#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:30:06 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180786 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/17/2011784.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011784_Fobs loop_ _publ_author_name 'Arendse, Malcolm J.' 'Anderson, Gordon K.' 'Rath, Nigam P.' _publ_section_title ; [Ethylene-1,2-bis(diphenylphosphine)-P,P']dinitratoplatinum(II) and cis-bis[(diphenylphosphinomethyl)diphenylphosphine oxide-O,P]platinum(II) dinitrate dihydrate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 237 _journal_page_last 239 _journal_volume 57 _journal_year 2001 _space_group_IT_number 9 _symmetry_space_group_name_Hall 'C -2yc' _symmetry_space_group_name_H-M 'C 1 c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.506 _cell_angle_gamma 90.000 _cell_length_a 10.4971 _cell_length_b 15.5281 _cell_length_c 16.3930 _exptl_crystal_F_000 1400.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file bk1556Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' gka10998s/lt/ccd in Cc' _shelx_refln_list_code 4 _shelx_f_calc_maximum 426.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 -20 3685.76 1187.19 1443.78 o 4 0 -20 6351.59 6223.17 1482.07 o 1 1 -20 1527.42 1267.61 842.52 o 3 1 -20 1444.90 1822.91 861.67 o 2 2 -20 644.97 19.15 727.63 o -1 1 -19 7103.88 6805.28 984.22 o 1 1 -19 6615.68 7230.37 1631.43 o 3 1 -19 3485.79 3239.88 758.27 o 5 1 -19 3765.48 4074.74 662.53 o 0 2 -19 6303.05 6598.48 1060.81 o 2 2 -19 3900.26 5154.70 827.20 o 4 2 -19 5045.96 4993.86 697.00 o 6 2 -19 3858.15 4901.95 742.95 o -1 3 -19 397.73 892.31 1344.21 o 1 3 -19 115.87 1685.04 1646.75 o 3 3 -19 152.33 482.54 754.44 o 5 3 -19 128.29 -455.73 704.65 o 0 4 -19 4064.41 4480.69 1018.69 o 2 4 -19 3676.36 5384.48 1194.85 o 4 4 -19 2719.89 3381.58 823.37 o 1 5 -19 2379.94 2990.95 850.18 o 3 5 -19 4645.10 5242.78 980.39 o 5 5 -19 3550.94 1991.42 731.46 o 2 6 -19 186.86 -134.04 1007.20 o 4 6 -19 134.62 1562.50 834.86 o -2 0 -18 7612.30 7529.08 1727.17 o 0 0 -18 11457.86 11699.57 1995.25 o 2 0 -18 7960.30 9106.90 2297.79 o 4 0 -18 3987.39 2470.12 792.74 o 6 0 -18 4878.80 6395.51 880.82 o 8 0 -18 2632.10 3936.88 746.78 o -3 1 -18 1886.50 1022.52 1635.26 o -1 1 -18 2437.80 2343.74 915.29 o 1 1 -18 1867.22 1037.83 834.86 o 3 1 -18 2015.76 2607.99 942.09 o 5 1 -18 1188.94 1363.35 582.11 o 7 1 -18 2069.25 1807.59 528.49 o -2 2 -18 1920.80 1688.87 700.83 o 0 2 -18 4053.51 3940.71 765.93 o 2 2 -18 2653.25 2730.54 750.61 o 4 2 -18 852.15 1466.75 593.60 o 6 2 -18 927.22 340.84 513.17 o -3 3 -18 5152.09 3550.08 2041.20 o -1 3 -18 6386.51 6295.94 773.59 o 1 3 -18 8697.47 10255.79 1003.37 o 3 3 -18 7745.30 8988.18 1022.52 o 5 3 -18 5211.20 6119.77 735.29 o 7 3 -18 8031.33 7552.06 819.54 o -2 4 -18 2237.75 2569.69 792.74 o 0 4 -18 414.52 310.20 628.06 o 2 4 -18 2520.03 1007.20 700.83 o 4 4 -18 2720.87 1302.08 788.91 o 6 4 -18 2489.43 1715.68 697.00 o -1 5 -18 490.45 -34.47 716.14 o 1 5 -18 1788.15 1171.87 777.42 o 3 5 -18 431.42 1761.64 808.06 o 5 5 -18 945.10 1034.00 681.68 o 7 5 -18 1033.14 2167.58 754.44 o 0 6 -18 2947.00 3519.44 942.09 o 2 6 -18 3123.15 5307.89 884.65 o 4 6 -18 7909.05 8655.00 1053.15 o 6 6 -18 6007.27 7084.84 926.77 o -1 7 -18 1601.79 788.91 769.76 o 1 7 -18 2351.82 945.92 785.08 o 3 7 -18 3718.05 4978.54 919.11 o 5 7 -18 3472.92 3975.17 869.33 o 0 8 -18 19.91 1056.98 850.18 o 2 8 -18 170.60 1049.32 815.71 o 4 8 -18 800.96 1677.38 919.11 o -3 1 -17 5644.50 4316.01 1734.83 o -1 1 -17 9053.53 9470.71 1577.81 o 1 1 -17 11235.72 12067.21 1187.19 o 3 1 -17 4917.35 3603.70 639.55 o 5 1 -17 3733.98 3929.22 562.96 o 7 1 -17 5310.09 4741.10 566.79 o 9 1 -17 2516.96 2286.30 578.28 o -4 2 -17 4490.49 6567.84 2113.96 o -2 2 -17 5790.84 5690.85 727.63 o 0 2 -17 8286.77 9060.94 911.46 o 2 2 -17 8349.46 9650.71 930.60 o 4 2 -17 6467.54 6885.70 620.40 o 6 2 -17 6506.03 5721.49 555.30 o 8 2 -17 6678.33 6012.54 651.04 o -3 3 -17 449.55 -1056.98 746.78 o -1 3 -17 37.51 -398.28 578.28 o 1 3 -17 339.23 268.08 677.85 o 3 3 -17 1049.84 1344.21 528.49 o 5 3 -17 879.66 1137.40 639.55 o 7 3 -17 293.99 566.79 509.34 o -4 4 -17 3684.96 3282.01 1072.30 o -2 4 -17 3853.53 2711.39 651.04 o 0 4 -17 4549.42 4787.06 808.06 o 2 4 -17 7500.26 7766.52 873.16 o 4 4 -17 5408.52 5541.50 873.16 o 6 4 -17 4259.74 5587.45 674.02 o 8 4 -17 2777.70 1428.46 543.81 o -3 5 -17 5012.48 5847.87 1236.98 o -1 5 -17 4151.01 5047.47 792.74 o 1 5 -17 6155.46 6908.68 880.82 o 3 5 -17 10097.80 11963.81 1114.43 o 5 5 -17 10837.88 11343.41 980.39 o 7 5 -17 6368.88 6943.15 903.80 o -2 6 -17 220.43 -359.99 643.38 o 0 6 -17 80.37 467.22 662.53 o 2 6 -17 1094.48 1206.34 674.02 o 4 6 -17 713.03 26.81 739.12 o 6 6 -17 317.68 585.94 712.31 o -1 7 -17 1802.04 2094.82 719.97 o 1 7 -17 2302.24 3251.37 758.27 o 3 7 -17 4067.20 5549.16 899.97 o 5 7 -17 7626.01 9267.74 934.43 o 7 7 -17 3765.94 2872.23 777.42 o -2 8 -17 4839.40 5350.01 831.03 o 0 8 -17 3420.69 3182.44 988.05 o 2 8 -17 6206.41 8731.59 1095.28 o 4 8 -17 9827.60 11661.27 1175.70 o 6 8 -17 4803.33 6154.24 934.43 o -1 9 -17 751.50 -294.88 716.14 o 1 9 -17 1080.73 61.27 788.91 o 3 9 -17 672.54 1585.47 907.63 o 5 9 -17 232.70 -471.05 758.27 o 2 10 -17 2378.40 3511.78 1068.47 o -4 0 -16 11503.20 11818.29 1834.40 o -2 0 -16 9928.26 8815.84 1631.43 o 0 0 -16 15245.46 16628.32 1409.31 o 2 0 -16 11985.25 9754.11 1355.69 o 4 0 -16 6205.55 5648.73 942.09 o 6 0 -16 10233.51 10428.12 1102.94 o 8 0 -16 7659.42 9704.32 1256.12 o -5 1 -16 1729.77 1118.26 762.10 o -3 1 -16 3542.91 2768.83 532.32 o -1 1 -16 1398.08 2274.81 788.91 o 1 1 -16 4456.98 5120.24 677.85 o 3 1 -16 3088.46 2313.11 612.74 o 5 1 -16 3583.12 4120.70 551.47 o 7 1 -16 2350.01 3205.41 536.15 o 9 1 -16 2771.43 2565.86 536.15 o -4 2 -16 1826.35 2171.41 907.63 o -2 2 -16 1190.07 379.13 455.73 o 0 2 -16 3524.32 5238.95 888.48 o 2 2 -16 3317.30 3661.14 842.52 o 4 2 -16 880.40 1711.85 444.24 o 6 2 -16 1539.84 846.35 425.09 o 8 2 -16 1828.02 2316.94 532.32 o -5 3 -16 5314.22 6537.20 1198.68 o -3 3 -16 6495.38 6407.00 815.71 o -1 3 -16 6543.56 8183.95 876.99 o 1 3 -16 13108.21 16057.70 1191.02 o 3 3 -16 12200.49 12021.26 861.67 o 5 3 -16 9325.14 10558.33 681.68 o 7 3 -16 9341.66 10167.71 677.85 o 9 3 -16 7853.59 8911.58 823.37 o -4 4 -16 2408.55 1983.76 693.17 o -2 4 -16 2802.09 2397.36 593.60 o 0 4 -16 3520.43 3592.21 654.87 o 2 4 -16 3891.55 4787.06 731.46 o 4 4 -16 7203.22 7789.50 777.42 o 6 4 -16 5257.19 5445.76 593.60 o 8 4 -16 2508.69 1842.06 505.51 o -3 5 -16 288.98 390.62 742.95 o -1 5 -16 1424.51 854.01 597.42 o 1 5 -16 1661.86 1202.51 639.55 o 3 5 -16 684.78 505.51 605.08 o 5 5 -16 1083.41 1608.45 762.10 o 7 5 -16 2046.60 681.68 578.28 o 9 5 -16 569.20 1133.58 547.64 o -4 6 -16 3209.66 2366.72 796.57 o -2 6 -16 6893.06 7027.40 785.08 o 0 6 -16 9481.92 10627.27 976.56 o 2 6 -16 8440.28 9221.79 968.90 o 4 6 -16 13355.32 14870.51 1225.49 o 6 6 -16 8570.88 9486.03 892.31 o 8 6 -16 3802.79 4044.11 842.52 o -3 7 -16 2607.46 2787.98 754.44 o -1 7 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2 -15 7142.31 6663.58 746.78 o -2 2 -15 5229.79 4706.63 520.83 o 0 2 -15 7074.59 6820.60 953.58 o 2 2 -15 9099.29 9723.47 796.57 o 4 2 -15 7831.37 7977.15 670.19 o 6 2 -15 5702.34 6177.22 513.17 o 8 2 -15 8733.17 7693.76 635.72 o 10 2 -15 4418.96 5353.84 800.40 o -5 3 -15 24.02 72.76 635.72 o -3 3 -15 720.40 938.26 428.92 o -1 3 -15 645.60 739.12 517.00 o 1 3 -15 90.50 225.95 543.81 o 3 3 -15 1080.28 827.20 371.48 o 5 3 -15 1111.66 1102.94 398.28 o 7 3 -15 745.46 1325.06 440.41 o 9 3 -15 127.88 153.19 478.71 o -6 4 -15 4546.32 5127.90 999.54 o -4 4 -15 4603.18 4599.40 708.48 o -2 4 -15 7261.89 7755.03 635.72 o 0 4 -15 6256.12 6713.37 762.10 o 2 4 -15 7069.18 7571.21 704.65 o 4 4 -15 7740.75 7475.47 693.17 o 6 4 -15 4264.27 4480.69 517.00 o 8 4 -15 7127.86 7892.90 639.55 o 10 4 -15 4353.56 4940.24 823.37 o -5 5 -15 2305.51 2366.72 750.61 o -3 5 -15 6171.92 6946.98 631.89 o -1 5 -15 10870.13 11887.22 976.56 o 1 5 -15 15149.13 17405.74 1225.49 o 3 5 -15 14487.96 15590.49 1152.72 o 5 5 -15 11904.37 13300.36 842.52 o 7 5 -15 4772.89 4530.47 532.32 o 9 5 -15 2899.78 4086.23 693.17 o -4 6 -15 441.98 1573.98 869.33 o -2 6 -15 891.61 536.15 566.79 o 0 6 -15 320.32 559.13 631.89 o 2 6 -15 1135.88 2290.13 700.83 o 4 6 -15 834.64 -26.81 578.28 o 6 6 -15 1115.62 1183.36 601.25 o 8 6 -15 130.44 413.60 612.74 o -5 7 -15 598.56 1095.28 719.97 o -3 7 -15 2978.56 2408.85 582.11 o -1 7 -15 6552.04 5790.42 777.42 o 1 7 -15 8482.15 7253.35 842.52 o 3 7 -15 4983.99 4955.56 742.95 o 5 7 -15 9169.77 9302.21 846.35 o 7 7 -15 2766.59 2906.70 685.51 o 9 7 -15 1159.65 1095.28 723.80 o -4 8 -15 3870.54 2971.80 811.88 o -2 8 -15 12855.25 12400.39 995.71 o 0 8 -15 7927.19 7923.54 884.65 o 2 8 -15 7684.88 7958.00 949.75 o 4 8 -15 13593.33 14912.64 1221.66 o 6 8 -15 7182.74 6962.30 834.86 o 8 8 -15 3258.73 3029.25 811.88 o -3 9 -15 693.58 892.31 593.60 o -1 9 -15 547.23 1129.75 624.23 o 1 9 -15 234.56 -7.66 685.51 o 3 9 -15 266.74 95.74 854.01 o 5 9 -15 773.55 1409.31 677.85 o 7 9 -15 994.39 1014.86 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490.19 o 9 1 -14 2696.66 1895.67 451.90 o -6 2 -14 2942.86 3354.77 968.90 o -4 2 -14 4697.86 5886.16 608.91 o -2 2 -14 1717.02 1367.18 421.26 o 0 2 -14 1266.09 850.18 451.90 o 2 2 -14 3085.52 2424.17 486.36 o 4 2 -14 1164.30 2068.01 440.41 o 6 2 -14 4205.93 3584.55 432.75 o 8 2 -14 4435.41 4821.52 562.96 o 10 2 -14 2609.65 3140.31 719.97 o -7 3 -14 4268.95 4810.03 1064.64 o -5 3 -14 9286.36 11017.89 1087.62 o -3 3 -14 14574.36 14920.30 762.10 o -1 3 -14 13109.24 12205.08 765.93 o 1 3 -14 14839.34 16348.76 1072.30 o 3 3 -14 9925.84 9715.81 620.40 o 5 3 -14 9039.83 8930.73 582.11 o 7 3 -14 8461.82 8942.22 624.23 o 9 3 -14 10437.44 11259.16 727.63 o -6 4 -14 1244.56 876.99 880.82 o -4 4 -14 3167.32 3216.90 612.74 o -2 4 -14 4468.38 3852.62 494.02 o 0 4 -14 7920.87 9137.53 819.54 o 2 4 -14 6942.02 7337.60 666.36 o 4 4 -14 8046.35 8092.04 589.77 o 6 4 -14 5463.71 5530.01 509.34 o 8 4 -14 1121.81 1095.28 463.39 o 10 4 -14 2775.98 3764.54 727.63 o -5 5 -14 1725.90 2041.20 716.14 o -3 5 -14 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