#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:31:24 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180787 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/18/2011868.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2011868_Fobs loop_ _publ_author_name 'Jameson, Geoffrey B.' 'Collman, James P.' 'Boulatov, Roman' _publ_section_title ; Superimposed saddle and ruffled distortions of the porphyrin in iodo(pyridine-N)(5,10,15,20-tetraphenylporphyrinato-\k^4^N)rhodium(III) toluene solvate ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 406 _journal_page_last 408 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.560 _cell_angle_gamma 90.000 _cell_length_a 13.3463 _cell_length_b 23.4600 _cell_length_c 14.5584 _exptl_crystal_F_000 2040.00 _reflns_d_resolution_high 0.8505 _cod_data_source_file fg1606Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Rb4 Rh(TPP)Ipy' _shelx_refln_list_code 4 _shelx_f_calc_maximum 350.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 22714.93 25399.07 704.21 o 4 0 0 94096.45 106669.37 2812.88 o 6 0 0 435.48 309.02 207.99 o 8 0 0 46.30 22.78 249.59 o 10 0 0 3695.70 2762.36 462.54 o 12 0 0 1569.61 2430.57 581.39 o 14 0 0 14643.40 16028.94 766.69 o 1 1 0 14618.09 13609.09 187.17 o 2 1 0 49516.25 55420.44 1031.33 o 3 1 0 21028.56 22871.01 1851.64 o 4 1 0 12377.57 12363.02 603.68 o 5 1 0 22604.20 21883.72 510.72 o 6 1 0 6069.16 6009.09 269.95 o 7 1 0 352.86 -28.22 153.39 o 8 1 0 56.69 -176.13 176.13 o 9 1 0 1451.32 748.08 777.50 o 10 1 0 3438.71 4267.90 301.19 o 11 1 0 1065.30 1736.97 516.56 o 12 1 0 3514.17 3483.42 304.45 o 13 1 0 1143.00 403.18 461.33 o 14 1 0 447.36 431.11 599.78 o 15 1 0 714.92 586.73 1190.52 o 0 2 0 63973.34 75173.70 4054.90 o 1 2 0 33996.79 34035.18 449.03 o 2 2 0 25586.39 23687.89 269.10 o 3 2 0 41463.79 43246.62 686.53 o 4 2 0 670.48 618.46 195.73 o 5 2 0 11614.87 11485.83 767.10 o 6 2 0 2405.66 1682.60 529.39 o 7 2 0 9565.65 10656.59 318.24 o 8 2 0 3652.08 4128.87 348.62 o 9 2 0 444.32 636.10 193.85 o 10 2 0 157.92 499.25 353.93 o 11 2 0 863.85 1902.36 290.98 o 12 2 0 1762.62 2576.44 435.32 o 13 2 0 4454.38 4341.71 395.57 o 14 2 0 1796.48 1562.35 468.72 o 15 2 0 2995.52 3395.90 1496.57 o 1 3 0 10836.76 12378.14 302.22 o 2 3 0 9217.52 9681.24 142.86 o 3 3 0 12950.11 13107.02 215.27 o 4 3 0 2830.21 2913.40 188.98 o 5 3 0 2076.35 2497.14 215.29 o 6 3 0 6314.71 5139.12 358.89 o 7 3 0 2119.26 2199.50 207.84 o 8 3 0 4237.49 4490.63 244.46 o 9 3 0 1129.69 1072.77 208.73 o 10 3 0 8164.20 7611.39 419.46 o 11 3 0 3494.39 2962.56 297.67 o 12 3 0 78.01 127.71 261.69 o 13 3 0 4088.64 3005.02 589.32 o 14 3 0 1478.76 2208.79 373.73 o 15 3 0 2614.03 3064.70 665.86 o 0 4 0 48.80 36.30 133.71 o 1 4 0 29234.83 28178.46 390.58 o 2 4 0 9850.07 11689.21 200.30 o 3 4 0 53.57 107.45 75.52 o 4 4 0 5751.41 5296.04 114.35 o 5 4 0 2535.42 2414.88 116.76 o 6 4 0 8939.11 9262.06 216.96 o 7 4 0 6072.26 6431.24 416.73 o 8 4 0 12534.54 12886.73 532.74 o 9 4 0 3398.96 2870.45 435.12 o 10 4 0 3351.93 2933.14 354.48 o 11 4 0 1712.25 1517.92 415.44 o 12 4 0 1916.08 2361.55 394.54 o 13 4 0 3300.34 3984.60 454.26 o 14 4 0 3021.65 2261.83 473.93 o 15 4 0 1863.36 1290.22 398.99 o 1 5 0 9615.10 9408.60 374.55 o 2 5 0 48024.60 48189.54 658.86 o 3 5 0 23704.13 23357.19 311.78 o 4 5 0 6058.25 6455.52 138.93 o 5 5 0 8890.26 8882.53 259.68 o 6 5 0 1545.79 1518.77 184.69 o 7 5 0 1377.44 1156.96 174.01 o 8 5 0 12837.99 13023.87 714.79 o 9 5 0 13176.06 13475.97 349.14 o 10 5 0 735.46 735.67 180.24 o 11 5 0 3398.92 3667.14 1662.96 o 12 5 0 5926.49 4856.81 677.47 o 13 5 0 459.86 -133.73 344.10 o 14 5 0 191.36 1243.08 422.83 o 15 5 0 2000.19 1850.95 658.75 o 0 6 0 2730.66 3668.37 164.16 o 1 6 0 334.09 585.81 181.41 o 2 6 0 7551.68 7820.70 426.77 o 3 6 0 25664.20 27078.68 410.81 o 4 6 0 7865.08 8085.97 325.46 o 5 6 0 6531.68 6573.46 175.13 o 6 6 0 5571.47 6630.39 191.11 o 7 6 0 67425.00 70670.27 2258.70 o 8 6 0 526.78 635.94 169.71 o 9 6 0 52.76 -186.15 199.12 o 10 6 0 2246.09 1911.67 347.29 o 11 6 0 10952.47 10435.70 908.74 o 12 6 0 1183.08 1531.77 361.41 o 13 6 0 1487.51 2258.94 663.60 o 14 6 0 1739.58 822.58 452.38 o 15 6 0 12.51 89.20 624.97 o 1 7 0 8469.73 8805.46 178.18 o 2 7 0 2326.61 2483.35 134.24 o 3 7 0 3693.66 4059.42 139.12 o 4 7 0 6291.43 6546.00 323.80 o 5 7 0 40122.11 41222.82 1195.70 o 6 7 0 2273.64 2447.85 151.79 o 7 7 0 2573.44 3011.27 237.26 o 8 7 0 3951.20 3454.67 249.56 o 9 7 0 31551.19 33572.45 1981.89 o 10 7 0 700.93 412.21 472.94 o 11 7 0 136.66 575.25 651.72 o 12 7 0 110.15 592.02 663.11 o 13 7 0 3450.55 2780.03 674.00 o 14 7 0 227.34 1166.38 455.01 o 0 8 0 593.48 784.38 127.27 o 1 8 0 16476.31 15671.17 770.55 o 2 8 0 3760.95 3599.47 125.52 o 3 8 0 10083.13 10083.58 267.76 o 4 8 0 199.34 399.91 96.14 o 5 8 0 1151.15 1220.88 179.13 o 6 8 0 38749.63 41553.76 1394.14 o 7 8 0 17191.39 15722.24 663.19 o 8 8 0 14538.55 15467.25 561.91 o 9 8 0 198.06 -162.50 224.21 o 10 8 0 5123.17 5101.87 415.97 o 11 8 0 5002.17 4038.91 893.88 o 12 8 0 460.96 -196.48 651.72 o 13 8 0 1610.14 748.80 367.54 o 14 8 0 373.09 -438.90 865.65 o 1 9 0 1601.84 1462.14 102.01 o 2 9 0 63.65 -8.64 150.18 o 3 9 0 5968.56 5940.19 253.18 o 4 9 0 44163.25 46656.57 1537.52 o 5 9 0 2.63 -81.43 140.67 o 6 9 0 11927.97 11572.94 297.51 o 7 9 0 331.89 841.79 245.84 o 8 9 0 13926.87 13426.60 606.65 o 9 9 0 69.51 -348.64 348.64 o 10 9 0 15490.01 14807.44 611.39 o 11 9 0 19.32 -137.48 270.31 o 12 9 0 2375.46 2970.24 435.59 o 13 9 0 1270.54 1587.10 438.58 o 14 9 0 1776.84 2298.25 726.99 o 0 10 0 13.55 343.69 146.59 o 1 10 0 7655.38 8109.89 194.96 o 2 10 0 11394.99 11303.99 303.64 o 3 10 0 49.02 401.19 140.40 o 4 10 0 141.82 459.17 267.91 o 5 10 0 4057.80 4731.25 183.80 o 6 10 0 33797.68 35084.30 887.49 o 7 10 0 5106.36 4495.95 284.32 o 8 10 0 7651.14 6941.07 318.07 o 9 10 0 250.30 599.48 282.91 o 10 10 0 1597.10 765.33 340.22 o 11 10 0 2934.42 2411.73 397.59 o 12 10 0 2849.07 2149.84 820.09 o 13 10 0 951.75 1287.93 448.72 o 14 10 0 284.83 1570.72 465.37 o 1 11 0 2137.56 1323.72 108.86 o 2 11 0 17400.55 17848.38 327.41 o 3 11 0 2192.03 2610.33 144.10 o 4 11 0 12788.85 12898.05 281.20 o 5 11 0 17744.29 18085.93 608.53 o 6 11 0 275.69 900.50 192.72 o 7 11 0 1683.61 1763.64 240.34 o 8 11 0 4314.74 4811.24 303.58 o 9 11 0 7650.32 8307.23 510.20 o 10 11 0 11322.88 10601.50 1392.57 o 11 11 0 116.89 56.83 313.31 o 12 11 0 1987.62 2714.62 477.24 o 13 11 0 4339.54 4093.64 532.30 o 14 11 0 558.92 990.15 524.65 o 0 12 0 80135.34 82689.73 1612.39 o 1 12 0 6907.27 7125.75 338.54 o 2 12 0 1178.74 1144.81 129.05 o 3 12 0 6300.74 5655.17 459.47 o 4 12 0 11370.39 11047.17 571.18 o 5 12 0 245.25 -40.76 203.77 o 6 12 0 6241.41 5939.81 303.47 o 7 12 0 7122.72 7859.70 615.26 o 8 12 0 170.83 238.20 262.63 o 9 12 0 419.61 787.43 325.43 o 10 12 0 91.35 -358.28 577.43 o 11 12 0 4324.70 4805.81 560.59 o 12 12 0 923.64 1710.99 479.35 o 13 12 0 834.22 141.93 421.68 o 1 13 0 3756.87 3636.64 179.90 o 2 13 0 42479.61 43394.66 861.76 o 3 13 0 1532.16 1360.66 186.29 o 4 13 0 1139.51 1335.70 191.96 o 5 13 0 2573.93 2648.55 242.53 o 6 13 0 6514.16 6633.46 618.04 o 7 13 0 446.02 396.22 212.85 o 8 13 0 839.03 1071.01 321.38 o 9 13 0 3438.08 3457.82 331.99 o 10 13 0 2872.83 2635.67 614.57 o 11 13 0 593.89 1574.82 405.15 o 12 13 0 6810.20 7272.17 600.02 o 13 13 0 189.85 802.52 1067.70 o 0 14 0 28523.39 30278.28 901.80 o 1 14 0 16240.99 15358.89 319.76 o 2 14 0 3.24 175.23 223.14 o 3 14 0 4166.24 4515.46 564.95 o 4 14 0 11732.13 13447.59 434.28 o 5 14 0 9359.90 9905.72 361.82 o 6 14 0 2.28 5.09 271.94 o 7 14 0 12.29 448.84 229.78 o 8 14 0 1008.44 885.20 259.56 o 9 14 0 833.63 822.12 263.22 o 10 14 0 3806.85 4209.60 459.37 o 11 14 0 135.44 -353.62 772.05 o 12 14 0 140.93 545.53 419.83 o 13 14 0 1569.36 2570.34 520.16 o 1 15 0 15987.31 15924.76 351.11 o 2 15 0 45.83 177.59 165.96 o 3 15 0 8668.66 8332.93 309.96 o 4 15 0 78.74 188.35 258.70 o 5 15 0 1371.05 1477.81 284.79 o 6 15 0 738.50 725.15 231.12 o 7 15 0 147.11 42.23 322.71 o 8 15 0 2384.22 2260.27 290.59 o 9 15 0 15.63 78.40 508.42 o 10 15 0 2261.66 1671.14 334.76 o 11 15 0 2933.97 2643.89 931.52 o 12 15 0 730.21 519.81 443.61 o 0 16 0 1588.36 1851.68 232.59 o 1 16 0 32220.02 32837.26 664.69 o 2 16 0 300.24 -153.62 153.62 o 3 16 0 4788.99 5268.82 573.73 o 4 16 0 1759.56 2187.88 370.48 o 5 16 0 14381.76 14145.24 479.12 o 6 16 0 273.65 -236.97 236.97 o 7 16 0 377.03 1306.27 365.09 o 8 16 0 1339.78 1261.64 441.97 o 9 16 0 3375.44 3072.12 366.46 o 10 16 0 29.13 -316.45 316.45 o 11 16 0 347.70 189.29 433.29 o 12 16 0 479.23 1669.90 797.81 o 1 17 0 7708.61 7864.90 328.28 o 2 17 0 12294.45 12466.10 488.77 o 3 17 0 17561.55 17611.33 484.23 o 4 17 0 371.99 725.35 787.58 o 5 17 0 2627.85 3345.48 352.92 o 6 17 0 1696.56 1932.23 309.92 o 7 17 0 74.50 -33.49 214.20 o 8 17 0 4474.34 4262.79 345.42 o 9 17 0 620.81 979.98 515.09 o 10 17 0 736.53 905.69 389.13 o 11 17 0 2758.72 4201.51 1467.35 o 12 17 0 3024.11 5109.33 583.68 o 0 18 0 12705.88 11979.48 783.45 o 1 18 0 3067.51 3281.95 393.94 o 2 18 0 176.24 -88.50 180.24 o 3 18 0 2169.71 2566.65 365.49 o 4 18 0 11271.24 11434.64 707.38 o 5 18 0 839.95 339.03 448.76 o 6 18 0 1602.37 1770.47 414.74 o 7 18 0 2058.58 2867.44 755.89 o 8 18 0 451.90 524.27 308.78 o 9 18 0 473.54 381.34 807.71 o 10 18 0 1411.59 1475.09 449.62 o 11 18 0 792.98 812.94 415.47 o 1 19 0 1059.35 469.64 266.67 o 2 19 0 10322.55 10504.99 519.97 o 3 19 0 1753.47 1369.27 271.43 o 4 19 0 444.41 571.73 247.45 o 5 19 0 5546.40 6253.97 546.57 o 6 19 0 80.98 312.76 397.98 o 7 19 0 42.68 561.40 346.72 o 8 19 0 195.81 633.08 304.59 o 9 19 0 3965.34 5655.36 1416.34 o 10 19 0 14.18 -375.67 375.67 o 11 19 0 66.73 -462.23 472.94 o 0 20 0 346.80 478.39 393.21 o 1 20 0 164.19 -187.55 774.04 o 2 20 0 1053.97 1401.81 359.82 o 3 20 0 3653.43 4047.71 578.42 o 4 20 0 980.24 959.86 315.13 o 5 20 0 32.84 429.05 272.79 o 6 20 0 5495.09 5725.56 532.56 o 7 20 0 11608.93 12331.84 511.15 o 8 20 0 1410.53 1150.83 408.11 o 9 20 0 91.34 -534.60 654.19 o 10 20 0 784.26 1278.34 480.70 o 1 21 0 1185.34 1342.90 368.42 o 2 21 0 169.31 21.42 347.65 o 3 21 0 27.87 738.25 359.46 o 4 21 0 17443.41 18372.47 2202.76 o 5 21 0 773.52 879.25 286.87 o 6 21 0 3075.02 2617.18 345.26 o 7 21 0 140.33 -491.26 491.26 o 8 21 0 4636.84 4937.41 972.13 o 9 21 0 599.09 271.81 714.11 o 10 21 0 4695.37 4726.42 794.34 o 0 22 0 190.47 41.60 501.17 o 1 22 0 248.92 322.63 584.86 o 2 22 0 1927.83 1906.97 561.09 o 3 22 0 74.48 154.65 459.07 o 4 22 0 1162.71 1014.71 791.86 o 5 22 0 6.03 384.95 1240.54 o 6 22 0 14936.21 14853.94 569.38 o 7 22 0 139.29 407.07 393.02 o 8 22 0 5492.17 5860.49 969.15 o 9 22 0 28.09 278.55 421.35 o 1 23 0 1337.73 1413.04 476.90 o 2 23 0 814.76 920.70 700.25 o 3 23 0 12.45 -79.96 356.61 o 4 23 0 10382.98 11862.76 810.68 o 5 23 0 2340.86 2958.30 757.69 o 6 23 0 2823.27 2691.65 516.58 o 7 23 0 6.83 384.29 588.33 o 8 23 0 3273.76 2974.43 627.94 o 0 24 0 242.00 797.31 570.50 o 1 24 0 9.64 556.78 955.29 o 2 24 0 136.86 -332.06 332.06 o 3 24 0 3341.62 2773.06 641.32 o 4 24 0 243.04 289.11 452.69 o 5 24 0 1389.53 770.41 451.67 o 6 24 0 3040.27 3504.68 572.17 o 7 24 0 4985.27 3718.15 795.33 o 1 25 0 108.53 -279.24 374.35 o 2 25 0 2775.80 2825.77 619.03 o 3 25 0 269.04 -220.97 419.58 o 4 25 0 735.70 59.95 426.58 o 5 25 0 5980.44 6728.88 960.74 o 6 25 0 228.49 593.28 779.48 o 0 26 0 5113.27 5513.83 865.65 o 1 26 0 456.75 176.84 426.79 o 2 26 0 5.46 115.46 692.32 o 3 26 0 109.48 340.71 615.07 o 4 26 0 1651.63 259.22 486.33 o 5 26 0 2107.85 4029.15 898.34 o 1 27 0 3679.02 4346.50 618.18 o 2 27 0 4012.55 4351.90 892.39 o 3 27 0 2667.01 2647.94 631.67 o -13 0 1 3014.12 3147.42 753.24 o -11 0 1 4148.81 3140.71 540.79 o -9 0 1 1054.12 1417.33 360.52 o -7 0 1 1484.26 1619.38 254.55 o -5 0 1 10205.63 9119.06 408.06 o -3 0 1 7123.37 6901.45 281.29 o -1 0 1 9746.01 9266.97 193.99 o 1 0 1 123188.91 125335.97 2270.60 o 3 0 1 1615.39 1807.62 112.94 o 5 0 1 522.32 289.21 197.10 o 7 0 1 11420.27 11198.02 569.51 o 9 0 1 20639.67 22129.23 700.74 o 11 0 1 19292.07 20265.11 951.82 o 13 0 1 4864.99 4485.78 471.30 o 15 0 1 7186.29 6126.86 1208.84 o -14 1 1 75.12 143.34 1022.14 o -13 1 1 200.06 -292.66 292.66 o -12 1 1 458.30 291.47 309.72 o -11 1 1 228.49 24.11 243.83 o -10 1 1 16.50 313.18 737.88 o -9 1 1 5.48 -259.38 415.49 o -8 1 1 230.47 381.59 533.85 o -7 1 1 1978.77 1820.89 196.66 o -6 1 1 1203.67 954.96 237.71 o -5 1 1 18621.15 20083.19 475.79 o -4 1 1 348.30 326.65 156.00 o -3 1 1 10901.52 10262.19 336.37 o -2 1 1 17055.71 16096.32 234.32 o -1 1 1 101548.62 103215.45 1515.43 o 0 1 1 17615.09 20910.93 278.41 o 1 1 1 1090.78 1085.67 76.05 o 2 1 1 22.85 216.78 62.78 o 3 1 1 432.12 383.13 82.97 o 4 1 1 2344.76 2745.33 265.86 o 5 1 1 400.07 119.17 112.20 o 6 1 1 1004.16 891.82 155.65 o 7 1 1 3051.33 3469.84 227.82 o 8 1 1 1578.97 1609.36 213.02 o 9 1 1 511.58 350.24 202.63 o 10 1 1 188.87 509.84 202.03 o 11 1 1 17552.62 16262.05 494.07 o 12 1 1 6162.67 6841.48 362.12 o 13 1 1 10092.30 10957.69 519.80 o 14 1 1 673.74 -255.76 566.55 o 15 1 1 1628.12 873.72 474.62 o -15 2 1 739.62 1664.37 529.88 o -14 2 1 5771.22 4678.67 492.25 o -13 2 1 415.67 -459.57 459.57 o -12 2 1 76.66 80.23 272.87 o -11 2 1 3335.04 2887.64 295.23 o -10 2 1 804.44 325.60 241.55 o -9 2 1 1582.75 1421.76 259.99 o -8 2 1 8880.45 9237.29 368.52 o -7 2 1 9.46 312.71 169.88 o -6 2 1 820.19 971.69 247.61 o -5 2 1 24197.56 26315.98 468.51 o -4 2 1 67446.16 71413.05 1416.72 o -3 2 1 31889.32 35633.12 493.95 o -2 2 1 13504.28 13996.33 513.12 o -1 2 1 825.82 1342.60 72.48 o 0 2 1 39272.03 36423.29 575.98 o 1 2 1 58274.74 54570.56 1371.48 o 2 2 1 1965.90 1801.78 91.83 o 3 2 1 4116.74 4570.28 205.75 o 4 2 1 13090.80 13540.76 441.84 o 5 2 1 69.60 -93.38 93.38 o 6 2 1 7528.38 8519.01 530.20 o 7 2 1 605.54 992.73 156.66 o 8 2 1 432.33 287.46 245.07 o 9 2 1 11597.28 11823.42 378.40 o 10 2 1 23398.90 24529.83 718.94 o 11 2 1 1892.56 1815.01 263.16 o 12 2 1 387.26 253.81 291.35 o 13 2 1 301.96 737.08 273.57 o 14 2 1 5072.49 4892.87 583.99 o 15 2 1 1405.93 3121.72 587.24 o -15 3 1 331.56 1019.69 366.19 o -14 3 1 1774.06 1800.02 436.88 o -13 3 1 4904.84 2724.28 1523.81 o -12 3 1 1919.05 2264.64 364.44 o -11 3 1 116.29 198.98 186.84 o -10 3 1 504.27 174.65 366.21 o -9 3 1 27254.31 29007.61 1143.82 o -8 3 1 107.00 486.27 372.90 o -7 3 1 13356.09 12454.91 435.62 o -6 3 1 15429.43 15519.00 297.89 o -5 3 1 8595.64 8871.60 272.67 o -4 3 1 2254.63 2601.79 104.99 o -3 3 1 4588.72 5387.94 114.19 o -2 3 1 12660.36 13519.83 204.96 o -1 3 1 9951.22 11208.77 293.95 o 0 3 1 32047.54 28436.02 385.45 o 1 3 1 20.61 108.76 43.35 o 2 3 1 50312.03 48777.61 761.77 o 3 3 1 12.59 111.48 79.42 o 4 3 1 514.72 617.62 190.17 o 5 3 1 29243.20 30977.87 562.21 o 6 3 1 4902.15 5330.53 216.78 o 7 3 1 268.65 217.93 129.63 o 8 3 1 6432.24 5981.05 276.02 o 9 3 1 6763.70 6338.14 387.82 o 10 3 1 2568.30 2427.80 267.57 o 11 3 1 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