#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/19/2011948.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2011948_Fobs
loop_
_publ_author_name
'Hirschle, Christian'
'Emmerling, Franziska'
'R\"ohr, Caroline'
_publ_section_title
;
 \b-Rubidium antimonide, Rb~4~Sb~4~
;
_journal_issue                   5
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              501
_journal_page_last               502
_journal_volume                  57
_journal_year                    2001
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 114.280
_cell_angle_gamma                90.000
_cell_length_a                   7.3566
_cell_length_b                   7.1341
_cell_length_c                   13.7930
_exptl_crystal_F_000             704.00
_reflns_d_resolution_high        0.7331
_[local]_cod_data_source_file    br1316Isup2.hkl
_[local]_cod_data_source_block   I
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     beta-RbSb
_shelx_refln_list_code           4
_shelx_f_calc_maximum            404.51
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 163626.28 162452.45 1290.65 o
3 0 0 43658.22 46667.84 924.93 o
4 0 0 749.52 544.11 154.83 o
5 0 0 2237.41 2102.99 202.44 o
6 0 0 11697.30 11434.87 428.92 o
7 0 0 9388.18 8885.90 346.87 o
8 0 0 3284.05 3124.76 348.17 o
9 0 0 11698.94 9355.76 478.96 o
1 1 0 80.48 78.80 239.97 o
2 1 0 553.03 626.48 112.10 o
3 1 0 1078.80 1360.84 126.08 o
4 1 0 76.62 319.25 153.05 o
5 1 0 2773.16 3108.03 203.57 o
6 1 0 245.93 423.56 231.52 o
7 1 0 1581.02 1202.11 298.29 o
8 1 0 420.69 155.00 327.70 o
9 1 0 345.54 283.67 382.78 o
0 2 0 2999.43 2476.19 158.57 o
1 2 0 527.06 616.24 87.57 o
2 2 0 1261.18 1250.85 108.69 o
3 2 0 1534.20 1393.01 138.91 o
4 2 0 103.30 84.65 459.95 o
5 2 0 444.90 665.80 195.12 o
6 2 0 38.94 -17.38 238.02 o
7 2 0 7.28 170.75 280.26 o
8 2 0 148.19 -1577.00 1051.33 o
1 3 0 892.06 988.30 80.58 o
2 3 0 22312.90 23830.75 661.41 o
3 3 0 3204.12 3171.06 154.83 o
4 3 0 20036.33 21079.50 648.58 o
5 3 0 9397.95 9698.24 293.09 o
6 3 0 2431.54 2358.72 271.97 o
7 3 0 3152.36 2956.44 301.87 o
8 3 0 160.60 -518.93 994.96 o
0 4 0 58915.05 50987.39 1297.80 o
1 4 0 2551.61 2608.92 100.08 o
2 4 0 24473.35 25512.30 746.87 o
3 4 0 6629.93 7072.10 204.39 o
4 4 0 141.34 339.72 184.89 o
5 4 0 298.32 -251.99 712.10 o
6 4 0 2659.85 2920.21 270.51 o
7 4 0 2256.60 1841.91 318.76 o
8 4 0 1043.26 862.87 361.98 o
1 5 0 558.10 414.62 109.83 o
2 5 0 6462.24 6962.27 177.74 o
3 5 0 1076.07 1184.07 176.93 o
4 5 0 6177.95 7038.47 254.59 o
5 5 0 4507.16 5112.73 276.20 o
6 5 0 624.95 340.53 282.53 o
7 5 0 2443.12 2377.73 339.07 o
0 6 0 304.08 -273.76 821.28 o
1 6 0 168.07 229.57 130.79 o
2 6 0 202.11 379.53 150.77 o
3 6 0 729.63 765.72 191.39 o
4 6 0 118.44 -154.18 616.57 o
5 6 0 494.18 328.35 255.40 o
6 6 0 164.19 -621.12 1010.88 o
7 6 0 130.24 -667.26 1051.98 o
1 7 0 909.19 1000.32 178.88 o
2 7 0 11937.76 12315.45 363.12 o
3 7 0 2423.71 2664.81 223.88 o
4 7 0 11485.30 11917.24 332.25 o
5 7 0 9348.75 10573.79 359.22 o
6 7 0 1011.42 619.01 339.40 o
0 8 0 1433.55 1532.40 360.52 o
1 8 0 142.87 -221.61 633.63 o
2 8 0 551.63 534.36 185.38 o
3 8 0 459.24 -382.13 692.93 o
4 8 0 2.02 -1226.48 844.19 o
5 8 0 89.08 54.91 302.19 o
1 9 0 54.72 0.00 768.96 o
2 9 0 544.68 0.00 615.76 o
3 9 0 1.31 -809.09 744.11 o
-9 1 1 26.40 180.99 1155.96 o
-8 1 1 1498.36 854.10 346.38 o
-7 1 1 3834.88 4341.00 307.72 o
-6 1 1 956.93 752.88 241.27 o
-5 1 1 12081.88 12673.21 385.05 o
-4 1 1 24994.85 24098.98 604.22 o
-3 1 1 2778.05 3064.65 153.53 o
-2 1 1 40532.29 39862.19 834.76 o
-1 1 1 6443.29 5231.66 183.59 o
1 1 1 7730.31 8913.36 222.09 o
2 1 1 33110.05 34952.05 672.62 o
3 1 1 1581.98 1863.35 125.75 o
4 1 1 33754.68 38279.42 1000.48 o
5 1 1 12855.55 13072.88 427.78 o
6 1 1 5871.96 5902.49 270.35 o
7 1 1 6649.23 5875.52 315.68 o
8 1 1 20.88 -1517.78 1011.86 o
-9 2 1 924.23 -1984.72 1323.15 o
-8 2 1 5224.41 5282.02 369.45 o
-7 2 1 325.20 -170.59 834.11 o
-6 2 1 2373.61 2515.83 256.54 o
-5 2 1 619.09 963.11 204.39 o
-4 2 1 2755.95 2632.64 184.56 o
-3 2 1 13281.64 13870.93 390.74 o
-2 2 1 23343.02 25576.47 740.21 o
-1 2 1 65565.48 68503.80 1173.02 o
0 2 1 16156.09 15667.02 336.55 o
1 2 1 66088.53 69404.68 760.03 o
2 2 1 299.90 77.17 312.43 o
3 2 1 10688.80 11300.51 327.05 o
4 2 1 667.90 714.54 167.02 o
5 2 1 668.11 -530.30 642.56 o
6 2 1 23.57 -271.16 679.77 o
7 2 1 3235.57 2821.76 309.34 o
8 2 1 842.17 1015.27 328.67 o
-8 3 1 3734.30 3347.51 378.55 o
-7 3 1 2811.65 2563.27 316.98 o
-6 3 1 2824.68 3278.62 265.96 o
-5 3 1 15123.78 15868.16 496.99 o
-4 3 1 657.48 1035.58 182.78 o
-3 3 1 10207.10 11046.57 329.32 o
-2 3 1 7807.52 8173.96 269.70 o
-1 3 1 1314.03 1148.65 108.20 o
0 3 1 88.84 41.42 121.02 o
1 3 1 15510.05 16877.25 468.56 o
2 3 1 19362.73 21298.67 631.03 o
3 3 1 3298.56 3364.24 151.75 o
4 3 1 28902.55 29294.08 695.20 o
5 3 1 1653.92 1882.85 219.98 o
6 3 1 8139.11 7669.50 301.54 o
7 3 1 3771.79 3527.20 325.91 o
8 3 1 101.32 158.57 1101.21 o
-8 4 1 701.76 328.67 369.29 o
-7 4 1 1805.19 2162.78 315.19 o
-6 4 1 6627.56 6421.41 311.61 o
-5 4 1 1110.74 636.71 241.43 o
-4 4 1 4204.64 4464.64 223.23 o
-3 4 1 21403.31 23382.98 650.85 o
-2 4 1 5863.99 6355.78 193.99 o
-1 4 1 25064.71 25340.24 628.43 o
0 4 1 46040.94 43496.95 710.88 o
1 4 1 1192.95 1305.92 94.23 o
2 4 1 30083.55 32082.86 790.90 o
3 4 1 3495.81 3823.70 169.94 o
4 4 1 601.25 747.36 179.69 o
5 4 1 875.95 832.98 218.36 o
6 4 1 3699.37 3811.68 287.08 o
7 4 1 1448.79 943.94 317.30 o
8 4 1 2392.93 2130.61 376.28 o
-8 5 1 548.86 1016.08 367.50 o
-7 5 1 424.01 -838.50 991.71 o
-6 5 1 8413.71 9114.98 355.48 o
-5 5 1 14.97 -369.21 246.14 o
-4 5 1 18379.27 19955.22 603.73 o
-3 5 1 2154.36 2408.44 196.26 o
-2 5 1 9327.04 10414.73 291.96 o
-1 5 1 1454.05 1605.19 150.12 o
0 5 1 113.07 -136.98 139.82 o
1 5 1 1383.96 1555.48 113.89 o
2 5 1 961.47 1223.39 139.40 o
3 5 1 8628.04 8782.90 304.30 o
4 5 1 75.36 -108.04 604.71 o
5 5 1 5819.19 6553.34 273.11 o
6 5 1 245.76 -447.76 872.46 o
7 5 1 640.64 730.30 330.14 o
-7 6 1 336.11 452.64 357.11 o
-6 6 1 695.04 576.93 314.70 o
-5 6 1 2.96 -150.77 265.80 o
-4 6 1 147.48 -1190.98 793.98 o
-3 6 1 495.38 27.46 608.28 o
-2 6 1 1216.55 1010.88 166.69 o
-1 6 1 89.66 315.03 200.16 o
0 6 1 4558.21 4324.52 433.30 o
1 6 1 746.01 487.24 129.97 o
2 6 1 2072.90 2119.24 168.32 o
3 6 1 1245.74 1654.26 189.76 o
4 6 1 9.19 -601.13 630.38 o
5 6 1 25.50 -184.08 803.73 o
6 6 1 192.81 -1398.04 936.96 o
-6 7 1 586.62 873.76 333.06 o
-5 7 1 274.83 608.28 291.14 o
-4 7 1 1032.74 620.63 265.96 o
-3 7 1 485.24 213.65 640.94 o
-2 7 1 448.64 22.58 482.86 o
-1 7 1 98.56 129.97 251.01 o
0 7 1 5.02 -259.60 326.94 o
1 7 1 302.66 373.03 159.06 o
2 7 1 68.71 45.82 524.77 o
3 7 1 1244.76 1131.43 211.86 o
4 7 1 0.25 -238.99 716.81 o
5 7 1 789.50 779.04 282.05 o
6 7 1 96.15 -838.18 954.34 o
-5 8 1 339.97 515.68 315.84 o
-4 8 1 590.77 -281.23 833.30 o
-3 8 1 3930.53 4427.11 264.82 o
-2 8 1 2629.55 2395.11 201.46 o
-1 8 1 2671.09 2263.68 323.96 o
0 8 1 11270.92 10183.13 775.14 o
1 8 1 38.05 70.51 195.12 o
2 8 1 6442.10 6151.07 238.99 o
3 8 1 1557.76 2056.37 228.43 o
4 8 1 88.85 -485.13 821.77 o
-3 9 1 784.05 917.79 248.41 o
-2 9 1 178.12 415.76 219.33 o
-1 9 1 42.48 -778.06 1172.05 o
0 9 1 19.45 -1188.95 792.64 o
1 9 1 858.25 764.09 242.40 o
2 9 1 58.83 -215.27 638.34 o
3 9 1 1810.08 2308.68 264.82 o
-9 0 2 1438.12 881.23 394.96 o
-8 0 2 4830.70 4223.54 356.29 o
-7 0 2 3158.69 3102.18 314.21 o
-6 0 2 28808.95 29037.71 903.81 o
-5 0 2 20.28 -297.32 220.31 o
-4 0 2 44388.93 47064.26 1236.06 o
-3 0 2 9500.21 9898.24 304.63 o
-2 0 2 7600.06 6815.24 220.47 o
1 0 2 1643.71 1832.65 81.23 o
2 0 2 20343.03 22200.37 559.05 o
3 0 2 17804.64 19656.11 463.36 o
4 0 2 514.02 542.97 152.88 o
5 0 2 7375.29 7602.88 238.99 o
6 0 2 3210.03 2820.29 258.98 o
7 0 2 28.40 210.40 280.58 o
8 0 2 2431.42 2221.92 360.19 o
-9 1 2 1929.16 303.33 1290.65 o
-8 1 2 1526.56 1258.16 340.86 o
-7 1 2 3232.80 2755.63 322.99 o
-6 1 2 21175.30 21445.22 653.61 o
-5 1 2 80.02 10.72 218.85 o
-4 1 2 37323.80 36710.29 782.29 o
-3 1 2 10461.43 10372.81 317.30 o
-2 1 2 6273.90 5988.11 214.46 o
-1 1 2 2513.69 2387.96 81.88 o
0 1 2 9525.57 9293.68 183.60 o
1 1 2 26620.71 29110.82 488.87 o
2 1 2 8255.32 9168.92 238.34 o
3 1 2 64488.84 70400.77 1118.27 o
4 1 2 402.32 254.43 159.54 o
5 1 2 28903.55 28196.93 763.93 o
6 1 2 4753.56 4588.60 271.16 o
7 1 2 2194.73 1999.66 290.33 o
8 1 2 1495.10 1537.77 345.41 o
-9 2 2 150.16 347.03 389.76 o
-8 2 2 1662.74 1741.01 360.68 o
-7 2 2 343.22 249.23 293.09 o
-6 2 2 202.22 -800.97 805.84 o
-5 2 2 1473.40 1450.03 232.49 o
-4 2 2 6035.08 6094.53 223.56 o
-3 2 2 365.46 547.36 182.45 o
-2 2 2 25938.10 22702.57 665.96 o
-1 2 2 17933.70 17655.64 404.22 o
0 2 2 15289.90 14742.34 274.09 o
1 2 2 23963.95 24626.68 501.87 o
2 2 2 367.00 363.93 97.32 o
3 2 2 3173.89 3247.26 143.78 o
4 2 2 332.05 312.59 161.66 o
5 2 2 917.21 723.47 195.94 o
6 2 2 77.01 -198.05 237.04 o
7 2 2 2035.10 2282.69 296.83 o
8 2 2 832.87 -1624.52 1083.02 o
-9 3 2 15.46 128.51 1161.65 o
-8 3 2 90.19 219.17 340.37 o
-7 3 2 372.70 71.32 303.98 o
-6 3 2 4782.52 4169.43 302.68 o
-5 3 2 16.72 -631.19 659.62 o
-4 3 2 25524.93 25003.12 775.95 o
-3 3 2 4679.73 4936.29 223.39 o
-2 3 2 24706.29 26089.55 765.88 o
-1 3 2 11771.25 10578.66 261.25 o
0 3 2 983.53 984.25 62.75 o
1 3 2 766.09 733.38 85.13 o
2 3 2 5304.67 5760.49 176.12 o
3 3 2 7829.65 8540.33 253.61 o
4 3 2 3590.60 3744.09 192.53 o
5 3 2 13747.35 13820.72 440.78 o
6 3 2 15.36 256.38 237.20 o
7 3 2 4211.68 3374.96 320.71 o
8 3 2 422.76 556.46 339.40 o
-8 4 2 2111.02 1701.86 387.00 o
-7 4 2 607.80 -1352.06 1019.82 o
-6 4 2 7261.78 7625.63 329.65 o
-5 4 2 155.86 -231.68 249.88 o
-4 4 2 4856.57 5375.44 254.43 o
-3 4 2 1925.20 1800.64 215.60 o
-2 4 2 182.00 -157.11 752.72 o
-1 4 2 116.53 406.82 103.17 o
0 4 2 6774.24 6683.91 131.42 o
1 4 2 3648.26 3719.23 145.25 o
2 4 2 4006.06 4348.47 147.20 o
3 4 2 6108.09 6319.06 186.35 o
4 4 2 32.51 168.16 563.60 o
5 4 2 1183.58 1373.84 223.72 o
6 4 2 410.00 587.81 262.06 o
7 4 2 127.99 -120.71 297.97 o
-8 5 2 1277.54 1865.14 379.36 o
-7 5 2 317.57 -711.13 1084.64 o
-6 5 2 3055.46 2829.55 324.29 o
-5 5 2 152.54 -1267.50 845.00 o
-4 5 2 943.55 1230.21 241.59 o
-3 5 2 667.71 1211.69 221.12 o
-2 5 2 1041.67 -524.77 694.88 o
-1 5 2 426.44 388.14 172.05 o
0 5 2 3769.39 3494.32 133.47 o
1 5 2 7700.88 7839.11 248.09 o
2 5 2 331.87 348.66 135.17 o
3 5 2 9343.64 9639.27 314.38 o
4 5 2 1325.22 1286.91 207.96 o
5 5 2 2271.53 2384.72 251.99 o
6 5 2 1956.52 1928.99 280.58 o
7 5 2 3.80 -612.34 971.56 o
-7 6 2 410.74 -1535.65 1188.13 o
-6 6 2 759.28 1006.01 320.88 o
-5 6 2 1821.43 1759.05 301.70 o
-4 6 2 5594.00 6200.78 299.75 o
-3 6 2 303.63 203.57 236.07 o
-2 6 2 25568.91 28091.65 738.26 o
-1 6 2 16698.39 17446.05 448.09 o
0 6 2 16096.46 15543.30 313.24 o
1 6 2 26575.58 26186.06 564.09 o
2 6 2 614.74 -287.24 503.49 o
3 6 2 5388.97 5908.34 222.26 o
4 6 2 642.16 533.22 219.01 o
5 6 2 1008.56 179.69 785.70 o
6 6 2 23.41 -258.49 293.09 o
-6 7 2 98.23 -1511.45 1060.92 o
-5 7 2 183.48 85.78 314.21 o
-4 7 2 1714.20 1349.46 287.24 o
-3 7 2 25.42 0.00 675.06 o
-2 7 2 6439.68 6768.45 202.76 o
-1 7 2 2741.13 2615.58 358.41 o
0 7 2 2879.92 3178.49 213.89 o
1 7 2 5298.81 5332.39 190.09 o
2 7 2 183.38 -401.62 526.89 o
3 7 2 1161.13 1061.90 213.00 o
4 7 2 2247.86 2710.30 250.53 o
5 7 2 309.22 -38.83 864.17 o
-5 8 2 229.95 379.53 339.88 o
-4 8 2 1201.84 1389.76 306.74 o
-3 8 2 27.30 -505.12 777.41 o
-2 8 2 2400.86 2522.81 209.75 o
-1 8 2 1498.33 -2080.49 1387.00 o
0 8 2 605.88 -78.61 593.03 o
1 8 2 1876.92 1954.34 199.84 o
2 8 2 64.66 -55.24 609.75 o
3 8 2 176.75 -106.42 223.72 o
4 8 2 103.98 -251.18 269.05 o
-3 9 2 317.52 -738.75 758.73 o
-2 9 2 732.88 779.20 265.15 o
-1 9 2 492.59 400.32 1420.95 o
0 9 2 13.62 208.04 306.01 o
1 9 2 9.99 130.46 218.36 o
2 9 2 289.68 -168.48 225.51 o
-9 1 3 221.34 -872.13 1185.05 o
-8 1 3 163.11 -50.53 1015.75 o
-7 1 3 463.74 -213.48 859.30 o
-6 1 3 1740.73 1529.16 280.10 o
-5 1 3 2828.54 3304.94 240.94 o
-4 1 3 13802.28 14733.15 469.53 o
-3 1 3 11384.64 11061.84 380.34 o
-2 1 3 25951.83 25683.54 688.38 o
-1 1 3 14157.62 12010.99 312.91 o
0 1 3 16008.94 15621.30 247.58 o
1 1 3 1854.34 2050.36 84.65 o
2 1 3 4129.69 4452.62 141.19 o
3 1 3 1412.82 1489.84 125.26 o
4 1 3 1302.23 1160.84 163.93 o
5 1 3 3726.25 3986.33 229.89 o
6 1 3 788.01 -303.82 753.85 o
7 1 3 1625.00 0.00 901.38 o
8 1 3 301.12 -866.61 1028.10 o
-9 2 3 602.04 488.22 398.21 o
-8 2 3 12343.57 13109.92 438.34 o
-7 2 3 3954.54 4034.75 319.41 o
-6 2 3 12192.16 13204.81 402.76 o
-5 2 3 30984.57 30140.05 906.09 o
-4 2 3 2752.72 3014.93 233.79 o
-3 2 3 20930.71 21804.11 574.33 o
-2 2 3 69891.84 61051.35 938.09 o
-1 2 3 9010.73 7592.49 220.96 o
0 2 3 61360.04 58416.98 492.19 o
1 2 3 67644.95 68559.03 808.44 o
2 2 3 751.17 977.90 102.36 o
3 2 3 24222.96 25001.01 548.33 o
4 2 3 8910.00 8873.23 276.03 o
5 2 3 717.68 559.22 207.96 o
6 2 3 2769.16 2559.21 260.27 o
7 2 3 10009.39 8511.08 357.27 o
8 2 3 547.33 761.82 328.19 o
-9 3 3 1890.73 1569.12 420.63 o
-8 3 3 42.94 10.07 359.87 o
-7 3 3 4587.97 4346.20 360.52 o
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-5 3 3 2248.10 2505.10 269.86 o
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2 3 3 29321.65 31588.79 762.95 o
3 3 3 5637.36 6082.02 180.18 o
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6 3 3 34.07 252.96 241.92 o
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-8 4 3 566.13 171.57 382.45 o
-7 4 3 433.76 -49.07 1027.13 o
-6 4 3 2383.34 2492.43 312.26 o
-5 4 3 3303.96 3302.01 312.91 o
-4 4 3 6704.20 7480.71 322.34 o
-3 4 3 6836.06 7942.77 334.20 o
-2 4 3 8157.38 8590.70 249.23 o
-1 4 3 6307.33 6251.96 186.19 o
0 4 3 1895.26 1876.63 1077.90 o
1 4 3 4490.92 4715.82 149.96 o
2 4 3 346.80 387.65 125.43 o
3 4 3 4116.68 4296.48 179.37 o
4 4 3 1426.92 1426.64 198.21 o
5 4 3 3027.99 2854.58 246.47 o
6 4 3 385.66 167.02 263.04 o
7 4 3 906.80 1079.44 301.70 o
-8 5 3 569.71 -1929.40 1286.26 o
-7 5 3 2585.71 2533.37 384.08 o
-6 5 3 3863.87 3554.98 352.07 o
-5 5 3 8.05 -152.40 299.59 o
-4 5 3 16131.29 18210.63 512.26 o
-3 5 3 12445.63 14004.64 459.95 o
-2 5 3 4468.80 4454.40 171.89 o
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2 5 3 11522.43 12066.88 322.18 o
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5 5 3 15184.58 14080.84 462.71 o
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