#------------------------------------------------------------------------------
#$Date: 2016-04-02 21:28:50 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180785 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/16/2011692.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2011692_Fobs
loop_
_publ_author_name
'Ar\?ic\?i, Cengiz'
'Svoboda, Ingrid'
'Sar\?i, Musa'
'Atakol, Orhan'
'Fuess, Hartmut'
_publ_section_title
;
 {Bis(<i>N</i>,<i>N</i>-dimethylformamide)[\m-<i>N</i>,<i>N</i>'-bis(salicylidene)-1,3-propanediaminato]nickel(II)}dibromozinc(II)
;
_journal_issue                   1
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              31
_journal_page_last               32
_journal_volume                  57
_journal_year                    2001
_space_group_IT_number           9
_symmetry_space_group_name_Hall  'C -2yc'
_symmetry_space_group_name_H-M   'C 1 c 1'
_exptl_crystal_F_000             1424.00
_cod_data_source_file            da1133Isup2.hkl
_cod_data_source_block           I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     ' DA1133 '
_shelx_refln_list_code           4
_shelx_f_calc_maximum            448.44
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
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1 1 -21 18.41 60.49 68.97 o
0 2 -21 448.54 516.31 39.70 o
2 2 -21 131.10 138.22 30.93 o
1 3 -21 617.37 647.78 40.52 o
-2 0 -20 1111.63 1082.89 42.18 o
0 0 -20 262.73 186.41 35.04 o
2 0 -20 184.42 169.16 27.37 o
-3 1 -20 181.74 172.44 43.79 o
-1 1 -20 521.34 528.11 39.42 o
1 1 -20 890.71 925.31 33.96 o
-2 2 -20 27.41 78.28 83.75 o
0 2 -20 311.33 312.61 37.23 o
2 2 -20 661.64 694.08 30.12 o
-1 3 -20 460.94 535.21 41.61 o
1 3 -20 810.90 843.11 38.61 o
-2 4 -20 181.27 129.19 45.16 o
0 4 -20 80.93 42.70 82.38 o
-1 5 -20 80.38 58.85 90.32 o
1 5 -20 1282.88 1311.17 45.47 o
0 6 -20 434.91 380.25 43.53 o
1 7 -20 343.48 307.96 40.79 o
-3 1 -19 283.11 214.61 42.16 o
-1 1 -19 994.39 1011.65 38.34 o
1 1 -19 190.44 211.04 29.56 o
-4 2 -19 69.40 -3.01 91.69 o
-2 2 -19 1112.02 1099.35 42.72 o
0 2 -19 1165.40 1177.74 39.71 o
2 2 -19 1146.13 1066.26 32.05 o
-3 3 -19 93.96 88.41 44.07 o
-1 3 -19 405.90 399.14 38.60 o
1 3 -19 669.48 637.42 36.42 o
-2 4 -19 532.28 522.91 44.35 o
0 4 -19 463.05 552.46 39.70 o
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-1 5 -19 23.33 65.41 40.51 o
1 5 -19 125.98 -22.72 81.29 o
-2 6 -19 78.27 124.26 38.04 o
0 6 -19 359.71 304.13 40.79 o
-1 7 -19 102.94 41.88 35.58 o
1 7 -19 1069.65 855.01 39.71 o
0 8 -19 138.73 70.89 37.77 o
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-2 0 -18 1895.89 1846.68 57.82 o
0 0 -18 3749.46 3950.34 81.22 o
2 0 -18 137.08 151.09 23.81 o
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-3 1 -18 16.68 70.34 78.82 o
-1 1 -18 1257.74 1307.41 47.39 o
1 1 -18 629.00 593.61 29.57 o
-4 2 -18 366.60 325.76 44.35 o
-2 2 -18 185.44 225.55 36.95 o
0 2 -18 99.20 89.78 32.57 o
2 2 -18 1052.72 1009.26 33.41 o
-5 3 -18 291.17 308.77 42.43 o
-3 3 -18 461.33 463.21 42.43 o
-1 3 -18 889.18 922.87 39.98 o
1 3 -18 797.59 868.06 34.78 o
-4 4 -18 106.06 47.62 82.39 o
-2 4 -18 389.96 345.75 40.24 o
0 4 -18 388.22 367.66 37.50 o
-3 5 -18 471.46 404.63 38.87 o
-1 5 -18 365.54 359.44 38.60 o
1 5 -18 537.14 525.12 39.70 o
-4 6 -18 741.01 603.75 44.63 o
-2 6 -18 409.81 334.53 36.41 o
0 6 -18 223.24 137.96 35.86 o
-3 7 -18 109.40 18.06 78.83 o
-1 7 -18 587.01 500.76 35.59 o
1 7 -18 120.76 171.34 33.94 o
-2 8 -18 380.50 313.72 39.42 o
0 8 -18 710.50 619.63 38.06 o
-1 9 -18 517.41 529.20 38.60 o
1 9 -18 340.41 349.30 35.59 o
0 10 -18 9.96 50.09 73.62 o
-5 1 -17 281.34 128.38 42.70 o
-3 1 -17 269.07 259.50 37.50 o
-1 1 -17 3612.57 3586.44 82.59 o
1 1 -17 1642.19 1729.01 53.71 o
-6 2 -17 215.34 110.04 42.43 o
-4 2 -17 1244.02 1180.26 43.55 o
-2 2 -17 66.39 112.76 35.85 o
0 2 -17 2640.76 2828.10 79.24 o
2 2 -17 1176.26 1188.26 41.64 o
-5 3 -17 288.09 220.36 40.51 o
-3 3 -17 976.30 990.01 42.17 o
-1 3 -17 994.32 981.57 38.62 o
1 3 -17 313.51 367.10 32.03 o
-4 4 -17 985.84 857.45 40.53 o
-2 4 -17 1386.47 1358.20 41.91 o
0 4 -17 1919.11 1996.19 66.87 o
-5 5 -17 156.18 197.62 43.79 o
-3 5 -17 1131.75 945.46 39.71 o
-1 5 -17 973.68 710.68 37.79 o
1 5 -17 23.83 -58.02 76.09 o
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0 6 -17 93.54 114.41 30.65 o
-3 7 -17 529.53 328.53 37.23 o
-1 7 -17 18.51 27.37 67.60 o
1 7 -17 486.29 410.66 33.13 o
-4 8 -17 79.19 84.03 38.87 o
-2 8 -17 310.91 298.92 36.68 o
0 8 -17 1344.40 1270.46 38.35 o
-3 9 -17 179.16 220.07 39.14 o
-1 9 -17 366.99 366.55 36.68 o
1 9 -17 738.67 801.46 34.50 o
-2 10 -17 112.15 184.75 37.50 o
0 10 -17 741.23 896.46 36.69 o
-1 11 -17 22.04 -59.66 74.44 o
1 11 -17 134.98 166.96 32.30 o
-6 0 -16 812.73 652.80 43.54 o
-4 0 -16 902.52 747.35 39.43 o
-2 0 -16 1843.81 1802.98 57.82 o
0 0 -16 5477.72 5773.91 81.35 o
2 0 -16 922.39 908.18 30.95 o
-7 1 -16 183.57 140.69 42.15 o
-5 1 -16 467.71 469.24 40.24 o
-3 1 -16 1620.88 1698.78 55.07 o
-1 1 -16 942.78 1064.84 33.14 o
1 1 -16 1498.59 1587.82 49.32 o
-6 2 -16 72.64 -35.03 40.78 o
-4 2 -16 678.43 635.79 39.98 o
-2 2 -16 761.00 776.33 36.69 o
0 2 -16 188.01 200.64 29.56 o
2 2 -16 1292.52 1171.15 38.63 o
-5 3 -16 516.82 561.79 39.42 o
-3 3 -16 1764.98 1723.85 60.56 o
-1 3 -16 981.14 1073.62 37.25 o
1 3 -16 201.15 173.82 30.11 o
-6 4 -16 58.99 -6.30 43.79 o
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-2 4 -16 166.66 143.43 35.31 o
0 4 -16 1735.30 1829.45 57.00 o
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1 5 -16 1396.93 1419.68 44.93 o
-6 6 -16 63.94 95.25 44.89 o
-4 6 -16 1402.97 1277.89 42.46 o
-2 6 -16 1982.88 1586.77 41.66 o
0 6 -16 370.18 316.74 30.66 o
-5 7 -16 34.19 61.03 84.02 o
-3 7 -16 189.98 185.04 34.49 o
-1 7 -16 27.08 -4.93 64.04 o
1 7 -16 2263.27 2230.19 64.97 o
-4 8 -16 287.15 203.11 38.05 o
-2 8 -16 85.99 132.47 34.21 o
0 8 -16 1196.10 1297.77 34.79 o
-3 9 -16 53.23 114.95 37.50 o
-1 9 -16 570.98 700.90 33.95 o
1 9 -16 1037.24 1174.64 36.70 o
-2 10 -16 129.76 133.02 35.86 o
0 10 -16 463.18 516.87 32.58 o
-1 11 -16 310.33 396.10 36.13 o
1 11 -16 1169.83 1222.08 39.44 o
0 12 -16 909.76 1094.52 37.52 o
-7 1 -15 365.86 332.33 41.61 o
-5 1 -15 1355.20 1096.84 40.54 o
-3 1 -15 849.92 799.12 36.97 o
-1 1 -15 2485.35 2505.53 71.57 o
1 1 -15 5175.86 5337.94 68.71 o
-6 2 -15 308.87 264.43 38.87 o
-4 2 -15 1639.28 1673.05 49.05 o
-2 2 -15 173.19 202.28 32.85 o
0 2 -15 452.58 499.93 29.30 o
2 2 -15 726.27 712.55 23.55 o
-7 3 -15 264.89 288.79 45.17 o
-5 3 -15 207.73 186.41 36.68 o
-3 3 -15 1795.05 1691.38 50.42 o
-1 3 -15 356.77 389.56 33.40 o
1 3 -15 3269.40 3705.12 75.73 o
-6 4 -15 709.96 730.25 43.54 o
-4 4 -15 16.24 -66.51 71.43 o
-2 4 -15 1274.72 1172.48 35.61 o
0 4 -15 4678.31 5055.29 95.31 o
-7 5 -15 68.86 -73.35 94.97 o
-5 5 -15 40.77 38.59 38.59 o
-3 5 -15 1375.37 1323.18 38.63 o
-1 5 -15 2418.50 1899.22 58.40 o
1 5 -15 28.44 2.74 66.51 o
-6 6 -15 192.01 229.38 43.52 o
-4 6 -15 282.59 236.24 36.41 o
-2 6 -15 304.05 261.70 30.93 o
0 6 -15 91.66 50.64 28.74 o
-5 7 -15 508.17 422.43 38.60 o
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1 7 -15 260.79 297.83 28.47 o
-6 8 -15 353.80 303.86 41.88 o
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-2 8 -15 208.51 227.74 32.30 o
0 8 -15 2610.20 2804.08 75.67 o
-5 9 -15 167.62 85.13 39.69 o
-3 9 -15 1099.03 1138.24 38.62 o
-1 9 -15 13.84 27.37 30.38 o
1 9 -15 2949.48 3250.24 71.03 o
-4 10 -15 570.49 634.35 39.70 o
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0 10 -15 668.45 808.00 31.49 o
-3 11 -15 13.10 19.16 35.85 o
-1 11 -15 72.01 101.00 32.02 o
1 11 -15 401.24 480.99 29.57 o
-2 12 -15 295.33 325.20 36.13 o
0 12 -15 238.18 310.68 31.48 o
-1 13 -15 70.55 4.38 70.34 o
1 13 -15 975.10 1015.70 34.78 o
-8 0 -14 144.97 78.28 87.31 o
-6 0 -14 2421.83 1907.67 70.18 o
-4 0 -14 4182.54 4123.18 92.79 o
-2 0 -14 600.20 573.93 27.66 o
0 0 -14 3097.95 3347.50 61.74 o
2 0 -14 15844.37 15392.19 95.70 o
-7 1 -14 10.37 -12.86 84.30 o
-5 1 -14 431.91 419.69 36.14 o
-3 1 -14 611.69 661.27 33.95 o
-1 1 -14 3717.03 3988.37 74.12 o
1 1 -14 2685.43 2889.65 53.77 o
-8 2 -14 188.99 225.54 46.81 o
-6 2 -14 628.44 563.48 38.88 o
-4 2 -14 518.69 511.99 35.05 o
-2 2 -14 1709.50 1827.16 52.89 o
0 2 -14 1340.19 1398.75 42.47 o
2 2 -14 56.65 32.84 17.52 o
-7 3 -14 289.29 287.42 43.25 o
-5 3 -14 777.59 824.24 38.61 o
-3 3 -14 432.77 408.20 32.31 o
-1 3 -14 3307.52 3516.98 80.95 o
1 3 -14 1187.82 1334.18 41.92 o
-8 4 -14 5.04 61.03 94.97 o
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-3 5 -14 735.70 644.06 33.41 o
-1 5 -14 2072.60 1668.62 53.73 o
1 5 -14 2726.97 2525.88 73.51 o
-6 6 -14 702.16 654.13 42.44 o
-4 6 -14 259.62 245.54 33.40 o
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0 6 -14 1255.72 1074.17 36.16 o
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0 8 -14 475.44 506.22 28.75 o
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-3 9 -14 12.73 -20.25 66.78 o
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1 9 -14 2023.33 2184.68 60.57 o
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1 11 -14 1816.66 2025.25 62.20 o
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0 12 -14 292.48 313.43 29.29 o
-1 13 -14 1226.29 1421.50 45.47 o
1 13 -14 78.50 48.44 60.21 o
0 14 -14 489.70 478.00 32.85 o
-9 1 -13 427.75 333.98 48.18 o
-7 1 -13 159.81 137.41 40.24 o
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-3 1 -13 342.52 369.03 29.57 o
-1 1 -13 4952.76 5532.33 77.52 o
1 1 -13 3743.11 3975.21 54.93 o
-8 2 -13 340.89 352.31 46.26 o
-6 2 -13 212.01 -39.96 79.93 o
-4 2 -13 204.65 237.60 31.48 o
-2 2 -13 5469.19 6112.69 92.11 o
0 2 -13 4277.93 4678.50 73.35 o
2 2 -13 3058.82 3113.28 46.93 o
-7 3 -13 239.30 202.83 42.15 o
-5 3 -13 2239.03 2250.87 71.55 o
-3 3 -13 746.90 777.19 31.22 o
-1 3 -13 6014.19 6606.06 94.09 o
1 3 -13 1540.86 1682.75 50.98 o
-8 4 -13 184.72 153.01 46.81 o
-6 4 -13 910.85 1026.14 40.80 o
-4 4 -13 2101.24 2133.18 68.80 o
-2 4 -13 1988.44 1942.22 59.76 o
0 4 -13 2449.13 2491.70 71.03 o
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-1 5 -13 4543.56 3778.34 76.09 o
1 5 -13 704.11 653.95 25.74 o
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-6 6 -13 128.38 136.03 38.59 o
-4 6 -13 715.26 589.00 32.31 o
-2 6 -13 407.25 330.72 28.75 o
0 6 -13 17.83 13.68 50.36 o
-7 7 -13 531.48 575.75 43.80 o
-5 7 -13 1769.84 1430.07 37.81 o
-3 7 -13 1560.97 1342.86 41.37 o
-1 7 -13 3840.71 3777.92 74.11 o
1 7 -13 638.42 762.88 24.92 o
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-4 8 -13 1327.71 1396.24 44.65 o
-2 8 -13 261.42 274.01 29.02 o
0 8 -13 327.80 347.12 26.01 o
-7 9 -13 37.87 -43.79 81.83 o
-5 9 -13 705.25 700.95 37.51 o
-3 9 -13 1035.66 992.82 33.14 o
-1 9 -13 1888.14 2117.38 57.28 o
1 9 -13 1285.92 1316.31 41.91 o
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-4 10 -13 484.09 499.63 34.50 o
-2 10 -13 1335.79 1549.66 44.65 o
0 10 -13 527.25 630.81 26.83 o
-5 11 -13 86.71 77.18 37.77 o
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1 11 -13 81.63 11.22 50.91 o
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1 13 -13 1048.69 1109.99 33.96 o
-2 14 -13 958.64 1095.92 37.52 o
0 14 -13 577.86 715.40 31.76 o
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-2 2 -12 1611.78 1817.18 57.01 o
0 2 -12 4538.28 5346.21 72.84 o
2 2 -12 1446.51 1322.94 36.18 o
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-5 3 -12 946.79 1081.01 37.52 o
-3 3 -12 1506.24 1410.73 44.39 o
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0 4 -12 1067.54 948.98 30.96 o
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0 12 -12 227.25 323.82 26.55 o
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1 13 -12 1703.61 1943.14 53.70 o
-2 14 -12 221.18 256.75 33.12 o
0 14 -12 948.88 967.51 31.49 o
-1 15 -12 380.05 355.05 32.30 o
1 15 -12 20.19 51.73 58.84 o
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1 1 -11 7556.80 8270.24 64.56 o
-8 2 -11 1055.22 1172.20 45.19 o
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2 2 -11 1502.08 1524.36 34.54 o
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-1 1 20 878.38 917.36 33.96 o
1 1 20 548.70 659.54 43.80 o
-6 2 20 23.68 2.74 28.46 o
-4 2 20 4.64 8.48 55.01 o
-2 2 20 722.18 758.18 30.94 o
0 2 20 287.62 292.90 36.41 o
2 2 20 23.29 58.30 86.49 o
-5 3 20 613.19 594.67 29.57 o
-3 3 20 899.28 811.11 30.67 o
-1 3 20 762.54 654.15 33.95 o
1 3 20 444.03 523.16 41.34 o
-6 4 20 140.12 122.90 29.01 o
-4 4 20 527.24 505.94 29.29 o
-2 4 20 39.18 58.57 60.49 o
0 4 20 58.08 58.57 35.03 o
2 4 20 181.57 168.34 42.15 o
-5 5 20 193.30 238.41 28.74 o
-3 5 20 240.39 265.52 29.56 o
-1 5 20 1246.60 1310.86 38.07 o
1 5 20 88.79 -26.28 79.92 o
-4 6 20 56.17 55.56 59.12 o
-2 6 20 1037.43 1115.70 34.78 o
0 6 20 470.66 465.95 36.14 o
-3 7 20 94.86 117.14 30.11 o
-1 7 20 346.10 403.77 33.67 o
-5 1 21 473.85 468.41 30.11 o
-3 1 21 414.74 437.46 30.39 o
-1 1 21 21.35 -42.97 68.97 o
1 1 21 186.19 219.25 43.25 o
-4 2 21 1827.33 1634.33 47.67 o
-2 2 21 115.63 41.06 63.23 o
0 2 21 437.26 549.98 39.15 o
-3 3 21 86.12 99.90 29.29 o
-1 3 21 625.96 648.88 35.87 o
-2 4 21 888.57 977.85 34.23 o