#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/16/2011679.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011679_Fobs loop_ _publ_author_name 'Hao, Qingli' 'Yang, Xujie' 'Jian, Fangfang' 'Lu, Lude' 'Wang, Xin' 'Razak, Ibrahim Abdul' 'Chantrapromma, Suchada' 'Fun, Hoong-Kun' _publ_section_title ; Bis(O,O'-diisopropyl dithiophosphato-S,S')(1,10-phenanthroline-N,N')metal(II) complexes with cadmium(II) and iron(II) ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 42 _journal_page_last 44 _journal_volume 57 _journal_year 2001 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.5761 _cell_length_b 18.8015 _cell_length_c 14.7098 _exptl_crystal_F_000 1384.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file bj1016IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' bj1016II in Pbcn 23/5/2000' _shelx_refln_list_code 4 _shelx_f_calc_maximum 308.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10011.64 9860.75 569.98 o 4 0 0 321.88 264.67 47.03 o 6 0 0 7.85 -33.11 32.66 o 8 0 0 1076.55 1080.69 115.72 o 10 0 0 4688.99 4846.47 346.61 o 12 0 0 630.47 939.15 159.05 o 1 1 0 2937.92 3208.18 337.46 o 3 1 0 12824.45 17069.67 694.57 o 5 1 0 2472.98 3086.31 149.05 o 7 1 0 59.26 132.50 41.25 o 9 1 0 235.42 292.31 59.15 o 11 1 0 217.92 216.68 111.57 o 13 1 0 407.91 448.93 96.86 o 0 2 0 4869.29 5493.71 255.44 o 2 2 0 25201.23 31671.79 1800.84 o 4 2 0 1160.76 1229.89 71.30 o 6 2 0 128.20 107.24 36.94 o 8 2 0 1697.00 2138.03 129.28 o 10 2 0 3645.74 3972.59 246.38 o 12 2 0 189.25 86.99 69.13 o 1 3 0 1994.57 1902.97 133.87 o 3 3 0 2753.69 2579.26 177.23 o 5 3 0 1352.29 1215.22 77.88 o 7 3 0 4.35 -3.93 30.44 o 9 3 0 3831.37 4219.03 215.87 o 11 3 0 611.44 571.50 79.68 o 13 3 0 598.84 366.42 84.95 o 0 4 0 29366.40 27048.34 3248.57 o 2 4 0 8972.38 8268.57 492.98 o 4 4 0 181.94 236.27 54.21 o 6 4 0 3076.74 4235.76 312.32 o 8 4 0 445.08 634.27 68.93 o 10 4 0 0.03 4.54 46.77 o 12 4 0 1.32 -17.49 55.00 o 1 5 0 1678.78 1618.29 62.48 o 3 5 0 25576.57 31366.26 1801.63 o 5 5 0 413.80 437.08 72.51 o 7 5 0 1541.81 1410.15 97.46 o 9 5 0 3333.27 3599.04 233.47 o 11 5 0 1197.01 1274.68 113.95 o 13 5 0 140.30 103.85 85.81 o 0 6 0 8876.39 9069.78 418.22 o 2 6 0 27292.90 36917.17 2111.87 o 4 6 0 1256.94 2171.02 170.05 o 6 6 0 0.66 18.18 48.60 o 8 6 0 183.55 110.20 48.09 o 10 6 0 1035.24 1174.27 105.67 o 12 6 0 729.60 876.44 105.73 o 1 7 0 1715.95 2329.20 214.03 o 3 7 0 8887.53 9968.50 608.81 o 5 7 0 283.58 239.87 71.16 o 7 7 0 6227.65 6884.71 452.79 o 9 7 0 1445.61 1631.57 117.50 o 11 7 0 3.04 32.40 93.89 o 13 7 0 136.28 28.73 103.38 o 0 8 0 3112.81 3194.35 166.79 o 2 8 0 11551.55 14738.42 504.44 o 4 8 0 545.49 474.90 81.38 o 6 8 0 366.07 523.84 96.98 o 8 8 0 5588.08 5532.51 386.46 o 10 8 0 1012.05 840.10 94.46 o 12 8 0 906.79 835.15 105.06 o 1 9 0 57.04 112.84 23.71 o 3 9 0 10373.78 10175.82 627.44 o 5 9 0 7411.26 7183.51 466.94 o 7 9 0 132.27 113.93 73.52 o 9 9 0 2812.34 2472.44 159.55 o 11 9 0 383.10 371.22 80.58 o 0 10 0 5217.76 6391.93 455.04 o 2 10 0 40.65 61.10 26.98 o 4 10 0 1092.89 1222.00 138.51 o 6 10 0 7370.55 7014.58 465.92 o 8 10 0 559.81 409.24 110.67 o 10 10 0 927.06 1044.84 104.84 o 12 10 0 0.89 -36.48 95.07 o 1 11 0 9068.86 10532.92 351.39 o 3 11 0 157.63 241.89 50.12 o 5 11 0 931.90 1266.11 156.58 o 7 11 0 3105.01 2590.48 226.51 o 9 11 0 32.03 77.11 91.37 o 11 11 0 781.77 711.74 92.73 o 0 12 0 77.40 99.88 44.58 o 2 12 0 2169.83 2774.80 116.62 o 4 12 0 3166.31 2948.56 238.01 o 6 12 0 0.52 60.39 83.85 o 8 12 0 15.05 134.02 91.93 o 10 12 0 161.53 38.72 93.50 o 1 13 0 7952.17 9073.26 313.43 o 3 13 0 152.31 124.02 51.17 o 5 13 0 5705.77 5489.90 380.84 o 7 13 0 23.38 67.68 90.02 o 9 13 0 836.69 607.24 136.60 o 11 13 0 323.52 153.89 113.25 o 0 14 0 10236.19 10724.43 519.97 o 2 14 0 24.06 36.26 31.62 o 4 14 0 12.88 86.99 51.55 o 6 14 0 423.95 543.26 126.95 o 8 14 0 133.59 223.70 106.07 o 10 14 0 228.48 178.58 118.08 o 1 15 0 4.78 12.52 34.17 o 3 15 0 1920.88 2635.60 245.93 o 5 15 0 623.32 883.14 156.13 o 7 15 0 42.46 -5.72 86.32 o 9 15 0 360.94 238.07 123.69 o 0 16 0 272.42 426.68 77.90 o 2 16 0 296.51 205.31 69.27 o 4 16 0 3290.23 4334.86 355.48 o 6 16 0 447.04 714.77 157.59 o 8 16 0 459.27 374.90 124.59 o 1 17 0 2608.97 2610.97 243.06 o 3 17 0 202.75 292.06 115.05 o 5 17 0 554.32 601.96 150.63 o 7 17 0 735.49 761.80 170.50 o 0 18 0 687.77 1226.15 167.24 o 2 18 0 3352.88 3453.46 214.00 o 4 18 0 244.31 292.28 125.60 o 6 18 0 189.83 245.25 128.86 o 8 18 0 553.64 633.17 173.42 o 1 19 0 265.11 80.86 143.62 o 3 19 0 1325.47 1714.64 223.48 o 5 19 0 62.39 247.61 136.83 o 7 19 0 55.21 134.92 136.38 o 0 20 0 59.65 -15.04 93.61 o 2 20 0 60.06 203.55 87.40 o 4 20 0 16.76 -14.82 104.61 o 6 20 0 422.78 267.25 146.03 o 1 21 0 779.38 585.06 114.14 o 3 21 0 477.17 413.96 154.45 o 0 22 0 33.14 -56.46 103.04 o 2 22 0 157.09 72.69 82.46 o 1 1 1 39623.39 43604.45 1285.76 o 2 1 1 1382.95 1276.36 93.99 o 3 1 1 289.30 594.60 29.42 o 4 1 1 517.71 588.35 33.06 o 5 1 1 3072.56 3117.20 105.76 o 6 1 1 262.09 216.47 30.34 o 7 1 1 4.90 6.43 20.81 o 8 1 1 1551.68 1453.92 70.88 o 9 1 1 3201.10 3321.04 127.27 o 10 1 1 4.74 14.25 30.81 o 11 1 1 622.43 653.17 59.23 o 12 1 1 27.12 112.36 46.60 o 13 1 1 166.99 203.06 54.24 o 0 2 1 43392.87 43751.04 1650.04 o 1 2 1 24157.80 27265.84 829.10 o 2 2 1 814.02 710.59 44.56 o 3 2 1 66.02 129.01 26.80 o 4 2 1 15.52 22.59 16.63 o 5 2 1 864.33 589.17 36.28 o 6 2 1 16205.11 19307.89 563.73 o 7 2 1 1285.93 1241.81 62.67 o 8 2 1 129.69 93.35 29.97 o 9 2 1 960.02 1064.51 64.34 o 10 2 1 906.71 991.73 65.63 o 11 2 1 486.92 467.66 56.54 o 12 2 1 657.96 749.52 75.72 o 13 2 1 8.02 -31.66 52.00 o 1 3 1 2365.00 2625.91 118.79 o 2 3 1 134.94 92.09 19.31 o 3 3 1 21049.51 25128.07 1759.71 o 4 3 1 786.32 1011.60 66.20 o 5 3 1 865.39 1082.04 62.02 o 6 3 1 801.85 842.80 47.92 o 7 3 1 393.07 366.34 36.81 o 8 3 1 713.74 772.08 51.38 o 9 3 1 734.91 847.78 58.31 o 10 3 1 71.12 98.46 50.41 o 11 3 1 652.00 685.64 62.41 o 12 3 1 7.98 28.78 46.91 o 13 3 1 7.38 135.50 55.67 o 0 4 1 10605.45 10421.69 431.97 o 1 4 1 11969.45 13502.27 361.72 o 2 4 1 27626.87 32351.46 1845.15 o 3 4 1 8598.69 9965.72 491.68 o 4 4 1 953.22 1460.66 86.93 o 5 4 1 363.68 246.14 40.08 o 6 4 1 1079.53 1163.04 69.60 o 7 4 1 826.78 902.91 52.39 o 8 4 1 1744.91 1877.54 83.70 o 9 4 1 457.29 474.50 52.05 o 10 4 1 3111.76 3366.80 133.38 o 11 4 1 16.12 49.37 37.98 o 12 4 1 541.27 557.40 62.73 o 13 4 1 172.10 120.89 67.28 o 1 5 1 2048.85 1832.91 72.51 o 2 5 1 6006.66 6597.01 497.45 o 3 5 1 2952.72 3985.87 268.94 o 4 5 1 1767.91 2490.90 181.55 o 5 5 1 36.31 0.29 29.39 o 6 5 1 49.16 101.06 39.41 o 7 5 1 324.05 340.21 38.96 o 8 5 1 2063.92 2129.84 92.65 o 9 5 1 176.74 157.52 39.37 o 10 5 1 2.95 30.42 33.67 o 11 5 1 99.86 62.00 41.64 o 12 5 1 21.12 77.67 45.42 o 13 5 1 28.17 -2.69 55.88 o 0 6 1 14572.96 15285.41 1060.81 o 1 6 1 580.34 805.88 31.38 o 2 6 1 8706.99 11095.46 504.37 o 3 6 1 591.27 1076.84 101.41 o 4 6 1 5994.50 6577.23 294.24 o 5 6 1 238.60 303.24 49.00 o 6 6 1 62.75 87.15 39.57 o 7 6 1 584.27 715.31 57.26 o 8 6 1 4565.18 5811.64 196.57 o 9 6 1 138.79 181.81 39.33 o 10 6 1 2.69 -16.16 31.53 o 11 6 1 16.48 27.97 39.36 o 12 6 1 429.36 527.37 63.04 o 13 6 1 95.69 39.18 58.34 o 1 7 1 686.29 904.26 42.61 o 2 7 1 1773.63 2784.99 167.15 o 3 7 1 44873.47 51631.62 2083.55 o 4 7 1 922.32 665.09 63.50 o 5 7 1 878.37 842.88 71.71 o 6 7 1 718.79 754.31 73.04 o 7 7 1 976.11 1193.00 96.67 o 8 7 1 77.83 26.86 35.70 o 9 7 1 636.02 605.12 54.13 o 10 7 1 3.09 -2.82 32.74 o 11 7 1 887.83 883.16 70.90 o 12 7 1 3.21 2.28 52.60 o 13 7 1 43.38 62.79 60.81 o 0 8 1 40.19 26.46 19.83 o 1 8 1 1192.80 1103.83 38.25 o 2 8 1 113.20 110.25 20.33 o 3 8 1 397.39 371.91 43.31 o 4 8 1 212.51 293.59 50.23 o 5 8 1 9.54 -25.19 31.77 o 6 8 1 1929.06 2145.26 131.91 o 7 8 1 124.22 199.32 57.18 o 8 8 1 468.12 601.86 84.46 o 9 8 1 45.04 50.47 36.28 o 10 8 1 1782.37 1810.30 94.51 o 11 8 1 370.56 379.33 55.98 o 12 8 1 0.08 49.05 53.24 o 1 9 1 9594.68 10791.14 431.95 o 2 9 1 18.02 25.14 15.72 o 3 9 1 74.16 71.49 31.26 o 4 9 1 889.12 912.16 78.11 o 5 9 1 810.92 951.54 126.39 o 6 9 1 158.41 220.45 54.15 o 7 9 1 4611.16 4743.65 299.35 o 8 9 1 12.92 -27.66 46.55 o 9 9 1 861.39 689.13 70.01 o 10 9 1 61.81 20.27 37.80 o 11 9 1 796.36 739.29 79.93 o 12 9 1 44.27 5.73 75.85 o 0 10 1 4164.66 4578.89 299.99 o 1 10 1 49.41 54.54 16.96 o 2 10 1 11081.49 13904.36 338.58 o 3 10 1 4419.15 4619.82 249.77 o 4 10 1 398.42 306.87 58.59 o 5 10 1 200.82 160.93 51.90 o 6 10 1 55.37 45.34 48.24 o 7 10 1 734.31 761.36 89.25 o 8 10 1 1186.03 1081.54 104.24 o 9 10 1 36.08 -8.76 69.09 o 10 10 1 255.71 224.67 49.38 o 11 10 1 26.13 -14.04 55.62 o 12 10 1 515.84 450.83 77.77 o 1 11 1 4163.45 4603.13 139.25 o 2 11 1 115.19 229.41 26.90 o 3 11 1 3210.99 3579.30 179.01 o 4 11 1 789.61 809.12 86.56 o 5 11 1 6255.85 7038.97 333.16 o 6 11 1 300.61 320.29 65.42 o 7 11 1 50.76 77.83 60.47 o 8 11 1 0.51 -13.04 47.15 o 9 11 1 257.84 296.49 74.08 o 10 11 1 47.24 -1.63 39.57 o 11 11 1 13.45 12.94 61.33 o 0 12 1 17643.81 21329.07 687.97 o 1 12 1 129.94 78.75 22.45 o 2 12 1 360.08 529.29 36.50 o 3 12 1 125.20 98.00 28.31 o 4 12 1 88.17 101.40 32.92 o 5 12 1 33.55 44.37 54.76 o 6 12 1 2309.48 2341.19 154.29 o 7 12 1 340.33 370.48 77.14 o 8 12 1 530.40 480.85 84.86 o 9 12 1 79.38 93.15 65.79 o 10 12 1 583.13 641.06 101.25 o 11 12 1 283.56 258.65 63.85 o 1 13 1 2873.77 3072.22 123.68 o 2 13 1 15.07 49.74 29.61 o 3 13 1 79.83 80.74 30.71 o 4 13 1 492.90 608.59 53.90 o 5 13 1 3.61 18.22 50.00 o 6 13 1 35.19 28.15 62.74 o 7 13 1 973.33 802.34 97.38 o 8 13 1 157.83 280.70 79.53 o 9 13 1 97.14 28.75 119.60 o 10 13 1 13.42 103.10 73.17 o 11 13 1 11.45 78.33 73.77 o 0 14 1 7688.29 8712.00 304.26 o 1 14 1 65.37 105.77 27.39 o 2 14 1 145.85 130.33 29.55 o 3 14 1 195.46 306.73 47.44 o 4 14 1 3485.72 3778.47 179.84 o 5 14 1 43.03 152.28 52.17 o 6 14 1 107.30 30.03 60.24 o 7 14 1 10.50 20.63 57.85 o 8 14 1 178.87 144.85 72.46 o 9 14 1 26.28 58.65 63.98 o 10 14 1 921.61 952.20 124.00 o 1 15 1 259.97 358.95 39.15 o 2 15 1 705.34 703.01 54.93 o 3 15 1 13.92 -0.45 44.75 o 4 15 1 375.93 359.51 63.21 o 5 15 1 4455.96 4717.63 261.94 o 6 15 1 180.03 96.91 67.72 o 7 15 1 339.53 240.53 79.76 o 8 15 1 282.17 319.57 86.82 o 9 15 1 456.47 329.34 102.70 o 10 15 1 30.40 132.77 84.88 o 0 16 1 3759.97 4221.10 206.37 o 1 16 1 303.75 417.20 46.24 o 2 16 1 651.23 766.72 56.69 o 3 16 1 25.08 -5.67 43.49 o 4 16 1 19.74 -5.40 60.47 o 5 16 1 123.29 73.36 120.49 o 6 16 1 43.93 -31.27 55.50 o 7 16 1 95.30 149.63 80.43 o 8 16 1 190.78 257.28 86.80 o 9 16 1 96.39 25.72 71.97 o 1 17 1 8.26 3.49 39.21 o 2 17 1 44.19 43.78 38.49 o 3 17 1 3385.73 3932.97 234.89 o 4 17 1 71.37 75.99 71.75 o 5 17 1 736.51 1049.02 127.06 o 6 17 1 17.86 -35.36 66.05 o 7 17 1 214.14 214.87 89.44 o 8 17 1 21.67 -16.82 72.94 o 0 18 1 879.92 1022.24 115.10 o 1 18 1 26.78 55.59 45.86 o 2 18 1 347.80 399.27 63.57 o 3 18 1 73.98 44.06 77.12 o 4 18 1 988.32 1183.51 131.47 o 5 18 1 41.62 22.95 72.21 o 6 18 1 247.62 120.72 94.12 o 7 18 1 0.00 -81.38 96.08 o 8 18 1 82.46 21.94 98.61 o 1 19 1 59.76 31.54 44.54 o 2 19 1 256.16 325.39 63.84 o 3 19 1 184.87 289.67 94.58 o 4 19 1 11.46 64.47 83.49 o 5 19 1 3.16 44.90 81.66 o 6 19 1 41.56 22.95 81.71 o 7 19 1 890.80 965.58 142.53 o 0 20 1 81.09 16.44 71.35 o 1 20 1 40.45 57.68 58.04 o 2 20 1 1347.81 1280.72 97.25 o 3 20 1 1.34 51.87 80.51 o 4 20 1 329.10 357.30 104.85 o 5 20 1 16.24 15.34 88.92 o 6 20 1 142.43 207.55 95.99 o 1 21 1 6.50 14.12 52.58 o 2 21 1 6.91 36.75 69.54 o 3 21 1 96.60 121.81 97.08 o 4 21 1 0.08 43.30 178.36 o 0 22 1 677.81 538.17 116.93 o 1 22 1 129.28 184.08 93.72 o 2 22 1 174.14 251.21 83.27 o 0 0 2 95275.90 51353.33 3565.88 o 1 0 2 29219.76 25373.52 1725.12 o 2 0 2 2346.43 2181.60 221.42 o 3 0 2 5783.73 6489.45 818.93 o 4 0 2 868.27 1091.61 65.18 o 5 0 2 229.27 67.17 35.92 o 6 0 2 8449.80 8319.91 360.47 o 7 0 2 890.99 824.47 68.59 o 8 0 2 172.63 135.21 45.72 o 9 0 2 2754.72 2811.88 159.73 o 10 0 2 146.41 201.54 61.72 o 11 0 2 678.72 662.84 87.75 o 12 0 2 185.12 203.35 72.04 o 13 0 2 38.26 18.83 67.14 o 1 1 2 366.35 319.97 20.93 o 2 1 2 10891.90 10742.28 849.54 o 3 1 2 337.47 443.54 54.29 o 4 1 2 1005.76 1061.27 45.47 o 5 1 2 6336.51 7827.22 237.39 o 6 1 2 2264.99 2743.72 99.10 o 7 1 2 2613.57 2855.66 105.59 o 8 1 2 4599.89 4808.58 164.31 o 9 1 2 62.21 73.94 31.88 o 10 1 2 101.43 86.93 37.51 o 11 1 2 7.94 39.21 38.94 o 12 1 2 121.83 136.92 47.58 o 13 1 2 291.62 317.54 69.06 o 0 2 2 5877.33 5715.31 175.15 o 1 2 2 2551.69 2263.80 98.45 o 2 2 2 105.92 52.12 16.95 o 3 2 2 14766.09 17146.29 569.62 o 4 2 2 6917.52 7846.20 271.55 o 5 2 2 2450.65 2802.33 98.16 o 6 2 2 1346.60 1541.65 66.26 o 7 2 2 153.84 165.19 30.59 o 8 2 2 679.42 718.47 50.26 o 9 2 2 35.66 40.54 38.55 o 10 2 2 713.29 769.04 60.06 o 11 2 2 1.19 37.74 55.65 o 12 2 2 151.05 136.26 49.07 o 13 2 2 57.89 79.97 60.17 o 1 3 2 6190.36 5561.67 510.07 o 2 3 2 157.80 118.07 21.52 o 3 3 2 4731.79 5683.25 641.87 o 4 3 2 2873.16 3685.18 138.06 o 5 3 2 12678.31 14503.34 492.12 o 6 3 2 179.91 144.33 27.80 o 7 3 2 3574.09 4233.76 145.60 o 8 3 2 3836.15 4045.14 143.42 o 9 3 2 942.55 948.81 62.60 o 10 3 2 91.98 99.61 36.58 o 11 3 2 136.73 189.65 45.77 o 12 3 2 202.25 190.98 51.36 o 13 3 2 361.49 328.57 70.06 o 0 4 2 14844.20 15344.44 483.60 o 1 4 2 0.20 35.79 17.69 o 2 4 2 13985.82 15404.45 548.17 o 3 4 2 763.59 987.81 56.32 o 4 4 2 830.19 1219.24 77.39 o 5 4 2 72.74 -21.10 36.14 o 6 4 2 2755.10 2846.27 120.16 o 7 4 2 156.11 223.47 33.01 o 8 4 2 285.27 306.67 39.14 o 9 4 2 2097.43 2291.48 99.82 o 10 4 2 341.47 319.72 47.48 o 11 4 2 969.41 966.44 69.81 o 12 4 2 0.03 48.79 51.42 o 13 4 2 102.25 47.58 60.00 o 1 5 2 1137.50 1328.67 62.68 o 2 5 2 5494.67 5991.94 191.86 o 3 5 2 25889.75 30424.94 1071.39 o 4 5 2 2355.18 2581.56 133.53 o 5 5 2 989.04 1220.03 83.04 o 6 5 2 2686.24 2588.73 113.30 o 7 5 2 1648.48 1966.93 83.59 o 8 5 2 612.95 580.37 49.50 o 9 5 2 2357.19 2573.26 109.28 o 10 5 2 527.87 590.88 57.12 o 11 5 2 333.40 314.46 50.70 o 12 5 2 27.01 1.33 46.94 o 13 5 2 49.26 46.09 59.68 o 0 6 2 2382.06 2104.28 217.34 o 1 6 2 7600.94 7881.85 209.89 o 2 6 2 6589.65 7014.70 403.32 o 3 6 2 5720.46 6374.00 333.93 o 4 6 2 13978.56 15211.24 637.03 o 5 6 2 3437.99 3192.74 182.62 o 6 6 2 407.09 429.94 59.16 o 7 6 2 249.27 308.26 44.84 o 8 6 2 100.73 145.10 44.33 o 9 6 2 333.40 336.41 46.54 o 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2 185.47 130.42 54.56 o 8 9 2 758.17 815.56 88.38 o 9 9 2 1401.14 1601.00 102.35 o 10 9 2 607.51 673.96 73.89 o 11 9 2 45.79 8.06 48.66 o 12 9 2 0.03 18.90 51.56 o 0 10 2 13227.63 16539.65 598.94 o 1 10 2 1998.91 2080.67 66.44 o 2 10 2 21.55 37.77 17.76 o 3 10 2 189.25 230.52 28.35 o 4 10 2 263.33 228.68 53.17 o 5 10 2 115.20 166.42 55.70 o 6 10 2 2267.73 2735.83 163.93 o 7 10 2 0.96 65.46 55.91 o 8 10 2 1035.62 855.89 93.45 o 9 10 2 28.59 39.92 43.60 o 10 10 2 312.75 210.97 53.59 o 11 10 2 344.27 378.85 67.15 o 12 10 2 293.62 334.08 68.92 o 1 11 2 4115.74 5168.31 140.68 o 2 11 2 108.72 171.24 23.50 o 3 11 2 494.86 589.51 38.33 o 4 11 2 252.50 226.80 59.56 o 5 11 2 1398.66 1437.17 158.83 o 6 11 2 65.17 -24.51 48.36 o 7 11 2 2804.65 3061.90 187.98 o 8 11 2 41.64 13.76 52.61 o 9 11 2 5.90 -18.30 49.83 o 10 11 2 10.17 -43.25 61.22 o 11 11 2 122.69 175.85 62.81 o 0 12 2 123.95 174.26 44.70 o 1 12 2 1416.16 1692.64 67.43 o 2 12 2 9.40 2.47 18.55 o 3 12 2 3618.94 3619.80 127.79 o 4 12 2 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14 131.08 237.96 96.50 o 0 4 14 100.46 80.03 93.16 o 1 4 14 413.20 616.42 85.14 o 2 4 14 13.23 7.06 51.10 o 3 4 14 16.37 23.68 65.11 o 4 4 14 14.13 -5.07 63.23 o 5 4 14 9.63 -35.06 59.55 o 6 4 14 66.90 101.93 65.98 o 7 4 14 1.52 51.99 60.21 o 1 5 14 689.24 732.35 111.78 o 2 5 14 2.48 21.55 69.54 o 3 5 14 6.43 81.07 71.15 o 4 5 14 261.56 448.35 119.15 o 5 5 14 60.00 109.55 58.96 o 6 5 14 79.11 118.01 63.22 o 7 5 14 363.36 463.43 84.27 o 0 6 14 618.55 779.53 156.69 o 1 6 14 48.51 -52.53 85.53 o 2 6 14 193.69 150.40 81.13 o 3 6 14 95.15 -0.35 106.18 o 4 6 14 84.47 82.91 93.72 o 5 6 14 0.11 5.31 75.95 o 6 6 14 259.91 357.79 74.65 o 7 6 14 128.53 96.14 65.27 o 1 7 14 60.68 78.62 73.93 o 2 7 14 73.97 12.42 66.23 o 3 7 14 30.92 -21.03 84.02 o 4 7 14 94.30 141.64 99.64 o 5 7 14 0.24 40.32 97.59 o 6 7 14 3.59 -11.00 214.50 o 7 7 14 34.23 63.27 62.97 o 0 8 14 668.86 590.63 144.46 o 1 8 14 21.49 10.33 101.92 o 2 8 14 141.69 227.04 84.63 o 3 8 14 346.46 476.89 116.79 o 4 8 14 63.58 144.35 197.21 o 5 8 14 3.41 44.90 192.50 o 6 8 14 191.08 93.54 89.23 o 1 9 14 104.33 119.59 77.57 o 2 9 14 19.37 -49.61 127.28 o 3 9 14 5.95 58.34 81.25 o 4 9 14 604.77 633.30 253.62 o 5 9 14 44.78 65.21 118.19 o 6 9 14 119.66 74.79 119.58 o 0 10 14 3.49 10.55 97.20 o 1 10 14 48.40 11.22 69.04 o 2 10 14 189.97 153.00 95.72 o 3 10 14 20.94 12.89 84.82 o 4 10 14 380.76 402.87 123.50 o 5 10 14 0.13 8.62 100.00 o 1 11 14 64.06 58.67 100.80 o 2 11 14 37.18 3.14 85.98 o 3 11 14 318.79 387.33 111.18 o 4 11 14 37.94 71.11 118.47 o 0 12 14 29.18 68.58 123.36 o 1 12 14 18.23 2.46 104.67 o 2 12 14 8.41 16.71 99.39 o 3 12 14 117.15 102.82 159.61 o 1 13 14 52.49 25.00 74.09 o 2 13 14 26.33 -1.98 85.88 o 1 1 15 24.99 52.26 54.67 o 2 1 15 207.99 324.21 68.58 o 3 1 15 547.62 780.30 81.86 o 4 1 15 7.58 69.02 58.64 o 5 1 15 386.31 646.13 107.10 o 6 1 15 63.26 36.60 68.63 o 7 1 15 159.16 110.45 85.94 o 0 2 15 45.47 92.67 82.34 o 1 2 15 634.50 1084.14 98.00 o 2 2 15 155.70 121.49 72.23 o 3 2 15 25.91 96.34 64.05 o 4 2 15 410.54 685.46 93.06 o 5 2 15 7.54 30.01 64.99 o 6 2 15 0.67 70.94 119.76 o 1 3 15 133.30 233.55 73.18 o 2 3 15 41.91 45.26 65.82 o 3 3 15 34.92 5.74 58.02 o 4 3 15 170.37 164.33 66.94 o 5 3 15 102.46 56.94 63.08 o 6 3 15 25.44 118.73 68.03 o 0 4 15 144.15 123.13 107.98 o 1 4 15 43.65 -12.64 69.42 o 2 4 15 66.53 177.98 94.62 o 3 4 15 185.86 234.29 78.95 o 4 4 15 208.91 227.77 115.47 o 5 4 15 3.55 88.21 75.29 o 6 4 15 489.46 898.69 111.58 o 1 5 15 4.27 -16.71 75.24 o 2 5 15 28.08 10.32 77.41 o 3 5 15 45.60 25.21 79.81 o 4 5 15 8.98 67.99 66.35 o 5 5 15 23.78 156.38 76.12 o 6 5 15 1.61 11.34 69.23 o 0 6 15 370.40 243.68 120.66 o 1 6 15 95.68 152.83 84.07 o 2 6 15 8.50 -7.81 63.47 o 3 6 15 39.28 141.75 93.92 o 4 6 15 40.46 131.82 101.73 o 5 6 15 0.27 80.27 110.24 o 6 6 15 177.65 156.58 87.48 o 1 7 15 133.66 44.58 73.63 o 2 7 15 9.52 25.84 70.95 o 3 7 15 0.80 59.22 84.97 o 4 7 15 115.41 261.27 112.76 o 5 7 15 426.89 468.19 200.41 o 0 8 15 29.06 11.22 98.89 o 1 8 15 10.37 27.42 75.92 o 2 8 15 127.83 137.59 86.54 o 3 8 15 314.15 301.24 111.02 o 4 8 15 12.10 87.27 119.99 o 5 8 15 14.35 -38.79 90.07 o 1 9 15 43.11 85.06 82.28 o 2 9 15 46.07 -53.39 78.80 o 3 9 15 242.23 186.60 162.81 o 4 9 15 47.20 99.37 99.34 o 0 10 15 5.92 32.10 109.66 o 1 10 15 15.34 -40.58 72.83 o 2 10 15 7.07 -59.64 69.61 o 3 10 15 260.04 161.95 105.39 o 1 11 15 28.32 14.45 79.98 o 2 11 15 46.20 46.11 82.01 o 0 0 16 877.64 965.64 195.98 o 1 0 16 125.28 415.40 181.72 o 2 0 16 213.60 103.67 94.50 o 3 0 16 4.98 64.59 99.48 o 4 0 16 595.57 906.26 249.52 o 5 0 16 73.33 25.70 209.90 o 1 1 16 5.45 14.10 68.17 o 2 1 16 19.74 2.76 72.90 o 3 1 16 199.46 231.09 100.73 o 4 1 16 24.18 85.40 93.14 o 5 1 16 0.64 77.59 82.81 o 0 2 16 5.46 14.59 110.00 o 1 2 16 3.53 56.31 73.13 o 2 2 16 14.41 59.49 99.11 o 3 2 16 3.16 -43.79 103.20 o 4 2 16 180.61 361.42 114.41 o 5 2 16 0.01 10.16 81.95 o 1 3 16 0.72 56.69 87.58 o 2 3 16 2.23 -49.43 78.33 o 3 3 16 312.60 446.53 116.36 o 4 3 16 16.61 22.17 71.01 o 5 3 16 165.90 107.62 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