#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/18/2011859.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011859_Fobs loop_ _publ_author_name 'Doma\'nski, Andrzej' 'Ejsmont, Krzysztof' 'Kyzio\/l, Janusz B.' 'Zaleski, Jacek' _publ_section_title ; Two trans-4-aminoazoxybenzenes ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 467 _journal_page_last 470 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.160 _cell_angle_gamma 90.000 _cell_length_a 5.7330 _cell_length_b 11.6020 _cell_length_c 16.0380 _exptl_crystal_F_000 448.00 _reflns_d_resolution_high 0.8392 _[local]_cod_data_source_file da1152Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' S1 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 138.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 693.08 739.13 8.38 o 4 0 0 9.22 7.70 0.44 o 6 0 0 133.01 135.10 2.19 o 1 1 0 1243.63 1187.86 11.21 o 2 1 0 38.62 49.17 0.70 o 3 1 0 130.13 136.43 4.22 o 4 1 0 2.56 3.33 0.93 o 5 1 0 211.67 222.50 3.99 o 6 1 0 15.82 14.41 0.64 o 0 2 0 391.33 381.99 2.91 o 1 2 0 836.76 812.41 2.52 o 2 2 0 809.70 813.72 12.41 o 3 2 0 133.08 140.53 1.34 o 4 2 0 0.36 0.72 0.73 o 5 2 0 270.18 281.89 2.58 o 6 2 0 3.41 4.06 0.48 o 1 3 0 17.23 23.21 0.80 o 2 3 0 1532.98 1511.09 10.95 o 3 3 0 0.73 0.71 0.61 o 4 3 0 33.98 36.27 1.07 o 5 3 0 37.91 35.49 1.28 o 6 3 0 45.43 48.31 1.52 o 0 4 0 1.63 0.13 0.73 o 1 4 0 2255.78 2334.67 40.63 o 2 4 0 40.37 57.01 0.91 o 3 4 0 298.76 323.09 2.16 o 4 4 0 0.13 -0.63 0.79 o 5 4 0 30.21 31.26 1.25 o 6 4 0 33.95 33.32 1.42 o 1 5 0 4.96 4.04 0.30 o 2 5 0 11.03 10.70 1.00 o 3 5 0 82.28 82.73 2.59 o 4 5 0 5.82 7.77 0.38 o 5 5 0 2.40 0.61 0.97 o 6 5 0 6.30 8.84 0.51 o 0 6 0 25.65 29.59 0.78 o 1 6 0 118.49 118.13 2.89 o 2 6 0 82.03 90.37 2.64 o 3 6 0 94.29 100.94 3.67 o 4 6 0 33.49 27.26 1.15 o 5 6 0 38.72 32.04 1.34 o 6 6 0 2.79 -0.45 1.72 o 1 7 0 160.41 172.96 3.29 o 2 7 0 49.61 46.08 1.12 o 3 7 0 2.11 2.16 0.34 o 4 7 0 38.37 34.13 3.29 o 5 7 0 40.64 36.69 1.43 o 0 8 0 72.58 79.58 1.65 o 1 8 0 34.68 41.13 1.10 o 2 8 0 13.27 13.86 0.63 o 3 8 0 35.08 29.22 1.20 o 4 8 0 101.57 89.71 1.79 o 5 8 0 2.99 1.36 1.08 o 1 9 0 16.81 16.22 0.90 o 2 9 0 56.51 59.17 3.92 o 3 9 0 6.73 6.49 0.43 o 4 9 0 4.32 2.09 0.52 o 5 9 0 2.72 2.46 0.62 o 0 10 0 1.35 0.48 1.52 o 1 10 0 36.25 42.67 1.35 o 2 10 0 85.90 85.55 1.72 o 3 10 0 102.69 101.27 1.91 o 4 10 0 1.34 2.00 0.62 o 1 11 0 199.24 213.54 5.27 o 2 11 0 125.46 118.37 2.08 o 3 11 0 0.30 1.33 1.11 o 4 11 0 0.85 1.63 1.28 o 0 12 0 2.45 3.79 0.83 o 1 12 0 1.48 -0.55 1.27 o 2 12 0 7.96 8.08 0.52 o 3 12 0 14.67 13.54 0.69 o 1 13 0 14.06 13.80 0.84 o 2 13 0 4.37 4.79 0.54 o -5 0 1 156.64 165.37 2.87 o -3 0 1 376.01 370.86 5.25 o -1 0 1 3487.06 3228.56 89.70 o 1 0 1 18011.64 16779.37 55.34 o 3 0 1 14.40 13.16 0.61 o 5 0 1 558.19 587.17 3.58 o -6 1 1 1.59 -1.18 1.18 o -5 1 1 200.21 206.21 2.27 o -4 1 1 16.16 12.53 0.72 o -3 1 1 400.22 416.88 4.85 o -2 1 1 663.19 639.81 3.10 o -1 1 1 2833.41 2785.06 7.60 o 0 1 1 433.25 20.73 1.53 o 1 1 1 165.17 155.03 1.08 o 2 1 1 0.03 0.88 0.40 o 3 1 1 5.05 3.65 0.23 o 4 1 1 120.19 115.17 1.49 o 5 1 1 46.82 49.06 1.52 o 6 1 1 72.91 76.67 1.80 o -6 2 1 5.76 4.52 0.83 o -5 2 1 0.05 0.43 0.93 o -4 2 1 6.15 4.40 0.31 o -3 2 1 47.42 46.31 0.89 o -2 2 1 121.01 129.69 1.63 o -1 2 1 370.56 341.54 10.56 o 0 2 1 1.09 0.67 0.10 o 1 2 1 27.62 21.10 0.65 o 2 2 1 15.51 19.16 0.76 o 3 2 1 40.35 41.48 1.99 o 4 2 1 0.01 0.11 0.75 o 5 2 1 12.67 14.35 0.71 o 6 2 1 139.11 142.45 2.28 o -6 3 1 0.04 -1.09 1.09 o -5 3 1 34.48 39.69 1.26 o -4 3 1 48.34 52.41 1.17 o -3 3 1 40.74 39.20 1.23 o -2 3 1 106.91 117.71 1.10 o -1 3 1 742.09 704.84 22.74 o 0 3 1 158.31 165.10 0.76 o 1 3 1 124.23 136.54 1.18 o 2 3 1 654.86 624.77 4.21 o 3 3 1 1293.02 1347.51 7.51 o 4 3 1 14.70 13.37 0.57 o 5 3 1 12.52 12.92 0.69 o 6 3 1 1.78 1.94 0.58 o -6 4 1 4.00 4.11 0.48 o -5 4 1 41.68 37.01 1.26 o -4 4 1 13.23 13.97 0.86 o -3 4 1 30.52 28.47 1.01 o -2 4 1 1039.26 1064.70 15.55 o -1 4 1 70.22 62.46 3.53 o 0 4 1 56.00 50.91 0.50 o 1 4 1 86.40 94.53 1.04 o 2 4 1 607.12 620.06 8.81 o 3 4 1 20.28 16.77 0.78 o 4 4 1 48.48 49.13 1.23 o 5 4 1 4.31 3.98 0.40 o 6 4 1 0.99 0.85 1.04 o -6 5 1 21.30 22.01 0.92 o -5 5 1 2.97 0.27 0.99 o -4 5 1 85.60 98.01 1.59 o -3 5 1 103.61 111.94 1.41 o -2 5 1 163.56 164.03 4.20 o -1 5 1 0.31 0.57 0.50 o 0 5 1 189.69 184.19 1.12 o 1 5 1 95.99 98.05 3.27 o 2 5 1 43.00 41.10 0.87 o 3 5 1 23.49 20.50 0.84 o 4 5 1 2.55 1.25 0.84 o 5 5 1 2.23 2.90 0.98 o 6 5 1 1.52 0.80 1.11 o -6 6 1 13.54 13.32 0.67 o -5 6 1 0.03 -1.02 1.02 o -4 6 1 10.11 11.22 0.52 o -3 6 1 7.21 9.59 0.51 o -2 6 1 0.02 0.56 0.60 o -1 6 1 44.99 52.17 2.20 o 0 6 1 328.86 357.79 1.40 o 1 6 1 290.16 308.61 5.58 o 2 6 1 18.11 18.59 0.78 o 3 6 1 0.34 0.04 0.75 o 4 6 1 0.54 0.15 1.22 o 5 6 1 29.61 30.68 1.30 o 6 6 1 1.78 3.63 0.49 o -5 7 1 11.65 10.43 0.54 o -4 7 1 24.27 20.70 1.00 o -3 7 1 10.25 8.35 0.45 o -2 7 1 13.46 14.92 3.94 o -1 7 1 137.31 137.45 1.48 o 0 7 1 204.37 243.97 1.30 o 1 7 1 671.71 705.83 16.42 o 2 7 1 157.99 177.85 1.77 o 3 7 1 1.16 1.07 0.44 o 4 7 1 8.99 8.44 0.43 o 5 7 1 9.62 8.77 0.84 o -5 8 1 0.87 -0.38 1.09 o -4 8 1 24.21 21.17 2.38 o -3 8 1 3.57 5.54 0.40 o -2 8 1 35.88 38.25 1.86 o -1 8 1 22.99 25.72 1.00 o 0 8 1 0.25 0.52 0.52 o 1 8 1 93.30 106.24 2.20 o 2 8 1 44.98 46.87 1.22 o 3 8 1 11.52 10.61 0.54 o 4 8 1 41.76 38.58 1.38 o 5 8 1 9.28 9.38 0.94 o -5 9 1 6.01 2.96 0.63 o -4 9 1 0.69 0.79 1.03 o -3 9 1 67.74 70.02 2.09 o -2 9 1 3.93 5.08 0.63 o -1 9 1 64.52 67.54 2.30 o 0 9 1 2.77 3.00 0.46 o 1 9 1 2.47 2.87 0.48 o 2 9 1 7.75 7.25 0.40 o 3 9 1 0.38 -0.08 1.02 o 4 9 1 9.48 9.21 0.96 o 5 9 1 1.12 1.13 0.64 o -4 10 1 5.67 5.73 0.48 o -3 10 1 0.02 0.37 1.07 o -2 10 1 189.86 194.10 7.74 o -1 10 1 134.70 147.28 4.38 o 0 10 1 19.59 21.70 0.74 o 1 10 1 32.60 36.98 2.64 o 2 10 1 0.07 0.13 0.99 o 3 10 1 0.10 1.41 1.11 o 4 10 1 44.36 39.76 1.63 o -4 11 1 2.10 0.75 1.29 o -3 11 1 0.81 1.81 1.08 o -2 11 1 99.94 97.01 5.14 o -1 11 1 164.69 168.76 6.04 o 0 11 1 125.94 135.41 1.46 o 1 11 1 9.24 12.19 0.61 o 2 11 1 0.70 -0.41 1.14 o 3 11 1 57.26 55.64 3.85 o 4 11 1 45.29 40.15 2.07 o -3 12 1 13.30 16.98 1.50 o -2 12 1 0.22 1.14 1.14 o -1 12 1 5.66 6.26 0.51 o 0 12 1 8.52 9.76 0.39 o 1 12 1 6.09 5.54 0.52 o 2 12 1 9.18 12.05 1.84 o 3 12 1 11.16 13.63 0.81 o -2 13 1 0.78 1.03 1.52 o -1 13 1 2.32 2.67 0.67 o 0 13 1 168.74 175.38 1.89 o 1 13 1 1.04 0.37 1.26 o 2 13 1 3.11 4.26 1.23 o -6 0 2 113.92 124.02 2.13 o -4 0 2 206.72 201.07 2.34 o -2 0 2 1136.89 1026.01 29.56 o 0 0 2 281.84 203.10 10.81 o 2 0 2 662.24 650.88 2.18 o 4 0 2 201.84 193.87 3.84 o 6 0 2 76.21 74.92 1.90 o -6 1 2 62.53 63.36 1.67 o -5 1 2 13.70 15.57 0.77 o -4 1 2 60.00 64.32 1.67 o -3 1 2 29.19 27.27 2.12 o -2 1 2 4.44 6.33 0.34 o -1 1 2 912.79 844.55 18.02 o 0 1 2 3.95 5.47 0.16 o 1 1 2 8.00 9.03 0.41 o 2 1 2 117.94 136.37 2.12 o 3 1 2 78.29 80.37 1.65 o 4 1 2 456.71 452.10 3.58 o 5 1 2 62.21 65.90 1.74 o 6 1 2 12.87 15.28 1.54 o -6 2 2 41.03 44.97 2.58 o -5 2 2 23.36 22.39 1.11 o -4 2 2 3.06 3.99 0.30 o -3 2 2 550.46 566.55 3.36 o -2 2 2 2481.97 2538.01 35.66 o -1 2 2 10575.91 9745.94 162.20 o 0 2 2 1321.75 1331.22 10.26 o 1 2 2 346.32 320.92 3.52 o 2 2 2 35.35 40.83 0.72 o 3 2 2 4.48 5.52 0.26 o 4 2 2 172.54 175.80 1.84 o 5 2 2 2.11 0.69 0.57 o 6 2 2 19.57 20.71 1.09 o -6 3 2 11.92 12.98 0.68 o -5 3 2 4.01 2.42 0.74 o -4 3 2 0.06 -0.08 0.74 o -3 3 2 50.28 48.21 1.08 o -2 3 2 548.53 535.52 7.52 o -1 3 2 415.29 422.76 21.09 o 0 3 2 2920.98 2733.79 79.02 o 1 3 2 1.16 0.53 0.40 o 2 3 2 828.88 825.83 9.75 o 3 3 2 404.24 433.04 5.85 o 4 3 2 396.18 396.85 4.60 o 5 3 2 192.00 192.87 2.24 o 6 3 2 0.17 0.55 1.33 o -6 4 2 65.44 60.19 3.89 o -5 4 2 6.33 6.55 0.43 o -4 4 2 24.82 23.95 0.99 o -3 4 2 28.92 22.82 1.16 o -2 4 2 316.73 313.87 3.89 o -1 4 2 7.19 6.03 0.48 o 0 4 2 0.32 1.00 0.26 o 1 4 2 118.28 131.42 3.46 o 2 4 2 12.03 16.56 0.70 o 3 4 2 7.08 7.73 0.56 o 4 4 2 30.23 31.28 1.11 o 5 4 2 39.43 42.67 1.35 o 6 4 2 8.32 8.15 0.48 o -6 5 2 1.43 1.52 1.16 o -5 5 2 19.31 17.27 0.83 o -4 5 2 85.51 77.46 1.48 o -3 5 2 85.76 77.43 1.24 o -2 5 2 20.90 23.70 0.96 o -1 5 2 105.73 107.08 6.38 o 0 5 2 88.38 94.38 0.88 o 1 5 2 810.28 812.59 6.07 o 2 5 2 9.29 13.14 0.61 o 3 5 2 45.39 49.10 1.10 o 4 5 2 3.60 4.55 0.35 o 5 5 2 0.22 -0.81 0.93 o 6 5 2 11.28 13.56 0.62 o -6 6 2 0.06 0.93 1.48 o -5 6 2 28.71 28.08 1.29 o -4 6 2 196.97 188.53 2.12 o -3 6 2 32.14 36.34 1.10 o -2 6 2 5.40 6.87 0.43 o -1 6 2 2.23 3.01 0.64 o 0 6 2 0.01 0.37 0.41 o 1 6 2 385.36 404.96 2.56 o 2 6 2 137.70 141.84 1.49 o 3 6 2 24.80 23.23 0.97 o 4 6 2 0.92 1.04 0.47 o 5 6 2 1.09 0.80 1.74 o 6 6 2 0.10 -1.14 1.14 o -5 7 2 1.76 1.84 0.42 o -4 7 2 28.78 28.19 1.23 o -3 7 2 18.99 17.90 0.89 o -2 7 2 7.57 6.52 0.36 o -1 7 2 112.45 115.18 5.34 o 0 7 2 37.89 38.34 0.67 o 1 7 2 544.91 568.62 12.50 o 2 7 2 8.65 7.87 0.35 o 3 7 2 1.11 1.41 0.81 o 4 7 2 0.01 1.32 0.98 o 5 7 2 7.01 6.79 0.47 o -5 8 2 8.18 7.77 0.48 o -4 8 2 14.15 10.86 0.52 o -3 8 2 3.17 1.90 0.96 o -2 8 2 127.88 107.32 65.07 o -1 8 2 32.48 31.16 1.04 o 0 8 2 108.55 119.43 1.54 o 1 8 2 7.68 9.07 0.54 o 2 8 2 4.71 5.08 0.36 o 3 8 2 9.55 9.87 0.47 o 4 8 2 22.27 19.84 1.13 o 5 8 2 2.11 1.96 0.62 o -5 9 2 8.20 7.41 0.51 o -4 9 2 1.13 1.49 0.55 o -3 9 2 54.67 56.01 2.36 o -2 9 2 123.93 118.34 4.93 o -1 9 2 114.92 118.54 6.49 o 0 9 2 56.67 60.66 0.94 o 1 9 2 4.98 6.74 0.38 o 2 9 2 1.65 1.69 0.95 o 3 9 2 7.89 8.19 0.49 o 4 9 2 1.22 -0.49 1.17 o 5 9 2 5.17 6.08 0.66 o -4 10 2 1.59 1.25 1.09 o -3 10 2 1.85 1.76 1.05 o -2 10 2 2.46 0.78 1.11 o -1 10 2 75.04 70.13 1.58 o 0 10 2 0.50 0.77 0.69 o 1 10 2 2.37 2.82 0.51 o 2 10 2 3.69 3.91 1.17 o 3 10 2 159.17 154.82 2.30 o 4 10 2 16.18 17.29 0.88 o -4 11 2 15.54 15.87 1.70 o -3 11 2 1.10 2.04 0.57 o -2 11 2 6.12 5.60 0.46 o -1 11 2 166.10 163.61 5.86 o 0 11 2 66.41 76.60 1.54 o 1 11 2 22.93 22.00 1.04 o 2 11 2 18.95 19.57 0.93 o 3 11 2 25.59 27.35 2.92 o 4 11 2 6.84 7.49 0.57 o -3 12 2 1.72 0.24 1.25 o -2 12 2 14.29 15.52 0.68 o -1 12 2 15.33 14.29 0.72 o 0 12 2 8.88 8.65 0.37 o 1 12 2 56.06 56.54 1.67 o 2 12 2 10.02 8.84 0.98 o 3 12 2 1.09 1.33 1.22 o -2 13 2 0.25 0.79 1.39 o -1 13 2 19.75 22.12 0.92 o 0 13 2 46.51 45.31 1.26 o 1 13 2 141.74 137.68 2.44 o 2 13 2 4.55 6.29 0.54 o -5 0 3 64.60 70.89 1.49 o -3 0 3 734.30 736.48 22.28 o -1 0 3 579.33 590.73 3.98 o 1 0 3 229.04 244.68 2.04 o 3 0 3 1.69 3.25 0.23 o 5 0 3 442.34 451.08 5.21 o -6 1 3 14.06 13.81 0.79 o -5 1 3 38.65 42.00 2.01 o -4 1 3 186.24 203.59 1.88 o -3 1 3 12.13 12.12 0.64 o -2 1 3 34.55 30.26 0.64 o -1 1 3 96.67 100.21 0.79 o 0 1 3 2695.45 2640.32 9.12 o 1 1 3 1319.02 1253.98 3.33 o 2 1 3 1242.28 1297.79 3.21 o 3 1 3 40.50 48.06 0.92 o 4 1 3 152.45 146.87 4.86 o 5 1 3 32.77 27.64 1.28 o 6 1 3 2.78 3.10 0.46 o -6 2 3 25.87 30.42 1.49 o -5 2 3 2.52 4.10 0.37 o -4 2 3 0.42 0.85 0.72 o -3 2 3 203.89 202.74 1.62 o -2 2 3 46.42 47.79 1.57 o -1 2 3 19073.80 17023.08 23.13 o 0 2 3 15959.02 13884.08 415.77 o 1 2 3 946.37 946.24 2.38 o 2 2 3 163.15 160.55 1.25 o 3 2 3 23.07 23.84 0.81 o 4 2 3 50.90 46.27 1.20 o 5 2 3 216.43 211.97 3.47 o 6 2 3 3.63 4.30 0.46 o -6 3 3 31.41 31.47 1.80 o -5 3 3 7.94 11.13 0.54 o -4 3 3 5.94 7.38 0.40 o -3 3 3 97.77 100.94 1.24 o -2 3 3 394.60 377.08 8.72 o -1 3 3 1682.84 1683.66 94.49 o 0 3 3 7.05 7.08 0.24 o 1 3 3 17.98 15.31 0.51 o 2 3 3 87.09 87.50 2.03 o 3 3 3 17.66 13.35 1.20 o 4 3 3 259.48 252.38 2.22 o 5 3 3 38.86 41.56 1.39 o 6 3 3 6.67 5.83 0.46 o -6 4 3 5.31 7.00 0.51 o -5 4 3 76.07 74.47 2.17 o -4 4 3 0.30 1.55 0.78 o -3 4 3 0.23 -0.39 0.96 o -2 4 3 255.20 244.47 7.64 o -1 4 3 50.79 58.77 3.12 o 0 4 3 259.03 231.69 9.14 o 1 4 3 20.69 18.13 1.48 o 2 4 3 685.36 729.24 26.13 o 3 4 3 0.92 1.02 0.66 o 4 4 3 38.74 36.45 1.17 o 5 4 3 7.46 7.30 0.62 o 6 4 3 1.18 0.23 1.07 o -6 5 3 78.01 73.85 1.91 o -5 5 3 15.30 14.87 0.81 o -4 5 3 36.70 35.18 1.16 o -3 5 3 77.84 81.31 3.43 o -2 5 3 17.68 13.03 1.40 o -1 5 3 20.02 25.58 1.95 o 0 5 3 800.98 847.78 33.23 o 1 5 3 32.95 26.91 1.50 o 2 5 3 323.79 329.21 12.66 o 3 5 3 16.70 21.30 0.90 o 4 5 3 14.35 14.18 1.59 o 5 5 3 11.11 11.75 0.59 o 6 5 3 4.54 4.33 0.49 o -6 6 3 9.05 11.49 0.54 o -5 6 3 64.48 63.26 3.36 o -4 6 3 0.02 0.75 0.90 o -3 6 3 82.57 92.38 3.48 o -2 6 3 42.59 36.94 1.47 o -1 6 3 0.01 -0.57 0.57 o 0 6 3 4.37 1.58 0.34 o 1 6 3 858.54 921.35 4.52 o 2 6 3 99.11 110.11 2.15 o 3 6 3 0.19 0.03 0.77 o 4 6 3 14.49 14.46 0.75 o 5 6 3 0.01 -1.00 1.00 o -5 7 3 1.08 -0.18 1.04 o -4 7 3 7.03 4.92 0.41 o -3 7 3 160.85 167.55 6.74 o -2 7 3 1.59 1.14 0.75 o -1 7 3 0.95 1.26 0.68 o 0 7 3 86.81 91.52 1.79 o 1 7 3 1.45 1.82 0.29 o 2 7 3 24.74 26.37 0.99 o 3 7 3 13.62 12.48 0.65 o 4 7 3 0.07 0.40 0.94 o 5 7 3 20.90 18.17 0.88 o -5 8 3 0.26 0.76 1.08 o -4 8 3 83.06 74.81 1.65 o -3 8 3 76.98 73.81 1.60 o -2 8 3 15.89 17.36 0.96 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