#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/18/2011805.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011805_Fobs loop_ _publ_author_name 'Cowan, John A.' 'Howard, J. A. K.' 'Leech, M. A.' _publ_section_title ; The 1:1 adduct of 2,5-dihydroxy-1,4-benzoquinone with 4,4'-bipyridine ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 302 _journal_page_last 303 _journal_volume 57 _journal_year 2001 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.843 _cell_angle_gamma 90.000 _cell_length_a 20.8676 _cell_length_b 7.0151 _cell_length_c 9.1087 _exptl_crystal_F_000 616.00 _reflns_d_resolution_high 0.7702 _[local]_cod_data_source_file gd1125Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'diqu in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 275.44 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1594.74 1549.71 43.54 o 4 0 0 107.31 89.68 2.54 o 6 0 0 22.23 15.07 2.01 o 8 0 0 4524.11 4903.07 108.46 o 10 0 0 448.35 516.18 15.73 o 12 0 0 3189.00 3604.92 77.91 o 14 0 0 1037.87 954.81 27.27 o 16 0 0 360.57 343.99 7.98 o 18 0 0 254.58 237.20 7.50 o 20 0 0 151.47 136.81 6.72 o 22 0 0 418.63 444.56 18.08 o 24 0 0 42.15 41.43 5.51 o 26 0 0 155.55 166.48 10.53 o 1 1 0 293.19 260.35 3.75 o 3 1 0 306.33 323.77 4.68 o 5 1 0 615.71 588.91 20.69 o 7 1 0 643.14 596.74 41.02 o 9 1 0 1274.74 1381.51 20.68 o 11 1 0 86.59 82.59 2.81 o 13 1 0 370.27 366.34 4.40 o 15 1 0 872.51 888.17 12.19 o 17 1 0 117.50 132.39 4.34 o 19 1 0 43.49 47.36 3.37 o 21 1 0 36.65 43.98 3.88 o 23 1 0 27.69 35.83 4.48 o 25 1 0 0.27 -0.60 3.98 o 0 2 0 75867.55 72644.16 2058.51 o 2 2 0 1639.62 1725.30 25.94 o 4 2 0 229.40 236.55 4.22 o 6 2 0 26.51 31.78 1.49 o 8 2 0 1906.53 2046.37 25.77 o 10 2 0 43.12 49.22 2.22 o 12 2 0 446.36 495.32 59.28 o 14 2 0 4.27 6.81 2.77 o 16 2 0 654.44 617.53 7.86 o 18 2 0 39.19 42.96 4.43 o 20 2 0 36.59 40.30 5.26 o 22 2 0 57.90 73.45 6.64 o 24 2 0 61.21 83.85 7.10 o 26 2 0 11.45 18.44 4.61 o 1 3 0 974.22 1028.35 15.34 o 3 3 0 57.25 84.22 2.93 o 5 3 0 773.19 880.62 7.97 o 7 3 0 595.68 534.44 6.17 o 9 3 0 2372.86 2467.13 62.66 o 11 3 0 260.70 253.62 4.23 o 13 3 0 682.90 655.95 10.26 o 15 3 0 1939.30 1827.69 31.43 o 17 3 0 184.53 206.72 7.89 o 19 3 0 215.04 190.03 12.31 o 21 3 0 121.50 103.22 17.02 o 23 3 0 49.84 58.19 6.59 o 25 3 0 3.70 9.54 4.92 o 0 4 0 59.71 49.57 3.66 o 2 4 0 5605.23 5546.13 62.23 o 4 4 0 386.71 409.87 9.68 o 6 4 0 182.46 195.30 4.07 o 8 4 0 13.47 18.11 2.03 o 10 4 0 14.68 18.62 2.94 o 12 4 0 279.81 257.56 8.00 o 14 4 0 707.81 669.07 9.94 o 16 4 0 582.49 559.40 12.86 o 18 4 0 185.10 170.33 6.46 o 20 4 0 4.63 2.39 4.38 o 22 4 0 129.67 116.10 7.35 o 24 4 0 50.93 64.18 7.68 o 1 5 0 575.56 627.06 8.27 o 3 5 0 13.12 9.24 1.93 o 5 5 0 337.23 327.42 8.26 o 7 5 0 52.06 66.87 3.53 o 9 5 0 649.21 646.42 12.22 o 11 5 0 293.49 291.09 14.87 o 13 5 0 22.27 25.83 3.67 o 15 5 0 190.56 172.91 5.72 o 17 5 0 8.69 5.71 3.00 o 19 5 0 127.87 118.45 7.47 o 21 5 0 69.67 64.63 7.52 o 0 6 0 1027.48 1013.56 18.95 o 2 6 0 1435.79 1386.15 21.46 o 4 6 0 378.25 355.64 8.11 o 6 6 0 118.05 118.66 3.87 o 8 6 0 63.84 70.29 4.15 o 10 6 0 0.08 -0.20 2.38 o 12 6 0 64.18 71.30 5.70 o 14 6 0 62.97 80.30 4.85 o 16 6 0 40.60 45.45 5.10 o 18 6 0 486.13 465.68 9.99 o 20 6 0 35.31 33.58 7.32 o 1 7 0 141.38 145.10 5.41 o 3 7 0 12.70 13.47 3.10 o 5 7 0 27.35 33.13 3.77 o 7 7 0 199.72 193.16 5.68 o 9 7 0 77.10 73.02 5.35 o 11 7 0 126.71 120.07 5.15 o 13 7 0 81.39 95.43 13.38 o 15 7 0 2.56 3.86 5.20 o 17 7 0 42.53 51.80 6.79 o 0 8 0 47.97 44.43 7.75 o 2 8 0 78.07 82.60 5.67 o 4 8 0 112.99 104.42 5.82 o 6 8 0 21.88 19.78 4.30 o 8 8 0 28.62 26.13 14.03 o 10 8 0 11.34 12.78 6.65 o 12 8 0 25.38 29.10 7.05 o 1 9 0 3.49 7.61 3.92 o 3 9 0 1.17 -1.85 4.69 o -25 1 1 209.20 210.09 10.81 o -23 1 1 48.01 43.82 4.16 o -21 1 1 26.84 36.79 3.36 o -19 1 1 1220.50 1207.43 10.82 o -17 1 1 1631.85 1468.03 13.27 o -15 1 1 30.50 42.26 2.51 o -13 1 1 168.61 152.86 3.97 o -11 1 1 6186.85 6416.10 88.53 o -9 1 1 755.37 951.16 10.84 o -7 1 1 239.25 229.89 2.71 o -5 1 1 0.69 -0.24 0.90 o -3 1 1 40284.28 38414.63 663.98 o -1 1 1 203.62 205.24 5.96 o 1 1 1 2041.29 1990.44 24.98 o 3 1 1 2067.45 2002.92 19.97 o 5 1 1 2015.98 2000.96 23.60 o 7 1 1 2384.77 2319.28 31.28 o 9 1 1 2073.05 2297.76 31.78 o 11 1 1 2190.16 2275.53 29.51 o 13 1 1 186.54 231.20 25.01 o 15 1 1 0.00 -1.65 1.65 o 17 1 1 921.00 852.53 14.05 o 19 1 1 1290.35 1191.97 11.87 o 21 1 1 329.80 322.82 8.18 o 23 1 1 0.86 -1.45 3.18 o 25 1 1 102.51 119.24 6.62 o -26 2 1 120.44 130.69 10.76 o -24 2 1 44.05 53.71 5.97 o -22 2 1 15.53 9.07 3.70 o -20 2 1 23.18 18.94 3.74 o -18 2 1 1284.20 1113.59 26.52 o -16 2 1 1341.20 1356.84 10.83 o -14 2 1 1065.58 1087.60 11.51 o -12 2 1 123.49 151.85 4.10 o -10 2 1 385.04 462.04 7.79 o -8 2 1 46.65 39.92 2.27 o -6 2 1 436.02 458.29 6.98 o -4 2 1 22787.75 20604.02 1250.85 o -2 2 1 36460.91 27374.58 4639.00 o 0 2 1 221.22 207.98 10.77 o 2 2 1 408.25 436.64 7.75 o 4 2 1 1766.28 1870.02 27.17 o 6 2 1 1692.93 1731.66 29.37 o 8 2 1 127.36 145.82 4.00 o 10 2 1 1603.30 1601.09 29.40 o 12 2 1 36.71 27.24 1.93 o 14 2 1 593.44 600.38 6.86 o 16 2 1 227.70 232.41 7.94 o 18 2 1 1271.33 1193.19 26.74 o 20 2 1 149.24 132.97 28.42 o 22 2 1 328.19 260.21 78.69 o 24 2 1 66.63 55.58 4.94 o 26 2 1 56.26 98.16 8.09 o -25 3 1 8.77 6.50 4.92 o -23 3 1 25.21 23.24 5.18 o -21 3 1 61.65 60.41 5.86 o -19 3 1 85.42 88.29 4.81 o -17 3 1 106.06 82.80 5.21 o -15 3 1 12.14 17.86 2.31 o -13 3 1 8.31 3.11 2.24 o -11 3 1 284.01 307.71 25.32 o -9 3 1 1101.43 1121.78 57.37 o -7 3 1 559.32 599.50 9.28 o -5 3 1 377.29 416.04 7.57 o -3 3 1 5135.59 5303.28 64.95 o -1 3 1 1259.06 1321.65 14.08 o 1 3 1 221.47 183.47 2.96 o 3 3 1 921.54 938.31 14.93 o 5 3 1 78.05 76.17 2.59 o 7 3 1 249.74 242.16 3.80 o 9 3 1 15.97 39.81 3.18 o 11 3 1 490.68 491.23 9.58 o 13 3 1 503.02 465.29 12.55 o 15 3 1 29.24 25.27 2.62 o 17 3 1 440.73 433.67 7.50 o 19 3 1 454.85 432.69 16.80 o 21 3 1 491.63 518.17 12.50 o 23 3 1 10.83 9.74 3.60 o 25 3 1 424.80 484.86 18.27 o -24 4 1 9.06 6.31 5.20 o -22 4 1 1.98 0.17 3.62 o -20 4 1 137.29 86.89 28.15 o -18 4 1 412.42 323.87 59.96 o -16 4 1 185.61 195.79 5.52 o -14 4 1 529.56 527.95 7.79 o -12 4 1 116.10 119.50 4.22 o -10 4 1 507.33 536.85 8.07 o -8 4 1 4.55 4.47 1.81 o -6 4 1 2.24 4.87 1.53 o -4 4 1 3146.68 3280.76 39.63 o -2 4 1 9061.76 9238.74 70.72 o 0 4 1 668.98 678.05 7.13 o 2 4 1 367.42 352.81 5.79 o 4 4 1 423.86 419.37 5.09 o 6 4 1 1715.01 1684.46 24.06 o 8 4 1 98.48 91.29 4.05 o 10 4 1 168.26 169.09 5.80 o 12 4 1 237.27 242.50 5.57 o 14 4 1 718.84 709.53 8.89 o 16 4 1 298.42 288.43 10.68 o 18 4 1 1028.84 955.15 14.97 o 20 4 1 56.42 62.91 5.22 o 22 4 1 198.50 202.37 7.94 o 24 4 1 18.11 22.59 5.61 o -21 5 1 194.15 172.22 8.85 o -19 5 1 15.35 24.81 4.68 o -17 5 1 149.84 165.32 10.87 o -15 5 1 40.80 45.27 4.38 o -13 5 1 4.23 9.82 3.92 o -11 5 1 59.65 68.11 3.97 o -9 5 1 389.27 380.84 10.04 o -7 5 1 420.85 456.86 11.30 o -5 5 1 890.91 913.30 14.57 o -3 5 1 39.39 50.64 3.95 o -1 5 1 457.38 491.31 7.73 o 1 5 1 342.17 338.25 5.19 o 3 5 1 275.77 261.76 7.05 o 5 5 1 343.16 332.54 6.87 o 7 5 1 0.01 4.09 2.08 o 9 5 1 57.05 63.76 3.29 o 11 5 1 928.48 875.22 13.97 o 13 5 1 404.84 378.10 7.14 o 15 5 1 10.33 7.91 4.14 o 17 5 1 36.19 34.61 3.97 o 19 5 1 106.30 104.81 5.95 o 21 5 1 306.01 315.42 19.10 o -20 6 1 77.95 78.10 11.10 o -18 6 1 15.05 24.19 4.84 o -16 6 1 247.74 258.13 8.07 o -14 6 1 24.27 26.15 4.03 o -12 6 1 51.74 61.10 4.96 o -10 6 1 127.68 135.19 5.02 o -8 6 1 19.61 21.49 2.57 o -6 6 1 60.71 70.88 4.04 o -4 6 1 314.87 278.06 4.92 o -2 6 1 194.78 181.18 6.18 o 0 6 1 232.16 241.66 7.62 o 2 6 1 56.54 58.49 3.86 o 4 6 1 66.37 71.16 4.07 o 6 6 1 378.97 367.04 12.32 o 8 6 1 331.22 314.89 7.62 o 10 6 1 142.66 149.41 8.36 o 12 6 1 743.97 713.77 32.45 o 14 6 1 158.08 161.71 9.15 o 16 6 1 56.85 54.56 5.36 o 18 6 1 159.71 153.24 7.40 o 20 6 1 5.56 -1.71 6.53 o -17 7 1 162.76 164.90 15.13 o -15 7 1 66.95 76.53 5.95 o -13 7 1 31.23 36.85 4.94 o -11 7 1 36.51 34.23 5.43 o -9 7 1 23.55 25.12 3.98 o -7 7 1 125.84 113.26 5.30 o -5 7 1 566.77 555.37 8.77 o -3 7 1 19.40 21.07 3.83 o -1 7 1 1.69 2.00 2.59 o 1 7 1 134.67 125.72 4.91 o 3 7 1 0.11 -1.81 2.53 o 5 7 1 30.00 32.22 3.69 o 7 7 1 48.70 62.81 4.59 o 9 7 1 26.36 29.71 4.35 o 11 7 1 8.58 11.58 3.50 o 13 7 1 15.06 19.69 5.02 o 15 7 1 31.71 33.52 5.70 o 17 7 1 2.87 4.99 6.12 o -12 8 1 31.14 37.08 7.61 o -10 8 1 4.38 4.63 5.72 o -8 8 1 23.30 25.20 6.64 o -6 8 1 1.72 -3.09 4.81 o -4 8 1 473.26 428.89 15.03 o -2 8 1 8.12 9.84 4.38 o 0 8 1 1.20 -3.40 3.40 o 2 8 1 4.96 0.30 3.70 o 4 8 1 171.32 176.74 6.38 o 6 8 1 39.13 48.87 4.80 o 8 8 1 44.27 53.89 5.47 o 10 8 1 9.22 10.89 3.84 o 12 8 1 196.84 185.60 8.46 o -3 9 1 32.23 19.00 5.74 o -1 9 1 8.06 5.05 5.10 o 1 9 1 27.07 32.37 6.81 o 3 9 1 2.89 7.93 4.61 o -26 0 2 21.15 41.30 10.10 o -24 0 2 4.73 -3.03 3.88 o -22 0 2 531.74 553.45 11.47 o -20 0 2 4701.56 4139.82 176.32 o -18 0 2 415.40 494.61 18.47 o -16 0 2 685.46 619.95 15.67 o -14 0 2 624.75 673.89 17.15 o -12 0 2 666.47 853.30 8.12 o -10 0 2 282.30 286.32 6.29 o -8 0 2 3523.60 3633.92 62.86 o -6 0 2 16935.32 16743.97 212.69 o -4 0 2 634.67 734.39 12.93 o -2 0 2 383.62 420.78 7.91 o 0 0 2 726.17 728.10 8.55 o 2 0 2 9402.41 9266.39 94.36 o 4 0 2 3785.08 3502.35 105.34 o 6 0 2 0.10 -1.71 1.71 o 8 0 2 3604.02 3759.73 145.86 o 10 0 2 1709.74 1831.55 45.91 o 12 0 2 571.35 563.99 97.27 o 14 0 2 334.30 327.64 13.51 o 16 0 2 8759.22 8498.04 285.44 o 18 0 2 1628.92 1500.08 58.73 o 20 0 2 988.52 904.37 41.47 o 22 0 2 13.10 1.04 7.32 o 24 0 2 220.35 252.51 16.03 o 26 0 2 30.89 41.13 9.76 o -25 1 2 14.25 9.32 4.45 o -23 1 2 46.08 49.82 4.32 o -21 1 2 28.10 45.75 3.60 o -19 1 2 5.80 5.98 2.42 o -17 1 2 77.52 76.20 3.57 o -15 1 2 66.46 73.31 2.97 o -13 1 2 461.28 442.38 5.66 o -11 1 2 1.33 1.02 1.24 o -9 1 2 85.48 87.79 2.43 o -7 1 2 1597.47 1684.77 20.96 o -5 1 2 3846.15 4075.58 58.32 o -3 1 2 581.30 603.56 4.28 o -1 1 2 718.07 734.52 6.88 o 1 1 2 350.02 363.67 3.23 o 3 1 2 8.81 6.37 1.30 o 5 1 2 128.19 125.80 4.81 o 7 1 2 2707.44 2932.04 51.33 o 9 1 2 1141.90 1214.45 15.65 o 11 1 2 0.10 -0.66 1.46 o 13 1 2 0.18 1.34 1.61 o 15 1 2 69.25 66.30 3.61 o 17 1 2 58.09 67.27 4.86 o 19 1 2 15.01 12.39 3.07 o 21 1 2 23.34 22.30 7.32 o 23 1 2 135.81 128.84 6.76 o 25 1 2 84.50 87.44 14.12 o -26 2 2 14.17 24.71 5.99 o -24 2 2 0.08 -2.54 4.34 o -22 2 2 48.20 58.70 4.92 o -20 2 2 1218.01 1072.65 21.75 o -18 2 2 0.12 1.00 2.05 o -16 2 2 254.06 215.68 4.39 o -14 2 2 349.99 369.95 10.27 o -12 2 2 695.69 784.21 12.71 o -10 2 2 90.03 95.31 2.46 o -8 2 2 105.69 122.02 3.36 o -6 2 2 843.93 811.46 17.17 o -4 2 2 94.50 83.92 2.73 o -2 2 2 3.31 10.15 1.84 o 0 2 2 1868.72 1895.14 23.59 o 2 2 2 1982.97 1983.25 14.22 o 4 2 2 2680.39 2753.83 24.71 o 6 2 2 542.05 639.25 13.44 o 8 2 2 692.41 637.91 7.74 o 10 2 2 917.69 968.39 13.61 o 12 2 2 14.45 18.76 2.14 o 14 2 2 686.65 648.67 7.59 o 16 2 2 3574.60 3402.07 25.29 o 18 2 2 1089.00 1031.86 12.27 o 20 2 2 253.28 244.13 6.68 o 22 2 2 40.83 45.68 4.64 o 24 2 2 28.00 33.08 4.59 o -25 3 2 26.33 28.88 7.55 o -23 3 2 117.09 116.54 8.10 o -21 3 2 96.92 120.71 6.93 o -19 3 2 112.83 98.08 9.64 o -17 3 2 200.49 202.78 6.07 o -15 3 2 68.88 76.25 4.08 o -13 3 2 859.62 775.32 15.57 o -11 3 2 30.65 44.28 2.30 o -9 3 2 304.02 324.11 7.55 o -7 3 2 3342.93 3547.60 30.52 o -5 3 2 7763.84 8128.27 57.22 o -3 3 2 197.73 206.41 4.32 o -1 3 2 522.82 584.11 5.89 o 1 3 2 969.53 945.09 10.57 o 3 3 2 1.34 1.89 1.07 o 5 3 2 29.97 37.18 2.22 o 7 3 2 2525.12 2625.91 44.34 o 9 3 2 396.32 392.13 9.67 o 11 3 2 165.78 164.77 4.40 o 13 3 2 0.49 -0.85 1.76 o 15 3 2 434.54 418.46 6.29 o 17 3 2 179.92 166.31 5.56 o 19 3 2 3.89 3.88 2.84 o 21 3 2 0.22 1.10 2.93 o 23 3 2 157.82 139.55 6.59 o -24 4 2 24.29 31.99 9.22 o -22 4 2 140.97 180.17 11.34 o -20 4 2 113.61 121.41 7.24 o -18 4 2 599.29 570.34 18.63 o -16 4 2 0.03 -0.39 3.21 o -14 4 2 78.32 73.26 4.32 o -12 4 2 270.29 271.56 6.30 o -10 4 2 6.71 14.67 2.19 o -8 4 2 955.56 914.36 17.43 o -6 4 2 2846.20 2839.64 83.72 o -4 4 2 595.49 572.82 27.14 o -2 4 2 861.34 821.06 31.43 o 0 4 2 1915.80 1838.80 35.54 o 2 4 2 326.31 303.28 4.63 o 4 4 2 257.98 290.95 4.36 o 6 4 2 842.93 848.33 22.46 o 8 4 2 48.88 65.55 3.27 o 10 4 2 231.59 240.59 6.60 o 12 4 2 391.53 393.87 8.12 o 14 4 2 855.31 821.77 29.50 o 16 4 2 160.18 158.21 5.21 o 18 4 2 235.42 261.56 7.71 o 20 4 2 91.40 89.89 6.12 o 22 4 2 73.98 94.79 9.36 o -21 5 2 16.89 28.29 5.46 o -19 5 2 183.27 182.12 7.22 o -17 5 2 50.47 39.73 9.71 o -15 5 2 1.94 -2.17 2.77 o -13 5 2 144.44 125.89 12.05 o -11 5 2 8.82 10.24 2.58 o -9 5 2 189.27 193.48 5.40 o -7 5 2 288.13 309.95 8.87 o -5 5 2 1349.31 1357.41 18.43 o -3 5 2 229.54 219.78 4.09 o -1 5 2 124.71 138.59 3.54 o 1 5 2 64.59 74.21 3.13 o 3 5 2 144.56 133.12 15.08 o 5 5 2 11.52 8.97 2.50 o 7 5 2 1.59 2.60 1.95 o 9 5 2 993.53 965.56 37.80 o 11 5 2 716.97 720.53 22.37 o 13 5 2 5.82 2.52 3.20 o 15 5 2 349.92 356.74 10.76 o 17 5 2 59.89 66.84 10.25 o 19 5 2 73.71 69.98 10.63 o 21 5 2 240.91 251.89 13.10 o -20 6 2 233.73 244.81 16.67 o -18 6 2 321.83 299.44 10.21 o -16 6 2 10.11 16.73 3.74 o -14 6 2 25.62 19.22 4.41 o -12 6 2 10.44 14.73 3.38 o -10 6 2 25.52 27.01 3.33 o -8 6 2 139.51 144.03 8.30 o -6 6 2 925.00 919.52 15.43 o -4 6 2 106.07 109.34 4.10 o -2 6 2 1304.61 1243.92 14.64 o 0 6 2 455.90 438.56 10.93 o 2 6 2 336.15 326.61 6.50 o 4 6 2 29.82 31.83 3.95 o 6 6 2 15.29 16.43 2.97 o 8 6 2 0.02 2.37 2.35 o 10 6 2 4.10 1.39 2.77 o 12 6 2 499.94 493.63 11.13 o 14 6 2 355.28 339.98 9.94 o 16 6 2 21.84 25.52 5.84 o 18 6 2 8.11 15.16 5.99 o -15 7 2 36.29 32.97 5.33 o -13 7 2 2.36 -1.63 3.92 o -11 7 2 4.88 5.62 3.67 o -9 7 2 54.56 52.11 4.50 o -7 7 2 70.87 82.22 5.77 o -5 7 2 199.35 164.27 6.34 o -3 7 2 228.58 211.58 7.05 o -1 7 2 8.97 16.57 3.14 o 1 7 2 0.67 -1.97 2.93 o 3 7 2 182.35 182.99 5.63 o 5 7 2 0.16 -0.84 2.84 o 7 7 2 124.27 125.76 4.94 o 9 7 2 1038.96 967.89 13.41 o 11 7 2 230.48 250.23 10.06 o 13 7 2 9.66 12.05 4.27 o 15 7 2 75.77 86.06 7.26 o -12 8 2 5.46 9.21 6.40 o -10 8 2 29.65 29.16 5.39 o -8 8 2 32.75 26.77 4.46 o -6 8 2 28.34 37.17 4.96 o -4 8 2 0.01 -3.33 3.33 o -2 8 2 563.40 509.77 10.99 o 0 8 2 37.94 38.41 4.60 o 2 8 2 14.92 15.66 4.22 o 4 8 2 165.56 147.21 8.33 o 6 8 2 176.89 181.07 6.74 o 8 8 2 77.00 84.86 7.02 o 10 8 2 8.69 7.21 4.09 o -25 1 3 47.15 66.36 6.02 o -23 1 3 389.51 333.28 7.88 o -21 1 3 4.05 2.30 2.37 o -19 1 3 440.33 387.25 9.90 o -17 1 3 12.85 12.59 2.37 o -15 1 3 269.72 258.39 4.06 o -13 1 3 138.44 138.77 3.10 o -11 1 3 575.16 579.42 4.98 o -9 1 3 5434.86 5634.40 44.06 o -7 1 3 1503.29 1597.53 21.60 o -5 1 3 942.76 973.60 11.55 o -3 1 3 288.06 301.68 3.38 o -1 1 3 966.77 1004.00 11.25 o 1 1 3 3935.29 4081.71 40.42 o 3 1 3 3.37 1.44 1.46 o 5 1 3 10085.86 10801.51 164.43 o 7 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6.03 4.34 o -5 1 11 33.21 25.82 4.91 o -3 1 11 40.57 54.82 6.02 o -1 1 11 199.99 212.63 11.65 o 1 1 11 215.81 242.87 8.27 o 3 1 11 15.28 22.07 5.06 o 5 1 11 1.49 1.41 4.24 o 7 1 11 98.80 118.46 7.03 o -8 2 11 45.46 60.11 6.39 o -6 2 11 16.57 32.58 5.12 o -4 2 11 49.46 60.24 5.81 o -2 2 11 3.34 3.43 4.18 o 0 2 11 16.69 14.01 5.13 o 2 2 11 91.54 91.81 6.90 o 4 2 11 9.80 8.54 5.45 o 6 2 11 187.55 229.33 9.05 o -5 3 11 211.81 218.79 8.01 o -3 3 11 89.31 94.67 6.88 o -1 3 11 184.46 212.79 7.02 o 1 3 11 72.33 101.89 8.05 o 3 3 11 58.19 75.42 9.37 o