#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/17/2011768.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011768_Fobs loop_ _publ_author_name 'Hao, Qingli' 'Jian, Fangfang' 'Wang, Xin' 'Razak, Ibrahim Abdul' 'Shanmuga Sundara Raj, S.' 'Fun, Hoong-Kun' _publ_section_title ; trans-Bis(2-aminopyridine-N)bis(O,O'-diisopropyl dithiophosphato-S,S')nickel(II) ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 160 _journal_page_last 161 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.938 _cell_angle_gamma 90.000 _cell_length_a 6.6296 _cell_length_b 16.3605 _cell_length_c 14.6386 _exptl_crystal_F_000 708.00 _reflns_d_resolution_high 0.7500 _[local]_cod_data_source_file ln1110Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' LN1110 in P2(1)/n 23/5/2000' _shelx_refln_list_code 4 _shelx_f_calc_maximum 161.24 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17.65 26.18 7.12 o 4 0 0 29.27 21.44 8.89 o 6 0 0 902.04 861.76 71.85 o 8 0 0 73.00 66.14 16.80 o 2 1 0 436.44 462.99 23.08 o 3 1 0 320.83 319.49 25.54 o 4 1 0 1800.60 1801.07 98.61 o 5 1 0 46.79 56.60 8.80 o 6 1 0 23.10 21.36 8.10 o 7 1 0 202.72 197.13 17.22 o 8 1 0 4.65 1.02 7.55 o 0 2 0 3646.36 3311.72 119.84 o 1 2 0 3590.15 3549.59 240.38 o 2 2 0 6.04 5.88 2.56 o 3 2 0 2567.51 2724.42 146.42 o 4 2 0 2213.00 2284.27 123.88 o 5 2 0 704.55 699.52 41.72 o 6 2 0 84.15 85.56 11.12 o 7 2 0 337.72 338.86 24.62 o 8 2 0 16.15 16.42 9.04 o 1 3 0 18.76 22.89 3.25 o 2 3 0 1217.20 1395.18 56.27 o 3 3 0 9632.55 10566.43 388.04 o 4 3 0 8085.45 7915.19 419.10 o 5 3 0 207.70 224.69 17.15 o 6 3 0 502.62 488.84 31.57 o 7 3 0 1054.00 1042.06 61.13 o 8 3 0 2.06 13.63 11.73 o 0 4 0 25.27 23.07 3.02 o 1 4 0 2696.30 2530.31 144.31 o 2 4 0 439.69 463.70 20.38 o 3 4 0 160.41 209.96 9.80 o 4 4 0 1590.84 1614.36 89.01 o 5 4 0 225.29 208.09 16.70 o 6 4 0 785.21 763.06 45.81 o 7 4 0 28.80 21.80 8.58 o 8 4 0 637.55 621.85 40.34 o 1 5 0 341.90 369.63 15.96 o 2 5 0 1343.33 1326.57 53.67 o 3 5 0 308.44 284.25 15.95 o 4 5 0 88.51 86.13 6.90 o 5 5 0 87.39 97.97 11.00 o 6 5 0 574.99 584.20 36.72 o 7 5 0 1177.35 1143.56 66.86 o 8 5 0 398.24 375.71 34.24 o 0 6 0 2551.74 2667.99 169.87 o 1 6 0 1591.70 1765.23 58.19 o 2 6 0 3805.51 3718.87 120.87 o 3 6 0 4446.13 4517.63 203.01 o 4 6 0 720.61 686.52 28.59 o 5 6 0 174.38 173.45 14.91 o 6 6 0 74.72 75.10 10.78 o 7 6 0 251.48 238.28 20.12 o 8 6 0 486.44 450.39 31.69 o 1 7 0 2708.98 2751.78 89.86 o 2 7 0 1145.26 1211.67 40.73 o 3 7 0 532.33 522.27 20.71 o 4 7 0 569.19 580.68 24.88 o 5 7 0 285.29 288.28 19.08 o 6 7 0 24.14 17.43 7.88 o 7 7 0 1.31 -2.86 6.75 o 8 7 0 117.08 105.87 14.39 o 0 8 0 6187.83 5970.78 444.06 o 1 8 0 560.08 534.36 17.66 o 2 8 0 5283.67 5198.29 167.96 o 3 8 0 1958.05 1977.12 71.65 o 4 8 0 4.29 9.12 6.59 o 5 8 0 0.26 5.64 5.71 o 6 8 0 25.03 20.28 8.40 o 7 8 0 171.93 177.84 23.04 o 8 8 0 103.64 87.88 18.52 o 1 9 0 14079.83 13948.42 417.48 o 2 9 0 1299.68 972.91 152.11 o 3 9 0 163.37 145.32 10.15 o 4 9 0 22.09 22.54 7.11 o 5 9 0 1502.61 1505.68 59.21 o 6 9 0 38.30 23.80 6.23 o 7 9 0 105.31 109.39 19.19 o 0 10 0 4147.03 4526.82 208.03 o 1 10 0 395.63 417.65 14.42 o 2 10 0 1889.31 1888.97 68.25 o 3 10 0 882.45 853.20 49.66 o 4 10 0 16.13 15.82 6.83 o 5 10 0 180.47 188.95 11.84 o 6 10 0 360.15 350.36 18.13 o 7 10 0 30.09 28.42 10.28 o 1 11 0 190.10 204.90 13.50 o 2 11 0 942.27 906.82 34.78 o 3 11 0 73.42 84.96 10.19 o 4 11 0 308.92 314.95 34.49 o 5 11 0 3071.58 3145.95 119.27 o 6 11 0 18.49 22.11 6.97 o 7 11 0 11.18 5.74 8.58 o 0 12 0 554.88 629.24 43.90 o 1 12 0 508.60 475.00 19.34 o 2 12 0 1026.27 1071.29 66.00 o 3 12 0 1072.25 994.25 57.47 o 4 12 0 1185.29 1191.82 68.35 o 5 12 0 22.70 34.11 6.77 o 6 12 0 823.01 893.54 38.11 o 7 12 0 136.78 140.12 16.18 o 1 13 0 3.83 12.72 8.30 o 2 13 0 104.16 92.42 9.05 o 3 13 0 573.78 553.06 34.73 o 4 13 0 0.55 2.10 6.07 o 5 13 0 883.57 832.02 50.24 o 6 13 0 52.60 60.10 7.97 o 0 14 0 5.47 5.06 5.98 o 1 14 0 2342.99 2473.30 170.17 o 2 14 0 100.59 100.50 11.36 o 3 14 0 28.54 27.18 7.86 o 4 14 0 39.80 37.45 8.35 o 5 14 0 21.86 34.87 9.81 o 6 14 0 228.98 205.68 13.59 o 1 15 0 242.37 261.81 16.38 o 2 15 0 432.03 430.05 28.47 o 3 15 0 320.64 326.94 23.33 o 4 15 0 372.54 357.33 25.45 o 5 15 0 6.46 3.87 7.19 o 6 15 0 74.77 85.31 9.60 o 0 16 0 430.54 424.21 39.88 o 1 16 0 152.36 142.72 19.43 o 2 16 0 495.80 535.10 34.33 o 3 16 0 62.46 63.72 10.08 o 4 16 0 339.15 309.11 23.39 o 5 16 0 37.55 33.02 9.33 o 1 17 0 278.56 296.19 22.06 o 2 17 0 130.81 134.73 14.11 o 3 17 0 1307.95 1226.69 70.95 o 4 17 0 292.59 272.28 21.76 o 5 17 0 228.60 233.25 20.32 o 0 18 0 992.36 1101.30 91.34 o 1 18 0 155.00 149.67 14.55 o 2 18 0 133.81 123.98 13.41 o 3 18 0 13.66 21.17 8.29 o 4 18 0 147.18 144.17 15.45 o 1 19 0 223.09 222.40 18.74 o 2 19 0 321.63 296.70 22.94 o 3 19 0 107.28 102.44 18.54 o 4 19 0 7.89 14.30 12.18 o 0 20 0 485.09 522.16 50.02 o 1 20 0 154.71 151.74 19.29 o 2 20 0 54.45 50.30 10.75 o 3 20 0 3.88 0.50 9.21 o 1 21 0 0.89 0.68 7.18 o -7 0 1 1863.74 1560.58 124.03 o -5 0 1 457.67 409.57 37.13 o -3 0 1 114.31 135.86 11.34 o -1 0 1 7276.34 6792.69 394.70 o 1 0 1 25997.56 20102.17 1493.95 o 3 0 1 6682.14 7113.00 532.55 o 5 0 1 1956.73 1743.27 136.13 o 7 0 1 13.91 9.03 10.42 o -8 1 1 4.10 3.76 10.59 o -7 1 1 181.19 166.50 15.57 o -6 1 1 3529.27 3166.92 171.36 o -5 1 1 391.34 363.62 24.02 o -4 1 1 213.86 193.28 14.47 o -3 1 1 399.81 412.93 16.68 o -2 1 1 633.22 676.73 23.38 o -1 1 1 5545.88 5230.64 204.59 o 1 1 1 379.83 309.78 17.43 o 2 1 1 766.27 762.69 45.69 o 3 1 1 2561.29 2876.82 154.53 o 4 1 1 7440.73 7405.60 392.49 o 5 1 1 1193.77 1134.35 64.42 o 6 1 1 1.91 3.26 9.88 o 7 1 1 0.09 0.69 10.13 o 8 1 1 28.30 24.22 9.79 o -8 2 1 167.14 153.02 16.01 o -7 2 1 535.98 496.48 32.39 o -6 2 1 1373.58 1302.70 73.85 o -5 2 1 55.18 48.34 8.99 o -4 2 1 1536.29 1543.59 71.59 o -3 2 1 9388.52 9864.83 383.45 o -2 2 1 405.05 453.72 14.82 o -1 2 1 104.95 97.89 5.37 o 0 2 1 2587.04 2420.60 149.00 o 1 2 1 10.58 9.12 3.87 o 2 2 1 79.25 84.61 5.81 o 3 2 1 3075.98 3080.40 165.10 o 4 2 1 4308.62 4239.29 226.59 o 5 2 1 718.61 780.95 46.17 o 6 2 1 7.42 2.06 6.35 o 7 2 1 370.56 345.32 25.02 o 8 2 1 194.35 178.35 17.42 o -8 3 1 82.20 95.96 13.45 o -7 3 1 165.66 161.52 15.55 o -6 3 1 158.87 131.89 18.37 o -5 3 1 15.72 17.83 6.93 o -4 3 1 4283.64 4432.25 199.31 o -3 3 1 28.48 31.71 3.99 o -2 3 1 10653.16 11154.76 389.06 o -1 3 1 4088.27 3596.80 169.88 o 0 3 1 11.77 17.37 2.75 o 1 3 1 7187.51 6000.41 351.70 o 2 3 1 229.92 213.66 10.46 o 3 3 1 414.61 441.34 19.10 o 4 3 1 1396.23 1312.08 73.10 o 5 3 1 1210.25 1132.34 64.46 o 6 3 1 922.23 906.39 53.39 o 7 3 1 1.12 -1.76 9.38 o 8 3 1 338.49 325.45 25.24 o -8 4 1 0.38 15.19 12.75 o -7 4 1 222.50 220.38 18.74 o -6 4 1 169.83 159.62 14.54 o -5 4 1 999.50 936.06 54.07 o -4 4 1 2230.80 2247.70 77.84 o -3 4 1 8361.73 8403.78 260.55 o -2 4 1 8684.95 9328.73 362.81 o -1 4 1 1706.86 1855.13 77.83 o 0 4 1 9362.61 8400.71 307.88 o 1 4 1 397.18 391.31 39.07 o 2 4 1 17.48 15.91 4.93 o 3 4 1 14.03 12.18 3.74 o 4 4 1 801.40 890.25 51.39 o 5 4 1 15.46 12.28 7.25 o 6 4 1 476.55 462.24 30.29 o 7 4 1 2043.36 1930.40 107.86 o 8 4 1 682.41 655.25 42.38 o -8 5 1 194.18 168.74 23.17 o -7 5 1 338.43 363.11 26.11 o -6 5 1 10.37 7.45 7.40 o -5 5 1 185.09 164.19 14.21 o -4 5 1 4560.94 4482.73 140.50 o -3 5 1 1740.16 1924.95 69.10 o -2 5 1 2197.06 2181.23 86.71 o -1 5 1 793.97 900.76 33.23 o 0 5 1 4719.03 4675.30 260.23 o 1 5 1 3937.58 3776.82 147.86 o 2 5 1 682.48 706.45 58.71 o 3 5 1 1.32 1.59 3.44 o 4 5 1 71.31 75.91 7.80 o 5 5 1 78.74 79.00 10.48 o 6 5 1 1168.91 1199.03 69.07 o 7 5 1 23.21 15.01 9.40 o 8 5 1 772.31 725.78 64.81 o -8 6 1 428.52 411.52 40.79 o -7 6 1 56.93 58.67 10.86 o -6 6 1 81.80 73.30 14.58 o -5 6 1 515.36 542.00 23.80 o -4 6 1 97.82 109.67 6.54 o -3 6 1 2063.22 2090.50 83.71 o -2 6 1 562.38 573.18 24.81 o -1 6 1 479.50 500.36 19.47 o 0 6 1 113.46 112.54 6.76 o 1 6 1 1686.46 1654.58 59.50 o 2 6 1 223.94 296.64 16.04 o 3 6 1 1465.50 1426.19 97.01 o 4 6 1 303.14 312.35 15.12 o 5 6 1 195.03 229.68 18.28 o 6 6 1 887.36 905.24 53.94 o 7 6 1 534.42 509.53 34.00 o 8 6 1 20.97 15.69 9.86 o -8 7 1 537.67 522.94 41.14 o -7 7 1 850.56 827.22 50.66 o -6 7 1 43.03 44.34 9.05 o -5 7 1 21.49 25.40 5.65 o -4 7 1 221.40 207.75 9.56 o -3 7 1 47.43 67.27 6.01 o -2 7 1 3125.14 769.36 953.32 o -1 7 1 35.23 46.61 4.00 o 0 7 1 42.24 32.87 3.49 o 1 7 1 1965.08 2031.99 72.66 o 2 7 1 4474.33 4249.22 166.52 o 3 7 1 5853.19 5979.01 266.94 o 4 7 1 224.82 229.24 17.44 o 5 7 1 64.26 55.71 6.81 o 6 7 1 470.40 451.30 42.29 o 7 7 1 11.88 8.10 7.95 o 8 7 1 95.45 86.64 18.96 o -8 8 1 60.92 69.64 12.48 o -7 8 1 72.79 76.52 12.28 o -6 8 1 0.04 3.30 7.44 o -5 8 1 817.75 823.70 34.31 o -4 8 1 102.23 94.29 7.65 o -3 8 1 1328.06 1360.05 55.73 o -2 8 1 0.28 3.40 3.30 o -1 8 1 4529.96 4514.03 158.50 o 0 8 1 21.11 22.79 3.68 o 1 8 1 4929.88 5238.16 184.06 o 2 8 1 186.27 192.46 10.00 o 3 8 1 1202.81 1184.36 48.43 o 4 8 1 626.24 608.30 26.06 o 5 8 1 1370.23 1449.60 62.11 o 6 8 1 30.98 31.88 8.67 o 7 8 1 196.39 188.58 18.85 o -7 9 1 0.47 -2.44 7.21 o -6 9 1 641.89 636.07 28.13 o -5 9 1 288.64 317.15 15.99 o -4 9 1 3.52 -0.40 3.85 o -3 9 1 12.02 16.03 4.39 o -2 9 1 567.58 633.22 27.55 o -1 9 1 462.66 457.92 18.36 o 0 9 1 4167.45 4361.43 153.57 o 1 9 1 104.18 90.56 5.71 o 2 9 1 7294.50 7225.73 281.79 o 3 9 1 328.39 335.16 18.33 o 4 9 1 1024.19 1026.93 59.12 o 5 9 1 267.51 270.07 14.55 o 6 9 1 122.33 152.19 15.63 o 7 9 1 104.09 110.51 20.22 o -7 10 1 49.15 37.59 9.98 o -6 10 1 251.70 270.92 22.42 o -5 10 1 2088.18 2147.09 82.58 o -4 10 1 262.15 269.43 14.47 o -3 10 1 227.25 226.80 12.44 o -2 10 1 2560.68 2747.83 109.41 o -1 10 1 6207.21 6457.84 226.89 o 0 10 1 1101.02 1098.23 40.61 o 1 10 1 293.71 363.91 17.40 o 2 10 1 22.86 20.19 3.87 o 3 10 1 637.51 628.47 37.99 o 4 10 1 597.00 550.84 34.33 o 5 10 1 2519.81 2518.15 96.40 o 6 10 1 525.01 508.92 23.80 o 7 10 1 231.46 240.23 20.64 o -7 11 1 333.90 320.73 28.86 o -6 11 1 406.92 398.37 19.78 o -5 11 1 113.46 116.91 12.73 o -4 11 1 654.29 685.48 41.55 o -3 11 1 420.80 443.33 20.79 o -2 11 1 2491.10 2494.23 99.74 o -1 11 1 485.95 544.41 24.21 o 0 11 1 188.22 179.54 12.53 o 1 11 1 2057.27 2076.55 82.89 o 2 11 1 96.31 101.11 10.15 o 3 11 1 1250.17 1253.75 82.97 o 4 11 1 224.01 209.34 23.14 o 5 11 1 265.44 262.90 14.52 o 6 11 1 353.64 378.03 19.42 o 7 11 1 0.55 1.41 8.06 o -7 12 1 8.26 9.80 8.29 o -6 12 1 20.60 33.72 6.89 o -5 12 1 1646.78 1647.28 152.56 o -4 12 1 85.94 89.12 11.20 o -3 12 1 1852.33 1828.40 74.32 o -2 12 1 11.53 16.71 4.64 o -1 12 1 3090.21 3241.23 128.43 o 0 12 1 511.42 581.04 25.56 o 1 12 1 130.60 145.46 12.75 o 2 12 1 27.63 25.23 7.07 o 3 12 1 54.59 51.86 8.50 o 4 12 1 107.50 107.20 11.92 o 5 12 1 1157.60 1227.41 49.68 o 6 12 1 29.54 28.69 7.11 o 7 12 1 140.37 145.64 22.03 o -7 13 1 95.52 100.76 19.18 o -6 13 1 183.98 208.90 14.50 o -5 13 1 331.30 323.48 23.87 o -4 13 1 1517.61 1473.66 83.06 o -3 13 1 324.57 372.21 21.82 o -2 13 1 1391.45 1416.71 58.42 o -1 13 1 745.93 802.71 37.52 o 0 13 1 58.28 65.22 7.47 o 1 13 1 1458.43 1589.27 75.91 o 2 13 1 70.89 65.71 13.15 o 3 13 1 1972.04 1907.66 105.59 o 4 13 1 14.11 11.11 7.01 o 5 13 1 409.51 418.71 20.51 o 6 13 1 382.91 400.21 20.54 o -6 14 1 316.94 368.11 19.75 o -5 14 1 222.89 211.69 18.11 o -4 14 1 17.01 22.04 7.75 o -3 14 1 609.01 651.87 33.65 o -2 14 1 753.87 738.98 32.30 o -1 14 1 58.07 62.14 7.82 o 0 14 1 221.17 244.89 18.92 o 1 14 1 227.53 253.73 15.60 o 2 14 1 47.74 60.78 9.50 o 3 14 1 48.54 53.66 9.16 o 4 14 1 139.49 145.18 14.63 o 5 14 1 6.41 5.58 7.40 o 6 14 1 25.53 27.11 7.30 o -6 15 1 6.06 1.19 5.67 o -5 15 1 88.58 85.05 11.87 o -4 15 1 208.78 217.10 18.33 o -3 15 1 0.20 -2.85 4.76 o -2 15 1 100.18 113.50 10.22 o -1 15 1 993.73 1050.81 55.71 o 0 15 1 612.91 611.57 32.28 o 1 15 1 164.00 161.76 14.47 o 2 15 1 457.14 458.85 30.05 o 3 15 1 111.93 107.33 12.01 o 4 15 1 94.31 98.84 12.40 o 5 15 1 380.25 272.81 32.83 o 6 15 1 93.88 81.65 17.08 o -5 16 1 126.89 133.16 14.92 o -4 16 1 57.65 62.16 10.63 o -3 16 1 525.03 535.72 34.84 o -2 16 1 303.25 358.84 39.00 o -1 16 1 44.43 54.91 7.84 o 0 16 1 474.82 522.68 27.70 o 1 16 1 1078.78 1001.50 58.28 o 2 16 1 15.82 15.42 6.89 o 3 16 1 1056.21 1005.88 59.18 o 4 16 1 426.10 406.41 28.23 o 5 16 1 10.67 17.74 8.60 o -5 17 1 42.92 44.19 9.96 o -4 17 1 30.84 24.13 8.82 o -3 17 1 77.66 84.26 11.71 o -2 17 1 80.55 78.70 11.17 o -1 17 1 4.74 1.18 5.37 o 0 17 1 552.16 588.35 37.26 o 1 17 1 61.89 60.15 9.76 o 2 17 1 359.50 354.64 25.36 o 3 17 1 106.90 110.04 13.14 o 4 17 1 574.61 497.55 33.17 o 5 17 1 7.98 2.82 7.49 o -4 18 1 132.21 132.49 14.92 o -3 18 1 366.22 373.65 27.03 o -2 18 1 544.55 530.82 34.66 o -1 18 1 15.34 16.95 7.80 o 0 18 1 1.41 4.42 6.60 o 1 18 1 735.76 733.78 45.09 o 2 18 1 0.00 1.32 7.31 o 3 18 1 677.04 660.10 41.63 o 4 18 1 3.43 3.68 7.28 o -4 19 1 187.45 192.82 25.57 o -3 19 1 61.46 69.47 11.95 o -2 19 1 15.49 18.41 8.36 o -1 19 1 628.08 620.63 39.63 o 0 19 1 1030.86 1046.82 62.23 o 1 19 1 2.92 7.90 10.90 o 2 19 1 9.06 9.39 7.78 o 3 19 1 0.01 10.32 7.72 o -3 20 1 404.01 396.85 28.78 o -2 20 1 101.54 95.38 15.10 o -1 20 1 238.86 223.51 19.19 o 0 20 1 149.42 151.95 15.64 o 1 20 1 3.58 5.08 9.61 o 2 20 1 20.19 17.64 8.64 o -1 21 1 0.15 3.24 9.91 o 0 21 1 257.97 284.80 33.00 o 1 21 1 75.92 64.91 11.73 o -8 0 2 14.25 19.04 13.49 o -6 0 2 7516.09 6967.96 523.93 o -4 0 2 1.60 3.13 4.85 o -2 0 2 858.46 845.25 40.64 o 0 0 2 504.39 456.06 28.35 o 2 0 2 3137.32 3828.74 288.59 o 4 0 2 12294.44 12468.29 930.63 o 6 0 2 375.96 358.16 35.20 o 8 0 2 168.39 147.68 24.02 o -8 1 2 5.62 6.32 10.45 o -7 1 2 2206.73 2033.98 112.71 o -6 1 2 215.06 177.56 22.45 o -5 1 2 248.83 233.91 17.21 o -4 1 2 259.42 255.94 11.68 o -3 1 2 1523.86 1548.23 51.37 o -2 1 2 1514.41 1714.76 56.41 o -1 1 2 341.22 308.52 13.62 o 0 1 2 1474.91 1356.09 52.15 o 1 1 2 73.85 59.07 4.59 o 2 1 2 1349.51 1558.84 85.00 o 3 1 2 5669.88 6003.45 318.57 o 4 1 2 132.50 135.10 12.64 o 5 1 2 627.24 616.73 37.59 o 6 1 2 50.36 47.65 13.44 o 7 1 2 318.54 313.81 23.73 o 8 1 2 301.07 291.15 23.63 o -8 2 2 21.28 14.61 8.87 o -7 2 2 26.11 11.69 14.76 o -6 2 2 2235.55 2123.58 116.62 o -5 2 2 695.13 671.01 33.54 o -4 2 2 541.80 550.24 21.86 o -3 2 2 4437.46 4681.21 151.55 o -2 2 2 2483.45 2521.62 69.75 o -1 2 2 649.89 664.44 58.76 o 0 2 2 1915.85 1880.40 74.91 o 1 2 2 3417.20 3332.06 187.58 o 2 2 2 151.22 184.97 9.50 o 3 2 2 272.16 324.15 21.15 o 4 2 2 6720.92 6719.59 356.67 o 5 2 2 784.45 799.55 47.30 o 6 2 2 100.69 97.91 11.91 o 7 2 2 266.34 234.05 19.65 o 8 2 2 72.52 51.20 11.27 o -8 3 2 241.58 233.06 19.79 o -7 3 2 35.71 22.04 7.94 o -6 3 2 273.15 253.86 26.73 o -5 3 2 489.29 463.41 24.48 o -4 3 2 814.77 773.85 32.83 o -3 3 2 6126.96 5881.56 171.29 o -2 3 2 4897.53 4622.24 175.12 o -1 3 2 3637.18 3177.92 154.19 o 0 3 2 200.13 196.84 11.59 o 1 3 2 3516.16 3710.75 166.36 o 2 3 2 63.59 80.00 5.73 o 3 3 2 268.33 258.31 17.72 o 4 3 2 0.50 5.22 8.73 o 5 3 2 445.08 457.99 29.60 o 6 3 2 150.73 144.85 14.59 o 7 3 2 846.10 835.04 50.78 o 8 3 2 1095.35 1021.29 61.49 o -8 4 2 1.24 2.45 10.78 o -7 4 2 172.52 168.43 23.01 o -6 4 2 50.03 38.34 14.70 o -5 4 2 25.87 30.38 7.71 o -4 4 2 3689.27 3598.18 113.19 o -3 4 2 969.45 1121.01 32.17 o -2 4 2 923.78 841.59 31.45 o -1 4 2 1618.43 1601.05 66.71 o 0 4 2 3489.53 3321.00 135.11 o 1 4 2 845.78 947.71 44.33 o 2 4 2 1457.65 1566.15 114.82 o 3 4 2 70.37 51.14 5.28 o 4 4 2 881.77 900.43 51.79 o 5 4 2 0.94 2.89 6.58 o 6 4 2 577.05 557.23 35.53 o 7 4 2 0.75 -1.08 6.86 o 8 4 2 365.84 337.66 28.13 o -8 5 2 0.00 11.89 12.06 o -7 5 2 164.03 141.78 14.49 o -6 5 2 25.50 28.99 8.15 o -5 5 2 1084.26 1037.05 49.94 o -4 5 2 277.96 292.32 11.82 o -3 5 2 2920.96 2779.65 110.20 o -2 5 2 2490.27 2695.81 96.36 o -1 5 2 217.05 242.90 17.97 o 0 5 2 12.00 25.60 4.21 o 1 5 2 7828.18 7963.07 354.46 o 2 5 2 2639.50 2993.90 135.18 o 3 5 2 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