#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/10/2011031.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011031_Fobs loop_ _publ_author_name 'Kani, Yoshiyuki' 'Ohba, Shigeru' 'Ito, Sayo' 'Nishida, Yuzo' _publ_section_title ; Four copper(II) complexes with potentially tetradentate tripodal ligands ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e233 _journal_page_last e235 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _[local]_cod_data_source_file qa0275IIIsup4.hkl _[local]_cod_data_source_block III loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma _refln_F_squared_calc _refln_observed_status 0 1 1 5338.12 534.18 5329.94 o 0 0 2 9623.14 1063.82 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91.76 924.57 o 2 1 -2 236.17 28.51 278.45 o 1 2 -3 263.05 31.89 318.30 o 2 1 2 792.33 73.93 691.21 o 1 2 3 4274.59 422.26 4181.75 o 0 3 1 1147.40 122.89 1249.02 o 0 2 4 7383.14 711.50 6946.45 o 0 1 5 16340.79 1605.40 15880.12 o 1 0 -5 29878.10 3039.63 30495.04 o 2 1 -3 8612.00 829.33 8102.04 o 2 2 0 14948.92 1463.49 14443.98 o 1 0 5 6621.75 747.38 7888.10 o 0 3 2 13671.68 1322.52 12962.42 o 2 1 3 1273.55 112.71 1032.78 o 1 3 0 29377.68 2820.34 27531.63 o 2 2 -1 15099.52 1468.91 14407.41 o 2 2 1 1734.04 176.69 1763.01 o 1 3 -1 64266.80 6686.79 67990.92 o 1 3 1 1237.81 114.56 1074.75 o 1 2 -4 859.31 91.20 918.71 o 1 1 -5 5044.35 505.52 5046.39 o 1 2 4 454.90 43.44 389.79 o 1 1 5 199.81 19.63 140.04 o 2 2 -2 9826.31 887.89 8368.38 o 2 0 -4 21582.90 2109.04 20766.37 o 2 2 2 5493.13 518.37 5009.67 o 1 3 -2 18768.46 2030.57 20998.66 o 2 0 4 4153.32 443.26 4557.88 o 1 3 2 881.48 85.49 812.08 o 0 3 3 491.46 61.66 649.39 o 0 0 6 2633.22 261.68 2591.74 o 2 1 -4 4703.07 454.31 4447.19 o 0 2 5 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