#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/18/2011830.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011830_Fobs loop_ _publ_author_name 'Suescun, Leopoldo' 'Mombr\'u, Alvaro W.' 'Mariezcurrena, Ra\'ul A.' 'Davyt, Danilo' 'Fern\'andez, Rafael' 'Manta, Eduardo' _publ_section_title ; Two natural products from the algae Laurencia scoparia ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 286 _journal_page_last 288 _journal_volume 57 _journal_year 2001 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.8720 _cell_length_b 11.8970 _cell_length_c 21.5750 _exptl_crystal_F_000 1312.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file sx1116Vsup3.hkl _[local]_cod_data_source_block V #BEGIN Tags that were not found in dictionaries: _shelx_title ' V redone by GF with riding H' _shelx_refln_list_code 4 _shelx_f_calc_maximum 235.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 65.58 61.18 6.48 o 4 0 0 3600.20 3469.84 114.20 o 6 0 0 10831.94 10290.85 301.81 o 8 0 0 1464.64 1251.18 86.80 o 10 0 0 4832.78 4874.64 203.19 o 12 0 0 5.51 0.00 89.50 o 14 0 0 553.20 556.24 65.19 o 1 1 0 13624.43 12690.14 163.54 o 2 1 0 19112.08 17786.94 325.53 o 3 1 0 18595.92 17509.79 325.51 o 4 1 0 7178.00 6331.37 133.35 o 5 1 0 2176.51 2127.46 62.58 o 6 1 0 1426.69 1358.21 52.61 o 7 1 0 494.82 493.55 23.84 o 8 1 0 2368.57 2232.28 81.62 o 9 1 0 453.51 392.58 25.74 o 10 1 0 364.60 363.99 26.44 o 11 1 0 376.36 414.88 43.22 o 12 1 0 10.53 0.00 54.05 o 13 1 0 99.43 102.38 86.24 o 14 1 0 26.07 0.00 76.32 o 15 1 0 32.48 112.79 70.05 o 0 2 0 4879.80 4470.22 127.19 o 1 2 0 1640.68 1709.74 44.27 o 2 2 0 23477.60 23138.09 599.53 o 3 2 0 5903.60 5936.40 176.32 o 4 2 0 4727.69 4258.29 140.71 o 5 2 0 13133.21 13307.18 373.61 o 6 2 0 6227.50 6045.40 199.31 o 7 2 0 1348.34 1094.52 77.44 o 8 2 0 1.74 48.50 44.37 o 9 2 0 170.41 145.59 32.07 o 10 2 0 271.94 298.81 37.58 o 11 2 0 328.24 298.54 42.62 o 12 2 0 2058.08 1878.58 110.20 o 13 2 0 339.83 256.94 56.30 o 14 2 0 82.49 0.00 116.94 o 15 2 0 121.51 0.00 132.86 o 1 3 0 833.47 813.92 30.36 o 2 3 0 6848.30 6589.54 193.80 o 3 3 0 107.43 112.83 15.12 o 4 3 0 320.16 304.88 20.85 o 5 3 0 1240.67 1164.80 70.40 o 6 3 0 10000.91 10178.21 309.76 o 7 3 0 9.86 0.00 42.89 o 8 3 0 3116.69 2904.29 140.80 o 9 3 0 1298.58 1458.25 100.63 o 10 3 0 165.44 225.82 38.37 o 11 3 0 441.57 576.69 50.01 o 12 3 0 25.75 0.00 88.99 o 13 3 0 213.87 221.24 56.47 o 14 3 0 1.15 72.84 58.87 o 15 3 0 43.00 0.00 140.47 o 0 4 0 6876.04 6563.66 195.80 o 1 4 0 89.71 90.15 10.01 o 2 4 0 404.54 400.97 24.65 o 3 4 0 5571.99 5811.07 185.36 o 4 4 0 604.26 671.76 41.44 o 5 4 0 8305.74 8409.50 264.40 o 6 4 0 4707.59 4483.68 172.73 o 7 4 0 790.18 772.93 48.26 o 8 4 0 376.27 367.72 33.51 o 9 4 0 3807.05 4088.14 188.39 o 10 4 0 292.27 259.53 43.41 o 11 4 0 14.32 21.08 86.41 o 12 4 0 55.23 0.00 99.87 o 13 4 0 279.40 351.44 57.85 o 14 4 0 26.62 81.43 108.34 o 1 5 0 2404.72 2415.79 69.32 o 2 5 0 2466.66 2557.71 103.89 o 3 5 0 13608.13 13983.54 398.63 o 4 5 0 5133.20 4892.49 173.09 o 5 5 0 1075.72 1183.85 81.78 o 6 5 0 507.77 472.77 35.12 o 7 5 0 1117.69 1197.37 68.74 o 8 5 0 3.68 0.00 64.02 o 9 5 0 401.41 445.10 43.82 o 10 5 0 671.62 697.59 55.24 o 11 5 0 2016.93 1944.73 113.00 o 12 5 0 11.71 0.00 116.30 o 13 5 0 199.84 165.80 59.85 o 14 5 0 13.61 143.28 111.49 o 0 6 0 7336.48 8256.94 255.05 o 1 6 0 450.60 421.34 26.62 o 2 6 0 2852.67 2774.84 118.43 o 3 6 0 71.70 37.63 41.06 o 4 6 0 6.69 42.71 21.30 o 5 6 0 28.61 67.28 46.27 o 6 6 0 492.90 511.02 37.93 o 7 6 0 5000.72 4940.77 209.63 o 8 6 0 1545.53 1517.71 85.57 o 9 6 0 7.03 0.00 79.25 o 10 6 0 254.48 252.75 47.99 o 11 6 0 17.08 163.09 89.62 o 12 6 0 69.98 118.48 73.88 o 13 6 0 16.90 0.00 128.78 o 14 6 0 0.78 17.07 135.94 o 1 7 0 7637.54 7587.91 175.85 o 2 7 0 289.71 300.40 28.30 o 3 7 0 507.80 494.27 33.75 o 4 7 0 5179.92 5133.09 196.87 o 5 7 0 970.67 869.88 51.76 o 6 7 0 252.67 103.45 69.08 o 7 7 0 844.02 921.51 60.64 o 8 7 0 434.89 359.13 47.09 o 9 7 0 850.12 916.15 60.80 o 10 7 0 180.23 165.17 91.92 o 11 7 0 74.36 19.76 104.97 o 12 7 0 3.56 117.62 94.65 o 13 7 0 214.06 147.94 136.07 o 0 8 0 19.02 0.00 53.48 o 1 8 0 1378.37 1372.18 56.89 o 2 8 0 467.21 449.36 35.18 o 3 8 0 1071.20 1071.75 64.44 o 4 8 0 828.39 840.47 52.33 o 5 8 0 5263.35 5151.39 213.01 o 6 8 0 319.98 336.18 36.49 o 7 8 0 355.65 293.00 44.22 o 8 8 0 119.62 188.01 40.03 o 9 8 0 106.63 32.12 94.95 o 10 8 0 1.86 0.00 97.51 o 11 8 0 402.30 451.31 59.86 o 12 8 0 33.64 122.83 60.35 o 13 8 0 10.62 107.60 141.21 o 1 9 0 385.09 386.55 26.45 o 2 9 0 5549.24 5907.69 226.64 o 3 9 0 805.74 760.41 53.59 o 4 9 0 416.64 396.25 41.53 o 5 9 0 0.58 123.29 64.13 o 6 9 0 582.77 591.79 51.16 o 7 9 0 63.39 90.99 80.57 o 8 9 0 814.79 807.51 61.14 o 9 9 0 1.28 79.77 47.01 o 10 9 0 143.58 59.39 117.40 o 11 9 0 70.74 0.00 129.31 o 12 9 0 19.18 0.00 129.47 o 0 10 0 169.07 138.71 79.72 o 1 10 0 2941.74 3072.80 111.52 o 2 10 0 22.27 89.67 61.73 o 3 10 0 7.83 41.92 67.86 o 4 10 0 33.49 0.00 73.98 o 5 10 0 64.40 107.14 75.19 o 6 10 0 38.34 100.04 75.64 o 7 10 0 948.80 926.39 65.28 o 8 10 0 96.26 69.75 106.98 o 9 10 0 4.90 0.00 113.89 o 10 10 0 147.90 0.00 134.69 o 11 10 0 82.05 0.00 140.41 o 1 11 0 59.41 83.49 54.40 o 2 11 0 1695.55 1733.51 98.99 o 3 11 0 208.98 174.17 88.03 o 4 11 0 2483.58 2544.02 169.13 o 5 11 0 4.07 0.00 93.85 o 6 11 0 145.28 118.14 74.45 o 7 11 0 24.09 119.10 94.88 o 8 11 0 14.27 64.48 103.47 o 9 11 0 20.34 0.00 119.57 o 10 11 0 344.09 271.03 145.08 o 0 12 0 844.46 817.79 62.64 o 1 12 0 1118.02 1237.45 56.02 o 2 12 0 59.61 50.91 90.31 o 3 12 0 3.47 0.00 95.57 o 4 12 0 83.08 84.23 79.14 o 5 12 0 565.16 517.20 63.01 o 6 12 0 1.09 0.00 112.74 o 7 12 0 169.50 106.70 123.59 o 8 12 0 106.81 25.08 140.76 o 9 12 0 16.69 120.08 130.32 o 1 13 0 86.69 123.62 47.85 o 2 13 0 907.57 766.43 70.08 o 3 13 0 21.44 0.00 109.03 o 4 13 0 329.25 262.22 62.66 o 5 13 0 0.85 60.41 125.92 o 6 13 0 32.62 0.00 131.76 o 7 13 0 49.94 0.00 147.80 o 8 13 0 293.76 203.89 75.55 o 0 14 0 5.57 0.00 115.50 o 1 14 0 394.75 354.04 58.71 o 2 14 0 44.28 37.16 114.18 o 3 14 0 30.26 75.58 115.33 o 4 14 0 14.79 0.00 131.82 o 5 14 0 443.19 341.05 75.26 o 6 14 0 78.69 101.53 137.49 o 1 15 0 90.38 0.00 100.02 o 2 15 0 98.16 133.83 132.57 o 3 15 0 17.05 88.99 125.23 o 2 0 1 55568.93 53594.98 1350.36 o 3 0 1 449.90 437.88 29.25 o 4 0 1 8896.55 8094.22 231.73 o 5 0 1 15748.26 14444.55 397.85 o 6 0 1 3361.77 3471.63 129.61 o 7 0 1 8138.95 7717.06 247.08 o 8 0 1 573.18 513.78 33.58 o 9 0 1 1388.40 1368.57 74.38 o 10 0 1 964.23 1021.41 59.44 o 11 0 1 58.97 82.06 72.10 o 12 0 1 3.14 35.96 74.32 o 13 0 1 271.27 302.30 52.52 o 14 0 1 23.80 0.00 114.41 o 15 0 1 166.95 150.04 123.99 o -15 1 1 20.54 127.52 84.47 o -14 1 1 109.56 190.07 106.00 o -13 1 1 797.65 938.21 67.16 o -12 1 1 15.76 33.15 74.95 o -11 1 1 1572.33 1813.97 128.80 o -10 1 1 478.54 524.43 41.19 o -9 1 1 658.51 701.86 46.07 o -8 1 1 500.95 457.98 34.27 o -7 1 1 4714.34 4794.39 175.11 o -6 1 1 146.05 152.24 19.24 o -5 1 1 4153.94 3958.08 138.35 o -4 1 1 7580.46 6873.00 203.97 o -3 1 1 3419.19 2943.36 97.48 o -2 1 1 2409.09 2326.43 75.66 o -1 1 1 5368.41 5162.98 158.49 o 1 1 1 3856.67 3586.73 179.51 o 2 1 1 2516.47 2412.42 78.41 o 3 1 1 3926.65 3679.87 116.11 o 4 1 1 7687.02 7167.93 209.27 o 5 1 1 3574.06 3274.46 116.69 o 6 1 1 155.93 195.14 19.65 o 7 1 1 4559.21 4692.21 168.79 o 8 1 1 393.16 386.08 31.45 o 9 1 1 797.23 906.75 58.29 o 10 1 1 512.65 598.24 42.63 o 11 1 1 1407.98 1571.89 90.71 o 12 1 1 28.82 0.00 88.07 o 13 1 1 804.04 875.88 64.40 o 14 1 1 130.88 40.77 115.00 o 15 1 1 23.77 0.00 124.55 o -1 2 1 1787.20 1912.76 64.74 o 0 2 1 36705.79 40864.87 1033.12 o 1 2 1 1861.76 1807.91 62.85 o 2 2 1 6947.21 7066.38 199.23 o 3 2 1 2822.90 2652.86 95.49 o 4 2 1 5255.04 5082.09 162.34 o 5 2 1 10282.41 10161.07 296.71 o 6 2 1 1260.19 1416.35 79.40 o 7 2 1 3113.55 2966.98 131.63 o 8 2 1 3880.79 3895.06 162.81 o 9 2 1 561.64 570.79 40.45 o 10 2 1 1814.67 1960.59 123.23 o 11 2 1 409.53 556.56 45.20 o 12 2 1 295.69 340.17 47.71 o 13 2 1 170.09 123.47 104.35 o 14 2 1 317.36 216.44 64.66 o 15 2 1 80.18 0.00 140.53 o -1 3 1 6366.18 6148.13 177.89 o 0 3 1 166.27 178.23 13.29 o 1 3 1 7094.81 7154.49 203.67 o 2 3 1 5047.72 4684.93 146.07 o 3 3 1 3700.63 3627.83 124.85 o 4 3 1 1595.04 1525.10 73.93 o 5 3 1 2461.04 2489.50 106.09 o 6 3 1 1575.63 1672.38 91.32 o 7 3 1 1605.17 1551.05 96.17 o 8 3 1 1305.98 1345.66 72.83 o 9 3 1 445.32 424.86 40.16 o 10 3 1 0.99 0.00 67.34 o 11 3 1 1250.85 1320.07 92.18 o 12 3 1 167.81 147.19 45.65 o 13 3 1 645.87 651.97 63.65 o 14 3 1 51.63 0.00 123.86 o 15 3 1 25.46 0.00 136.80 o -1 4 1 5625.20 5654.36 173.24 o 0 4 1 1230.02 1263.53 61.11 o 1 4 1 5048.63 5172.26 161.48 o 2 4 1 5717.58 5464.64 172.12 o 3 4 1 682.56 757.10 39.68 o 4 4 1 5170.99 4906.15 169.16 o 5 4 1 2442.67 2404.41 108.46 o 6 4 1 196.27 216.79 25.38 o 7 4 1 1090.97 1078.21 64.04 o 8 4 1 2515.65 2425.14 136.38 o 9 4 1 277.70 332.28 40.67 o 10 4 1 1512.27 1756.06 97.89 o 11 4 1 24.27 0.00 80.52 o 12 4 1 375.63 394.42 55.73 o 13 4 1 3.19 0.00 102.04 o 14 4 1 181.19 198.90 139.97 o -1 5 1 1858.48 1551.07 76.03 o 0 5 1 18282.40 20162.20 543.13 o 1 5 1 1499.29 1317.09 71.43 o 2 5 1 4290.46 4446.99 154.09 o 3 5 1 279.84 437.58 31.10 o 4 5 1 2515.63 2257.29 107.79 o 5 5 1 124.96 132.30 23.31 o 6 5 1 5349.64 5092.76 195.33 o 7 5 1 1182.41 1182.78 71.85 o 8 5 1 2445.94 2462.01 140.71 o 9 5 1 283.15 207.46 41.69 o 10 5 1 417.52 447.85 49.38 o 11 5 1 135.55 117.51 99.08 o 12 5 1 167.55 87.28 99.88 o 13 5 1 98.46 59.10 114.99 o 14 5 1 90.17 233.59 121.35 o -1 6 1 1874.12 1962.02 93.97 o 0 6 1 1561.66 1419.84 80.43 o 1 6 1 1972.64 1994.33 98.58 o 2 6 1 6795.71 7089.63 229.16 o 3 6 1 6680.57 6769.94 226.16 o 4 6 1 2349.71 2695.04 123.63 o 5 6 1 973.69 959.70 60.49 o 6 6 1 22.93 0.00 62.48 o 7 6 1 699.32 712.49 45.73 o 8 6 1 1906.04 1870.20 100.52 o 9 6 1 310.11 299.63 44.85 o 10 6 1 570.95 578.18 55.80 o 11 6 1 338.37 320.02 53.90 o 12 6 1 222.41 178.18 112.03 o 13 6 1 79.70 0.00 129.59 o 14 6 1 132.14 189.78 71.19 o -1 7 1 464.42 495.35 31.29 o 0 7 1 7567.10 7896.24 255.57 o 1 7 1 490.32 464.71 32.66 o 2 7 1 3917.31 4234.21 163.43 o 3 7 1 872.45 934.84 58.70 o 4 7 1 2354.83 2062.52 120.48 o 5 7 1 1354.47 1446.44 76.97 o 6 7 1 3243.25 3400.36 162.40 o 7 7 1 120.58 83.61 82.29 o 8 7 1 983.48 1041.67 69.81 o 9 7 1 329.36 371.63 48.05 o 10 7 1 399.35 328.79 51.72 o 11 7 1 430.46 425.20 62.38 o 12 7 1 131.73 33.50 127.36 o 13 7 1 231.27 180.86 146.10 o -1 8 1 1134.52 1176.38 64.97 o 0 8 1 10.69 0.00 51.65 o 1 8 1 949.84 989.50 59.97 o 2 8 1 2858.00 2878.39 138.88 o 3 8 1 2240.82 2233.31 124.87 o 4 8 1 303.32 240.64 35.23 o 5 8 1 933.71 971.97 59.04 o 6 8 1 53.92 72.44 71.07 o 7 8 1 522.68 532.80 48.35 o 8 8 1 620.40 645.36 53.74 o 9 8 1 640.38 458.98 56.78 o 10 8 1 580.81 504.60 61.98 o 11 8 1 10.30 199.56 102.39 o 12 8 1 160.47 145.24 130.17 o 13 8 1 86.93 16.55 136.93 o -1 9 1 2863.04 2907.97 144.65 o 0 9 1 1703.72 1934.39 116.87 o 1 9 1 2855.59 3010.03 146.77 o 2 9 1 550.93 514.76 41.31 o 3 9 1 209.32 193.47 36.08 o 4 9 1 1138.72 1044.95 74.24 o 5 9 1 526.64 576.70 44.35 o 6 9 1 2464.27 2477.16 162.89 o 7 9 1 18.32 49.42 81.03 o 8 9 1 467.48 506.45 55.85 o 9 9 1 387.30 506.53 53.32 o 10 9 1 68.97 125.47 111.95 o 11 9 1 95.27 120.95 71.35 o 12 9 1 118.25 173.23 131.32 o -1 10 1 417.82 478.34 43.08 o 0 10 1 1178.13 1144.55 76.14 o 1 10 1 441.43 515.59 42.97 o 2 10 1 43.61 2.98 73.76 o 3 10 1 1459.42 1518.18 88.89 o 4 10 1 167.43 212.47 37.97 o 5 10 1 485.79 495.43 48.06 o 6 10 1 402.32 366.38 47.89 o 7 10 1 215.81 210.07 45.01 o 8 10 1 11.22 0.00 108.34 o 9 10 1 284.22 158.93 110.66 o 10 10 1 66.57 217.03 113.96 o 11 10 1 218.59 68.78 144.38 o -1 11 1 578.54 581.92 49.10 o 0 11 1 2879.24 3073.55 172.65 o 1 11 1 598.56 609.49 50.36 o 2 11 1 210.13 121.71 91.35 o 3 11 1 453.63 427.93 49.90 o 4 11 1 231.49 254.35 47.48 o 5 11 1 72.75 19.01 89.33 o 6 11 1 793.10 811.31 66.53 o 7 11 1 78.05 0.00 121.17 o 8 11 1 336.69 280.03 61.92 o 9 11 1 15.34 180.78 107.13 o 10 11 1 78.44 113.90 94.72 o -1 12 1 30.88 60.29 85.61 o 0 12 1 2.15 0.00 97.12 o 1 12 1 57.53 152.90 86.01 o 2 12 1 20.87 15.00 92.82 o 3 12 1 870.33 849.71 67.67 o 4 12 1 80.18 0.00 104.28 o 5 12 1 198.90 167.18 56.64 o 6 12 1 18.19 93.57 51.25 o 7 12 1 122.18 123.64 67.46 o 8 12 1 10.38 0.00 128.90 o 9 12 1 210.30 14.32 148.28 o -1 13 1 274.62 225.72 56.30 o 0 13 1 696.20 654.35 64.86 o 1 13 1 310.59 139.24 121.42 o 2 13 1 169.01 177.14 54.18 o 3 13 1 5.99 0.00 111.04 o 4 13 1 279.66 253.78 60.48 o 5 13 1 45.90 49.94 110.80 o 6 13 1 289.76 284.48 142.90 o 7 13 1 26.90 0.00 138.92 o 8 13 1 95.26 0.00 155.99 o -1 14 1 130.49 118.14 131.71 o 0 14 1 36.75 187.25 100.84 o 1 14 1 147.01 155.14 107.61 o 2 14 1 186.20 49.14 124.62 o 3 14 1 538.23 598.98 69.09 o 4 14 1 249.76 18.15 144.16 o 5 14 1 119.29 98.61 139.91 o 6 14 1 73.14 156.16 128.62 o -1 15 1 200.97 0.00 138.42 o 0 15 1 53.73 127.30 145.33 o 1 15 1 219.49 0.00 140.60 o 2 15 1 53.81 0.00 147.80 o 3 15 1 94.50 143.39 136.12 o 1 0 2 2400.97 2342.63 48.40 o 2 0 2 35886.87 36360.83 922.04 o 3 0 2 7294.21 6523.23 188.52 o 4 0 2 3158.54 2829.78 100.84 o 5 0 2 3764.21 3701.20 130.12 o 6 0 2 51.07 8.65 39.45 o 7 0 2 947.81 1133.69 76.61 o 8 0 2 716.27 808.80 51.87 o 9 0 2 402.42 366.92 36.15 o 10 0 2 741.10 720.67 48.19 o 11 0 2 1307.37 1363.92 85.94 o 12 0 2 2439.92 2299.79 120.28 o 13 0 2 84.22 0.00 114.71 o 14 0 2 307.12 292.68 62.83 o 15 0 2 9.84 0.00 133.36 o -15 1 2 102.88 186.23 62.02 o -14 1 2 90.39 154.39 111.09 o -13 1 2 19.75 38.31 91.39 o -12 1 2 2.37 0.00 83.72 o -11 1 2 19.85 106.28 62.48 o -10 1 2 845.06 897.20 58.17 o -9 1 2 1609.17 1576.02 80.88 o -8 1 2 2778.02 2580.27 129.34 o -7 1 2 1042.74 938.45 55.79 o -6 1 2 9951.78 9480.17 287.35 o -5 1 2 2939.56 2900.50 112.34 o -4 1 2 1548.67 1401.24 64.59 o -3 1 2 23418.50 21843.36 571.80 o -2 1 2 1912.98 1854.44 65.25 o -1 1 2 7265.76 6839.00 129.94 o 0 1 2 1044.75 917.86 38.51 o 1 1 2 9679.66 9246.75 333.21 o 2 1 2 1802.16 1838.19 64.81 o 3 1 2 21655.49 20995.59 550.42 o 4 1 2 1279.51 1193.23 59.61 o 5 1 2 3110.49 3022.90 112.08 o 6 1 2 9360.37 9235.86 276.28 o 7 1 2 958.34 993.79 52.01 o 8 1 2 3029.51 3054.95 135.07 o 9 1 2 1597.26 1745.74 110.71 o 10 1 2 665.46 640.90 46.53 o 11 1 2 26.62 42.15 69.18 o 12 1 2 0.58 0.00 84.17 o 13 1 2 9.48 0.00 105.99 o 14 1 2 66.04 0.00 116.47 o 15 1 2 145.22 154.57 90.54 o -1 2 2 2702.53 2676.07 85.75 o 0 2 2 40131.54 45675.38 1154.14 o 1 2 2 3023.23 2934.00 92.82 o 2 2 2 887.87 920.59 44.79 o 3 2 2 4420.84 4228.62 134.60 o 4 2 2 4163.53 4475.36 148.64 o 5 2 2 4889.36 4766.99 163.18 o 6 2 2 9278.60 9159.13 282.14 o 7 2 2 529.36 564.55 39.14 o 8 2 2 1962.84 1847.74 107.85 o 9 2 2 1035.58 1080.72 68.67 o 10 2 2 1690.07 1914.05 94.01 o 11 2 2 76.16 124.03 38.36 o 12 2 2 177.18 168.60 47.02 o 13 2 2 271.69 235.51 58.60 o 14 2 2 333.83 284.20 62.03 o 15 2 2 61.86 195.33 132.28 o -1 3 2 3239.01 3286.19 106.99 o 0 3 2 145.01 141.96 12.89 o 1 3 2 3550.20 3534.95 113.86 o 2 3 2 2407.27 2433.28 90.17 o 3 3 2 23648.26 23891.82 631.56 o 4 3 2 3226.32 2848.51 110.97 o 5 3 2 7724.01 7303.52 232.16 o 6 3 2 2114.89 2088.42 105.57 o 7 3 2 571.94 563.82 35.53 o 8 3 2 1367.05 1395.35 74.67 o 9 3 2 875.37 902.66 63.97 o 10 3 2 48.89 34.99 69.87 o 11 3 2 513.10 467.82 49.72 o 12 3 2 180.40 43.99 91.63 o 13 3 2 340.75 407.53 55.79 o 14 3 2 69.28 12.94 122.20 o 15 3 2 16.55 0.00 131.53 o -1 4 2 8174.45 8047.05 233.32 o 0 4 2 23.69 37.11 12.88 o 1 4 2 7671.43 7759.60 227.35 o 2 4 2 22826.42 24250.19 641.85 o 3 4 2 3832.76 3970.92 137.81 o 4 4 2 734.18 711.58 42.42 o 5 4 2 565.40 522.91 35.19 o 6 4 2 2399.02 2430.75 118.92 o 7 4 2 4818.75 4683.65 188.53 o 8 4 2 2286.33 2389.52 131.75 o 9 4 2 705.32 782.94 48.60 o 10 4 2 56.08 0.00 74.73 o 11 4 2 65.22 76.45 48.97 o 12 4 2 326.07 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94.38 o -5 1 22 16.57 18.33 89.27 o -4 1 22 146.69 96.96 96.84 o -3 1 22 125.14 104.75 53.71 o -2 1 22 53.22 38.36 81.60 o -1 1 22 47.42 0.00 62.57 o 0 1 22 149.41 124.46 59.20 o 1 1 22 28.36 35.14 80.43 o 2 1 22 49.13 11.46 78.51 o 3 1 22 139.53 132.69 95.13 o 4 1 22 126.39 152.91 87.96 o 5 1 22 14.93 0.00 96.38 o 6 1 22 229.49 52.81 117.12 o 7 1 22 158.76 54.30 113.16 o 8 1 22 31.46 0.00 121.91 o 9 1 22 62.89 11.97 126.38 o -1 2 22 369.75 389.50 50.98 o 0 2 22 3.57 92.65 79.37 o 1 2 22 372.77 462.37 48.11 o 2 2 22 3.01 48.28 79.19 o 3 2 22 115.70 69.35 88.59 o 4 2 22 109.15 0.00 98.10 o 5 2 22 245.46 234.25 49.26 o 6 2 22 24.19 0.00 106.62 o 7 2 22 88.31 79.71 96.89 o 8 2 22 4.14 184.10 113.73 o 9 2 22 262.99 205.21 144.10 o -1 3 22 158.52 157.49 94.21 o 0 3 22 195.18 151.37 93.82 o 1 3 22 160.83 83.90 86.14 o 2 3 22 308.62 142.04 106.59 o 3 3 22 53.12 103.37 86.58 o 4 3 22 139.20 88.77 69.87 o 5 3 22 212.47 113.17 99.08 o 6 3 22 28.15 128.21 100.33 o 7 3 22 53.27 47.82 111.55 o 8 3 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51.26 101.13 o 1 5 23 36.06 48.91 103.36 o 2 5 23 47.30 41.11 99.01 o 3 5 23 156.37 171.00 105.72 o 4 5 23 236.97 214.14 128.69 o 5 5 23 112.50 0.00 121.70 o 6 5 23 29.11 93.74 128.56 o 7 5 23 34.84 11.11 124.89 o -1 6 23 114.60 141.39 107.89 o 0 6 23 106.23 19.64 107.38 o 1 6 23 126.56 143.74 112.30 o 2 6 23 20.39 4.86 118.31 o 3 6 23 110.96 130.05 102.74 o 4 6 23 109.43 0.00 138.19 o 5 6 23 11.16 70.26 117.28 o 6 6 23 59.38 28.35 125.58 o -1 7 23 13.12 48.67 109.03 o 0 7 23 1.57 130.04 104.62 o 1 7 23 13.48 18.38 113.09 o 2 7 23 45.74 0.00 124.55 o 3 7 23 511.21 334.70 69.77 o 4 7 23 24.56 0.00 125.52 o 5 7 23 13.51 0.00 137.31 o -1 8 23 10.57 173.05 109.77 o 0 8 23 267.79 92.27 133.39 o 1 8 23 8.04 101.87 86.86 o 2 8 23 77.10 0.00 132.68 o 3 8 23 95.44 103.53 131.88 o 0 0 24 468.68 178.95 96.35 o 1 0 24 495.34 524.21 40.92 o 2 0 24 0.90 0.00 101.24 o 3 0 24 125.18 114.19 100.11 o 4 0 24 10.12 0.00 98.72 o 5 0 24 29.60 0.00 112.01 o 6 0 24 10.56 119.10 110.35 o 7 0 24 59.62 0.00 122.26 o -7 1 24 19.13 135.71 114.99 o -6 1 24 229.98 198.10 59.16 o -5 1 24 103.38 71.87 115.34 o -4 1 24 215.89 222.90 53.09 o -3 1 24 31.23 37.85 94.14 o -2 1 24 122.90 9.56 96.89 o -1 1 24 22.70 0.00 73.00 o 0 1 24 402.46 422.71 38.58 o 1 1 24 26.05 117.79 67.52 o 2 1 24 127.31 130.17 95.01 o 3 1 24 31.63 141.56 101.12 o 4 1 24 253.07 101.43 102.86 o 5 1 24 77.52 123.58 77.25 o 6 1 24 221.26 319.40 58.99 o 7 1 24 12.06 0.00 122.42 o -1 2 24 5.68 25.88 88.99 o 0 2 24 33.24 152.84 102.39 o 1 2 24 9.30 1.09 92.19 o 2 2 24 54.35 140.93 94.54 o 3 2 24 332.45 318.52 59.11 o 4 2 24 43.29 75.42 72.16 o 5 2 24 64.13 38.36 116.53 o 6 2 24 49.07 0.00 122.49 o 7 2 24 66.28 228.31 122.77 o -1 3 24 17.77 70.60 100.04 o 0 3 24 402.01 380.80 54.19 o 1 3 24 41.20 108.69 57.95 o 2 3 24 22.47 51.82 95.12 o 3 3 24 44.57 108.00 93.28 o 4 3 24 20.81 165.32 97.69 o 5 3 24 7.14 33.15 121.05 o 6 3 24 60.86 0.00 117.97 o 7 3 24 44.39 41.05 125.69 o -1 4 24 197.15 202.16 113.22 o 0 4 24 0.42 0.69 100.78 o 1 4 24 195.03 73.08 116.43 o 2 4 24 35.80 0.00 120.66 o 3 4 24 87.11 0.00 121.17 o 4 4 24 205.01 239.16 56.75 o 5 4 24 72.93 0.00 120.89 o 6 4 24 97.54 0.00 125.69 o -1 5 24 2.42 152.89 102.55 o 0 5 24 1.11 82.57 100.10 o 1 5 24 15.77 84.98 100.33 o 2 5 24 48.43 46.44 117.68 o 3 5 24 113.32 151.53 126.10 o 4 5 24 203.34 121.70 83.85 o 5 5 24 25.10 0.00 132.85 o 6 5 24 55.61 0.00 127.47 o -1 6 24 58.71 129.65 116.13 o 0 6 24 154.53 0.00 124.79 o 1 6 24 54.25 0.00 116.19 o 2 6 24 87.50 74.67 137.09 o 3 6 24 81.97 155.07 116.59 o 4 6 24 26.40 104.34 131.76 o 5 6 24 27.89 0.00 127.81 o -1 7 24 183.41 122.84 139.63 o 0 7 24 31.97 0.00 144.82 o 1 7 24 227.72 244.43 141.86 o 2 7 24 49.99 221.96 115.10 o 3 7 24 126.83 203.93 124.50 o 1 0 25 201.38 252.45 37.07 o 2 0 25 12.92 0.00 101.58 o 3 0 25 0.88 64.59 100.55 o 4 0 25 6.49 34.07 115.39 o 5 0 25 389.33 259.07 63.69 o 6 0 25 50.29 175.12 110.80 o -6 1 25 21.93 1.54 122.43 o -5 1 25 103.04 0.00 139.38 o -4 1 25 182.53 194.48 123.47 o -3 1 25 0.79 91.22 104.27 o -2 1 25 247.22 342.49 54.87 o -1 1 25 14.52 24.58 73.97 o 0 1 25 82.79 15.33 76.99 o 1 1 25 2.46 95.66 41.89 o 2 1 25 240.69 272.56 56.01 o 3 1 25 0.54 0.00 99.58 o 4 1 25 207.50 277.59 57.50 o 5 1 25 123.79 14.89 125.76 o 6 1 25 24.95 159.88 115.27 o -1 2 25 124.48 0.00 106.00 o 0 2 25 2.58 79.88 92.08 o 1 2 25 132.27 0.00 112.99 o 2 2 25 64.90 55.09 107.20 o 3 2 25 2.20 0.00 116.99 o 4 2 25 102.48 0.00 123.64 o 5 2 25 2.00 0.00 123.11 o 6 2 25 39.41 131.36 59.32 o -1 3 25 6.17 21.65 108.79 o 0 3 25 56.96 0.00 110.29 o 1 3 25 3.58 31.78 107.54 o 2 3 25 18.24 0.00 123.69 o 3 3 25 144.23 184.41 54.69 o 4 3 25 237.79 292.38 59.79 o 5 3 25 27.78 0.00 134.68 o 6 3 25 77.77 106.91 119.00 o -1 4 25 138.12 39.98 110.75 o 0 4 25 480.87 364.66 59.92 o 1 4 25 163.58 94.04 113.05 o 2 4 25 33.99 77.20 114.41 o 3 4 25 13.92 34.07 112.75 o 4 4 25 54.28 0.00 128.33 o 5 4 25 124.86 246.54 129.88 o -1 5 25 62.73 29.49 110.75 o 0 5 25 64.34 0.00 120.03 o 1 5 25 76.28 0.00 122.15 o 2 5 25 364.92 154.60 83.97 o 3 5 25 42.20 0.12 116.25 o 4 5 25 21.34 0.00 138.92 o -1 6 25 18.24 109.38 108.85 o 0 6 25 14.07 95.28 118.19 o 1 6 25 6.90 16.26 130.22 o 2 6 25 30.13 0.00 135.02 o 3 6 25 32.62 0.00 146.36 o 0 0 26 3.96 79.37 78.17 o 1 0 26 3.01 0.00 83.34 o 2 0 26 149.20 0.00 127.25 o 3 0 26 74.24 0.57 118.03 o 4 0 26 11.60 0.00 121.39 o 5 0 26 18.62 0.00 139.27 o -5 1 26 49.47 65.17 121.80 o -4 1 26 22.43 0.00 131.07 o -3 1 26 10.15 26.23 112.92 o -2 1 26 75.90 13.23 107.89 o -1 1 26 83.64 101.00 81.70 o 0 1 26 13.46 3.59 140.15 o 1 1 26 110.25 118.14 80.33 o 2 1 26 97.25 153.47 59.04 o 3 1 26 6.04 0.00 130.16 o 4 1 26 11.78 65.33 116.93 o 5 1 26 40.20 66.08 125.98 o -1 2 26 134.81 199.41 124.10 o 0 2 26 190.74 199.18 55.55 o 1 2 26 119.17 0.00 127.70 o 2 2 26 33.63 125.01 127.53 o 3 2 26 117.03 183.88 58.01 o 4 2 26 4.41 28.29 114.36 o 5 2 26 145.10 187.67 123.99 o -1 3 26 10.73 0.00 121.97 o 0 3 26 146.86 130.05 108.35 o 1 3 26 4.96 0.00 113.27 o 2 3 26 68.87 191.67 109.89 o 3 3 26 10.98 0.00 136.68 o 4 3 26 91.64 0.00 130.57 o -1 4 26 27.41 50.05 120.25 o 0 4 26 36.07 0.00 122.77 o 1 4 26 19.49 0.00 117.85 o 2 4 26 21.58 0.00 146.54 o 3 4 26 202.49 133.90 146.78 o 4 4 26 2.81 0.00 126.84 o -1 5 26 104.49 208.68 130.51 o 0 5 26 121.81 221.51 133.03 o 1 5 26 83.14 0.00 134.06 o 2 5 26 70.64 0.00 125.06 o 1 0 27 110.00 122.09 106.03 o 2 0 27 43.85 0.00 137.21 o 3 0 27 63.11 0.00 125.81 o 4 0 27 3.69 138.40 123.63 o -4 1 27 77.73 39.45 118.31 o -3 1 27 27.05 0.00 132.79 o -2 1 27 55.38 0.00 125.18 o -1 1 27 107.48 0.00 86.90 o 0 1 27 21.21 0.00 84.67 o 1 1 27 89.03 60.17 79.04 o 2 1 27 61.05 124.37 108.00 o 3 1 27 19.10 41.92 112.46 o 4 1 27 49.75 0.00 128.38 o -1 2 27 39.77 172.36 121.45 o 0 2 27 80.27 0.00 133.71 o 1 2 27 41.88 0.00 111.26 o 2 2 27 15.51 0.00 124.14 o 3 2 27 14.92 0.00 132.57 o -1 3 27 37.72 0.00 131.82 o 0 3 27 0.05 0.00 134.45 o 1 3 27 43.14 83.44 60.64 o 2 3 27 37.80 221.03 124.89 o -1 4 27 60.33 96.38 126.56 o 0 4 27 2.79 0.00 134.33 o 1 4 27 71.79 223.67 126.38 o 0 0 28 4.60 45.06 124.60 o