#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:31:24 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180787 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/18/2011861.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011861_Fobs loop_ _publ_author_name 'Cai, Jiwen' 'Hu, Xiaopeng' 'Chen, Cai-Hong' 'Ji, Liang-Nian' _publ_section_title ; trans-(DL-Isoleucinato-N,O)[tris(2-aminoethyl)amine-\k^4^N]cobalt(III) diperchlorate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 394 _journal_page_last 396 _journal_volume 57 _journal_year 2001 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.4330 _cell_length_b 25.2657 _cell_length_c 27.2578 _exptl_crystal_F_000 3336.00 _reflns_d_resolution_high 0.8000 _cod_data_source_file da1160Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 05031M in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 690.49 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5167.97 6684.70 123.79 o 6 0 0 355.98 590.00 69.63 o 8 0 0 4533.85 5072.25 159.85 o 10 0 0 1524.51 1478.80 181.26 o 2 1 0 30.73 208.89 37.58 o 3 1 0 755.01 769.30 37.70 o 4 1 0 1265.75 1712.96 56.66 o 5 1 0 753.86 627.67 47.54 o 6 1 0 2326.80 1971.21 64.87 o 7 1 0 2143.00 2032.55 101.30 o 8 1 0 104.26 103.28 50.54 o 9 1 0 697.76 664.95 94.05 o 10 1 0 945.35 1062.34 115.82 o 11 1 0 25.57 51.48 83.61 o 2 2 0 9863.26 8798.75 160.26 o 3 2 0 25924.96 26711.17 402.46 o 4 2 0 63.33 10.78 23.98 o 5 2 0 12381.00 13015.97 213.79 o 6 2 0 1387.17 1664.06 61.22 o 7 2 0 5502.56 5445.12 107.34 o 8 2 0 1434.80 1663.55 89.88 o 9 2 0 52.75 48.32 64.85 o 10 2 0 107.63 99.60 71.07 o 11 2 0 4752.07 5235.96 218.91 o 2 3 0 1970.54 1864.30 82.34 o 3 3 0 2625.94 3019.86 61.59 o 4 3 0 3717.24 2890.17 68.96 o 5 3 0 3865.60 3802.46 87.12 o 6 3 0 5716.92 5691.22 115.16 o 7 3 0 232.74 221.21 42.01 o 8 3 0 797.45 727.53 75.74 o 9 3 0 483.06 575.77 127.10 o 10 3 0 2126.93 2194.82 116.75 o 11 3 0 56.16 47.68 85.36 o 1 4 0 12302.78 12266.97 175.73 o 2 4 0 55211.25 65926.20 651.54 o 3 4 0 1413.55 1591.30 42.39 o 4 4 0 20366.54 21645.23 362.80 o 5 4 0 1606.39 1748.75 64.16 o 6 4 0 1190.56 1469.83 68.76 o 7 4 0 1171.29 1130.55 94.88 o 8 4 0 3003.46 3879.57 122.60 o 9 4 0 157.45 95.32 49.10 o 10 4 0 2277.36 2416.09 153.91 o 11 4 0 848.68 864.29 175.73 o 1 5 0 44148.99 49033.57 311.38 o 2 5 0 8147.00 6654.27 113.71 o 3 5 0 7095.83 8257.67 110.71 o 4 5 0 260.19 354.32 46.90 o 5 5 0 3371.59 3616.36 74.71 o 6 5 0 6177.05 7325.82 113.45 o 7 5 0 6048.62 6050.42 141.88 o 8 5 0 787.39 897.51 66.70 o 9 5 0 36.74 15.23 45.43 o 10 5 0 232.44 272.23 90.26 o 11 5 0 0.10 -107.21 107.21 o 0 6 0 10343.33 10562.71 173.52 o 1 6 0 24547.93 25078.23 369.15 o 2 6 0 497.34 478.20 27.68 o 3 6 0 3211.69 3177.09 60.78 o 4 6 0 949.00 1054.02 44.34 o 5 6 0 1200.67 1470.00 63.49 o 6 6 0 109.37 100.01 33.70 o 7 6 0 31.08 58.20 46.10 o 8 6 0 656.34 784.05 64.41 o 9 6 0 469.97 548.76 62.71 o 10 6 0 390.29 407.83 141.47 o 11 6 0 807.57 868.71 181.26 o 1 7 0 2666.20 3342.60 63.17 o 2 7 0 32623.79 31758.15 191.47 o 3 7 0 552.90 659.35 35.28 o 4 7 0 42.31 101.25 25.79 o 5 7 0 2.08 -11.40 26.38 o 6 7 0 17975.12 18751.78 181.86 o 7 7 0 1113.86 1341.58 83.14 o 8 7 0 166.37 34.06 49.80 o 9 7 0 941.54 1226.12 95.80 o 10 7 0 450.90 409.65 98.43 o 11 7 0 60.98 44.21 124.89 o 0 8 0 170982.41 177453.55 856.15 o 1 8 0 8251.27 8091.72 86.59 o 2 8 0 450.56 563.69 29.38 o 3 8 0 397.65 390.55 29.33 o 4 8 0 127.40 126.28 26.98 o 5 8 0 2.10 35.95 28.03 o 6 8 0 60.17 7.09 38.74 o 7 8 0 1369.20 1444.33 86.18 o 8 8 0 221.07 536.35 71.42 o 9 8 0 139.54 208.50 134.29 o 10 8 0 339.97 351.05 120.47 o 11 8 0 202.53 678.61 177.94 o 1 9 0 7144.76 7786.06 95.96 o 2 9 0 1869.18 2147.83 45.44 o 3 9 0 1877.62 1569.17 41.98 o 4 9 0 696.09 672.12 42.14 o 5 9 0 56339.17 54414.80 1126.63 o 6 9 0 97.53 140.34 46.70 o 7 9 0 3395.57 3555.46 120.96 o 8 9 0 53.40 60.22 53.69 o 9 9 0 727.32 815.39 107.46 o 10 9 0 106.57 59.79 82.38 o 11 9 0 24.22 -75.16 118.26 o 0 10 0 2593.35 2194.86 78.14 o 1 10 0 9863.68 10315.56 232.59 o 2 10 0 1796.73 2087.99 47.22 o 3 10 0 2712.18 2114.07 49.68 o 4 10 0 3688.58 2949.06 69.17 o 5 10 0 421.45 426.23 41.51 o 6 10 0 1032.79 943.24 73.21 o 7 10 0 47.09 8.99 47.36 o 8 10 0 486.79 411.98 90.24 o 9 10 0 0.61 10.71 72.37 o 10 10 0 0.98 -20.07 85.14 o 11 10 0 2.58 -18.79 142.57 o 1 11 0 2308.08 2336.18 59.61 o 2 11 0 3511.37 3554.57 60.97 o 3 11 0 5811.46 5181.24 113.70 o 4 11 0 11363.11 8977.02 115.68 o 5 11 0 1014.82 1163.10 57.45 o 6 11 0 27076.91 24362.18 272.86 o 7 11 0 726.10 691.84 98.03 o 8 11 0 9.17 -8.55 66.99 o 9 11 0 618.71 685.89 109.40 o 10 11 0 882.46 879.85 130.12 o 11 11 0 15.90 28.49 101.16 o 0 12 0 39242.61 35251.73 320.28 o 1 12 0 7437.54 7383.73 101.51 o 2 12 0 3122.79 2604.74 65.58 o 3 12 0 5236.15 5216.69 77.61 o 4 12 0 315.91 285.64 36.76 o 5 12 0 6011.25 5771.40 129.30 o 6 12 0 1017.55 868.38 98.98 o 7 12 0 84.54 108.83 70.63 o 8 12 0 1760.24 2087.36 146.97 o 9 12 0 13.08 29.94 75.27 o 10 12 0 26.60 -43.49 88.27 o 1 13 0 26852.84 26307.63 249.08 o 2 13 0 678.03 692.77 44.66 o 3 13 0 1453.68 1679.75 52.15 o 4 13 0 3212.08 2864.81 83.43 o 5 13 0 6345.02 6196.99 136.60 o 6 13 0 2436.44 2247.99 134.18 o 7 13 0 1983.17 2216.83 138.30 o 8 13 0 117.68 73.55 80.08 o 9 13 0 19.63 -31.36 79.70 o 10 13 0 974.16 1039.46 141.40 o 0 14 0 45343.34 41800.92 525.54 o 1 14 0 614.35 721.83 53.33 o 2 14 0 15.60 83.77 30.40 o 3 14 0 1712.43 1873.38 56.60 o 4 14 0 6713.66 7284.14 115.76 o 5 14 0 431.22 375.06 78.14 o 6 14 0 1109.10 1374.02 118.49 o 7 14 0 3659.54 3707.90 249.78 o 8 14 0 2203.48 2828.65 164.03 o 9 14 0 1103.21 1310.32 142.07 o 10 14 0 418.56 615.71 125.43 o 1 15 0 702.55 608.15 45.48 o 2 15 0 1353.15 1472.13 61.39 o 3 15 0 2691.99 3033.95 131.45 o 4 15 0 1672.63 1644.09 68.10 o 5 15 0 2868.47 2914.34 145.26 o 6 15 0 4594.31 4473.65 328.81 o 7 15 0 1543.57 1581.10 137.02 o 8 15 0 293.43 180.74 85.99 o 9 15 0 6.53 -19.46 85.96 o 10 15 0 65.70 4.40 97.24 o 0 16 0 3282.69 3438.51 144.79 o 1 16 0 2037.33 1901.85 69.86 o 2 16 0 262.42 364.14 42.04 o 3 16 0 10458.09 10402.28 200.84 o 4 16 0 6562.70 6748.38 190.65 o 5 16 0 468.69 382.43 80.86 o 6 16 0 228.18 173.54 78.19 o 7 16 0 3935.83 4060.74 197.84 o 8 16 0 1401.56 1727.92 154.18 o 9 16 0 2.57 -58.05 112.73 o 10 16 0 136.39 67.59 95.98 o 1 17 0 312.39 509.66 47.88 o 2 17 0 825.35 765.58 54.72 o 3 17 0 1836.89 2069.15 75.31 o 4 17 0 653.55 480.84 85.55 o 5 17 0 200.00 168.35 74.83 o 6 17 0 263.65 243.81 85.76 o 7 17 0 722.21 984.26 123.02 o 8 17 0 226.45 190.82 94.48 o 9 17 0 86.77 159.42 100.93 o 0 18 0 5681.27 5521.26 298.41 o 1 18 0 1607.43 1552.88 70.54 o 2 18 0 1127.19 1093.60 62.22 o 3 18 0 16390.27 15070.68 343.70 o 4 18 0 2075.28 1999.49 149.76 o 5 18 0 4035.32 3671.24 169.82 o 6 18 0 28.12 55.35 76.12 o 7 18 0 851.36 781.64 161.36 o 8 18 0 118.23 122.03 95.33 o 9 18 0 5.26 -18.53 98.32 o 1 19 0 3750.76 3589.07 97.22 o 2 19 0 298.42 290.25 45.41 o 3 19 0 6816.92 6716.97 128.46 o 4 19 0 656.61 805.07 105.11 o 5 19 0 296.84 208.06 83.23 o 6 19 0 1859.23 1887.78 142.27 o 7 19 0 1.64 -53.48 81.10 o 8 19 0 305.49 222.24 98.50 o 9 19 0 962.29 1273.73 153.57 o 0 20 0 123.70 137.48 58.55 o 1 20 0 5366.08 5425.69 116.89 o 2 20 0 486.39 602.31 55.75 o 3 20 0 2399.94 2629.17 108.63 o 4 20 0 1829.79 1774.53 181.81 o 5 20 0 254.50 151.97 80.50 o 6 20 0 1063.94 1126.81 129.98 o 7 20 0 163.91 139.78 123.79 o 8 20 0 294.62 347.33 107.03 o 9 20 0 73.80 45.56 103.37 o 1 21 0 3531.79 3634.77 101.23 o 2 21 0 2207.32 1993.98 82.77 o 3 21 0 270.37 353.62 83.01 o 4 21 0 3.46 6.26 72.26 o 5 21 0 59.85 35.75 76.91 o 6 21 0 360.85 318.31 99.02 o 7 21 0 13.66 23.78 87.71 o 8 21 0 401.07 483.42 116.04 o 0 22 0 2892.79 3367.16 144.18 o 1 22 0 138.35 263.82 50.45 o 2 22 0 323.06 476.79 68.67 o 3 22 0 334.34 387.14 85.01 o 4 22 0 302.30 217.46 86.36 o 5 22 0 72.79 58.86 80.21 o 6 22 0 195.71 206.00 90.63 o 7 22 0 226.75 190.62 94.55 o 8 22 0 1.96 -80.31 87.48 o 1 23 0 25.28 -38.27 41.12 o 2 23 0 3780.90 3619.03 129.03 o 3 23 0 926.82 967.44 112.13 o 4 23 0 297.92 228.23 86.74 o 5 23 0 1410.06 1412.23 140.57 o 6 23 0 7.12 -44.37 85.24 o 7 23 0 38.17 16.21 88.65 o 8 23 0 196.00 222.57 110.84 o 0 24 0 272.63 259.63 75.80 o 1 24 0 948.45 854.31 83.14 o 2 24 0 301.99 430.83 69.20 o 3 24 0 19.02 -28.70 67.63 o 4 24 0 8.93 30.22 76.95 o 5 24 0 0.34 22.05 83.52 o 6 24 0 66.87 115.78 97.65 o 7 24 0 73.57 -52.85 91.73 o 1 25 0 2335.87 2517.97 115.69 o 2 25 0 1406.30 1397.68 125.04 o 3 25 0 2123.50 2694.10 158.24 o 4 25 0 59.84 -29.99 77.18 o 5 25 0 27.70 -53.84 81.66 o 6 25 0 297.03 179.60 100.03 o 7 25 0 231.47 61.74 107.29 o 0 26 0 1061.76 1048.87 165.78 o 1 26 0 106.57 188.35 66.15 o 2 26 0 66.57 115.61 77.36 o 3 26 0 312.50 326.41 94.26 o 4 26 0 59.21 -20.35 78.89 o 5 26 0 114.69 58.17 89.46 o 6 26 0 9.27 -18.78 94.41 o 1 27 0 217.30 234.76 72.10 o 2 27 0 2500.33 2261.03 148.97 o 3 27 0 24.87 13.60 79.32 o 4 27 0 11.65 -5.44 83.58 o 5 27 0 324.00 390.51 111.08 o 6 27 0 39.68 -9.10 94.50 o 0 28 0 3.28 -2.21 102.79 o 1 28 0 233.15 328.42 101.68 o 2 28 0 990.18 1128.33 130.95 o 3 28 0 28.60 59.45 90.57 o 4 28 0 1889.50 1745.59 155.12 o 5 28 0 29.57 3.89 88.86 o 1 29 0 1583.16 1482.12 204.47 o 2 29 0 166.82 137.52 92.49 o 3 29 0 1104.65 1280.72 144.35 o 4 29 0 253.33 128.16 100.00 o 0 30 0 499.37 669.77 164.68 o 1 30 0 112.13 118.26 131.52 o 2 30 0 53.42 -29.84 127.10 o 3 30 0 1628.28 1836.01 161.31 o 1 31 0 200.22 185.68 154.73 o 2 31 0 202.20 245.36 158.05 o 3 0 1 14555.94 15138.26 173.26 o 4 0 1 5257.31 6071.09 172.47 o 5 0 1 7740.28 7140.12 122.04 o 6 0 1 8956.80 9510.95 127.62 o 7 0 1 138.05 171.17 39.87 o 8 0 1 2049.83 2310.57 98.24 o 9 0 1 610.59 496.73 86.58 o 10 0 1 4479.39 4604.29 184.83 o 11 0 1 458.43 549.50 106.57 o -11 1 1 690.18 777.60 116.04 o -10 1 1 193.89 213.67 83.01 o -9 1 1 3262.92 3144.47 148.06 o -8 1 1 2187.30 1855.60 93.02 o -7 1 1 6287.01 5567.70 100.09 o -6 1 1 2989.51 2850.07 84.26 o -5 1 1 11821.74 10649.19 174.43 o -4 1 1 14344.21 13644.97 242.05 o -3 1 1 6888.12 8981.67 125.36 o -2 1 1 22037.45 29504.18 309.47 o 3 1 1 6301.80 7712.00 112.77 o 4 1 1 15549.24 15341.05 160.16 o 5 1 1 11540.28 10489.39 106.64 o 6 1 1 3014.67 2840.55 76.69 o 7 1 1 6101.20 5256.47 124.32 o 8 1 1 2247.24 1950.08 80.01 o 9 1 1 3202.55 3349.99 152.25 o 10 1 1 187.03 239.17 82.80 o 11 1 1 672.86 825.45 121.89 o -11 2 1 298.18 218.16 93.60 o -10 2 1 642.02 714.93 104.50 o -9 2 1 1966.23 1700.03 176.28 o -8 2 1 1194.12 1263.36 72.09 o -7 2 1 428.76 332.18 44.39 o -6 2 1 2480.04 2588.09 80.59 o -5 2 1 15693.74 16251.03 169.67 o -4 2 1 1641.62 1821.13 55.51 o -3 2 1 1450.15 1575.07 60.12 o -2 2 1 10629.51 11430.31 183.47 o 2 2 1 11840.04 13007.51 140.20 o 3 2 1 1284.57 1179.16 45.08 o 4 2 1 1313.69 1440.08 54.63 o 5 2 1 15168.33 15770.94 150.25 o 6 2 1 2541.52 2625.32 73.76 o 7 2 1 474.88 364.79 45.12 o 8 2 1 1383.69 1284.13 103.18 o 9 2 1 1982.62 1846.26 124.64 o 10 2 1 598.02 593.51 147.00 o 11 2 1 286.52 381.96 108.24 o -11 3 1 3.07 -79.30 79.30 o -10 3 1 848.27 855.85 108.85 o -9 3 1 123.50 91.01 48.41 o -8 3 1 3260.58 3422.82 167.75 o -7 3 1 152.83 97.04 54.70 o -6 3 1 557.01 562.61 49.67 o -5 3 1 1397.39 1541.04 81.72 o -4 3 1 11200.20 11255.15 124.60 o -3 3 1 2215.86 2205.48 72.92 o -2 3 1 15589.67 17979.50 552.62 o 2 3 1 14261.68 17718.63 268.69 o 3 3 1 2036.27 2003.56 47.47 o 4 3 1 10246.81 10301.26 126.39 o 5 3 1 1630.85 1922.55 72.29 o 6 3 1 590.52 563.21 45.86 o 7 3 1 197.24 218.09 42.34 o 8 3 1 2994.80 3047.08 110.35 o 9 3 1 152.74 260.27 78.47 o 10 3 1 821.20 837.35 111.36 o 11 3 1 0.52 -56.62 82.56 o -11 4 1 167.66 151.42 135.94 o -10 4 1 656.41 487.50 100.42 o -9 4 1 732.57 825.13 71.48 o -8 4 1 870.36 669.41 72.82 o -7 4 1 7261.06 8355.13 200.56 o -6 4 1 2598.44 2516.15 81.50 o -5 4 1 4647.09 4073.34 89.20 o -4 4 1 1967.85 1903.81 57.52 o -3 4 1 894.41 1095.95 60.26 o -2 4 1 2757.09 3238.39 76.98 o 2 4 1 3117.10 3587.05 62.93 o 3 4 1 893.02 1098.89 39.85 o 4 4 1 1614.50 1573.30 55.52 o 5 4 1 4377.74 3699.65 88.45 o 6 4 1 2329.62 2062.33 79.31 o 7 4 1 7116.83 7541.10 125.84 o 8 4 1 887.52 794.19 64.72 o 9 4 1 794.97 806.44 80.24 o 10 4 1 616.20 575.40 104.69 o 11 4 1 155.90 141.49 90.74 o -11 5 1 732.30 574.72 169.10 o -10 5 1 1036.23 1233.74 202.81 o -9 5 1 1233.32 1343.38 83.26 o -8 5 1 1941.29 2489.03 107.00 o -7 5 1 10371.73 11248.35 233.79 o -6 5 1 567.69 694.86 53.75 o -5 5 1 259.68 401.72 41.13 o -4 5 1 40.35 47.07 21.87 o -3 5 1 4957.59 5636.23 111.60 o -2 5 1 19338.38 20549.71 203.18 o -1 5 1 26177.33 28522.33 223.10 o 1 5 1 25082.16 28568.10 217.98 o 2 5 1 18250.80 19717.67 190.91 o 3 5 1 5845.49 6378.75 127.14 o 4 5 1 18.90 87.54 24.84 o 5 5 1 167.52 301.41 35.11 o 6 5 1 537.80 634.73 47.98 o 7 5 1 10771.41 11461.87 162.11 o 8 5 1 1756.92 2152.42 86.67 o 9 5 1 1370.57 1409.91 81.07 o 10 5 1 903.69 989.95 120.59 o 11 5 1 767.40 946.08 184.57 o -11 6 1 93.68 169.10 133.73 o -10 6 1 1.27 -8.84 106.10 o -9 6 1 1090.14 1358.36 85.51 o -8 6 1 32.66 -28.56 48.34 o -7 6 1 4176.18 4617.72 128.02 o -6 6 1 277.65 307.01 37.10 o -5 6 1 896.27 902.44 49.13 o -4 6 1 3082.34 2397.88 55.82 o -3 6 1 908.96 1129.21 48.30 o -2 6 1 6962.26 5732.93 112.54 o -1 6 1 9337.56 9573.76 129.33 o 0 6 1 9413.21 8763.42 92.47 o 1 6 1 8433.16 9277.29 100.98 o 2 6 1 6441.07 5259.43 59.55 o 3 6 1 565.03 729.91 35.57 o 4 6 1 3156.13 2487.82 60.72 o 5 6 1 923.73 922.42 49.30 o 6 6 1 288.01 280.46 40.89 o 7 6 1 4448.97 4715.12 130.36 o 8 6 1 41.22 -24.74 39.88 o 9 6 1 1095.12 1346.14 97.90 o 10 6 1 5.60 -10.06 61.32 o 11 6 1 102.96 134.84 134.84 o -11 7 1 265.94 152.52 140.36 o -10 7 1 522.22 780.29 163.57 o -9 7 1 209.12 192.36 76.91 o -8 7 1 595.68 565.22 69.06 o -7 7 1 1322.39 1283.92 80.90 o -6 7 1 1713.40 1921.14 94.36 o -5 7 1 1544.20 1676.23 55.63 o -4 7 1 25453.70 27260.99 182.63 o -3 7 1 5640.30 5211.32 70.70 o -2 7 1 1610.15 1491.10 86.21 o -1 7 1 12705.62 11277.64 114.53 o 0 7 1 46554.47 47981.12 224.82 o 1 7 1 12506.02 11454.63 202.04 o 2 7 1 1854.50 1993.25 41.71 o 3 7 1 5942.16 5651.89 79.07 o 4 7 1 24653.53 26614.20 189.43 o 5 7 1 1470.14 1661.14 59.29 o 6 7 1 1661.72 1945.46 69.43 o 7 7 1 1404.54 1440.70 85.39 o 8 7 1 328.15 352.86 56.63 o 9 7 1 268.42 182.78 65.74 o 10 7 1 561.05 560.35 149.21 o 11 7 1 266.94 303.94 149.21 o -11 8 1 146.72 99.47 145.89 o -10 8 1 532.61 640.28 112.68 o -9 8 1 655.20 674.67 106.07 o -8 8 1 657.04 733.15 75.57 o -7 8 1 6693.56 6991.56 153.10 o -6 8 1 700.90 970.60 70.54 o -5 8 1 249.64 126.27 30.53 o -4 8 1 4512.22 4400.30 75.11 o -3 8 1 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