40 27.85 0.50 o 10 5 1 45.60 36.55 0.56 o -10 6 1 4.52 5.18 0.19 o -9 6 1 34.35 41.86 0.65 o -8 6 1 58.40 60.32 0.86 o -7 6 1 134.79 157.74 11.02 o -6 6 1 219.25 232.99 10.83 o -5 6 1 86.26 115.93 3.93 o -4 6 1 90.41 78.72 4.08 o -3 6 1 3.27 4.68 0.34 o -2 6 1 687.51 925.81 17.44 o -1 6 1 619.60 806.34 7.13 o 0 6 1 619.48 805.44 26.61 o 1 6 1 106.81 120.53 5.07 o 2 6 1 184.69 150.31 11.15 o 3 6 1 95.49 75.81 7.04 o 4 6 1 260.64 272.71 31.68 o 5 6 1 20.12 24.73 5.62 o 6 6 1 318.31 289.87 39.58 o 7 6 1 16.56 15.44 0.37 o 8 6 1 11.41 9.36 0.28 o 9 6 1 1.34 0.46 0.14 o 10 6 1 20.31 18.28 0.33 o -10 7 1 3.60 4.73 0.17 o -9 7 1 15.19 17.00 0.35 o -8 7 1 11.26 15.34 0.36 o -7 7 1 17.61 17.79 0.40 o -6 7 1 45.84 44.50 1.91 o -5 7 1 75.29 79.81 2.07 o -4 7 1 124.19 128.77 3.45 o -3 7 1 22.48 31.22 0.34 o -2 7 1 174.60 187.76 1.46 o -1 7 1 44.01 48.15 0.46 o 0 7 1 13.09 6.66 0.26 o 1 7 1 134.01 127.29 5.16 o 2 7 1 105.99 106.06 7.75 o 3 7 1 124.21 133.35 9.04 o 4 7 1 67.65 67.63 5.96 o 5 7 1 134.72 129.35 14.94 o 6 7 1 110.10 103.14 1.30 o 7 7 1 23.80 21.85 0.44 o 8 7 1 6.13 5.95 0.23 o 9 7 1 36.83 33.63 0.52 o -9 8 1 6.87 9.11 0.24 o -8 8 1 25.30 32.89 0.54 o -7 8 1 72.94 79.32 1.05 o -6 8 1 87.31 96.24 1.24 o -5 8 1 484.95 516.60 14.56 o -4 8 1 146.27 163.57 3.38 o -3 8 1 44.09 48.01 1.47 o -2 8 1 17.04 17.01 0.30 o -1 8 1 60.54 62.21 1.11 o 0 8 1 59.75 62.45 0.80 o 1 8 1 86.43 81.11 3.36 o 2 8 1 198.40 189.02 13.01 o 3 8 1 78.77 78.22 6.86 o 4 8 1 39.98 41.98 4.09 o 5 8 1 16.87 15.60 0.37 o 6 8 1 30.44 28.24 0.52 o 7 8 1 2.65 1.60 0.16 o 8 8 1 2.30 2.46 0.16 o 9 8 1 2.69 2.23 0.12 o -8 9 1 2.97 3.11 0.16 o -7 9 1 21.68 23.19 0.43 o -6 9 1 83.46 89.24 1.17 o -5 9 1 23.29 28.67 0.53 o -4 9 1 107.62 114.34 1.42 o -3 9 1 17.09 23.62 0.33 o -2 9 1 5.54 5.83 0.60 o -1 9 1 1.47 2.24 0.22 o 0 9 1 109.29 120.91 1.38 o 1 9 1 20.81 27.29 0.35 o 2 9 1 50.07 45.04 3.08 o 3 9 1 79.53 87.88 5.95 o 4 9 1 63.28 58.88 0.85 o 5 9 1 17.97 17.91 0.39 o 6 9 1 0.76 0.94 0.15 o 7 9 1 3.38 2.99 0.17 o 8 9 1 8.93 7.52 0.21 o -8 10 1 23.21 23.07 0.37 o -7 10 1 44.14 46.51 0.66 o -6 10 1 3.51 3.51 0.19 o -5 10 1 16.99 21.29 0.43 o -4 10 1 16.08 17.59 0.40 o -3 10 1 113.43 116.09 1.45 o -2 10 1 8.97 9.12 0.28 o -1 10 1 63.35 65.82 0.93 o 0 10 1 10.05 11.34 0.32 o 1 10 1 51.03 54.90 0.81 o 2 10 1 104.41 103.51 1.32 o 3 10 1 42.91 42.60 0.68 o 4 10 1 36.01 31.53 0.55 o 5 10 1 17.82 18.06 0.39 o 6 10 1 15.70 16.10 0.34 o 7 10 1 3.37 4.90 0.17 o -6 11 1 5.37 7.75 0.21 o -5 11 1 5.33 7.02 0.22 o -4 11 1 8.52 9.37 0.27 o -3 11 1 27.93 28.66 0.51 o -2 11 1 16.43 18.50 0.40 o -1 11 1 69.76 77.70 1.05 o 0 11 1 37.03 38.70 0.63 o 1 11 1 8.21 11.83 0.32 o 2 11 1 19.39 21.81 0.43 o 3 11 1 5.54 5.42 0.22 o 4 11 1 8.15 8.20 0.25 o 5 11 1 0.68 0.51 0.11 o 6 11 1 0.08 0.12 0.09 o -5 12 1 3.15 3.09 0.14 o -4 12 1 12.78 13.45 0.29 o -3 12 1 33.85 40.47 0.60 o -2 12 1 0.87 1.01 0.14 o -1 12 1 23.53 24.36 0.44 o 0 12 1 5.67 6.75 0.23 o 1 12 1 3.87 4.43 0.20 o 2 12 1 23.71 24.03 0.43 o 3 12 1 17.34 16.08 0.33 o 4 12 1 4.17 4.76 0.17 o 5 12 1 5.77 4.97 0.16 o -2 13 1 7.79 7.19 0.20 o -1 13 1 1.51 1.39 0.12 o 0 13 1 6.86 6.74 0.20 o 1 13 1 3.09 3.26 0.15 o 2 13 1 22.04 20.33 0.35 o -11 0 2 5.02 3.58 0.20 o -10 0 2 479.11 479.28 5.14 o -9 0 2 6.12 4.91 0.23 o -8 0 2 207.09 204.21 2.30 o -7 0 2 87.78 97.35 1.17 o -6 0 2 9.25 7.89 0.20 o -5 0 2 710.98 981.13 11.64 o -4 0 2 2073.54 2815.68 29.68 o -3 0 2 2971.88 3317.61 34.35 o -2 0 2 3258.54 3383.73 34.73 o -1 0 2 8116.30 4336.97 44.20 x 0 0 2 0.08 24.53 0.28 x 1 0 2 2661.82 2065.06 21.42 o 2 0 2 129.88 75.58 0.82 o 3 0 2 40.44 18.03 0.25 o 4 0 2 1021.32 1220.90 13.88 o 5 0 2 1104.36 1284.17 15.01 o 6 0 2 431.42 396.62 4.16 o 7 0 2 168.61 153.49 1.76 o 8 0 2 483.59 429.18 4.59 o 9 0 2 0.14 0.53 0.15 o 10 0 2 11.96 10.09 0.28 o 11 0 2 5.03 4.61 0.17 o -11 1 2 27.14 31.11 0.51 o -10 1 2 35.15 43.57 0.69 o -9 1 2 8.93 8.81 0.28 o -8 1 2 34.68 35.60 0.41 o -7 1 2 70.04 69.46 0.66 o -6 1 2 152.11 141.60 2.71 o -5 1 2 173.30 138.42 4.07 o -4 1 2 222.17 167.38 5.50 o -3 1 2 1231.97 1466.81 43.00 o -2 1 2 1670.76 1860.16 83.49 o -1 1 2 62.10 49.44 3.71 o 0 1 2 4901.42 3370.96 67.05 o 1 1 2 4305.98 3151.58 161.44 o 2 1 2 1857.77 1786.98 30.25 o 3 1 2 90.89 115.38 10.48 o 4 1 2 185.49 157.11 2.32 o 5 1 2 306.81 254.29 4.24 o 6 1 2 74.79 72.77 1.30 o 7 1 2 175.81 147.77 3.00 o 8 1 2 20.70 15.43 0.58 o 9 1 2 39.32 34.15 0.58 o 10 1 2 35.86 33.63 0.55 o 11 1 2 5.71 4.74 0.17 o -11 2 2 13.01 14.31 0.31 o -10 2 2 32.11 32.06 0.55 o -9 2 2 9.81 13.18 0.34 o -8 2 2 260.79 273.59 5.79 o -7 2 2 504.69 681.14 6.89 o -6 2 2 278.70 282.98 4.81 o -5 2 2 383.53 611.61 13.97 o -4 2 2 12.37 9.83 0.13 o -3 2 2 2507.12 2834.12 23.32 o -2 2 2 3882.02 3615.39 414.59 o -1 2 2 416.53 451.47 30.93 o 0 2 2 426.49 452.41 32.22 o 1 2 2 1406.67 1512.15 103.33 o 2 2 2 78.38 83.54 2.95 o 3 2 2 600.42 660.54 30.77 o 4 2 2 91.23 64.62 4.12 o 5 2 2 221.13 215.03 11.06 o 6 2 2 125.43 106.49 5.68 o 7 2 2 109.15 93.19 4.03 o 8 2 2 22.25 19.69 1.36 o 9 2 2 33.88 26.71 0.49 o 10 2 2 1.72 1.50 0.15 o 11 2 2 5.62 4.09 0.16 o -11 3 2 17.44 19.20 0.36 o -10 3 2 37.91 37.99 0.61 o -9 3 2 211.17 221.61 2.51 o -8 3 2 92.75 101.74 1.17 o -7 3 2 79.50 82.94 0.74 o -6 3 2 107.24 115.24 3.22 o -5 3 2 81.52 82.59 23.72 o -4 3 2 214.18 158.57 2.46 o -3 3 2 944.54 1275.22 19.93 o -2 3 2 41.57 43.31 0.72 o -1 3 2 1398.22 1605.66 49.56 o 0 3 2 2118.57 2545.19 153.06 o 1 3 2 327.37 428.43 41.37 o 2 3 2 1173.11 1490.16 142.80 o 3 3 2 908.11 1073.21 69.52 o 4 3 2 893.44 1104.39 89.93 o 5 3 2 411.59 440.15 121.59 o 6 3 2 8.46 8.98 1.20 o 7 3 2 32.96 31.06 3.09 o 8 3 2 217.97 193.02 2.22 o 9 3 2 0.58 0.98 0.15 o 10 3 2 20.27 21.23 0.40 o 11 3 2 1.39 1.13 0.11 o -11 4 2 6.32 7.46 0.21 o -10 4 2 5.41 4.65 0.21 o -9 4 2 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