#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:30:06 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180786 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/17/2011745.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011745_Fobs loop_ _publ_author_name 'Casta\~neda, Fernando' 'Terraza, Claudio A.' 'Garland, Maria Teresa' 'Bunton, Clifford A.' 'Baggio, Ricardo F.' _publ_section_title ; Methyl, ethyl, isopropyl and tert-butyl 3-oxo-2-(triphenylphosphoranylidene)butyrates, a common pattern for a preferred conformation ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 180 _journal_page_last 184 _journal_volume 57 _journal_year 2001 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.9325 _cell_length_b 16.3429 _cell_length_c 17.7804 _exptl_crystal_F_000 1712.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file bk1566IVsup4.hkl _cod_data_source_block IV #BEGIN Tags that were not found in dictionaries: _shelx_refln_list_code 4 _shelx_f_calc_maximum 317.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 100867.49 100115.24 335.85 o 4 0 0 2523.30 2556.06 62.29 o 6 0 0 0.79 101.44 53.49 o 8 0 0 992.93 887.12 65.25 o 10 0 0 444.82 296.60 78.89 o 12 0 0 502.70 328.83 95.41 o 14 0 0 1492.69 1580.46 98.27 o 16 0 0 434.64 353.84 100.25 o 2 1 0 994.17 996.76 36.98 o 4 1 0 5244.71 5266.26 67.13 o 6 1 0 8229.76 8613.64 83.74 o 8 1 0 3054.46 2886.17 71.08 o 10 1 0 5950.98 5402.79 97.28 o 12 1 0 1503.90 1503.25 99.26 o 14 1 0 140.11 143.06 89.57 o 16 1 0 0.94 90.17 100.25 o 0 2 0 28540.86 29949.16 158.68 o 2 2 0 1565.21 1457.57 43.80 o 4 2 0 28390.66 28511.37 157.69 o 6 2 0 5018.26 5137.93 68.12 o 8 2 0 2087.97 2078.15 71.08 o 10 2 0 54.10 33.32 74.05 o 12 2 0 309.35 293.73 90.56 o 14 2 0 171.01 46.27 90.56 o 16 2 0 380.71 435.50 99.26 o 2 3 0 21751.16 21784.87 135.35 o 4 3 0 19664.44 19425.55 123.68 o 6 3 0 4266.88 4464.95 67.13 o 8 3 0 369.45 422.85 56.45 o 10 3 0 657.80 617.31 82.75 o 12 3 0 1029.29 995.67 90.56 o 14 3 0 326.93 223.53 88.58 o 16 3 0 21.95 90.46 96.39 o 0 4 0 7407.83 7377.82 67.13 o 2 4 0 2972.98 2746.87 58.43 o 4 4 0 406.82 325.86 51.61 o 6 4 0 33.52 -5.04 51.61 o 8 4 0 1384.63 1496.72 68.12 o 10 4 0 382.64 364.12 75.93 o 12 4 0 249.63 407.03 88.58 o 14 4 0 73.80 156.70 84.73 o 16 4 0 13.95 37.77 97.28 o 2 5 0 24149.93 23771.17 132.38 o 4 5 0 276.07 200.00 49.63 o 6 5 0 1211.48 1129.04 60.31 o 8 5 0 129.92 95.70 61.30 o 10 5 0 652.16 491.46 80.77 o 12 5 0 274.42 319.04 90.56 o 14 5 0 65.30 -59.32 84.73 o 16 5 0 116.77 44.29 98.27 o 0 6 0 11298.40 11861.66 90.56 o 2 6 0 3183.63 3194.14 59.32 o 4 6 0 93.16 117.75 51.61 o 6 6 0 947.53 973.53 59.32 o 8 6 0 2154.39 2380.18 74.05 o 10 6 0 663.01 666.25 85.72 o 12 6 0 512.07 453.40 88.58 o 14 6 0 765.80 665.56 91.55 o 16 6 0 183.82 54.47 87.59 o 2 7 0 1654.82 1700.29 57.44 o 4 7 0 1149.98 996.07 56.45 o 6 7 0 727.23 601.69 59.32 o 8 7 0 0.16 69.21 63.27 o 10 7 0 427.12 374.01 83.74 o 12 7 0 107.21 83.54 83.74 o 14 7 0 3.83 29.86 88.58 o 16 7 0 0.60 35.49 94.42 o 0 8 0 2474.17 2534.81 63.27 o 2 8 0 8674.90 8889.18 90.56 o 4 8 0 3299.45 3566.76 74.94 o 6 8 0 185.55 204.26 60.31 o 8 8 0 713.99 567.39 74.94 o 10 8 0 1689.93 1546.15 92.44 o 12 8 0 117.66 4.45 80.77 o 14 8 0 32.21 213.25 94.42 o 16 8 0 97.98 263.77 99.26 o 2 9 0 406.55 453.10 57.44 o 4 9 0 3013.44 3139.17 70.10 o 6 9 0 999.92 1073.97 72.07 o 8 9 0 164.42 164.02 72.07 o 10 9 0 263.70 177.76 86.61 o 12 9 0 272.73 224.03 84.73 o 14 9 0 15.49 36.48 88.58 o 0 10 0 28.11 84.33 52.60 o 2 10 0 1125.94 1260.63 63.27 o 4 10 0 195.35 117.75 60.31 o 6 10 0 74.98 114.29 66.24 o 8 10 0 245.00 165.80 80.77 o 10 10 0 893.53 1050.44 93.43 o 12 10 0 470.57 453.40 90.56 o 14 10 0 6.07 90.56 93.43 o 2 11 0 451.98 403.67 61.30 o 4 11 0 528.42 371.24 67.13 o 6 11 0 23.16 56.75 69.11 o 8 11 0 1.31 43.30 76.92 o 10 11 0 45.98 88.29 80.77 o 12 11 0 80.18 120.22 83.74 o 14 11 0 58.08 134.16 90.56 o 0 12 0 15.71 -55.76 61.30 o 2 12 0 98.47 79.49 65.25 o 4 12 0 133.76 116.86 74.05 o 6 12 0 5.84 -76.13 79.88 o 8 12 0 506.40 472.18 80.77 o 10 12 0 6.02 118.54 79.88 o 12 12 0 64.01 250.03 87.59 o 2 13 0 620.72 665.76 74.05 o 4 13 0 52.82 88.48 74.05 o 6 13 0 3.96 -72.17 77.91 o 8 13 0 194.29 254.97 74.94 o 10 13 0 109.70 162.53 85.72 o 12 13 0 14.00 121.41 86.61 o 0 14 0 1077.11 867.44 79.88 o 2 14 0 2269.74 2330.65 94.42 o 4 14 0 286.23 368.47 77.91 o 6 14 0 80.79 48.05 77.91 o 8 14 0 0.06 0.99 76.92 o 10 14 0 90.59 205.05 86.61 o 12 14 0 92.35 36.09 93.43 o 2 15 0 135.66 35.10 73.06 o 4 15 0 355.70 253.10 75.93 o 6 15 0 478.66 594.38 82.75 o 8 15 0 66.77 14.34 83.74 o 10 15 0 3.83 -38.95 90.56 o 0 16 0 1020.74 882.47 82.75 o 2 16 0 116.82 26.20 79.88 o 4 16 0 429.42 512.81 86.61 o 6 16 0 794.08 740.60 84.73 o 8 16 0 572.69 506.49 94.42 o 10 16 0 377.32 472.28 90.56 o 2 17 0 1460.65 1695.24 92.44 o 4 17 0 696.89 673.77 86.61 o 6 17 0 194.72 158.68 89.57 o 8 17 0 47.50 54.77 77.91 o 0 18 0 156.81 104.90 90.56 o 2 18 0 40.39 -55.27 87.59 o 4 18 0 64.34 -13.74 85.72 o 6 18 0 138.86 215.92 92.44 o 2 19 0 1.03 -6.23 91.55 o 1 1 1 0.42 3.26 27.29 o 2 1 1 787.27 925.97 37.96 o 3 1 1 3651.30 3417.28 58.43 o 4 1 1 12659.62 13173.90 100.25 o 5 1 1 410.90 443.81 52.60 o 6 1 1 114.73 111.12 52.60 o 7 1 1 54.92 248.25 56.45 o 8 1 1 396.01 416.91 63.27 o 9 1 1 41.22 -7.71 65.25 o 10 1 1 107.18 35.49 74.05 o 11 1 1 747.07 662.20 87.59 o 12 1 1 222.02 198.42 87.59 o 13 1 1 98.13 186.95 89.57 o 14 1 1 27.35 101.83 85.72 o 15 1 1 23.66 143.65 92.44 o 16 1 1 6.26 19.67 102.23 o 17 1 1 2.40 -42.61 98.27 o 0 2 1 23654.52 22304.70 111.03 o 1 2 1 5315.57 5315.29 51.61 o 2 2 1 16303.75 16868.79 104.11 o 3 2 1 3180.66 3569.73 60.31 o 4 2 1 342.45 379.94 51.61 o 5 2 1 471.33 387.06 52.60 o 6 2 1 258.55 271.39 52.60 o 7 2 1 612.25 649.45 59.32 o 8 2 1 1617.55 1631.08 67.13 o 9 2 1 304.57 420.28 65.25 o 10 2 1 14.55 82.85 76.92 o 11 2 1 1.71 86.80 86.61 o 12 2 1 74.82 16.81 87.59 o 13 2 1 421.38 379.25 88.58 o 14 2 1 334.54 217.21 90.56 o 15 2 1 532.82 462.99 94.42 o 16 2 1 224.16 278.70 96.39 o 17 2 1 12.09 127.24 102.23 o 1 3 1 2583.57 2475.59 49.63 o 2 3 1 86035.99 86362.78 447.76 o 3 3 1 5125.65 4950.78 63.27 o 4 3 1 5700.12 5575.11 65.25 o 5 3 1 1484.56 1542.10 55.46 o 6 3 1 210.48 290.96 52.60 o 7 3 1 8.48 284.73 55.46 o 8 3 1 1646.38 1834.84 68.12 o 9 3 1 1346.78 1441.75 70.10 o 10 3 1 2062.61 2177.31 85.72 o 11 3 1 1729.04 1657.97 87.59 o 12 3 1 181.06 194.67 85.72 o 13 3 1 6.39 4.94 87.59 o 14 3 1 0.59 169.16 85.72 o 15 3 1 195.84 204.16 89.57 o 16 3 1 144.23 205.34 96.39 o 17 3 1 3.19 46.66 99.26 o 1 4 1 391.45 291.36 48.64 o 2 4 1 13562.88 13816.03 104.11 o 3 4 1 615.31 605.45 48.64 o 4 4 1 528.09 496.80 49.63 o 5 4 1 122.29 38.26 52.60 o 6 4 1 4655.23 4640.04 74.94 o 7 4 1 3.46 -9.10 59.32 o 8 4 1 5320.97 5043.41 85.72 o 9 4 1 1069.53 999.23 71.08 o 10 4 1 1800.74 1734.00 85.72 o 11 4 1 1145.32 1283.96 90.56 o 12 4 1 264.31 250.13 89.57 o 13 4 1 86.68 122.79 87.59 o 14 4 1 112.44 22.05 82.75 o 15 4 1 183.89 83.74 93.43 o 16 4 1 235.49 214.83 92.44 o 17 4 1 48.65 74.25 95.41 o 1 5 1 606.79 742.97 47.65 o 2 5 1 543.50 549.10 49.63 o 3 5 1 108.75 176.57 46.76 o 4 5 1 5317.87 5704.82 75.93 o 5 5 1 1955.48 2029.51 61.30 o 6 5 1 2203.46 2302.57 65.25 o 7 5 1 1.09 42.71 53.49 o 8 5 1 282.35 205.94 62.29 o 9 5 1 127.38 114.68 68.12 o 10 5 1 462.59 433.52 77.91 o 11 5 1 198.78 298.18 85.72 o 12 5 1 39.13 212.46 86.61 o 13 5 1 38.56 36.88 77.91 o 14 5 1 53.65 47.85 84.73 o 15 5 1 34.20 -0.79 86.61 o 16 5 1 6.06 131.00 100.25 o 17 5 1 2.96 -74.35 95.41 o 0 6 1 596.28 585.18 49.63 o 1 6 1 650.79 574.01 48.64 o 2 6 1 11352.35 11260.66 85.72 o 3 6 1 817.24 761.76 51.61 o 4 6 1 8871.97 9007.02 87.59 o 5 6 1 416.57 312.41 58.43 o 6 6 1 306.64 297.58 58.43 o 7 6 1 1996.67 1965.84 68.12 o 8 6 1 161.73 245.98 62.29 o 9 6 1 19.59 55.76 71.08 o 10 6 1 2036.49 2111.56 93.43 o 11 6 1 750.92 726.66 90.56 o 12 6 1 154.14 121.90 83.74 o 13 6 1 3.56 79.09 79.88 o 14 6 1 0.43 167.18 88.58 o 15 6 1 2.00 110.04 94.42 o 16 6 1 3.67 21.35 94.42 o 1 7 1 0.07 17.99 44.79 o 2 7 1 604.57 549.30 51.61 o 3 7 1 751.46 896.61 52.60 o 4 7 1 3532.96 3326.32 66.24 o 5 7 1 243.95 494.72 55.46 o 6 7 1 19.32 36.88 56.45 o 7 7 1 115.28 280.09 59.32 o 8 7 1 0.34 -2.77 63.27 o 9 7 1 376.61 485.23 74.05 o 10 7 1 34.36 -63.57 81.76 o 11 7 1 125.37 143.95 83.74 o 12 7 1 19.20 66.93 83.74 o 13 7 1 5.15 -17.80 83.74 o 14 7 1 4.87 -69.11 85.72 o 15 7 1 0.06 -75.04 91.55 o 16 7 1 6.15 12.36 97.28 o 0 8 1 1324.51 1263.60 53.49 o 1 8 1 1600.96 1553.57 57.44 o 2 8 1 224.61 235.79 52.60 o 3 8 1 424.64 357.60 52.60 o 4 8 1 1486.20 1584.71 63.27 o 5 8 1 575.86 592.70 58.43 o 6 8 1 6.09 -6.72 59.32 o 7 8 1 252.60 190.91 60.31 o 8 8 1 36.59 85.42 68.12 o 9 8 1 199.44 172.52 75.93 o 10 8 1 289.32 421.76 80.77 o 11 8 1 153.64 262.59 82.75 o 12 8 1 578.50 718.36 88.58 o 13 8 1 618.53 582.91 87.59 o 14 8 1 95.56 78.99 88.58 o 15 8 1 81.52 -14.34 92.44 o 16 8 1 2.12 54.87 94.42 o 1 9 1 35.11 137.62 48.64 o 2 9 1 6.23 -28.47 53.49 o 3 9 1 574.36 656.56 54.47 o 4 9 1 213.77 202.28 54.47 o 5 9 1 156.69 213.65 60.31 o 6 9 1 207.55 193.87 63.27 o 7 9 1 226.86 303.22 67.13 o 8 9 1 42.41 18.49 72.07 o 9 9 1 279.35 272.87 81.76 o 10 9 1 211.43 120.81 80.77 o 11 9 1 194.76 309.74 75.93 o 12 9 1 41.21 95.21 83.74 o 13 9 1 189.95 63.57 85.72 o 14 9 1 14.69 26.20 87.59 o 15 9 1 2.69 -89.08 92.44 o 0 10 1 1072.28 1072.69 60.31 o 1 10 1 1517.23 1601.52 62.29 o 2 10 1 492.47 436.59 59.32 o 3 10 1 944.48 850.54 61.30 o 4 10 1 12.52 80.87 59.32 o 5 10 1 582.95 474.75 68.12 o 6 10 1 64.88 136.24 67.13 o 7 10 1 0.19 158.88 71.08 o 8 10 1 237.89 431.55 76.92 o 9 10 1 9.34 8.40 81.76 o 10 10 1 86.44 113.50 80.77 o 11 10 1 45.82 165.80 83.74 o 12 10 1 68.41 -1.88 86.61 o 13 10 1 183.34 207.72 87.59 o 14 10 1 156.57 243.11 95.41 o 15 10 1 14.34 72.96 94.42 o 1 11 1 9.61 -52.99 57.44 o 2 11 1 14.93 96.10 64.26 o 3 11 1 50.34 85.62 60.31 o 4 11 1 37.68 125.86 63.27 o 5 11 1 61.08 200.30 67.13 o 6 11 1 186.40 198.92 71.08 o 7 11 1 62.25 42.51 74.05 o 8 11 1 0.67 -8.40 78.89 o 9 11 1 71.12 -26.89 77.91 o 10 11 1 44.61 -28.08 80.77 o 11 11 1 0.58 -80.97 83.74 o 12 11 1 412.73 426.01 91.55 o 13 11 1 537.11 493.24 92.44 o 14 11 1 176.66 237.87 94.42 o 0 12 1 4696.24 4349.38 90.56 o 1 12 1 2004.88 1874.68 73.06 o 2 12 1 2887.07 3016.38 85.72 o 3 12 1 812.39 794.28 71.08 o 4 12 1 1891.34 1902.96 79.88 o 5 12 1 324.51 395.86 74.05 o 6 12 1 127.61 62.48 80.77 o 7 12 1 50.52 30.55 73.06 o 8 12 1 3.24 41.03 79.88 o 9 12 1 0.80 126.15 80.77 o 10 12 1 25.05 2.57 77.91 o 11 12 1 125.70 88.39 80.77 o 12 12 1 176.26 63.27 91.55 o 13 12 1 81.42 23.83 89.57 o 1 13 1 109.19 65.75 73.06 o 2 13 1 652.87 585.08 74.94 o 3 13 1 45.87 217.21 72.07 o 4 13 1 97.52 93.92 72.07 o 5 13 1 38.89 44.49 72.07 o 6 13 1 14.25 16.41 72.07 o 7 13 1 0.55 -24.32 72.07 o 8 13 1 0.28 118.14 70.10 o 9 13 1 31.20 93.53 81.76 o 10 13 1 18.45 -65.55 86.61 o 11 13 1 0.31 68.22 80.77 o 12 13 1 70.62 -2.08 82.75 o 13 13 1 113.52 142.46 88.58 o 0 14 1 3162.93 2685.08 90.56 o 1 14 1 548.03 617.91 77.91 o 2 14 1 51.27 24.72 70.10 o 3 14 1 1.45 -66.34 73.06 o 4 14 1 37.96 -31.24 75.93 o 5 14 1 108.26 30.25 72.07 o 6 14 1 70.49 41.13 73.06 o 7 14 1 357.80 331.20 74.94 o 8 14 1 24.16 69.50 76.92 o 9 14 1 76.48 106.48 80.77 o 10 14 1 0.06 16.91 82.75 o 11 14 1 44.31 -26.50 93.43 o 12 14 1 17.25 37.96 97.28 o 1 15 1 324.77 362.84 71.08 o 2 15 1 289.45 328.73 71.08 o 3 15 1 263.54 200.70 72.07 o 4 15 1 105.16 120.22 69.11 o 5 15 1 0.21 36.88 74.94 o 6 15 1 41.02 19.08 77.91 o 7 15 1 108.65 87.69 75.93 o 8 15 1 0.00 24.91 81.76 o 9 15 1 1.50 61.89 82.75 o 10 15 1 15.93 -34.21 93.43 o 11 15 1 8.46 129.81 92.44 o 0 16 1 0.44 -32.82 72.07 o 1 16 1 0.55 18.69 75.93 o 2 16 1 179.98 284.34 74.05 o 3 16 1 42.04 111.72 73.06 o 4 16 1 80.13 183.10 77.91 o 5 16 1 0.25 56.95 79.88 o 6 16 1 0.14 -65.15 75.93 o 7 16 1 19.03 260.71 89.57 o 8 16 1 14.18 -32.13 88.58 o 9 16 1 3.41 1.58 91.55 o 10 16 1 10.86 135.45 89.57 o 1 17 1 78.27 129.91 82.75 o 2 17 1 12.84 18.49 82.75 o 3 17 1 6.26 -1.09 75.93 o 4 17 1 304.33 460.02 89.57 o 5 17 1 4.24 39.74 81.76 o 6 17 1 173.62 199.02 79.88 o 7 17 1 20.65 -49.23 90.56 o 8 17 1 41.50 -48.35 85.72 o 0 18 1 14.67 -48.44 81.76 o 1 18 1 14.88 -67.13 84.73 o 2 18 1 180.03 175.98 78.89 o 3 18 1 134.65 163.52 85.72 o 4 18 1 438.52 539.90 90.56 o 5 18 1 198.94 317.26 90.56 o 6 18 1 242.15 336.34 82.75 o 1 19 1 3.87 -64.76 83.74 o 2 19 1 22.48 76.32 81.76 o 3 19 1 47.18 -32.72 80.77 o 0 0 2 27131.76 26877.02 155.81 o 1 0 2 45418.36 45304.03 248.25 o 2 0 2 46760.29 46595.50 237.57 o 3 0 2 6265.56 6305.33 71.08 o 4 0 2 2055.22 2163.17 59.32 o 5 0 2 72.13 71.38 52.60 o 6 0 2 13378.09 12813.53 104.11 o 7 0 2 102.78 150.37 59.32 o 8 0 2 79.25 166.19 59.32 o 9 0 2 82.29 147.21 66.24 o 10 0 2 95.62 -1.88 74.05 o 11 0 2 913.90 849.06 85.72 o 12 0 2 23.46 52.30 90.56 o 13 0 2 990.59 858.25 92.44 o 14 0 2 0.47 93.72 89.57 o 15 0 2 402.16 464.27 92.44 o 16 0 2 165.66 137.23 100.25 o 17 0 2 80.42 128.33 103.22 o 1 1 2 1501.26 1694.06 36.98 o 2 1 2 32.16 37.57 40.93 o 3 1 2 25316.72 24951.42 155.81 o 4 1 2 5046.68 5219.10 69.11 o 5 1 2 1687.10 1882.00 57.44 o 6 1 2 379.18 519.44 54.47 o 7 1 2 3689.23 3899.05 74.05 o 8 1 2 87.70 270.89 59.32 o 9 1 2 1234.91 1392.72 71.08 o 10 1 2 47.63 133.67 76.92 o 11 1 2 659.76 550.78 87.59 o 12 1 2 2.27 -81.07 89.57 o 13 1 2 972.05 830.07 94.42 o 14 1 2 118.11 65.35 88.58 o 15 1 2 58.26 171.73 89.57 o 16 1 2 3.04 126.65 97.28 o 17 1 2 54.98 110.23 95.41 o 0 2 2 2807.80 2667.88 42.81 o 1 2 2 7974.58 7878.28 63.27 o 2 2 2 212.65 287.40 46.76 o 3 2 2 1732.71 1726.88 58.43 o 4 2 2 348.00 318.25 52.60 o 5 2 2 949.08 1116.49 54.47 o 6 2 2 6541.87 6796.30 77.91 o 7 2 2 281.44 384.09 56.45 o 8 2 2 289.41 397.14 61.30 o 9 2 2 11.34 8.11 64.26 o 10 2 2 147.48 362.64 73.06 o 11 2 2 483.55 371.54 80.77 o 12 2 2 137.62 36.98 89.57 o 13 2 2 271.61 385.77 84.73 o 14 2 2 151.01 192.49 82.75 o 15 2 2 75.70 15.72 93.43 o 16 2 2 16.19 45.87 96.39 o 17 2 2 113.62 137.32 97.28 o 2 3 2 2573.42 2442.57 57.44 o 3 3 2 622.62 648.95 51.61 o 4 3 2 38.73 61.00 48.64 o 5 3 2 8.36 79.49 49.63 o 6 3 2 5275.28 5116.48 74.05 o 7 3 2 93.67 226.80 54.47 o 8 3 2 26.41 185.97 60.31 o 9 3 2 577.11 569.66 67.13 o 10 3 2 165.28 118.93 75.93 o 11 3 2 335.10 323.49 80.77 o 12 3 2 51.12 117.16 86.61 o 13 3 2 992.71 972.14 89.57 o 14 3 2 4.16 203.07 87.59 o 15 3 2 7.91 -86.90 91.55 o 16 3 2 9.80 33.81 92.44 o 17 3 2 13.18 122.79 102.23 o 0 4 2 11093.82 9718.26 80.77 o 1 4 2 10580.86 9510.35 88.58 o 2 4 2 10413.55 10238.49 81.76 o 3 4 2 15769.70 16164.47 104.11 o 4 4 2 99.14 165.50 48.64 o 5 4 2 262.09 272.87 49.63 o 6 4 2 499.75 442.92 56.45 o 7 4 2 2855.61 2778.71 71.08 o 8 4 2 170.08 135.35 62.29 o 9 4 2 187.79 236.09 67.13 o 10 4 2 0.05 -76.42 76.92 o 11 4 2 19.85 90.36 81.76 o 12 4 2 3.26 -41.52 86.61 o 13 4 2 47.51 89.37 79.88 o 14 4 2 312.14 255.17 81.76 o 15 4 2 0.05 17.20 91.55 o 16 4 2 0.73 43.60 88.58 o 17 4 2 42.45 254.48 99.26 o 1 5 2 3184.90 2977.92 62.29 o 2 5 2 856.40 953.75 50.62 o 3 5 2 594.82 721.72 50.62 o 4 5 2 13883.37 13737.92 100.25 o 5 5 2 228.00 356.11 53.49 o 6 5 2 1370.57 1383.82 62.29 o 7 5 2 38.23 268.12 57.44 o 8 5 2 654.07 660.32 65.25 o 9 5 2 28.43 42.31 67.13 o 10 5 2 1010.08 993.99 84.73 o 11 5 2 21.01 -60.60 80.77 o 12 5 2 25.06 99.16 85.72 o 13 5 2 42.01 29.26 83.74 o 14 5 2 0.89 10.97 84.73 o 15 5 2 198.49 131.99 91.55 o 16 5 2 0.03 0.10 94.42 o 17 5 2 63.19 -52.20 99.26 o 0 6 2 291.27 247.95 46.76 o 1 6 2 559.35 510.84 49.63 o 2 6 2 278.93 157.49 48.64 o 3 6 2 13088.97 12506.06 94.42 o 4 6 2 1349.88 1308.09 58.43 o 5 6 2 8393.98 7949.36 84.73 o 6 6 2 214.19 203.46 54.47 o 7 6 2 2256.62 2258.97 68.12 o 8 6 2 796.60 842.73 66.24 o 9 6 2 3024.97 2600.55 84.73 o 10 6 2 400.57 389.53 84.73 o 11 6 2 0.86 179.34 88.58 o 12 6 2 72.66 134.65 81.76 o 13 6 2 3.08 9.10 80.77 o 14 6 2 25.21 124.17 89.57 o 15 6 2 256.56 211.28 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