#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:30:06 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180786 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/17/2011783.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011783_Fobs loop_ _publ_author_name 'Sim, Wonbo' 'Lee, Jai Young' 'Kim, Jong Seung' 'Kim, Jin-Gyu' 'Suh, Il-Hwan' _publ_section_title ; 6,7-Bis(bromomethyl)-2,11,18,21,24-pentaoxatetracyclo[23.4.0.0^4,9^.0^12,17^]nonacosa-1(25),4(9),5,7,12(17),13,15,26,28-nonaene ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 293 _journal_page_last 294 _journal_volume 57 _journal_year 2001 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.1410 _cell_length_b 13.7976 _cell_length_c 21.8520 _exptl_crystal_F_000 1168.00 _reflns_d_resolution_high 0.8420 _cod_data_source_file bj1007Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' foo in P 21 21 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 336.63 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7650.01 7681.12 73.23 o 4 0 0 21578.40 22448.03 205.78 o 6 0 0 2747.31 2879.79 115.87 o 8 0 0 24.60 -15.94 127.17 o 1 1 0 1223.62 1155.89 17.24 o 2 1 0 52843.05 53805.23 480.80 o 3 1 0 4861.59 5298.89 80.09 o 4 1 0 10658.79 10763.89 132.74 o 5 1 0 7494.62 7387.45 148.12 o 6 1 0 3196.31 3200.13 143.49 o 7 1 0 229.71 159.43 119.76 o 8 1 0 368.95 558.38 121.98 o 9 1 0 357.42 299.40 135.89 o 0 2 0 0.32 -6.38 11.73 o 1 2 0 1461.61 1540.78 23.25 o 2 2 0 1170.16 1173.97 30.13 o 3 2 0 33815.91 33051.56 252.50 o 4 2 0 2195.63 2233.16 70.26 o 5 2 0 70.72 99.18 58.58 o 6 2 0 848.68 935.83 86.39 o 7 2 0 4849.03 4526.57 162.21 o 8 2 0 9.51 159.62 104.00 o 9 2 0 3.23 -13.16 156.47 o 1 3 0 113316.61 132555.03 1918.28 o 2 3 0 29757.30 31242.44 347.32 o 3 3 0 1638.73 1604.89 54.13 o 4 3 0 3087.57 2889.06 91.40 o 5 3 0 3716.02 3556.08 112.90 o 6 3 0 643.81 557.64 85.65 o 7 3 0 309.93 134.78 102.89 o 8 3 0 382.23 667.58 119.20 o 9 3 0 332.35 202.07 132.37 o 0 4 0 31585.41 30461.61 400.16 o 1 4 0 1811.80 2104.23 98.72 o 2 4 0 31.33 -22.43 26.87 o 3 4 0 651.45 633.65 45.42 o 4 4 0 11485.49 12179.87 168.33 o 5 4 0 7.40 -71.74 73.78 o 6 4 0 928.74 946.21 94.18 o 7 4 0 0.72 37.82 111.42 o 8 4 0 250.45 225.99 119.94 o 9 4 0 0.13 205.41 130.14 o 1 5 0 10990.91 11021.02 114.20 o 2 5 0 5773.65 5620.16 90.84 o 3 5 0 10.13 0.00 55.06 o 4 5 0 1910.89 1807.51 82.68 o 5 5 0 2105.88 1981.22 100.48 o 6 5 0 1902.87 1915.97 112.34 o 7 5 0 13.76 -108.08 117.35 o 8 5 0 172.27 172.41 115.50 o 9 5 0 53.03 66.74 158.32 o 0 6 0 2881.45 2982.31 68.59 o 1 6 0 17866.17 18331.72 178.90 o 2 6 0 456.00 411.93 42.45 o 3 6 0 26018.27 25554.54 240.07 o 4 6 0 241.71 297.17 65.63 o 5 6 0 415.48 374.85 81.01 o 6 6 0 0.12 52.09 90.84 o 7 6 0 1322.73 1420.61 127.36 o 8 6 0 7.23 23.91 132.74 o 1 7 0 14301.45 14597.49 175.93 o 2 7 0 1989.08 2053.52 81.76 o 3 7 0 1366.47 1490.87 82.13 o 4 7 0 219.57 103.07 71.37 o 5 7 0 1281.25 1157.18 97.33 o 6 7 0 397.50 360.39 103.63 o 7 7 0 17.27 149.61 102.15 o 8 7 0 284.99 415.08 129.58 o 0 8 0 6898.09 6772.52 133.66 o 1 8 0 640.95 664.05 61.55 o 2 8 0 774.55 772.13 70.08 o 3 8 0 370.96 242.49 73.78 o 4 8 0 1650.40 1864.61 104.74 o 5 8 0 0.54 -100.29 100.29 o 6 8 0 1158.41 1259.88 122.54 o 7 8 0 95.85 -11.31 122.17 o 8 8 0 39.35 190.58 130.33 o 1 9 0 979.97 847.59 75.82 o 2 9 0 3912.58 4177.49 123.10 o 3 9 0 18.37 36.89 77.86 o 4 9 0 4090.96 3653.22 140.34 o 5 9 0 226.22 205.04 100.29 o 6 9 0 120.98 42.45 125.14 o 7 9 0 5.10 -54.13 130.88 o 8 9 0 89.65 133.48 145.71 o 0 10 0 771.90 762.31 85.83 o 1 10 0 710.22 845.36 85.09 o 2 10 0 292.58 237.29 75.64 o 3 10 0 845.52 1046.88 93.62 o 4 10 0 77.31 108.08 90.84 o 5 10 0 267.27 255.65 105.86 o 6 10 0 20.93 8.53 109.38 o 7 10 0 136.16 172.97 128.29 o 1 11 0 686.04 516.67 90.84 o 2 11 0 695.80 710.77 94.92 o 3 11 0 451.96 500.17 104.19 o 4 11 0 180.26 155.35 100.48 o 5 11 0 64.54 -27.07 131.81 o 6 11 0 43.09 42.64 135.70 o 7 11 0 27.07 199.48 132.92 o 0 12 0 2411.67 2405.76 138.67 o 1 12 0 0.40 -55.43 104.56 o 2 12 0 715.96 718.74 102.33 o 3 12 0 256.03 258.80 103.45 o 4 12 0 210.83 533.73 117.16 o 5 12 0 105.91 220.61 110.49 o 6 12 0 217.27 270.85 136.07 o 1 13 0 57.49 46.35 120.50 o 2 13 0 58.96 -31.33 118.65 o 3 13 0 135.52 16.50 133.11 o 4 13 0 129.83 57.47 118.46 o 5 13 0 247.04 454.38 128.84 o 0 14 0 36.95 -78.97 124.76 o 1 14 0 440.15 538.18 116.98 o 2 14 0 12.17 -120.87 134.96 o 3 14 0 361.82 235.25 121.80 o 4 14 0 17.48 -149.79 149.79 o 5 14 0 0.14 -34.48 154.43 o 1 15 0 693.18 739.69 135.52 o 2 15 0 85.60 38.00 145.53 o 3 15 0 2.30 19.84 148.87 o 0 16 0 22.61 -130.14 162.58 o 1 16 0 43.01 202.07 136.81 o 2 16 0 14.73 -172.97 172.97 o 1 0 1 96.61 85.15 13.27 o 2 0 1 476.29 479.73 37.54 o 3 0 1 2.39 -2.04 40.97 o 4 0 1 435.06 416.38 47.64 o 5 0 1 212.76 127.92 65.63 o 6 0 1 1952.85 1893.90 108.82 o 7 0 1 105.40 143.86 96.40 o 8 0 1 1000.19 1017.58 128.10 o 9 0 1 14.20 -166.48 166.48 o -2 1 1 891.52 887.63 34.11 o -1 1 1 854.77 921.55 24.29 o 1 1 1 727.28 747.66 23.91 o 2 1 1 794.60 795.86 34.30 o 3 1 1 8391.81 8684.04 107.52 o 4 1 1 2737.22 2712.75 83.42 o 5 1 1 140.10 153.87 76.94 o 6 1 1 998.07 789.93 118.65 o 7 1 1 862.46 950.66 140.89 o 8 1 1 25.59 194.28 129.21 o 9 1 1 116.46 -67.67 177.97 o -2 2 1 8891.12 9406.49 90.65 o -1 2 1 22594.02 22751.32 144.42 o 0 2 1 287.68 274.65 11.99 o 1 2 1 23055.15 24152.65 149.98 o 2 2 1 8812.61 9477.12 91.95 o 3 2 1 2395.06 2486.95 62.66 o 4 2 1 1193.96 1142.53 59.14 o 5 2 1 5391.95 5288.69 129.96 o 6 2 1 59.53 82.87 75.45 o 7 2 1 60.10 4.82 109.01 o 8 2 1 264.92 117.53 120.13 o 9 2 1 246.13 474.96 147.01 o -2 3 1 3155.79 3356.04 61.36 o -1 3 1 1291.07 1282.50 36.52 o 0 3 1 16616.52 16514.15 374.67 o 1 3 1 1531.74 1542.78 40.41 o 2 3 1 3173.66 3514.55 63.59 o 3 3 1 5714.55 5884.90 91.77 o 4 3 1 6969.49 6799.78 127.17 o 5 3 1 96.36 185.57 60.81 o 6 3 1 1464.15 1481.05 100.11 o 7 3 1 1270.55 1174.98 114.20 o 8 3 1 10.06 29.66 108.08 o 9 3 1 55.70 -24.84 138.85 o -2 4 1 17263.48 16747.96 154.80 o -1 4 1 355.40 336.48 29.29 o 0 4 1 31.74 64.55 38.00 o 1 4 1 325.30 305.15 28.92 o 2 4 1 17239.66 17988.20 160.54 o 3 4 1 1707.39 1753.01 60.25 o 4 4 1 3486.46 3444.66 101.96 o 5 4 1 125.05 138.85 65.44 o 6 4 1 1369.93 1449.35 96.96 o 7 4 1 451.66 403.77 107.52 o 8 4 1 372.74 403.77 124.39 o 9 4 1 52.40 6.67 162.58 o 0 5 1 12162.79 12322.43 130.33 o 1 5 1 1956.41 1950.63 56.54 o 2 5 1 1179.57 1172.38 50.43 o 3 5 1 10405.14 10222.19 147.57 o 4 5 1 716.71 805.50 65.63 o 5 5 1 59.81 154.43 62.48 o 6 5 1 484.13 357.98 87.69 o 7 5 1 1658.32 1878.33 129.96 o 8 5 1 81.95 213.19 107.89 o 9 5 1 83.17 202.63 143.86 o 0 6 1 335.79 370.77 38.75 o 1 6 1 2723.64 2662.89 69.89 o 2 6 1 537.87 524.83 47.83 o 3 6 1 5393.38 5470.56 119.94 o 4 6 1 1325.27 1362.22 86.39 o 5 6 1 3965.35 3958.18 128.84 o 6 6 1 169.73 134.22 86.76 o 7 6 1 138.49 213.01 101.41 o 8 6 1 38.85 -60.07 140.52 o 0 7 1 10661.96 10618.17 134.03 o 1 7 1 1710.99 1832.91 74.34 o 2 7 1 201.43 113.46 53.02 o 3 7 1 2236.00 2178.29 88.80 o 4 7 1 961.63 999.42 80.27 o 5 7 1 563.05 708.17 85.28 o 6 7 1 118.00 231.36 92.14 o 7 7 1 327.11 454.57 113.09 o 8 7 1 153.24 107.71 126.06 o 0 8 1 3.25 -60.44 61.18 o 1 8 1 198.50 260.10 56.91 o 2 8 1 7343.08 7343.88 148.68 o 3 8 1 184.13 270.66 62.85 o 4 8 1 1875.40 1780.45 104.00 o 5 8 1 1084.52 1149.95 103.82 o 6 8 1 1227.41 1321.62 119.94 o 7 8 1 180.75 158.32 115.87 o 8 8 1 245.94 411.19 136.63 o 0 9 1 1997.82 2004.95 95.29 o 1 9 1 1409.35 1480.49 86.95 o 2 9 1 70.99 135.33 61.36 o 3 9 1 1550.97 1608.97 98.07 o 4 9 1 2141.68 2091.34 113.09 o 5 9 1 118.48 27.99 93.25 o 6 9 1 555.62 538.73 113.83 o 7 9 1 353.31 348.90 122.35 o 8 9 1 33.42 133.66 139.97 o 0 10 1 22.48 -10.75 78.79 o 1 10 1 3407.92 3428.53 123.84 o 2 10 1 20.42 117.35 68.22 o 3 10 1 886.24 1085.44 92.32 o 4 10 1 196.70 13.53 106.41 o 5 10 1 575.82 545.96 107.15 o 6 10 1 132.91 68.41 129.40 o 7 10 1 9.72 51.35 148.49 o 0 11 1 1199.14 1151.99 103.63 o 1 11 1 795.51 828.86 96.40 o 2 11 1 208.12 315.90 85.09 o 3 11 1 1447.86 1478.27 115.68 o 4 11 1 700.35 784.74 112.71 o 5 11 1 57.25 48.94 106.78 o 6 11 1 390.81 206.33 124.76 o 7 11 1 119.33 158.69 145.16 o 0 12 1 122.92 281.60 86.95 o 1 12 1 159.30 -23.17 108.45 o 2 12 1 891.55 995.89 113.83 o 3 12 1 146.20 45.05 101.59 o 4 12 1 186.96 32.26 128.84 o 5 12 1 40.84 -58.95 134.78 o 6 12 1 529.56 576.55 138.48 o 0 13 1 636.83 661.46 111.23 o 1 13 1 221.67 220.24 109.75 o 2 13 1 2.73 20.95 115.12 o 3 13 1 33.57 103.26 109.38 o 4 13 1 383.95 322.57 124.95 o 5 13 1 56.62 119.57 129.58 o 0 14 1 5.00 50.80 124.95 o 1 14 1 536.77 722.63 120.50 o 2 14 1 13.41 86.39 105.48 o 3 14 1 171.66 -54.32 144.60 o 4 14 1 35.30 -152.39 152.39 o 5 14 1 135.30 96.59 166.11 o 0 15 1 68.28 -81.01 139.04 o 1 15 1 107.23 367.81 126.43 o 2 15 1 17.27 -147.20 147.20 o 3 15 1 108.03 99.18 155.72 o 0 16 1 0.66 113.09 135.52 o 1 16 1 3.76 -82.87 158.69 o 2 16 1 38.67 229.32 137.74 o 1 0 2 61.03 62.83 14.61 o 2 0 2 27606.92 28119.47 467.36 o 3 0 2 631.92 653.30 48.76 o 4 0 2 1234.90 1311.61 70.45 o 5 0 2 231.84 250.09 70.26 o 6 0 2 1486.75 1293.81 104.19 o 7 0 2 229.94 187.43 104.19 o 8 0 2 7.33 273.63 114.01 o 9 0 2 174.16 171.30 144.04 o -2 1 2 7268.21 7442.51 87.32 o -1 1 2 834.51 897.64 27.25 o 0 1 2 26.08 15.46 10.51 o 1 1 2 797.66 813.47 27.81 o 2 1 2 7332.79 7908.20 90.47 o 3 1 2 317.39 404.14 43.94 o 4 1 2 615.21 672.21 59.51 o 5 1 2 954.84 834.79 90.28 o 6 1 2 82.20 120.32 92.32 o 7 1 2 202.67 131.07 129.40 o 8 1 2 125.14 175.38 141.08 o 9 1 2 75.05 48.94 177.79 o -2 2 2 238.61 236.55 28.73 o -1 2 2 7672.85 8068.56 81.20 o 0 2 2 54.24 41.26 11.93 o 1 2 2 7597.14 7980.69 80.64 o 2 2 2 225.97 219.87 29.29 o 3 2 2 3857.41 4111.12 78.23 o 4 2 2 648.47 647.74 59.32 o 5 2 2 322.00 361.13 66.18 o 6 2 2 547.90 352.05 86.02 o 7 2 2 409.01 283.64 110.86 o 8 2 2 10.41 13.35 143.30 o 9 2 2 43.53 -126.06 172.97 o -2 3 2 4288.70 4415.90 70.82 o -1 3 2 17880.19 18456.11 155.17 o 0 3 2 7.40 12.43 21.32 o 1 3 2 18055.39 18900.48 157.95 o 2 3 2 4206.17 4432.58 72.12 o 3 3 2 182.91 132.92 35.78 o 4 3 2 522.35 709.29 61.55 o 5 3 2 1629.24 1722.24 88.61 o 6 3 2 120.47 78.60 77.68 o 7 3 2 414.15 233.22 106.97 o 8 3 2 238.67 84.17 122.17 o 9 3 2 25.13 -27.99 163.88 o -2 4 2 2215.26 2238.17 58.95 o -1 4 2 930.39 976.06 38.19 o 0 4 2 9533.35 10344.10 131.53 o 1 4 2 920.15 856.11 38.56 o 2 4 2 2090.99 2275.24 59.32 o 3 4 2 1665.02 1643.45 60.62 o 4 4 2 309.05 273.82 57.47 o 5 4 2 230.53 152.02 64.51 o 6 4 2 43.93 55.06 74.34 o 7 4 2 63.49 14.65 111.60 o 8 4 2 10.71 58.21 128.66 o 9 4 2 51.55 -129.58 169.26 o 0 5 2 1667.27 1683.49 51.35 o 1 5 2 676.31 655.90 41.90 o 2 5 2 744.76 757.12 46.90 o 3 5 2 260.82 304.59 52.84 o 4 5 2 643.97 646.81 66.18 o 5 5 2 599.94 596.20 76.56 o 6 5 2 581.72 483.86 88.43 o 7 5 2 2.61 30.22 96.77 o 8 5 2 75.15 64.89 135.52 o 9 5 2 65.82 216.35 135.89 o 0 6 2 2111.46 2087.63 62.85 o 1 6 2 139.18 192.25 37.45 o 2 6 2 383.90 342.22 44.49 o 3 6 2 5533.71 5798.14 122.91 o 4 6 2 88.10 45.79 58.03 o 5 6 2 453.98 426.94 76.56 o 6 6 2 754.79 795.68 102.15 o 7 6 2 300.26 149.05 107.15 o 8 6 2 42.09 -48.57 132.92 o 0 7 2 1823.00 1763.95 66.37 o 1 7 2 1208.04 1316.80 69.33 o 2 7 2 410.13 307.00 56.91 o 3 7 2 651.20 569.32 71.74 o 4 7 2 232.90 269.18 71.56 o 5 7 2 105.48 169.44 78.23 o 6 7 2 10.66 42.64 105.86 o 7 7 2 27.90 -43.75 122.54 o 8 7 2 37.90 198.55 116.98 o 0 8 2 2043.22 2246.14 85.65 o 1 8 2 28.15 -46.35 61.18 o 2 8 2 841.99 829.05 71.19 o 3 8 2 103.20 68.04 64.14 o 4 8 2 212.86 293.47 71.19 o 5 8 2 375.66 405.81 94.36 o 6 8 2 55.40 -30.03 110.68 o 7 8 2 146.75 233.03 115.68 o 8 8 2 19.66 261.58 127.17 o 0 9 2 140.89 131.44 59.32 o 1 9 2 156.57 334.07 60.62 o 2 9 2 661.15 733.20 79.53 o 3 9 2 524.18 552.08 76.38 o 4 9 2 2280.32 2250.22 113.09 o 5 9 2 429.11 388.57 97.14 o 6 9 2 219.36 58.77 126.06 o 7 9 2 16.29 78.97 134.96 o 8 9 2 28.07 13.90 161.47 o 0 10 2 349.11 351.86 71.56 o 1 10 2 1147.50 1134.75 91.95 o 2 10 2 25.67 15.39 78.05 o 3 10 2 73.71 124.21 76.19 o 4 10 2 0.77 105.48 83.61 o 5 10 2 129.45 83.24 101.41 o 6 10 2 120.20 244.71 113.64 o 7 10 2 70.08 -51.54 156.84 o 0 11 2 205.68 324.43 80.27 o 1 11 2 328.92 316.45 89.73 o 2 11 2 193.67 73.78 90.28 o 3 11 2 223.15 208.93 93.43 o 4 11 2 112.27 39.67 115.68 o 5 11 2 73.19 21.88 121.61 o 6 11 2 171.31 129.03 129.96 o 7 11 2 47.53 51.54 141.82 o 0 12 2 297.50 196.88 96.77 o 1 12 2 3.42 27.99 102.15 o 2 12 2 516.87 608.81 105.11 o 3 12 2 260.36 312.93 104.37 o 4 12 2 158.93 231.55 106.60 o 5 12 2 83.88 -136.63 136.63 o 6 12 2 68.16 33.00 155.72 o 0 13 2 194.60 157.39 102.89 o 1 13 2 9.42 56.91 117.35 o 2 13 2 36.41 177.23 93.43 o 3 13 2 35.42 95.29 104.37 o 4 13 2 126.17 208.37 109.01 o 5 13 2 33.92 9.45 126.25 o 0 14 2 77.40 -132.18 132.18 o 1 14 2 156.13 57.10 136.26 o 2 14 2 15.50 57.84 128.10 o 3 14 2 49.19 -12.05 136.44 o 4 14 2 34.52 6.49 149.05 o 0 15 2 12.89 -99.92 135.52 o 1 15 2 203.70 94.55 147.01 o 2 15 2 57.19 224.13 121.24 o 3 15 2 25.81 149.24 133.29 o 0 16 2 0.86 -151.28 167.96 o 1 16 2 53.69 -175.38 175.38 o 1 0 3 1071.93 942.80 26.40 o 2 0 3 1206.16 1386.98 43.47 o 3 0 3 259.74 317.94 44.86 o 4 0 3 731.17 784.92 62.29 o 5 0 3 510.74 537.99 86.58 o 6 0 3 63.09 43.94 100.29 o 7 0 3 36.44 75.45 127.92 o 8 0 3 156.68 -158.69 158.69 o 9 0 3 138.97 23.17 173.89 o -2 1 3 4447.03 4625.75 76.56 o -1 1 3 18522.21 17387.54 143.86 o 0 1 3 10505.28 10784.83 69.02 o 1 1 3 18715.95 18199.54 147.94 o 2 1 3 4485.81 4790.19 79.35 o 3 1 3 4416.90 4490.79 95.47 o 4 1 3 395.08 350.75 64.51 o 5 1 3 100.20 49.87 84.35 o 6 1 3 460.38 574.14 101.41 o 7 1 3 209.31 248.79 125.88 o 8 1 3 24.36 34.11 172.41 o 9 1 3 146.72 138.48 170.37 o -2 2 3 2039.24 2075.21 52.46 o -1 2 3 19479.90 18307.99 149.05 o 0 2 3 368.29 378.84 16.39 o 1 2 3 19489.41 19320.94 154.43 o 2 2 3 1972.66 2048.15 51.17 o 3 2 3 272.61 204.30 39.12 o 4 2 3 223.22 176.67 60.62 o 5 2 3 1914.21 1790.46 101.22 o 6 2 3 175.55 167.77 86.02 o 7 2 3 13.06 111.05 103.82 o 8 2 3 163.41 231.36 129.58 o 9 2 3 49.40 333.14 149.98 o -2 3 3 918.63 951.59 42.27 o -1 3 3 4093.69 3729.23 60.44 o 0 3 3 1185.06 1081.07 25.37 o 1 3 3 4111.82 4120.58 63.77 o 2 3 3 942.72 1017.77 44.68 o 3 3 3 764.87 685.37 45.98 o 4 3 3 300.95 277.34 55.43 o 5 3 3 36.27 59.69 62.10 o 6 3 3 687.13 806.99 94.73 o 7 3 3 34.74 15.57 114.20 o 8 3 3 77.71 -142.75 142.75 o 9 3 3 45.05 261.39 135.89 o -2 4 3 5470.75 5122.59 84.91 o -1 4 3 632.52 555.23 35.96 o 0 4 3 751.09 798.76 25.82 o 1 4 3 629.62 666.28 35.96 o 2 4 3 5559.24 5415.31 86.95 o 3 4 3 23.84 33.74 38.93 o 4 4 3 1022.84 997.19 72.49 o 5 4 3 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