#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2011812.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011812_Fobs loop_ _publ_author_name 'Burgess, John' 'Fawcett, John' 'Palma, Vitor' 'Gilani, Syeda R.' _publ_section_title ; Fluoro derivatives of bis(salicylideneaminato-N,O)copper(II) and -oxovanadium(IV) ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 277 _journal_page_last 280 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.840 _cell_angle_gamma 90.000 _cell_length_a 27.3920 _cell_length_b 10.0480 _cell_length_c 9.6540 _exptl_crystal_F_000 1268.00 _reflns_d_resolution_high 0.8737 _[local]_cod_data_source_file gg1032Vsup6.hkl _[local]_cod_data_source_block V #BEGIN Tags that were not found in dictionaries: _shelx_title ' OV(C14H12NO2) P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 315.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 27864.33 29416.77 146.36 o 5 0 0 1210.06 1270.90 38.56 o 6 0 0 5441.41 5929.77 83.55 o 7 0 0 1938.11 2088.68 56.85 o 8 0 0 18846.11 19152.92 169.59 o 9 0 0 1268.07 1317.28 43.55 o 10 0 0 880.59 923.98 43.27 o 11 0 0 1769.90 1970.48 63.91 o 12 0 0 2518.71 2430.62 78.38 o 13 0 0 12671.12 13679.38 346.83 o 14 0 0 5890.61 7098.44 142.94 o 15 0 0 208.36 382.35 38.51 o 16 0 0 6586.99 6346.88 147.15 o 17 0 0 4270.41 4437.03 128.83 o 18 0 0 567.56 590.77 21.84 o 19 0 0 921.54 882.86 32.68 o 20 0 0 208.35 219.08 15.03 o 21 0 0 1152.24 1122.85 44.77 o 22 0 0 46.11 58.22 29.89 o 23 0 0 555.42 588.32 27.93 o 24 0 0 114.36 101.47 14.99 o 25 0 0 518.43 548.25 22.81 o 26 0 0 204.04 229.03 21.03 o 27 0 0 1436.84 1407.45 50.06 o 28 0 0 21.03 30.24 16.39 o 29 0 0 287.26 282.48 21.36 o 30 0 0 5.78 5.29 17.36 o 31 0 0 61.21 94.54 28.22 o 2 1 0 2068.29 2108.43 27.49 o 3 1 0 4437.95 4674.93 43.12 o 4 1 0 606.37 631.49 16.07 o 5 1 0 2981.54 2904.83 41.74 o 6 1 0 145.20 183.79 23.93 o 7 1 0 2849.65 2939.12 47.70 o 8 1 0 2470.06 2422.68 48.88 o 9 1 0 163.99 221.10 6.90 o 10 1 0 429.84 452.66 10.19 o 11 1 0 3795.63 3801.69 66.32 o 12 1 0 4413.24 4771.46 77.97 o 13 1 0 38.40 49.53 13.43 o 14 1 0 6674.82 7194.26 102.98 o 15 1 0 6490.15 6739.07 172.65 o 16 1 0 7.02 -6.05 15.15 o 17 1 0 469.98 436.62 11.87 o 18 1 0 1531.23 1555.21 39.75 o 19 1 0 2219.17 2102.80 52.19 o 20 1 0 940.43 903.04 31.93 o 21 1 0 42.59 46.21 10.76 o 22 1 0 502.10 491.73 20.34 o 23 1 0 1.82 0.56 9.75 o 24 1 0 745.56 720.93 18.88 o 25 1 0 575.24 552.67 16.80 o 26 1 0 81.43 66.33 20.69 o 27 1 0 281.92 260.25 14.46 o 28 1 0 382.89 404.71 17.29 o 29 1 0 168.41 195.90 14.70 o 30 1 0 97.88 99.77 13.93 o 31 1 0 68.66 45.36 18.34 o 0 2 0 3471.46 3479.80 89.78 o 1 2 0 630.04 643.55 20.64 o 2 2 0 4097.34 4415.27 91.87 o 3 2 0 28340.59 28584.11 416.15 o 4 2 0 5271.25 5299.72 114.37 o 5 2 0 12176.86 12365.68 132.79 o 6 2 0 3860.39 4066.32 242.13 o 7 2 0 1355.19 1388.70 87.99 o 8 2 0 4.50 13.42 7.60 o 9 2 0 40.96 52.18 8.19 o 10 2 0 6.96 15.35 8.01 o 11 2 0 2349.56 2637.24 84.36 o 12 2 0 1203.00 1309.33 46.79 o 13 2 0 146.57 186.63 11.67 o 14 2 0 237.09 243.26 12.84 o 15 2 0 839.29 798.12 30.30 o 16 2 0 164.75 194.97 12.82 o 17 2 0 3212.33 3551.03 117.28 o 18 2 0 126.92 111.22 35.10 o 19 2 0 263.84 271.46 16.97 o 20 2 0 129.13 127.41 36.39 o 21 2 0 4739.58 4830.99 159.51 o 22 2 0 119.45 73.42 26.84 o 23 2 0 1.11 2.43 14.53 o 24 2 0 1051.55 1026.85 38.50 o 25 2 0 2.44 -10.08 18.84 o 26 2 0 18.27 6.78 29.34 o 27 2 0 88.82 87.18 17.45 o 28 2 0 130.33 111.35 18.06 o 29 2 0 14.67 -1.22 20.84 o 30 2 0 3.82 3.50 17.03 o 1 3 0 261.42 274.12 11.01 o 2 3 0 18478.96 19447.76 176.63 o 3 3 0 29611.04 30697.47 621.59 o 4 3 0 5790.10 6139.40 105.56 o 5 3 0 2015.00 2111.91 66.35 o 6 3 0 5171.74 5435.67 105.51 o 7 3 0 7321.33 7074.63 123.88 o 8 3 0 556.44 517.77 15.13 o 9 3 0 1338.20 1361.92 71.73 o 10 3 0 703.48 687.63 23.05 o 11 3 0 695.16 600.51 46.52 o 12 3 0 259.83 232.35 12.38 o 13 3 0 2162.06 2340.81 98.49 o 14 3 0 3179.54 3502.67 240.67 o 15 3 0 1651.26 1668.42 59.65 o 16 3 0 391.82 392.19 16.56 o 17 3 0 107.14 99.90 16.55 o 18 3 0 200.74 186.02 15.01 o 19 3 0 1230.06 1238.89 62.11 o 20 3 0 1966.42 1987.43 62.05 o 21 3 0 104.32 88.65 23.72 o 22 3 0 2604.29 2812.80 192.53 o 23 3 0 437.12 419.08 39.76 o 24 3 0 1145.60 1130.16 45.68 o 25 3 0 12.74 -12.61 21.97 o 26 3 0 1018.86 997.47 37.19 o 27 3 0 0.63 -4.73 22.84 o 28 3 0 18.92 0.80 17.40 o 29 3 0 26.26 6.92 17.41 o 30 3 0 97.06 95.97 19.27 o 0 4 0 3584.96 3563.75 129.80 o 1 4 0 884.29 938.05 29.66 o 2 4 0 6515.25 6921.53 123.12 o 3 4 0 1533.08 1538.32 60.02 o 4 4 0 7709.40 7843.20 167.48 o 5 4 0 4285.92 4690.38 106.81 o 6 4 0 6457.66 6728.22 255.01 o 7 4 0 382.54 472.18 18.51 o 8 4 0 5799.40 5913.12 289.98 o 9 4 0 3080.72 3343.82 101.46 o 10 4 0 6208.44 6769.01 214.12 o 11 4 0 510.48 587.27 20.59 o 12 4 0 1973.61 2018.75 114.62 o 13 4 0 796.75 828.00 26.52 o 14 4 0 1154.30 1159.13 39.69 o 15 4 0 719.31 682.38 25.54 o 16 4 0 974.35 956.77 41.35 o 17 4 0 1637.41 1660.17 60.84 o 18 4 0 908.37 942.98 37.01 o 19 4 0 111.68 136.58 15.65 o 20 4 0 4.49 -15.24 23.88 o 21 4 0 768.12 768.69 27.72 o 22 4 0 227.01 248.35 33.30 o 23 4 0 592.98 631.75 32.18 o 24 4 0 295.49 287.64 36.43 o 25 4 0 477.65 474.70 24.87 o 26 4 0 437.76 413.09 44.64 o 27 4 0 132.88 113.76 21.01 o 28 4 0 53.45 73.05 17.70 o 29 4 0 145.20 160.82 20.73 o 1 5 0 6222.48 6320.57 133.40 o 2 5 0 3154.57 3504.03 100.57 o 3 5 0 6.09 34.92 9.34 o 4 5 0 71.29 60.15 27.26 o 5 5 0 36.96 103.47 11.46 o 6 5 0 3456.44 3687.63 273.64 o 7 5 0 499.58 821.20 48.56 o 8 5 0 92.62 104.19 10.96 o 9 5 0 607.16 610.25 21.99 o 10 5 0 45.75 38.38 10.41 o 11 5 0 4383.80 4602.23 134.83 o 12 5 0 236.50 206.97 14.74 o 13 5 0 182.70 177.24 23.67 o 14 5 0 21.57 1.99 30.93 o 15 5 0 387.92 404.24 18.26 o 16 5 0 571.29 612.02 23.45 o 17 5 0 223.26 230.34 16.70 o 18 5 0 2.52 24.77 20.88 o 19 5 0 1.08 14.41 16.92 o 20 5 0 606.26 580.68 60.81 o 21 5 0 924.11 999.66 40.26 o 22 5 0 1864.68 2011.98 143.18 o 23 5 0 93.96 98.16 25.30 o 24 5 0 298.77 307.40 22.66 o 25 5 0 179.59 232.72 32.89 o 26 5 0 237.63 278.20 21.78 o 27 5 0 498.13 560.38 27.64 o 28 5 0 381.34 365.16 25.77 o 0 6 0 6321.60 6912.84 220.58 o 1 6 0 387.34 354.21 15.86 o 2 6 0 12.05 12.58 10.24 o 3 6 0 806.06 820.42 27.34 o 4 6 0 57.74 48.22 10.42 o 5 6 0 202.86 208.06 13.34 o 6 6 0 203.22 198.01 13.44 o 7 6 0 472.28 436.34 16.58 o 8 6 0 101.90 94.39 12.35 o 9 6 0 26.36 20.88 11.40 o 10 6 0 0.08 18.81 10.96 o 11 6 0 321.21 317.92 16.95 o 12 6 0 121.08 131.08 22.22 o 13 6 0 227.17 191.50 15.03 o 14 6 0 713.05 720.34 32.26 o 15 6 0 66.95 46.01 13.82 o 16 6 0 61.02 64.83 15.88 o 17 6 0 95.14 96.08 15.15 o 18 6 0 1189.00 1132.27 50.87 o 19 6 0 1090.14 1063.87 35.72 o 20 6 0 2.21 -20.84 25.51 o 21 6 0 165.00 155.80 19.57 o 22 6 0 37.89 16.47 17.63 o 23 6 0 4.86 10.19 26.93 o 24 6 0 162.42 129.48 20.69 o 25 6 0 1.60 -21.49 32.51 o 26 6 0 25.55 22.66 19.74 o 1 7 0 940.13 912.97 30.41 o 2 7 0 215.98 212.83 15.42 o 3 7 0 95.81 65.29 36.68 o 4 7 0 284.50 315.50 17.06 o 5 7 0 468.48 453.56 18.29 o 6 7 0 23.80 24.56 12.67 o 7 7 0 1158.80 1238.37 37.78 o 8 7 0 103.19 89.98 13.91 o 9 7 0 1774.77 1811.97 61.66 o 10 7 0 196.10 240.93 16.34 o 11 7 0 574.82 479.98 20.17 o 12 7 0 33.02 48.38 13.96 o 13 7 0 299.11 303.64 36.14 o 14 7 0 32.19 5.74 14.20 o 15 7 0 463.22 416.81 21.30 o 16 7 0 317.65 325.87 20.71 o 17 7 0 1024.51 1077.90 39.52 o 18 7 0 2616.86 2768.58 87.41 o 19 7 0 2.05 -2.59 29.30 o 20 7 0 1469.47 1339.43 44.41 o 21 7 0 129.03 124.93 19.04 o 22 7 0 556.44 565.67 47.27 o 23 7 0 0.84 9.76 16.80 o 24 7 0 29.55 42.53 17.62 o 0 8 0 926.87 944.33 54.77 o 1 8 0 536.78 495.94 20.89 o 2 8 0 349.62 416.24 19.59 o 3 8 0 27.87 55.67 14.70 o 4 8 0 2261.33 2130.40 99.70 o 5 8 0 461.24 436.70 20.15 o 6 8 0 1607.53 1728.31 61.83 o 7 8 0 118.62 167.84 17.65 o 8 8 0 3187.62 3104.88 131.34 o 9 8 0 39.59 28.46 15.11 o 10 8 0 737.56 800.28 28.16 o 11 8 0 1.23 -14.78 23.72 o 12 8 0 1025.97 922.69 32.68 o 13 8 0 214.52 220.27 53.44 o 14 8 0 433.83 448.78 22.30 o 15 8 0 105.55 143.51 18.30 o 16 8 0 561.42 507.02 64.23 o 17 8 0 2.75 23.28 16.59 o 18 8 0 15.35 8.76 16.58 o 19 8 0 3.53 6.14 16.77 o 20 8 0 313.68 338.69 53.19 o 21 8 0 1.51 15.13 29.01 o 22 8 0 99.77 120.13 23.09 o 1 9 0 12.05 -8.93 15.81 o 2 9 0 574.95 509.61 23.93 o 3 9 0 1285.09 1287.03 41.52 o 4 9 0 175.10 208.90 18.21 o 5 9 0 338.81 358.41 20.57 o 6 9 0 0.16 19.12 14.10 o 7 9 0 586.47 615.34 25.79 o 8 9 0 5.30 -15.90 15.90 o 9 9 0 1353.35 1360.31 50.84 o 10 9 0 0.22 -1.64 15.50 o 11 9 0 318.84 324.29 22.05 o 12 9 0 306.28 350.32 25.97 o 13 9 0 718.53 689.67 36.51 o 14 9 0 69.02 63.00 18.71 o 15 9 0 214.05 239.19 29.59 o 16 9 0 402.76 388.69 35.10 o 17 9 0 1322.81 1238.89 41.20 o 18 9 0 108.01 112.04 21.04 o 19 9 0 0.33 -7.45 23.72 o 0 10 0 1528.90 1749.61 88.11 o 1 10 0 322.79 433.92 24.64 o 2 10 0 542.63 460.49 24.13 o 3 10 0 55.74 78.45 33.97 o 4 10 0 298.49 240.09 20.84 o 5 10 0 0.02 -16.10 16.46 o 6 10 0 2.50 5.39 15.41 o 7 10 0 0.73 -11.00 16.65 o 8 10 0 8.78 -5.53 16.41 o 9 10 0 15.50 -14.16 21.26 o 10 10 0 28.04 23.30 17.88 o 11 10 0 3.04 -14.50 25.18 o 12 10 0 1.08 15.94 17.88 o 13 10 0 28.02 -4.98 19.11 o 14 10 0 139.19 168.76 21.01 o 15 10 0 141.00 134.36 21.40 o 1 11 0 85.25 92.42 18.70 o 2 11 0 390.72 373.35 25.31 o 3 11 0 0.86 1.17 22.72 o 4 11 0 2.78 -7.95 18.80 o 5 11 0 127.94 151.52 20.42 o 6 11 0 36.41 27.79 19.17 o 7 11 0 165.24 169.21 19.83 o 8 11 0 0.15 9.84 26.47 o 9 11 0 18.68 31.60 23.30 o -31 1 1 10.46 5.36 12.21 o -30 1 1 84.31 121.76 12.89 o -29 1 1 239.03 259.19 14.52 o -28 1 1 192.85 210.11 13.56 o -27 1 1 260.79 225.82 13.93 o -26 1 1 89.56 87.10 13.24 o -25 1 1 153.75 155.47 12.03 o -24 1 1 496.38 520.70 17.23 o -23 1 1 82.04 86.36 10.22 o -22 1 1 474.56 497.93 14.65 o -21 1 1 69.41 93.11 9.50 o -20 1 1 324.72 317.21 12.11 o -19 1 1 361.69 351.63 14.68 o -18 1 1 2067.34 2067.50 51.99 o -17 1 1 86.62 90.79 9.21 o -16 1 1 3326.64 3102.59 71.46 o -15 1 1 629.29 626.86 15.93 o -14 1 1 191.04 262.08 52.67 o -13 1 1 14635.61 16088.36 206.11 o -12 1 1 1881.47 1855.55 46.44 o -11 1 1 9142.79 9375.73 99.86 o -10 1 1 540.29 522.25 16.89 o -9 1 1 32.91 36.47 5.34 o -8 1 1 456.27 418.80 9.88 o -7 1 1 2539.81 2458.71 43.42 o -6 1 1 1393.39 1380.30 35.24 o -5 1 1 1663.14 1780.99 58.66 o -4 1 1 6162.92 5914.38 81.00 o -3 1 1 19.47 23.36 4.12 o -2 1 1 1.02 -0.54 3.82 o -1 1 1 1201.01 1219.79 31.98 o 0 1 1 13583.30 11966.21 69.97 o 1 1 1 21.19 47.31 8.32 o 2 1 1 2630.31 2717.25 36.12 o 3 1 1 4348.62 4730.24 63.83 o 4 1 1 5815.40 5348.29 72.05 o 5 1 1 19277.67 19211.25 109.83 o 6 1 1 4764.05 4857.55 60.60 o 7 1 1 412.75 369.03 11.92 o 8 1 1 6.94 16.73 5.47 o 9 1 1 2637.33 2775.70 59.54 o 10 1 1 719.58 732.50 21.91 o 11 1 1 1031.44 1109.68 27.32 o 12 1 1 36.42 34.74 9.52 o 13 1 1 80.85 151.53 8.31 o 14 1 1 529.77 646.87 15.66 o 15 1 1 81.29 99.51 7.63 o 16 1 1 1.84 -7.13 7.13 o 17 1 1 1317.36 1197.86 30.87 o 18 1 1 301.22 309.72 11.20 o 19 1 1 14.87 18.90 9.67 o 20 1 1 1185.13 1266.03 30.87 o 21 1 1 3231.10 3181.65 86.71 o 22 1 1 391.25 423.89 32.96 o 23 1 1 463.46 446.38 15.65 o 24 1 1 138.51 148.72 11.75 o 25 1 1 217.70 185.47 18.43 o 26 1 1 16.12 17.93 10.80 o 27 1 1 3.65 16.28 11.10 o 28 1 1 185.97 202.28 13.69 o 29 1 1 0.58 2.00 15.56 o 30 1 1 18.62 32.87 12.09 o -30 2 1 75.81 85.44 19.32 o -29 2 1 413.04 420.79 25.76 o -28 2 1 122.32 94.66 18.98 o -27 2 1 6.19 5.64 16.58 o -26 2 1 397.57 367.30 21.13 o -25 2 1 90.06 112.83 17.70 o -24 2 1 243.93 235.34 18.74 o -23 2 1 161.42 150.88 28.26 o -22 2 1 52.20 20.52 43.56 o -21 2 1 2924.10 2784.10 107.50 o -20 2 1 104.89 14.98 36.80 o -19 2 1 7031.73 6596.88 247.71 o -18 2 1 990.00 953.65 28.16 o -17 2 1 2201.83 2036.06 113.12 o -16 2 1 44.80 56.11 12.05 o -15 2 1 13734.94 14042.36 215.94 o -14 2 1 2504.74 2475.78 99.91 o -13 2 1 1531.72 1487.77 51.55 o -12 2 1 112.82 138.03 10.36 o -11 2 1 3445.70 3384.94 94.53 o -10 2 1 3793.94 3755.72 95.11 o -9 2 1 1123.94 1092.94 114.62 o -8 2 1 708.24 780.91 37.55 o -7 2 1 396.20 370.51 12.56 o -6 2 1 5089.47 5031.48 92.16 o -5 2 1 156.41 162.12 8.83 o -4 2 1 566.92 595.96 22.87 o -3 2 1 17828.19 17081.78 151.28 o -2 2 1 31509.31 29890.38 300.73 o -1 2 1 14685.12 14090.93 261.47 o 0 2 1 9226.49 8828.53 150.64 o 1 2 1 4130.10 4110.77 94.07 o 2 2 1 21597.67 21418.78 720.00 o 3 2 1 429.88 464.74 15.49 o 4 2 1 2650.12 2572.24 65.03 o 5 2 1 1330.84 1184.72 74.82 o 6 2 1 5873.15 5742.80 100.54 o 7 2 1 533.59 630.94 24.09 o 8 2 1 11673.22 11763.90 153.57 o 9 2 1 2928.67 3254.76 86.75 o 10 2 1 354.05 302.59 11.79 o 11 2 1 61.76 94.67 9.22 o 12 2 1 395.98 304.42 12.00 o 13 2 1 866.21 1013.68 36.36 o 14 2 1 4673.86 4785.63 125.13 o 15 2 1 156.15 158.06 23.09 o 16 2 1 4302.93 4413.05 243.42 o 17 2 1 483.00 447.55 68.61 o 18 2 1 6051.91 5796.38 188.40 o 19 2 1 893.63 831.98 59.56 o 20 2 1 1141.04 1101.79 107.62 o 21 2 1 49.33 46.85 16.55 o 22 2 1 28.82 28.63 13.72 o 23 2 1 80.61 75.68 15.71 o 24 2 1 1414.96 1522.78 66.19 o 25 2 1 1364.90 1250.33 43.87 o 26 2 1 4.67 -2.14 35.64 o 27 2 1 82.47 81.30 17.02 o 28 2 1 280.58 304.23 23.13 o 29 2 1 225.39 285.59 22.02 o 30 2 1 45.81 51.75 23.17 o -30 3 1 228.09 209.19 21.22 o -29 3 1 0.30 22.39 20.59 o -28 3 1 26.29 56.05 16.94 o -27 3 1 152.19 144.29 18.18 o -26 3 1 2.45 15.32 15.43 o -25 3 1 3.27 14.83 21.76 o -24 3 1 80.10 73.64 16.71 o -23 3 1 167.36 113.41 19.47 o -22 3 1 691.64 682.51 24.26 o -21 3 1 609.09 581.53 59.90 o -20 3 1 2767.77 2773.78 117.25 o -19 3 1 37.09 19.95 18.84 o -18 3 1 1123.06 1076.42 39.46 o -17 3 1 1072.55 1089.45 36.80 o -16 3 1 836.04 956.49 55.39 o -15 3 1 0.36 4.23 10.67 o -14 3 1 5818.66 5932.40 248.50 o -13 3 1 836.77 776.31 31.17 o -12 3 1 13.17 1.16 9.28 o -11 3 1 222.74 281.23 18.05 o -10 3 1 1978.90 1750.28 60.63 o -9 3 1 6.33 -6.32 8.35 o -8 3 1 39.82 95.65 13.63 o -7 3 1 5698.48 5722.88 112.52 o -6 3 1 8458.15 8574.38 133.43 o -5 3 1 2792.82 2681.84 108.16 o -4 3 1 4055.83 3968.81 87.42 o -3 3 1 4291.03 4194.77 88.15 o -2 3 1 449.96 387.25 14.81 o -1 3 1 58.69 89.14 8.51 o 0 3 1 4.69 3.25 7.37 o 1 3 1 362.56 382.76 25.47 o 2 3 1 118.89 123.27 8.75 o 3 3 1 9608.36 9354.25 184.02 o 4 3 1 4267.96 4363.67 95.12 o 5 3 1 91.41 116.86 23.72 o 6 3 1 4045.23 4596.26 98.51 o 7 3 1 4432.59 4218.11 225.20 o 8 3 1 6418.13 6854.92 230.25 o 9 3 1 663.21 634.04 26.53 o 10 3 1 605.13 701.00 50.81 o 11 3 1 3202.86 3363.14 156.14 o 12 3 1 32.26 23.14 9.79 o 13 3 1 3586.18 3781.06 144.63 o 14 3 1 297.11 351.57 31.14 o 15 3 1 2260.14 2248.34 77.97 o 16 3 1 557.34 601.10 20.84 o 17 3 1 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35.51 o 7 0 10 114.71 107.29 31.34 o 8 0 10 167.64 212.57 33.01 o 9 0 10 37.40 9.59 27.68 o 10 0 10 816.98 934.74 49.02 o -15 1 10 21.67 9.84 27.43 o -14 1 10 202.93 197.49 32.93 o -13 1 10 210.21 268.93 32.93 o -12 1 10 122.21 110.96 29.43 o -11 1 10 386.20 353.29 36.60 o -10 1 10 0.82 -15.59 23.84 o -9 1 10 100.91 114.46 25.59 o -8 1 10 17.62 -14.00 26.09 o -7 1 10 129.83 118.71 28.26 o -6 1 10 173.51 219.41 32.09 o -5 1 10 124.86 109.79 27.59 o -4 1 10 75.33 53.44 25.84 o -3 1 10 137.83 146.38 30.93 o -2 1 10 803.82 741.76 46.60 o -1 1 10 419.25 501.70 27.22 o 0 1 10 49.39 46.07 24.30 o 1 1 10 52.26 93.36 17.65 o 2 1 10 14.58 -1.84 17.74 o 3 1 10 170.12 157.70 20.89 o 4 1 10 0.07 17.57 16.72 o 5 1 10 145.71 218.27 20.54 o 6 1 10 5.54 -8.53 26.30 o 7 1 10 165.00 161.87 28.01 o 8 1 10 14.59 26.39 17.48 o 9 1 10 299.75 390.66 38.51 o 10 1 10 47.72 82.60 28.01 o -1 2 10 12.84 -7.59 24.01 o 0 2 10 14.50 -24.18 24.18 o 1 2 10 37.15 39.51 25.43 o 2 2 10 23.14 21.84 25.34 o 3 2 10 33.53 11.67 26.76 o 4 2 10 90.33 66.61 27.59 o 5 2 10 105.19 106.95 26.59 o 6 2 10 3.89 54.77 22.17 o 7 2 10 92.28 74.61 27.84 o 8 2 10 2.22 -6.92 23.84 o 9 2 10 10.51 25.18 24.93 o -1 3 10 409.05 500.76 38.18 o 0 3 10 8.10 35.26 24.26 o 1 3 10 8.01 13.17 24.84 o 2 3 10 146.42 158.64 30.34 o 3 3 10 673.46 772.10 51.93 o 4 3 10 187.46 150.64 31.01 o 5 3 10 64.94 70.69 29.18 o 6 3 10 9.97 31.59 23.34 o 7 3 10 52.94 40.43 28.51 o 8 3 10 2.29 -2.83 23.93 o -1 4 10 0.03 -27.26 27.26 o 0 4 10 311.96 315.94 33.60 o 1 4 10 78.53 129.96 28.01 o 2 4 10 179.28 258.67 33.43 o 3 4 10 0.57 -16.59 26.68 o 4 4 10 353.57 316.03 34.35 o 5 4 10 81.90 74.86 28.93 o