#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/17/2011729.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011729_Fobs loop_ _publ_author_name 'Janczak, Jan' 'Kubiak, Ryszard' _publ_section_title ; [Phthalocyaninato(2--)]antimony(III) chloride ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 55 _journal_page_last 57 _journal_volume 57 _journal_year 2001 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 91.960 _cell_angle_beta 96.210 _cell_angle_gamma 92.370 _cell_length_a 9.5600 _cell_length_b 10.8060 _cell_length_c 12.4620 _exptl_crystal_F_000 664.00 _reflns_d_resolution_high 0.7214 _[local]_cod_data_source_file na1489Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sbpcicl in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 240.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 3595.92 3648.61 64.73 o 5 0 0 2164.38 2140.36 45.33 o 6 0 0 29.21 2.11 23.13 o 7 0 0 206.62 156.81 20.54 o 8 0 0 139.19 138.30 15.75 o 9 0 0 204.52 166.26 20.05 o 10 0 0 5.16 10.28 31.90 o 11 0 0 31.85 22.43 38.41 o 12 0 0 0.96 14.70 42.27 o -12 1 0 0.14 14.70 42.21 o -11 1 0 35.32 18.19 34.59 o -10 1 0 166.57 109.99 24.09 o -9 1 0 421.90 406.20 38.01 o -8 1 0 28.08 21.89 15.89 o -7 1 0 305.97 293.11 20.64 o -6 1 0 270.19 235.63 21.40 o -5 1 0 272.36 262.84 14.59 o -4 1 0 539.31 540.49 17.52 o -3 1 0 3097.41 3007.02 36.93 o -2 1 0 122.25 141.32 19.62 o 3 1 0 0.42 18.52 11.04 o 4 1 0 30.16 42.81 9.21 o 5 1 0 5226.50 5327.91 56.13 o 6 1 0 2371.53 2369.32 50.72 o 7 1 0 8.36 11.04 22.97 o 8 1 0 92.88 71.23 19.06 o 9 1 0 543.99 600.89 40.44 o 10 1 0 71.40 70.79 21.14 o 11 1 0 0.34 3.70 50.60 o 12 1 0 6.08 0.82 68.52 o -12 2 0 4.73 14.13 69.78 o -11 2 0 3.20 0.34 39.54 o -10 2 0 10.67 4.10 28.99 o -9 2 0 401.62 384.21 32.64 o -8 2 0 116.23 132.28 18.97 o -6 2 0 989.00 1030.24 39.77 o -5 2 0 3539.66 3490.12 50.92 o -4 2 0 1067.49 1006.19 26.99 o -3 2 0 224.72 205.20 10.95 o -2 2 0 27770.38 27194.18 96.91 o 2 2 0 3995.09 3991.76 52.81 o 3 2 0 959.22 999.37 41.42 o 4 2 0 50.06 75.56 11.33 o 5 2 0 1645.18 1694.60 33.18 o 6 2 0 926.43 920.74 30.18 o 7 2 0 661.16 546.15 123.78 o 8 2 0 10.07 2.24 28.17 o 9 2 0 326.53 242.97 39.97 o 10 2 0 191.08 208.69 32.24 o 11 2 0 64.71 30.72 42.20 o 12 2 0 0.44 11.17 73.19 o -12 3 0 10.76 7.00 64.29 o -11 3 0 35.10 73.19 31.18 o -10 3 0 28.42 13.88 31.53 o -9 3 0 57.14 12.35 25.09 o -8 3 0 401.63 383.58 26.44 o -7 3 0 177.80 158.72 18.68 o -6 3 0 80.55 71.71 12.87 o -5 3 0 1954.08 1998.94 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