#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:34:15 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180790 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/21/2012182.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012182_Fobs loop_ _publ_author_name 'Jeanneau, Erwann' 'Audebrand, Nathalie' 'Lou\"er, Daniel' _publ_section_title ; \b-CdC~2~O~4~ ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1012 _journal_page_last 1013 _journal_volume 57 _journal_year 2001 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 113.865 _cell_angle_gamma 90.000 _cell_length_a 5.8260 _cell_length_b 5.2520 _cell_length_c 5.8320 _exptl_crystal_F_000 184.00 _reflns_d_resolution_high 0.6204 _cod_data_source_file br1339Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' test structure: cd' _shelx_refln_list_code 4 _shelx_f_calc_maximum 99.56 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4108.92 4708.30 157.10 o 4 0 0 1036.84 960.86 25.23 o 6 0 0 662.34 679.55 41.61 o 8 0 0 188.69 189.17 28.09 o 1 1 0 9911.24 11253.46 246.24 o 2 1 0 1905.14 1951.95 41.41 o 3 1 0 2691.90 2614.57 52.98 o 4 1 0 0.63 1.99 0.71 o 5 1 0 1135.62 1160.05 27.21 o 6 1 0 0.69 3.30 1.67 o 7 1 0 355.11 368.76 17.91 o 8 1 0 3.21 5.15 4.83 o 0 2 0 873.23 1121.42 36.94 o 1 2 0 484.04 491.75 9.41 o 2 2 0 4747.16 4543.39 97.11 o 3 2 0 84.46 91.21 3.55 o 4 2 0 2609.10 2733.99 52.35 o 5 2 0 1.15 1.04 0.79 o 6 2 0 617.05 656.12 23.27 o 7 2 0 1.32 8.78 4.07 o 8 2 0 250.28 218.87 17.11 o 1 3 0 1940.35 1819.18 31.45 o 2 3 0 93.53 91.24 2.77 o 3 3 0 2982.52 2990.05 151.08 o 4 3 0 39.14 40.37 3.69 o 5 3 0 902.71 940.62 35.10 o 6 3 0 16.89 19.45 6.24 o 7 3 0 421.88 458.82 39.61 o 8 3 0 0.08 4.09 9.12 o 0 4 0 2727.26 2770.63 100.13 o 1 4 0 114.53 118.22 3.13 o 2 4 0 1655.49 1608.76 29.13 o 3 4 0 2.12 1.82 1.10 o 4 4 0 817.22 835.40 42.31 o 5 4 0 34.38 35.72 8.63 o 6 4 0 561.31 595.12 36.58 o 7 4 0 0.04 -2.28 4.61 o 1 5 0 1537.03 1549.14 34.65 o 2 5 0 10.22 7.39 0.96 o 3 5 0 563.56 549.00 53.48 o 4 5 0 5.61 4.20 2.28 o 5 5 0 670.41 650.56 34.88 o 6 5 0 0.44 6.80 5.17 o 0 6 0 779.71 773.74 25.72 o 1 6 0 20.82 18.35 2.42 o 2 6 0 609.97 606.98 22.90 o 3 6 0 0.19 0.39 2.33 o 4 6 0 609.65 644.62 57.21 o 5 6 0 4.90 4.18 3.85 o 6 6 0 317.98 311.69 103.94 o 1 7 0 471.76 491.39 22.01 o 2 7 0 2.45 1.53 3.71 o 3 7 0 553.63 575.62 35.66 o 4 7 0 10.57 11.17 8.03 o 0 8 0 412.81 381.80 32.43 o 1 8 0 4.14 6.20 3.73 o 2 8 0 428.14 418.10 36.10 o -7 0 1 1194.44 1316.07 95.93 o -5 0 1 1463.91 1499.20 43.53 o -3 0 1 3218.58 3175.49 114.30 o -1 0 1 2913.09 2734.68 61.27 o 1 0 1 3682.47 3365.45 90.60 o 3 0 1 6059.95 6471.61 178.91 o 5 0 1 1188.51 1265.63 47.00 o 7 0 1 272.22 269.74 27.25 o -8 1 1 429.71 458.30 31.27 o -7 1 1 1.84 0.65 3.73 o -6 1 1 1129.90 1215.57 35.69 o -5 1 1 88.92 85.65 3.33 o -4 1 1 2330.84 2374.00 45.44 o -3 1 1 14.15 7.84 1.05 o -2 1 1 5012.70 5025.58 81.61 o -1 1 1 34.50 71.67 1.63 o 0 1 1 3956.23 3863.04 81.70 o 1 1 1 679.97 1132.63 22.83 o 2 1 1 4055.83 4050.64 80.08 o 3 1 1 26.66 21.91 2.40 o 4 1 1 2114.14 2209.23 53.10 o 5 1 1 118.42 120.99 5.95 o 6 1 1 645.12 734.55 38.43 o 7 1 1 0.26 -3.36 3.81 o 8 1 1 233.69 224.49 20.68 o -8 2 1 21.38 14.10 4.56 o -7 2 1 286.84 295.32 18.27 o -6 2 1 13.63 10.43 1.35 o -5 2 1 1575.79 1604.59 38.09 o -4 2 1 4.13 4.96 0.53 o -3 2 1 3517.02 3458.54 70.04 o -2 2 1 71.07 73.72 1.86 o -1 2 1 6415.61 6506.97 157.07 o 0 2 1 0.20 0.86 0.33 o 1 2 1 4597.70 4556.73 104.11 o 2 2 1 280.29 276.51 5.82 o 3 2 1 961.27 913.96 21.56 o 4 2 1 5.69 4.92 1.05 o 5 2 1 1008.98 1058.54 45.42 o 6 2 1 6.91 4.53 4.57 o 7 2 1 508.14 525.66 35.63 o -8 3 1 136.00 127.08 14.41 o -7 3 1 13.83 14.67 3.91 o -6 3 1 531.25 527.44 24.82 o -5 3 1 14.37 12.85 2.98 o -4 3 1 1822.83 1684.10 109.69 o -3 3 1 6.27 0.68 1.89 o -2 3 1 2634.67 2592.92 86.52 o -1 3 1 24.39 15.67 2.93 o 0 3 1 5490.46 5564.65 95.79 o 1 3 1 75.86 85.70 5.22 o 2 3 1 2097.61 2000.15 40.97 o 3 3 1 9.77 9.51 1.48 o 4 3 1 715.13 713.15 38.60 o 5 3 1 34.95 24.70 5.08 o 6 3 1 556.83 593.50 42.55 o 7 3 1 15.32 14.85 11.02 o -7 4 1 309.34 304.43 18.99 o -6 4 1 41.09 31.59 5.27 o -5 4 1 636.77 622.62 31.28 o -4 4 1 1.42 0.29 1.85 o -3 4 1 1312.30 1219.87 81.35 o -2 4 1 3.44 4.85 0.83 o -1 4 1 2241.70 2212.18 41.95 o 0 4 1 1.43 2.38 0.90 o 1 4 1 2692.28 2678.79 61.30 o 2 4 1 88.17 90.25 3.09 o 3 4 1 1561.88 1527.85 62.69 o 4 4 1 14.36 4.14 2.81 o 5 4 1 405.14 426.11 36.90 o 6 4 1 1.18 10.53 5.70 o 7 4 1 103.43 80.07 8.70 o -7 5 1 2.92 0.42 9.31 o -6 5 1 301.67 293.04 21.50 o -5 5 1 2.75 4.83 4.46 o -4 5 1 587.08 556.79 32.15 o -3 5 1 1.07 1.58 0.80 o -2 5 1 1637.02 1640.70 44.33 o -1 5 1 39.09 36.99 1.94 o 0 5 1 1292.88 1296.35 29.82 o 1 5 1 0.18 3.15 1.04 o 2 5 1 1357.49 1341.93 31.09 o 3 5 1 33.43 25.69 2.82 o 4 5 1 694.20 696.45 59.01 o 5 5 1 28.01 24.56 7.59 o 6 5 1 104.52 54.34 18.78 o -6 6 1 0.07 -5.67 5.67 o -5 6 1 293.13 268.73 23.87 o -4 6 1 37.57 26.09 6.64 o -3 6 1 862.31 872.74 47.78 o -2 6 1 10.55 9.63 2.17 o -1 6 1 1099.11 1139.15 38.26 o 0 6 1 0.80 2.46 1.68 o 1 6 1 625.46 592.02 20.43 o 2 6 1 1.42 -1.63 1.63 o 3 6 1 505.82 500.66 28.54 o 4 6 1 69.79 68.20 10.65 o 5 6 1 250.35 235.97 40.16 o -5 7 1 20.93 13.80 7.06 o -4 7 1 390.97 383.23 41.57 o -3 7 1 51.60 59.15 7.76 o -2 7 1 446.79 440.95 30.76 o -1 7 1 10.36 13.22 3.11 o 0 7 1 535.37 566.33 26.02 o 1 7 1 13.94 17.82 3.75 o 2 7 1 333.63 345.81 24.24 o 3 7 1 10.66 8.21 6.89 o 4 7 1 235.82 236.19 28.86 o -3 8 1 170.49 128.50 18.29 o -2 8 1 2.38 -2.00 4.51 o -1 8 1 185.85 150.62 15.73 o 0 8 1 4.16 2.71 6.71 o 1 8 1 340.00 380.64 21.33 o 2 8 1 10.10 8.49 7.44 o -8 0 2 148.16 128.58 11.12 o -6 0 2 850.02 837.04 39.03 o -4 0 2 5670.24 5755.01 134.52 o -2 0 2 3483.41 3918.71 77.27 o 0 0 2 6057.30 5109.33 124.77 o 2 0 2 3614.99 3826.81 115.13 o 4 0 2 916.17 949.07 39.94 o 6 0 2 552.90 582.17 46.00 o -9 1 2 201.34 175.65 15.44 o -8 1 2 2.49 -3.39 6.47 o -7 1 2 411.05 400.83 19.15 o -6 1 2 176.40 170.78 5.88 o -5 1 2 1696.38 1688.15 34.07 o -4 1 2 1.93 0.05 1.92 o -3 1 2 4350.74 4358.81 77.98 o -2 1 2 569.24 574.93 11.84 o -1 1 2 5875.16 5712.54 94.55 o 0 1 2 150.30 147.79 3.32 o 1 1 2 5302.17 5516.82 108.36 o 2 1 2 14.63 12.63 0.91 o 3 1 2 1696.10 1714.44 44.54 o 4 1 2 0.41 -1.30 1.30 o 5 1 2 600.56 624.17 23.34 o 6 1 2 0.68 -2.38 2.38 o 7 1 2 260.25 251.49 24.08 o -8 2 2 500.70 514.28 31.85 o -7 2 2 4.35 8.20 2.69 o -6 2 2 819.29 845.10 30.64 o -5 2 2 110.56 109.44 4.83 o -4 2 2 884.11 874.68 17.23 o -3 2 2 7.43 9.59 2.27 o -2 2 2 5679.35 5518.60 89.82 o -1 2 2 13.79 13.33 0.83 o 0 2 2 5817.51 6337.53 103.28 o 1 2 2 19.63 18.13 2.21 o 2 2 2 2303.92 2272.08 41.69 o 3 2 2 91.27 93.52 3.26 o 4 2 2 1065.50 1139.15 33.54 o 5 2 2 0.75 0.33 1.63 o 6 2 2 272.29 297.97 26.00 o 7 2 2 0.01 -4.98 4.98 o -8 3 2 0.08 0.57 6.54 o -7 3 2 798.74 901.72 81.70 o -6 3 2 11.52 7.57 3.21 o -5 3 2 865.13 850.61 73.73 o -4 3 2 97.34 87.93 6.38 o -3 3 2 1751.40 1775.55 32.72 o -2 3 2 297.77 292.09 6.68 o -1 3 2 3776.25 3783.67 80.55 o 0 3 2 59.73 58.02 1.62 o 1 3 2 1681.11 1711.40 35.30 o 2 3 2 115.14 120.71 4.11 o 3 3 2 1547.73 1527.18 37.54 o 4 3 2 34.61 26.07 2.03 o 5 3 2 694.75 829.61 64.24 o 6 3 2 0.03 1.67 4.37 o 7 3 2 188.85 180.04 20.66 o -8 4 2 233.88 203.58 37.79 o -7 4 2 0.02 -2.74 6.80 o -6 4 2 868.32 886.03 51.42 o -5 4 2 7.91 8.03 5.37 o -4 4 2 1639.79 1741.68 109.35 o -3 4 2 141.96 142.62 5.84 o -2 4 2 1278.01 1280.12 30.15 o -1 4 2 4.45 3.92 1.07 o 0 4 2 952.56 929.93 24.10 o 1 4 2 35.09 30.87 4.19 o 2 4 2 1221.42 1257.26 30.87 o 3 4 2 0.05 1.97 2.00 o 4 4 2 1002.24 1042.76 34.57 o 5 4 2 21.63 21.61 6.61 o 6 4 2 447.58 449.84 43.01 o -7 5 2 240.99 209.55 17.33 o -6 5 2 8.05 -2.09 5.78 o -5 5 2 988.81 1014.80 87.30 o -4 5 2 5.97 -3.28 3.28 o -3 5 2 1060.15 1130.68 40.94 o -2 5 2 27.13 26.28 4.04 o -1 5 2 579.64 579.62 22.15 o 0 5 2 1.46 1.91 1.44 o 1 5 2 1152.60 1164.07 29.62 o 2 5 2 32.65 31.13 2.83 o 3 5 2 737.10 782.11 29.30 o 4 5 2 0.04 2.16 3.91 o 5 5 2 437.68 420.28 43.64 o -6 6 2 245.43 213.51 20.80 o -5 6 2 4.00 4.11 4.21 o -4 6 2 523.66 507.77 25.89 o -3 6 2 67.27 60.76 6.85 o -2 6 2 656.21 681.66 27.34 o -1 6 2 0.00 -1.45 1.45 o 0 6 2 995.71 1116.55 49.17 o 1 6 2 23.84 26.94 2.74 o 2 6 2 711.72 736.23 46.74 o 3 6 2 0.03 3.18 3.66 o 4 6 2 252.68 254.19 24.29 o -5 7 2 160.85 118.65 17.41 o -4 7 2 0.73 -1.00 5.76 o -3 7 2 418.86 434.78 59.26 o -2 7 2 0.01 3.59 6.14 o -1 7 2 800.99 918.79 58.00 o 0 7 2 13.59 14.59 4.64 o 1 7 2 501.76 510.29 32.86 o 2 7 2 8.02 -4.27 8.41 o 3 7 2 265.34 232.52 24.48 o -2 8 2 470.16 478.22 57.69 o -1 8 2 0.70 4.93 7.22 o 0 8 2 327.60 315.74 29.79 o 1 8 2 5.50 4.25 4.67 o -9 0 3 236.96 216.94 34.51 o -7 0 3 952.36 1019.53 37.53 o -5 0 3 1447.76 1374.21 45.74 o -3 0 3 2953.58 2718.54 59.29 o -1 0 3 7654.02 8095.08 212.01 o 1 0 3 1588.52 1485.20 35.06 o 3 0 3 1086.73 1069.55 32.27 o 5 0 3 1025.50 1117.10 134.44 o -9 1 3 0.20 0.60 5.09 o -8 1 3 503.33 519.07 21.52 o -7 1 3 0.66 -1.31 3.52 o -6 1 3 1353.13 1379.61 49.63 o -5 1 3 17.96 17.32 1.51 o -4 1 3 2001.59 1936.71 38.12 o -3 1 3 202.14 226.63 4.80 o -2 1 3 3602.91 3329.21 62.92 o -1 1 3 42.08 57.93 1.79 o 0 1 3 3404.99 3305.46 58.87 o 1 1 3 264.23 240.41 7.08 o 2 1 3 1790.41 1784.13 40.67 o 3 1 3 107.50 119.79 5.24 o 4 1 3 1187.22 1197.74 43.83 o 5 1 3 1.46 1.61 3.19 o 6 1 3 416.38 438.49 49.50 o -9 2 3 286.94 251.19 29.90 o -8 2 3 12.13 6.63 4.04 o -7 2 3 654.01 663.85 25.08 o -6 2 3 13.34 10.34 2.26 o -5 2 3 1824.65 1768.07 41.93 o -4 2 3 26.97 27.82 1.85 o -3 2 3 2411.25 2366.62 39.91 o -2 2 3 31.38 29.01 1.30 o -1 2 3 1311.47 1148.66 20.55 o 0 2 3 31.87 28.63 1.60 o 1 2 3 3389.93 3382.93 84.54 o 2 2 3 29.79 25.84 1.78 o 3 2 3 1820.83 1833.28 46.94 o 4 2 3 9.74 6.35 1.77 o 5 2 3 391.45 385.89 23.90 o 6 2 3 21.70 20.58 7.03 o -8 3 3 289.26 265.21 21.59 o -7 3 3 1.61 -3.16 3.16 o -6 3 3 570.73 578.23 36.01 o -5 3 3 16.00 12.80 1.28 o -4 3 3 2195.55 2204.04 61.36 o -3 3 3 149.02 153.52 4.00 o -2 3 3 2098.16 2055.09 43.47 o -1 3 3 39.13 33.53 1.91 o 0 3 3 2137.47 2089.64 41.71 o 1 3 3 194.12 191.57 4.88 o 2 3 3 2025.36 2086.58 47.66 o 3 3 3 8.16 7.12 1.46 o 4 3 3 431.13 439.84 21.85 o 5 3 3 24.23 24.44 6.79 o 6 3 3 203.06 203.56 22.80 o -8 4 3 0.02 2.32 7.43 o -7 4 3 233.15 200.61 14.99 o -6 4 3 12.57 12.13 3.12 o -5 4 3 635.12 583.95 29.47 o -4 4 3 0.04 -0.02 0.72 o -3 4 3 2079.25 2100.21 60.41 o -2 4 3 50.28 47.02 2.67 o -1 4 3 2875.93 3018.59 60.86 o 0 4 3 84.07 76.82 3.35 o 1 4 3 1240.12 1287.41 31.18 o 2 4 3 3.77 3.04 3.82 o 3 4 3 396.39 384.11 18.38 o 4 4 3 36.22 36.57 5.55 o 5 4 3 261.92 263.86 22.71 o -7 5 3 1.19 1.68 6.31 o -6 5 3 408.61 394.48 31.47 o -5 5 3 59.73 53.17 7.84 o -4 5 3 603.86 629.91 58.20 o -3 5 3 28.62 31.06 3.42 o -2 5 3 1768.36 1818.27 67.24 o -1 5 3 16.16 13.00 2.72 o 0 5 3 1460.26 1512.95 54.31 o 1 5 3 59.76 59.80 3.72 o 2 5 3 379.51 373.25 16.63 o 3 5 3 17.62 17.12 5.52 o 4 5 3 360.80 389.32 33.38 o 5 5 3 0.82 -2.59 6.78 o -6 6 3 6.41 -0.56 11.30 o -5 6 3 468.61 522.01 48.46 o -4 6 3 43.08 40.08 20.73 o -3 6 3 470.36 491.78 27.06 o -2 6 3 23.95 21.78 7.87 o -1 6 3 726.93 752.35 42.79 o 0 6 3 94.41 98.92 8.88 o 1 6 3 597.73 608.82 38.89 o 2 6 3 31.56 22.94 5.82 o 3 6 3 466.65 470.35 42.88 o 4 6 3 0.05 1.48 6.18 o -5 7 3 0.02 -14.43 15.29 o -4 7 3 400.10 406.08 39.30 o -3 7 3 9.32 5.65 4.49 o -2 7 3 256.53 217.74 40.63 o -1 7 3 0.19 4.06 4.56 o 0 7 3 331.89 331.96 25.82 o 1 7 3 13.17 10.43 6.15 o 2 7 3 495.89 499.56 46.91 o -1 8 3 177.65 147.54 27.96 o -8 0 4 578.67 585.81 51.13 o -6 0 4 515.82 502.80 24.93 o -4 0 4 2105.81 2088.63 57.77 o -2 0 4 4319.27 4288.21 109.21 o 0 0 4 3208.77 3293.56 100.05 o 2 0 4 2159.88 2146.23 101.08 o 4 0 4 313.82 295.72 38.53 o 6 0 4 112.78 90.09 12.20 o -9 1 4 259.78 249.02 18.24 o -8 1 4 14.94 6.90 3.40 o -7 1 4 571.30 566.39 19.29 o -6 1 4 7.60 10.24 4.05 o -5 1 4 1359.03 1341.78 37.93 o -4 1 4 154.55 146.29 5.97 o -3 1 4 3406.75 3345.70 84.56 o -2 1 4 2.34 2.12 0.85 o -1 1 4 3218.10 3212.35 56.19 o 0 1 4 7.78 7.35 0.88 o 1 1 4 2101.56 2107.85 52.15 o 2 1 4 48.89 41.49 2.91 o 3 1 4 880.88 889.54 44.71 o 4 1 4 58.92 53.71 6.70 o 5 1 4 269.81 263.74 22.40 o 6 1 4 18.84 9.83 10.35 o -9 2 4 0.42 -0.29 8.09 o -8 2 4 238.30 208.27 15.41 o -7 2 4 1.03 0.77 2.54 o -6 2 4 1334.08 1267.94 39.01 o -5 2 4 74.96 76.24 4.04 o -4 2 4 2188.21 2172.54 49.79 o -3 2 4 23.03 23.80 1.66 o -2 2 4 2407.98 2374.10 47.15 o -1 2 4 33.29 31.67 5.62 o 0 2 4 1958.46 1989.19 45.31 o 1 2 4 7.96 7.22 2.62 o 2 2 4 780.63 765.28 27.64 o 3 2 4 49.75 47.85 4.15 o 4 2 4 736.54 791.03 32.22 o 5 2 4 0.04 2.28 6.82 o -8 3 4 16.53 6.99 5.63 o -7 3 4 643.24 651.20 42.59 o -6 3 4 61.46 49.08 4.63 o -5 3 4 1412.32 1408.89 37.75 o -4 3 4 1.10 -1.18 1.18 o -3 3 4 1127.07 1132.74 33.00 o -2 3 4 12.97 11.08 1.52 o -1 3 4 1862.29 1889.34 42.55 o 0 3 4 68.55 71.88 3.04 o 1 3 4 1192.54 1211.71 30.17 o 2 3 4 3.67 1.28 1.29 o 3 3 4 718.68 738.42 28.75 o 4 3 4 5.49 -0.83 3.52 o 5 3 4 531.06 608.04 58.30 o -8 4 4 456.77 427.55 47.30 o -7 4 4 40.00 36.45 8.99 o -6 4 4 608.62 667.61 37.42 o -5 4 4 1.24 1.55 2.74 o -4 4 4 697.36 697.35 23.59 o -3 4 4 0.15 -1.44 1.44 o -2 4 4 974.56 949.83 29.75 o -1 4 4 0.91 1.26 1.59 o 0 4 4 1310.36 1305.80 36.81 o 1 4 4 35.12 28.77 4.60 o 2 4 4 1054.80 1108.15 48.26 o 3 4 4 3.54 5.99 4.10 o 4 4 4 454.83 484.26 33.70 o 5 4 4 2.37 0.42 20.65 o -7 5 4 383.47 370.37 41.30 o -6 5 4 4.25 1.21 5.14 o -5 5 4 439.35 409.70 33.65 o -4 5 4 2.75 1.08 1.26 o -3 5 4 873.46 880.53 27.66 o -2 5 4 23.11 27.04 7.38 o -1 5 4 653.71 681.35 33.05 o 0 5 4 3.66 7.66 4.00 o 1 5 4 811.29 807.63 32.14 o 2 5 4 6.13 7.46 4.04 o 3 5 4 596.64 656.32 35.73 o 4 5 4 11.00 6.95 6.21 o -6 6 4 309.22 276.94 31.41 o -5 6 4 0.17 -4.94 7.01 o -4 6 4 668.67 691.81 44.48 o -3 6 4 0.09 -1.33 5.73 o -2 6 4 659.31 703.33 29.91 o -1 6 4 0.59 0.08 2.77 o 0 6 4 376.27 379.15 24.45 o 1 6 4 11.30 12.93 5.24 o 2 6 4 403.71 392.23 36.87 o 3 6 4 12.04 12.87 6.98 o -4 7 4 0.27 6.22 7.53 o -3 7 4 434.49 441.32 34.94 o -2 7 4 20.70 8.08 6.87 o -1 7 4 471.42 500.81 49.80 o 0 7 4 0.71 -5.75 5.75 o 1 7 4 276.91 269.02 29.65 o -9 0 5 303.99 303.32 43.20 o -7 0 5 1024.87 1062.41 51.49 o -5 0 5 2280.92 2386.94 87.80 o -3 0 5 709.12 678.29 23.51 o -1 0 5 1185.81 1106.57 37.06 o 1 0 5 2009.42 1960.22 91.06 o 3 0 5 924.37 967.06 59.78 o 5 0 5 452.41 462.21 44.16 o -9 1 5 0.93 3.67 6.25 o -8 1 5 503.57 530.51 25.22 o -7 1 5 24.39 18.05 4.10 o -6 1 5 1192.19 1240.28 38.60 o -5 1 5 111.75 105.78 4.73 o -4 1 5 1551.59 1564.63 38.11 o -3 1 5 152.34 152.35 5.08 o -2 1 5 1453.84 1369.60 31.93 o -1 1 5 209.43 185.75 7.49 o 0 1 5 1793.14 1752.77 49.87 o 1 1 5 23.76 21.91 5.58 o 2 1 5 1108.09 1104.55 43.24 o 3 1 5 0.08 1.23 2.92 o 4 1 5 547.00 558.77 54.82 o 5 1 5 5.07 10.93 6.88 o -9 2 5 336.96 302.39 30.43 o -8 2 5 0.87 8.11 4.97 o -7 2 5 505.68 524.50 28.44 o -6 2 5 0.57 -1.38 6.28 o -5 2 5 696.53 661.00 22.67 o -4 2 5 96.71 94.87 4.54 o -3 2 5 2675.28 2612.29 72.11 o -2 2 5 11.25 6.99 1.29 o -1 2 5 2259.89 2229.89 59.49 o 0 2 5 47.84 40.52 5.22 o 1 2 5 879.68 839.67 30.33 o 2 2 5 0.07 2.43 4.05 o 3 2 5 578.59 604.91 26.09 o 4 2 5 0.17 -0.07 4.13 o -8 3 5 385.88 372.02 23.35 o -7 3 5 16.99 18.31 7.54 o -6 3 5 488.10 506.43 22.81 o -5 3 5 8.27 -0.72 6.90 o -4 3 5 1317.93 1306.53 38.92 o -3 3 5 27.62 24.85 3.20 o -2 3 5 2377.74 2352.08 65.53 o -1 3 5 20.89 22.25 2.14 o 0 3 5 985.60 980.80 36.77 o 1 3 5 1.71 1.65 2.05 o 2 3 5 646.78 694.87 32.72 o 3 3 5 0.01 0.09 0.87 o 4 3 5 301.97 312.56 28.24 o -8 4 5 0.04 -1.35 9.82 o -7 4 5 443.73 445.07 41.46 o -6 4 5 2.88 -1.31 4.72 o -5 4 5 985.24 1006.61 47.24 o -4 4 5 58.16 61.81 5.19 o -3 4 5 1046.66 1054.53 45.11 o -2 4 5 10.19 9.14 2.91 o -1 4 5 975.93 983.44 47.11 o 0 4 5 22.76 19.85 3.35 o 1 4 5 812.61 881.82 35.12 o 2 4 5 1.44 1.41 3.74 o 3 4 5 393.80 379.61 28.76 o 4 4 5 9.10 11.54 11.60 o -7 5 5 12.09 10.35 8.65 o -6 5 5 585.65 630.76 46.60 o -5 5 5 0.16 -0.98 4.79 o -4 5 5 778.48 843.64 41.87 o -3 5 5 2.38 3.90 4.94 o -2 5 5 607.96 642.48 32.88 o -1 5 5 2.83 0.97 5.83 o 0 5 5 903.18 945.77 60.08 o 1 5 5 0.02 1.59 3.13 o 2 5 5 397.07 422.51 32.58 o 3 5 5 9.05 7.40 7.90 o -6 6 5 27.28 21.26 8.86 o -5 6 5 389.93 353.80 40.97 o -4 6 5 4.80 -0.09 4.74 o -3 6 5 545.36 587.93 32.76 o -2 6 5 0.18 0.24 3.55 o -1 6 5 672.32 744.25 60.23 o 0 6 5 1.49 5.85 4.19 o 1 6 5 403.90 439.24 42.73 o -3 7 5 1.72 -6.93 6.93 o -2 7 5 433.61 425.65 48.18 o -1 7 5 0.97 -7.55 11.35 o -8 0 6 340.92 322.34 31.69 o -6 0 6 900.03 925.62 56.03 o -4 0 6 1928.16 1952.85 69.28 o -2 0 6 2849.57 2860.73 112.60 o 0 0 6 711.44 666.21 35.94 o 2 0 6 380.80 401.54 39.15 o 4 0 6 392.11 341.31 51.80 o -8 1 6 19.19 19.27 5.39 o -7 1 6 619.23 641.86 34.05 o -6 1 6 10.67 8.76 2.69 o -5 1 6 1136.68 1178.55 37.64 o -4 1 6 46.55 50.67 3.77 o -3 1 6 1917.11 1935.13 62.30 o -2 1 6 63.89 51.51 4.10 o -1 1 6 1602.25 1634.42 51.78 o 0 1 6 117.04 117.61 6.93 o 1 1 6 729.07 712.04 35.86 o 2 1 6 24.88 17.61 3.54 o 3 1 6 421.56 404.47 40.10 o 4 1 6 2.05 -2.01 5.20 o -8 2 6 414.85 401.71 34.11 o -7 2 6 10.06 12.26 3.59 o -6 2 6 780.83 872.29 33.43 o -5 2 6 14.87 16.34 3.14 o -4 2 6 1023.07 1120.37 56.58 o -3 2 6 9.55 9.97 3.18 o -2 2 6 918.45 891.09 30.64 o -1 2 6 78.96 73.53 12.25 o 0 2 6 1560.79 1606.10 65.03 o 1 2 6 12.27 11.21 3.26 o 2 2 6 796.88 811.30 38.64 o 3 2 6 0.37 4.86 4.16 o -8 3 6 0.14 -7.47 7.47 o -7 3 6 444.59 440.08 32.14 o -6 3 6 3.22 6.19 3.56 o -5 3 6 923.84 1017.12 35.89 o -4 3 6 0.06 5.17 2.66 o -3 3 6 729.98 728.56 32.03 o -2 3 6 9.99 6.42 1.47 o -1 3 6 853.11 841.76 31.60 o 0 3 6 0.02 0.78 1.11 o 1 3 6 1042.48 1108.96 42.16 o 2 3 6 52.62 37.82 6.57 o 3 3 6 349.78 319.27 27.55 o -7 4 6 3.06 5.09 5.69 o -6 4 6 532.32 501.55 47.91 o -5 4 6 1.44 -2.87 7.36 o -4 4 6 805.93 819.20 40.45 o -3 4 6 7.32 6.57 3.27 o -2 4 6 764.91 766.56 41.80 o -1 4 6 18.33 7.53 5.19 o 0 4 6 492.22 511.82 27.35 o 1 4 6 11.25 13.04 5.79 o 2 4 6 412.97 385.14 40.62 o -6 5 6 5.70 -0.91 6.39 o -5 5 6 376.44 326.56 34.15 o -4 5 6 0.39 4.26 3.24 o -3 5 6 635.52 690.60 40.89 o -2 5 6 8.45 7.53 4.69 o -1 5 6 532.01 524.11 43.88 o 0 5 6 0.70 -4.84 4.84 o 1 5 6 275.23 243.06 28.73 o -5 6 6 0.95 3.61 7.19 o -4 6 6 264.32 205.78 24.90 o -3 6 6 0.49 -3.74 5.38 o -2 6 6 440.44 435.22 33.89 o -1 6 6 7.76 0.49 7.13 o 0 6 6 390.36 392.42 33.37 o -7 0 7 328.55 352.79 23.33 o -5 0 7 733.02 765.77 50.86 o -3 0 7 1200.97 1257.31 54.73 o -1 0 7 951.70 885.90 52.61 o 1 0 7 929.16 945.51 86.65 o -8 1 7 466.46 469.36 28.87 o -7 1 7 21.49 28.68 5.17 o -6 1 7 648.63 671.85 32.52 o -5 1 7 30.87 27.20 6.66 o -4 1 7 986.77 1010.60 33.95 o -3 1 7 0.37 5.27 5.48 o -2 1 7 898.45 878.65 40.67 o -1 1 7 4.01 5.26 4.05 o 0 1 7 840.83 839.12 32.70 o 1 1 7 0.85 7.77 3.75 o 2 1 7 579.24 593.51 55.61 o -8 2 7 15.86 9.59 8.18 o -7 2 7 830.10 898.22 49.70 o -6 2 7 0.58 0.99 4.28 o -5 2 7 918.13 981.22 41.78 o -4 2 7 0.10 -0.54 5.19 o -3 2 7 752.75 733.18 32.19 o -2 2 7 0.01 1.05 4.10 o -1 2 7 789.94 859.26 39.71 o 0 2 7 18.09 13.51 4.45 o 1 2 7 495.59 497.80 28.19 o 2 2 7 1.89 1.25 7.37 o -7 3 7 0.27 -7.79 7.79 o -6 3 7 776.48 803.93 50.24 o -5 3 7 38.76 37.90 10.59 o -4 3 7 715.87 732.67 43.83 o -3 3 7 3.17 4.64 4.02 o -2 3 7 982.63 1048.96 52.16 o -1 3 7 5.05 0.72 3.83 o 0 3 7 595.55 616.11 44.19 o 1 3 7 8.75 -3.65 5.55 o 2 3 7 276.34 193.21 27.18 o -6 4 7 5.86 -0.32 6.00 o -5 4 7 561.31 580.07 37.07 o -4 4 7 3.34 -4.49 4.49 o -3 4 7 959.99 1112.70 78.93 o -2 4 7 2.50 5.17 3.84 o -1 4 7 794.59 814.33 50.01 o 0 4 7 6.50 11.25 5.52 o 1 4 7 338.04 264.87 41.96 o -5 5 7 8.24 9.62 13.23 o -4 5 7 720.49 791.49 63.16 o -3 5 7 5.15 3.24 5.32 o -2 5 7 561.99 594.92 42.02 o -1 5 7 14.76 13.99 6.47 o -6 0 8 932.60 1067.78 89.26 o -4 0 8 570.37 589.30 39.75 o -2 0 8 837.30 872.37 79.40 o 0 0 8 824.69 782.61 117.93 o -7 1 8 525.21 551.60 36.15 o -6 1 8 9.52 8.36 4.46 o -5 1 8 833.77 916.59 51.96 o -4 1 8 9.63 15.89 4.53 o -3 1 8 857.00 903.58 49.93 o -2 1 8 35.42 26.56 8.64 o -1 1 8 787.15 821.99 67.73 o 0 1 8 5.41 7.82 7.66 o 1 1 8 372.89 387.24 37.32 o -7 2 8 18.85 20.75 8.71 o -6 2 8 434.71 417.97 28.16 o -5 2 8 1.40 4.60 5.43 o -4 2 8 1158.91 1271.54 68.35 o -3 2 8 0.13 6.89 5.64 o -2 2 8 799.01 823.64 60.33 o -1 2 8 4.97 6.22 4.56 o 0 2 8 322.11 288.95 27.42 o -6 3 8 42.97 42.40 7.46 o -5 3 8 505.13 507.18 39.52 o -4 3 8 4.66 7.94 7.16 o -3 3 8 738.60 775.20 57.57 o -2 3 8 60.00 62.00 15.55 o -1 3 8 379.99 288.44 25.56 o 0 3 8 17.15 15.62 6.61 o -5 4 8 23.35 26.19 9.63 o -4 4 8 247.42 216.62 22.57 o -3 4 8 9.69 -1.00 6.86 o -2 4 8 351.66 309.34 30.87 o -5 0 9 493.19 509.78 51.68 o -3 0 9 592.96 527.03 85.43 o -5 1 9 0.41 0.62 5.21 o -4 1 9 519.42 537.00 44.52 o -3 1 9 5.22 5.98 6.64 o -2 1 9 517.73 514.70 58.38 o -5 2 9 457.74 476.62 31.12 o -4 2 9 1.63 2.26 5.90 o -3 2 9 484.17 455.50 47.05 o