#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/10/2011039.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011039_Fobs loop_ _publ_author_name 'Sa\&smannshausen, J\"org' 'Rust, J\"org' 'Goddard, Richard' _publ_section_title ; Tribenzyl{\h^5^-[2-(p-tolyl)prop-2-yl]cyclopentadienyl}zirconium ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e236 _journal_page_last e237 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.395 _cell_angle_gamma 90.000 _cell_length_a 25.0892 _cell_length_b 11.0572 _cell_length_c 22.0033 _exptl_crystal_F_000 2352.00 _reflns_d_resolution_high 0.7570 _[local]_cod_data_source_file qa0288Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 3324' _shelx_refln_list_code 4 _shelx_f_calc_maximum 421.61 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 0.40 74.67 13.75 o 4 0 0 53270.16 53705.36 2231.59 o 5 0 0 2789.98 2942.63 78.48 o 6 0 0 45312.94 45457.30 1287.49 o 7 0 0 11521.12 12475.32 256.62 o 8 0 0 12341.62 13409.78 277.99 o 9 0 0 14992.28 14798.94 748.68 o 10 0 0 20659.00 19245.88 391.75 o 11 0 0 993.90 1145.41 71.62 o 12 0 0 12385.68 12873.63 288.61 o 13 0 0 24721.96 25035.79 509.89 o 14 0 0 3166.95 3283.81 243.42 o 15 0 0 2707.77 2482.30 95.16 o 16 0 0 6699.30 6337.80 137.02 o 17 0 0 1146.68 1113.02 67.02 o 18 0 0 12.50 63.69 52.83 o 19 0 0 11057.72 10634.28 234.30 o 20 0 0 693.61 695.63 97.92 o 21 0 0 1500.61 1518.09 129.17 o 22 0 0 2868.50 2840.21 159.42 o 23 0 0 5237.99 4933.75 207.42 o 24 0 0 941.78 841.32 121.33 o 1 1 0 33.92 114.69 17.60 o 2 1 0 50232.33 49580.63 905.04 o 3 1 0 25.71 25.19 8.45 o 4 1 0 2415.93 2659.24 49.68 o 5 1 0 550.37 577.02 27.34 o 6 1 0 3576.60 3456.24 65.70 o 7 1 0 273.60 269.56 23.57 o 8 1 0 28050.09 26607.22 362.68 o 9 1 0 415.99 406.88 38.18 o 10 1 0 14279.71 14675.23 292.86 o 11 1 0 20048.61 20368.94 295.16 o 12 1 0 7999.38 7366.04 154.55 o 13 1 0 746.69 808.13 49.96 o 14 1 0 27572.71 26467.91 376.25 o 15 1 0 1755.67 1804.67 70.65 o 16 1 0 4060.63 4105.34 81.93 o 17 1 0 11340.68 10984.76 151.13 o 18 1 0 1960.91 1928.31 72.17 o 19 1 0 642.01 693.96 53.28 o 20 1 0 3157.37 3142.80 91.01 o 21 1 0 6096.69 5669.79 171.59 o 22 1 0 116.51 37.79 68.64 o 23 1 0 2114.78 2123.03 157.83 o 24 1 0 4306.95 4365.40 245.62 o 25 1 0 399.14 434.61 123.33 o 26 1 0 712.28 686.24 191.98 o 0 2 0 14430.71 14810.17 405.14 o 1 2 0 72.27 61.51 13.05 o 2 2 0 89730.70 91025.91 1341.40 o 3 2 0 56.63 150.85 14.16 o 4 2 0 5610.08 6034.32 86.59 o 5 2 0 190.46 191.80 17.45 o 6 2 0 160.83 157.43 18.18 o 7 2 0 1722.29 1719.73 49.52 o 8 2 0 5462.56 5739.83 102.85 o 9 2 0 4413.30 4521.83 91.08 o 10 2 0 607.07 496.22 35.98 o 11 2 0 74.87 126.38 32.59 o 12 2 0 5461.60 5109.61 124.50 o 13 2 0 758.69 927.90 47.68 o 14 2 0 593.28 639.64 39.96 o 15 2 0 162.58 123.98 43.13 o 16 2 0 758.28 927.36 51.74 o 17 2 0 84.86 0.88 39.62 o 18 2 0 803.03 846.04 87.99 o 19 2 0 294.25 353.66 51.11 o 20 2 0 151.41 75.82 62.80 o 21 2 0 85.59 268.36 66.13 o 22 2 0 2197.22 2068.89 109.70 o 23 2 0 380.87 435.55 131.05 o 24 2 0 182.64 295.59 202.02 o 25 2 0 2573.04 2325.07 179.90 o 26 2 0 132.88 111.37 131.17 o 27 2 0 91.99 24.71 140.22 o 28 2 0 258.25 271.75 210.96 o 29 2 0 261.10 138.07 217.84 o 1 3 0 412.67 411.00 35.12 o 2 3 0 16139.61 16612.69 267.39 o 3 3 0 141.13 210.29 24.03 o 4 3 0 3141.70 3353.95 65.70 o 5 3 0 4836.75 4952.37 79.30 o 6 3 0 2176.67 2162.44 56.03 o 7 3 0 7639.35 8098.74 118.54 o 8 3 0 685.33 731.21 37.06 o 9 3 0 8100.80 7816.28 134.51 o 10 3 0 5562.30 5580.18 152.61 o 11 3 0 4447.40 4450.19 97.67 o 12 3 0 14.25 56.23 28.76 o 13 3 0 941.26 977.98 46.85 o 14 3 0 1562.73 1659.46 67.14 o 15 3 0 688.99 745.38 52.90 o 16 3 0 21.05 -7.66 39.58 o 17 3 0 427.49 389.57 46.76 o 18 3 0 1203.13 1299.38 74.43 o 19 3 0 3.95 -20.43 58.25 o 20 3 0 39.94 172.10 65.89 o 21 3 0 136.72 70.53 84.44 o 22 3 0 23.12 -48.75 71.22 o 23 3 0 44.55 0.96 72.79 o 24 3 0 81.12 68.86 79.74 o 25 3 0 80.56 20.50 86.24 o 26 3 0 15.88 173.56 134.51 o 27 3 0 86.69 115.24 193.91 o 28 3 0 29.28 -149.08 211.24 o 29 3 0 1.08 54.46 220.04 o 30 3 0 18.00 -16.78 236.54 o 0 4 0 18415.35 18605.81 531.67 o 1 4 0 31.19 95.43 35.55 o 2 4 0 1943.82 2039.30 65.10 o 3 4 0 2262.21 2407.30 78.46 o 4 4 0 5345.22 5318.70 113.20 o 5 4 0 5386.19 5389.50 116.01 o 6 4 0 46511.13 48557.30 830.55 o 7 4 0 5061.80 5329.79 91.56 o 8 4 0 218.18 197.57 47.52 o 9 4 0 542.67 516.74 34.87 o 10 4 0 8563.80 8101.23 121.46 o 11 4 0 1302.24 1253.64 49.90 o 12 4 0 557.96 520.73 44.78 o 13 4 0 2608.27 2868.64 82.93 o 14 4 0 107.53 44.70 38.46 o 15 4 0 4679.98 4432.74 105.07 o 16 4 0 6740.19 6334.33 129.83 o 17 4 0 57.42 27.77 57.75 o 18 4 0 126.16 168.98 60.80 o 19 4 0 3829.93 3874.97 128.14 o 20 4 0 4185.67 3992.73 133.92 o 21 4 0 1813.59 1908.92 113.77 o 22 4 0 1095.50 1049.70 109.72 o 23 4 0 25.17 74.64 79.78 o 24 4 0 1466.80 1438.91 108.10 o 25 4 0 2111.63 2061.63 234.66 o 26 4 0 334.73 568.74 123.00 o 27 4 0 2.15 -145.68 145.68 o 28 4 0 65.69 1.38 217.29 o 29 4 0 1460.74 2062.85 286.05 o 1 5 0 713.29 716.52 68.62 o 2 5 0 31082.70 31417.43 498.59 o 3 5 0 919.61 890.07 53.40 o 4 5 0 22285.72 23042.86 504.89 o 5 5 0 2055.95 2161.98 77.14 o 6 5 0 146.40 207.38 32.48 o 7 5 0 11032.71 11437.23 248.85 o 8 5 0 32781.40 32375.72 341.93 o 9 5 0 0.40 -22.81 35.83 o 10 5 0 4805.98 4920.62 92.69 o 11 5 0 3200.82 3383.55 84.93 o 12 5 0 866.22 775.21 56.15 o 13 5 0 549.60 579.09 48.82 o 14 5 0 3259.28 3254.88 96.85 o 15 5 0 29.28 -21.43 55.03 o 16 5 0 88.56 103.89 54.67 o 17 5 0 339.21 281.09 59.88 o 18 5 0 1464.43 1567.81 96.59 o 19 5 0 1018.58 1094.18 88.17 o 20 5 0 86.16 104.83 71.07 o 21 5 0 3148.77 3036.21 131.58 o 22 5 0 2621.31 2479.15 123.63 o 23 5 0 1320.16 1296.96 106.33 o 24 5 0 2663.42 2644.01 144.10 o 25 5 0 512.53 405.50 119.97 o 26 5 0 317.46 395.10 153.52 o 27 5 0 3705.47 3582.99 387.95 o 28 5 0 817.36 1319.46 263.08 o 0 6 0 28190.37 27465.07 787.46 o 1 6 0 80.34 54.39 40.95 o 2 6 0 172.14 164.40 40.30 o 3 6 0 1319.95 1435.64 74.70 o 4 6 0 9792.60 9691.25 193.55 o 5 6 0 2913.17 2807.54 83.97 o 6 6 0 13960.74 13238.53 194.36 o 7 6 0 93.45 103.75 33.39 o 8 6 0 1438.73 1427.90 55.67 o 9 6 0 530.11 585.62 41.55 o 10 6 0 10939.68 11093.39 162.67 o 11 6 0 57.75 39.53 41.48 o 12 6 0 25537.64 24242.56 447.38 o 13 6 0 10840.21 10688.67 209.20 o 14 6 0 1202.04 1275.20 79.29 o 15 6 0 1642.64 1597.02 89.96 o 16 6 0 3881.08 3672.81 129.32 o 17 6 0 232.53 287.94 65.13 o 18 6 0 558.93 603.99 76.12 o 19 6 0 9285.35 9029.82 226.17 o 20 6 0 66.33 -45.51 76.87 o 21 6 0 106.98 224.02 86.69 o 22 6 0 2120.78 2150.87 142.12 o 23 6 0 1704.31 1614.57 136.05 o 24 6 0 631.16 725.66 142.13 o 25 6 0 2283.13 2623.36 220.40 o 26 6 0 57.65 123.12 159.63 o 27 6 0 0.10 12.61 164.29 o 28 6 0 83.81 57.29 175.90 o 1 7 0 149.92 133.73 38.11 o 2 7 0 11809.27 11995.70 214.42 o 3 7 0 984.51 1044.27 59.72 o 4 7 0 6023.82 5549.89 124.16 o 5 7 0 1589.43 1651.63 88.29 o 6 7 0 12.28 44.34 35.01 o 7 7 0 55.91 57.03 40.22 o 8 7 0 2364.67 2264.50 78.05 o 9 7 0 4598.72 4568.11 140.48 o 10 7 0 3692.07 3838.38 100.30 o 11 7 0 1117.55 1049.46 70.79 o 12 7 0 5119.57 4730.03 170.79 o 13 7 0 17.75 83.53 63.57 o 14 7 0 5181.20 4804.74 142.31 o 15 7 0 1960.26 2041.32 106.50 o 16 7 0 16.85 49.42 65.33 o 17 7 0 2656.22 2453.78 166.91 o 18 7 0 0.41 -39.10 132.24 o 19 7 0 909.51 781.90 98.65 o 20 7 0 1941.28 1874.94 154.03 o 21 7 0 815.48 884.87 101.55 o 22 7 0 845.36 1159.90 166.23 o 23 7 0 307.21 504.53 149.70 o 24 7 0 453.07 505.80 159.69 o 25 7 0 463.46 571.68 159.77 o 26 7 0 554.51 763.60 178.84 o 27 7 0 1233.99 1315.21 241.63 o 0 8 0 1564.37 1608.87 116.26 o 1 8 0 4835.43 4437.22 322.76 o 2 8 0 1410.38 1320.16 66.30 o 3 8 0 1574.54 1528.92 71.98 o 4 8 0 833.23 914.21 69.20 o 5 8 0 4216.98 4454.82 155.29 o 6 8 0 312.01 299.41 44.61 o 7 8 0 600.83 654.75 56.73 o 8 8 0 87.70 77.55 47.24 o 9 8 0 3386.86 3167.01 110.95 o 10 8 0 79.23 3.83 59.65 o 11 8 0 5736.42 5505.07 148.75 o 12 8 0 3519.76 3488.03 127.56 o 13 8 0 1175.79 1238.63 85.91 o 14 8 0 2697.89 2712.07 123.16 o 15 8 0 6.45 -67.63 67.63 o 16 8 0 2.42 115.38 76.34 o 17 8 0 4342.90 4158.64 160.43 o 18 8 0 2167.89 2300.65 123.91 o 19 8 0 16.40 -74.69 89.41 o 20 8 0 1415.99 1284.74 114.65 o 21 8 0 225.91 117.90 130.50 o 22 8 0 267.31 475.28 156.36 o 23 8 0 1463.67 1258.16 177.02 o 24 8 0 1685.72 1524.49 197.35 o 25 8 0 358.76 699.01 169.92 o 1 9 0 6338.06 6815.19 160.08 o 2 9 0 378.07 476.28 65.86 o 3 9 0 18703.29 19407.07 320.08 o 4 9 0 2.11 -31.47 60.01 o 5 9 0 1483.29 1470.12 76.34 o 6 9 0 2234.79 2354.15 94.82 o 7 9 0 5170.96 4971.21 190.60 o 8 9 0 3171.17 3047.30 116.94 o 9 9 0 4210.39 4267.04 136.34 o 10 9 0 1171.74 1149.98 84.79 o 11 9 0 14.24 11.42 67.12 o 12 9 0 1064.42 1111.46 89.00 o 13 9 0 1965.34 1962.03 132.27 o 14 9 0 1082.70 1106.29 94.23 o 15 9 0 1064.35 1101.57 96.92 o 16 9 0 3157.40 3205.14 150.78 o 17 9 0 1424.25 1333.06 108.41 o 18 9 0 609.78 838.23 111.96 o 19 9 0 1139.61 837.95 141.68 o 20 9 0 739.42 394.15 136.31 o 21 9 0 21.12 -28.14 176.99 o 22 9 0 3684.94 3908.86 271.06 o 23 9 0 274.66 316.99 160.11 o 24 9 0 5.35 -82.17 162.62 o 0 10 0 1668.72 1852.94 151.02 o 1 10 0 2921.69 3158.74 121.46 o 2 10 0 1845.87 1732.98 130.41 o 3 10 0 1709.27 1688.87 106.91 o 4 10 0 659.77 661.28 69.07 o 5 10 0 1482.19 1553.07 95.70 o 6 10 0 4493.51 4314.76 140.77 o 7 10 0 274.19 427.86 88.57 o 8 10 0 33.82 -59.57 73.10 o 9 10 0 2487.50 2348.43 122.69 o 10 10 0 220.89 223.54 81.21 o 11 10 0 3731.96 3396.45 134.51 o 12 10 0 0.83 -2.33 75.03 o 13 10 0 8.43 111.56 86.68 o 14 10 0 1170.99 1478.99 113.04 o 15 10 0 1055.88 1198.54 106.66 o 16 10 0 223.07 137.62 236.27 o 17 10 0 701.53 638.58 145.67 o 18 10 0 434.45 546.82 417.11 o 19 10 0 895.17 1020.90 166.29 o 20 10 0 1195.42 1009.37 175.62 o 21 10 0 646.10 956.23 204.63 o 22 10 0 169.75 296.22 160.56 o 1 11 0 101.34 44.29 91.32 o 2 11 0 1651.75 1761.37 275.05 o 3 11 0 126.16 85.63 78.20 o 4 11 0 1879.98 2044.47 147.68 o 5 11 0 7.89 134.14 79.40 o 6 11 0 1538.05 1659.26 168.01 o 7 11 0 707.59 824.27 90.25 o 8 11 0 3545.61 3704.71 194.25 o 9 11 0 167.73 123.30 81.72 o 10 11 0 144.77 230.85 93.12 o 11 11 0 48.77 98.07 85.46 o 12 11 0 1152.49 1152.92 129.78 o 13 11 0 355.66 433.81 182.80 o 14 11 0 886.53 1257.80 218.66 o 15 11 0 187.08 214.81 145.65 o 16 11 0 35.80 -133.11 133.11 o 17 11 0 2178.44 2577.93 212.99 o 18 11 0 791.68 730.95 159.96 o 19 11 0 250.48 168.38 155.48 o 20 11 0 735.08 928.89 179.09 o 1 12 0 1351.53 330.06 191.71 o 2 12 0 50.55 148.48 178.64 o 3 12 0 275.59 319.02 137.65 o 4 12 0 7.23 121.00 238.05 o 5 12 0 4.00 136.49 108.04 o 6 12 0 3232.84 3534.17 175.11 o 7 12 0 395.62 401.63 98.62 o 8 12 0 191.88 294.71 101.59 o 9 12 0 353.61 260.77 104.26 o 10 12 0 645.05 1089.43 151.78 o 11 12 0 453.52 445.76 145.03 o 12 12 0 1450.38 1355.85 163.75 o 13 12 0 43.69 217.96 146.98 o 14 12 0 354.98 382.93 149.54 o 15 12 0 22.50 40.63 169.79 o 16 12 0 760.91 1156.59 189.12 o 17 12 0 493.35 702.95 195.42 o 3 13 0 2850.08 2687.21 298.98 o 4 13 0 971.60 1383.76 231.86 o 5 13 0 1633.75 1665.13 250.84 o 6 13 0 0.47 -178.51 191.16 o 7 13 0 1004.88 1012.56 165.01 o 8 13 0 1468.33 1702.62 180.25 o 9 13 0 1082.45 1360.77 182.71 o 10 13 0 960.93 1403.80 184.96 o 11 13 0 150.02 181.14 161.45 o 12 13 0 3.34 -165.82 165.82 o 13 13 0 1600.42 1921.94 208.09 o 14 13 0 208.70 -47.01 190.29 o 6 14 0 16.08 57.21 235.44 o 7 14 0 548.59 1063.88 254.42 o 8 14 0 476.89 647.46 235.99 o -25 1 1 12.64 -39.90 244.79 o -24 1 1 1145.82 1291.76 209.72 o -23 1 1 61.55 40.39 147.95 o -22 1 1 483.69 630.38 73.80 o -21 1 1 2390.66 2377.69 98.51 o -20 1 1 478.16 450.14 52.52 o -19 1 1 267.35 287.50 43.26 o -18 1 1 2407.51 2291.84 81.44 o -17 1 1 53.60 83.01 34.05 o -16 1 1 1074.32 1067.44 46.92 o -15 1 1 1725.23 1481.03 56.46 o -14 1 1 2317.32 2295.79 75.82 o -13 1 1 7778.03 7452.80 142.08 o -12 1 1 6243.46 6047.77 117.19 o -11 1 1 2064.31 2075.98 64.81 o -10 1 1 7521.56 8035.13 135.53 o -9 1 1 24.08 23.27 22.73 o -8 1 1 1302.42 1305.16 45.36 o -7 1 1 10824.20 11061.47 163.42 o -6 1 1 604.04 618.61 29.61 o -5 1 1 23876.14 23619.59 440.20 o -4 1 1 459.25 536.03 23.15 o -3 1 1 32747.71 33523.74 646.81 o -2 1 1 405.38 444.01 19.83 o -1 1 1 75.01 80.12 20.96 o 0 1 1 1655.12 1559.53 79.90 o 1 1 1 23316.06 24191.51 366.17 o 2 1 1 53.34 134.57 13.27 o 3 1 1 21787.27 22372.74 343.74 o 4 1 1 481.35 488.75 23.07 o 5 1 1 33.97 49.38 14.57 o 6 1 1 23.08 34.12 16.46 o 7 1 1 2436.58 2425.26 57.15 o 8 1 1 392.44 365.09 66.50 o 9 1 1 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2122.16 2263.07 66.00 o -14 2 1 8918.53 9366.19 137.90 o -13 2 1 16476.73 15910.63 246.22 o -12 2 1 99.57 50.16 32.53 o -11 2 1 3726.03 3187.62 100.01 o -10 2 1 4480.75 4211.15 88.80 o -9 2 1 1702.31 1705.08 68.88 o -8 2 1 2499.60 2497.98 61.25 o -7 2 1 46115.86 44997.34 629.52 o -6 2 1 303.87 266.67 22.56 o -5 2 1 23809.35 24492.18 295.53 o -4 2 1 530.31 535.15 23.77 o -3 2 1 10938.62 10661.63 170.08 o -2 2 1 277.53 291.15 16.77 o -1 2 1 11452.96 11294.17 337.76 o 0 2 1 985.82 1016.01 44.61 o 1 2 1 54263.75 56248.90 1021.47 o 2 2 1 119.97 122.05 19.56 o 3 2 1 216.34 236.03 34.62 o 4 2 1 356.87 389.05 45.10 o 5 2 1 4168.23 4003.76 141.82 o 6 2 1 8865.92 9049.24 124.96 o 7 2 1 1720.26 1660.87 91.59 o 8 2 1 2823.37 2963.66 69.90 o 9 2 1 31966.36 31452.54 553.77 o 10 2 1 486.88 477.45 38.71 o 11 2 1 10227.10 9818.25 208.34 o 12 2 1 2383.61 2155.06 75.05 o 13 2 1 9805.09 9340.76 136.69 o 14 2 1 233.65 190.22 54.31 o 15 2 1 23478.25 23002.87 336.95 o 16 2 1 1205.11 1195.83 56.17 o 17 2 1 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