data_2011857
_journal_name_full  'Acta Crystallographica, Section C'
_journal_year  2001
_journal_volume  57
_journal_page_first  397
_journal_page_last  399
_publ_section_title
;
Sodium 4-(2-pyridinylazo)resorcinolate monohydrate and ammonium
2,4-dinitro-1-naphthalenolate from powder diffraction data
;
loop_
_publ_author_name
  'Yatsenko, A. V.'
  'Paseshnichenko, K. A.'
  'Chernyshev, V. V.'
  'Schenk, H.'
_chemical_name_common  'Acid Yellow 24'
_chemical_formula_moiety  'N H4 + , C10 H5 N2 O5 - '
_chemical_formula_sum  'C10 H9 N3 O5'
_chemical_formula_iupac  'N H4 + , C10 H5 N2 O5 - '
_chemical_formula_weight  251.20
_symmetry_cell_setting  'monoclinic'
_symmetry_space_group_name_H-M  'P 21/c'
loop_
_symmetry_equiv_pos_as_xyz
  'x, y, z'
  '-x, 1/2+y, 1/2-z'
  '-x, -y, -z'
  'x, 1/2-y, 1/2+z'
_cell_length_a  3.9240(10)
_cell_length_b  20.314(4)
_cell_length_c  13.336(3)
_cell_angle_alpha  90.0
_cell_angle_beta  94.310(10)
_cell_angle_gamma  90.0
_cell_volume  1060.0(10)
_cell_formula_units_Z  4
_cell_measurement_temperature  295(2)
_exptl_crystal_density_diffrn  1.574
_diffrn_ambient_temperature  295(2)
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_occupancy
_atom_site_type_symbol
  O1 .049(4) .0265(3) .2437(5)  .064(3) Uiso 1 O
  O21 .420(3) .1504(3) .0309(5)  .092(2) Uiso 1 O
  O22 .179(3) .0589(3) .0503(6)  .092(2) Uiso 1 O
  O41 -.129(4) .3244(3) .3512(5)  .092(2) Uiso 1 O
  O42 .195(3) .3263(4) .2255(5)  .092(2) Uiso 1 O
  N1 .466(4) .4475(4) .3438(7)  .087(5) Uiso 1 N
  N2 .269(2) .1127(4) .0847(5)  .064(3) Uiso 1 N
  N4 .032(3) .2985(4) .2905(6)  .064(3) Uiso 1 N
  C1 .046(2) .0875(4) .2534(6)  .046(2) Uiso 1 C
  C2 .156(3) .1321(4) .1790(5)  .046(2) Uiso 1 C
  C3 .133(3) .1991(4) .1964(6)  .046(2) Uiso 1 C
  C4 .029(3) .2250(3) .2861(6)  .046(2) Uiso 1 C
  C5 -.208(2) .2048(3) .4530(6)  .046(2) Uiso 1 C
  C6 -.308(3) .1611(4) .5264(6)  .046(2) Uiso 1 C
  C7 -.301(3) .0953(4) .5029(6)  .046(2) Uiso 1 C
  C8 -.181(2) .0687(3) .4189(6)  .046(2) Uiso 1 C
  C9 -.067(3) .1149(4) .3463(5)  .046(2) Uiso 1 C
  C10 -.086(4) .1817(4) .3635(6)  .046(2) Uiso 1 C
  H3 .2168 .2328 .1375  .076 Uiso 1 H
  H5 -.2154 .2587 .4669  .076 Uiso 1 H
  H6 -.4052 .1806 .5938  .076 Uiso 1 H
  H7 -.3798 .0586 .5624  .076 Uiso 1 H
  H8 -.1628 .0170 .4031  .076 Uiso 1 H
  H11 .6091 .4445 .2879  .095 Uiso 1 H
  H12 .2522 .4234 .3352  .095 Uiso 1 H
  H13 .4004 .4978 .3502  .095 Uiso 1 H
  H14 .5937 .4358 .4099  .095 Uiso 1 H
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
  N1 O41 1_555 3.430(10)
  yes
  N1 O42 1_555 3.070(10)
  yes
  N1 O1 2_555 2.770(10)
  yes
  N1 O1 2_655 2.810(10)
  yes
  N1 O22 2_655 2.960(10)
  yes
  N1 O41 1_655 2.960(10)
  yes
  N1 O22 4_555 3.060(10)
  yes
  N1 O21 4_555 3.210(10)
  yes
  C1 C2 . 1.434(12) no
  C1 C9 . 1.457(11) no
  C1 O1 . 1.246(10) no
  C2 C3 . 1.385(12) no
  C2 N2 . 1.420(11) no
  C3 C4 . 1.396(12) no
  C3 H3 . 1.109 no
  C4 C10 . 1.454(13) no
  C4 N4 . 1.494(10) no
  C5 C6 . 1.401(12) no
  C5 C10 . 1.400(13) no
  C5 H5 . 1.111 no
  C6 C7 . 1.372(12) no
  C6 H6 . 1.078 no
  C7 C8 . 1.361(12) no
  C7 H7 . 1.149 no
  C8 C9 . 1.444(11) no
  C8 H8 . 1.073 no
  C9 C10 . 1.378(12) no
  N1 H11 . .970 no
  N1 H12 . .971 no
  N1 H13 . 1.058 no
  N1 H14 . 1.009 no
  N2 O21 . 1.230(11) no
  N2 O22 . 1.228(10) no
  N4 O41 . 1.188(14) no
  N4 O42 . 1.250(13) no