#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/24/2012407.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012407_Fobs loop_ _publ_author_name 'McMullen, Sarah E.' 'Hagen, Karl S.' _publ_section_title ; trans-Bis(benzoato-O)tetrakis(methanol-O)iron(II): ligand bulk is not structure-determining ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m48 _journal_page_last m49 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 101.445 _cell_angle_gamma 90.000 _cell_length_a 9.8627 _cell_length_b 12.0652 _cell_length_c 8.6045 _exptl_crystal_F_000 448.00 _reflns_d_resolution_high 0.7108 _[local]_cod_data_source_file bk1620Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sd3141s Fe(PhCOO)2(MeOH)4 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 125.08 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5690.53 5662.02 65.76 o 2 0 0 6563.96 6333.04 260.66 o 3 0 0 1189.40 1273.50 27.99 o 4 0 0 1378.97 1461.03 34.81 o 5 0 0 11.03 6.29 0.54 o 6 0 0 380.71 398.96 5.22 o 7 0 0 328.62 309.24 4.03 o 8 0 0 5.64 7.21 0.76 o 9 0 0 1367.34 1335.50 36.25 o 10 0 0 873.27 858.53 11.96 o 11 0 0 1095.69 1113.02 12.63 o 12 0 0 616.31 671.63 10.96 o 13 0 0 1.65 6.31 2.16 o 1 1 0 1442.91 1624.97 18.11 o 2 1 0 5.53 4.62 0.63 o 3 1 0 475.01 509.41 6.32 o 4 1 0 876.58 945.23 13.60 o 5 1 0 118.85 125.03 1.67 o 6 1 0 6.40 4.98 0.40 o 7 1 0 24.07 15.61 0.63 o 8 1 0 367.33 363.32 4.00 o 9 1 0 2.51 2.55 0.57 o 10 1 0 44.43 41.09 2.79 o 11 1 0 7.85 8.77 1.80 o 12 1 0 1.15 1.83 2.16 o 13 1 0 34.03 35.61 40.14 o 0 2 0 3167.57 3565.10 38.67 o 1 2 0 1820.06 1963.84 10.58 o 2 2 0 3942.49 4071.04 29.35 o 3 2 0 1095.23 1090.87 17.01 o 4 2 0 907.02 969.12 8.67 o 5 2 0 2968.36 3202.60 32.15 o 6 2 0 316.14 279.96 3.10 o 7 2 0 1861.67 1827.60 16.44 o 8 2 0 24.39 27.84 0.99 o 9 2 0 246.21 237.99 3.36 o 10 2 0 136.67 138.88 2.54 o 11 2 0 136.09 128.35 5.54 o 12 2 0 243.08 237.50 8.60 o 13 2 0 232.42 229.91 7.97 o 1 3 0 2592.34 2819.90 13.28 o 2 3 0 3899.15 3990.51 43.80 o 3 3 0 139.67 178.27 2.62 o 4 3 0 20.73 19.42 1.06 o 5 3 0 292.75 306.74 4.01 o 6 3 0 314.08 335.76 3.96 o 7 3 0 153.48 133.44 2.17 o 8 3 0 77.20 67.54 2.40 o 9 3 0 408.51 401.07 4.64 o 10 3 0 47.97 51.87 2.12 o 11 3 0 25.57 26.94 1.46 o 12 3 0 0.01 -0.22 0.80 o 13 3 0 74.33 71.22 12.71 o 0 4 0 875.81 947.38 6.89 o 1 4 0 151.67 158.58 2.18 o 2 4 0 1899.80 1991.67 20.06 o 3 4 0 393.41 340.36 3.07 o 4 4 0 2544.16 2694.98 34.90 o 5 4 0 2430.44 2612.75 17.79 o 6 4 0 1602.31 1669.96 9.10 o 7 4 0 758.16 763.84 7.25 o 8 4 0 609.60 593.46 9.66 o 9 4 0 15.00 15.23 1.45 o 10 4 0 18.90 23.74 1.72 o 11 4 0 302.61 290.85 4.52 o 12 4 0 89.20 88.99 2.74 o 13 4 0 216.92 232.65 19.36 o 1 5 0 588.32 673.99 8.33 o 2 5 0 728.72 840.97 7.36 o 3 5 0 1302.16 1375.22 17.11 o 4 5 0 2.25 1.00 0.26 o 5 5 0 5.93 4.47 0.32 o 6 5 0 54.59 52.69 1.59 o 7 5 0 319.33 313.60 4.31 o 8 5 0 23.15 18.93 1.51 o 9 5 0 32.71 37.24 1.63 o 10 5 0 11.51 8.58 1.11 o 11 5 0 8.25 7.67 1.16 o 12 5 0 18.70 16.48 1.38 o 0 6 0 928.34 928.85 13.37 o 1 6 0 719.68 712.11 6.90 o 2 6 0 1713.21 1751.58 14.20 o 3 6 0 1052.29 1102.64 6.13 o 4 6 0 690.98 680.23 4.50 o 5 6 0 521.61 520.23 4.97 o 6 6 0 469.64 469.03 11.18 o 7 6 0 566.68 546.55 7.51 o 8 6 0 796.01 785.74 6.12 o 9 6 0 417.52 394.99 4.87 o 10 6 0 207.20 198.21 3.29 o 11 6 0 121.91 115.42 3.15 o 12 6 0 53.41 55.07 2.29 o 1 7 0 167.99 171.91 1.90 o 2 7 0 49.82 39.90 0.79 o 3 7 0 336.61 382.30 3.23 o 4 7 0 276.96 292.35 4.45 o 5 7 0 48.33 51.41 1.40 o 6 7 0 3.37 2.92 0.63 o 7 7 0 66.15 65.43 1.51 o 8 7 0 111.19 104.80 2.46 o 9 7 0 0.48 1.38 0.89 o 10 7 0 0.02 0.10 0.75 o 11 7 0 27.91 32.39 1.66 o 12 7 0 17.29 17.52 1.47 o 0 8 0 480.85 455.17 9.60 o 1 8 0 374.08 394.24 7.28 o 2 8 0 203.89 178.16 2.23 o 3 8 0 1092.42 1135.54 11.66 o 4 8 0 901.69 939.79 9.72 o 5 8 0 1149.79 1093.53 6.57 o 6 8 0 706.01 664.86 7.40 o 7 8 0 693.54 704.47 9.41 o 8 8 0 46.62 46.64 1.71 o 9 8 0 275.30 257.62 5.35 o 10 8 0 243.55 252.48 6.14 o 11 8 0 21.44 21.08 1.47 o 1 9 0 115.08 109.15 1.68 o 2 9 0 262.32 256.45 4.45 o 3 9 0 1099.08 1178.10 12.55 o 4 9 0 335.58 308.13 10.45 o 5 9 0 43.42 36.48 1.30 o 6 9 0 279.14 241.61 3.14 o 7 9 0 265.86 255.77 3.73 o 8 9 0 611.97 576.94 7.07 o 9 9 0 41.01 39.08 2.22 o 10 9 0 5.39 7.63 1.22 o 11 9 0 71.92 75.31 3.18 o 0 10 0 863.18 876.50 28.65 o 1 10 0 359.77 359.70 3.94 o 2 10 0 618.44 620.27 15.95 o 3 10 0 967.27 982.81 7.47 o 4 10 0 469.39 449.35 4.99 o 5 10 0 158.35 164.82 4.11 o 6 10 0 455.00 403.15 4.30 o 7 10 0 6.41 6.98 0.98 o 8 10 0 324.68 310.95 5.91 o 9 10 0 261.18 250.48 6.34 o 10 10 0 196.87 219.20 6.08 o 1 11 0 304.12 292.04 3.88 o 2 11 0 7.80 6.19 0.62 o 3 11 0 23.63 22.70 1.44 o 4 11 0 23.68 20.28 1.11 o 5 11 0 125.76 105.31 2.50 o 6 11 0 0.01 0.02 0.63 o 7 11 0 8.56 8.78 0.88 o 8 11 0 73.33 75.73 2.39 o 9 11 0 0.78 0.56 0.86 o 10 11 0 0.15 0.85 1.16 o 0 12 0 309.47 296.17 5.28 o 1 12 0 884.01 912.59 12.23 o 2 12 0 493.08 514.30 10.91 o 3 12 0 887.71 917.75 8.82 o 4 12 0 624.32 592.26 6.14 o 5 12 0 83.25 80.39 2.15 o 6 12 0 18.30 19.87 1.12 o 7 12 0 132.95 124.82 4.63 o 8 12 0 561.84 554.74 5.99 o 9 12 0 68.12 68.58 2.41 o 1 13 0 0.06 0.25 0.82 o 2 13 0 84.22 79.10 2.15 o 3 13 0 17.13 13.73 1.39 o 4 13 0 0.04 -0.39 0.82 o 5 13 0 4.22 4.16 0.91 o 6 13 0 2.23 2.24 0.87 o 7 13 0 60.87 62.81 2.15 o 8 13 0 4.12 5.75 1.07 o 0 14 0 103.99 109.18 3.83 o 1 14 0 463.87 458.50 8.97 o 2 14 0 235.06 246.86 3.48 o 3 14 0 304.94 307.30 5.04 o 4 14 0 161.80 156.31 3.66 o 5 14 0 42.22 41.57 1.81 o 6 14 0 173.62 172.59 4.15 o 7 14 0 43.10 42.72 2.46 o 1 15 0 192.23 191.86 5.72 o 2 15 0 150.22 163.53 3.66 o 3 15 0 0.42 0.44 0.82 o 4 15 0 3.81 3.09 0.96 o 5 15 0 60.75 65.98 4.24 o 6 15 0 1.16 1.60 1.22 o 0 16 0 115.52 117.78 9.80 o 1 16 0 154.06 162.65 4.81 o 2 16 0 104.44 105.79 3.72 o 3 16 0 326.89 344.73 6.92 o 4 16 0 171.28 179.02 3.45 o -13 1 1 16.62 16.62 2.03 o -12 1 1 289.02 322.20 5.96 o -11 1 1 494.92 511.02 7.60 o -10 1 1 370.06 379.89 8.14 o -9 1 1 380.84 347.56 4.15 o -8 1 1 21.34 22.57 0.74 o -7 1 1 142.04 155.22 2.14 o -6 1 1 383.22 349.67 3.38 o -5 1 1 4942.47 5107.80 42.73 o -4 1 1 2156.97 1949.56 17.51 o -3 1 1 3696.52 3573.40 25.97 o -2 1 1 2580.03 2668.65 24.08 o -1 1 1 3444.30 3661.84 23.56 o 0 1 1 5735.95 6102.02 30.88 o 1 1 1 7796.92 8556.88 90.05 o 2 1 1 11.24 11.01 0.40 o 3 1 1 788.96 771.20 4.14 o 4 1 1 5.21 5.34 0.32 o 5 1 1 172.29 148.18 1.69 o 6 1 1 2480.29 2641.38 17.67 o 7 1 1 1904.35 1941.42 25.61 o 8 1 1 895.91 916.29 11.59 o 9 1 1 114.59 114.11 2.47 o 10 1 1 447.64 424.02 5.22 o 11 1 1 222.40 229.73 7.31 o 12 1 1 154.88 153.37 5.81 o 13 1 1 189.34 215.71 6.40 o -13 2 1 107.12 103.06 4.25 o -12 2 1 10.11 14.05 1.50 o -11 2 1 40.69 37.41 1.97 o -10 2 1 13.48 8.51 0.93 o -9 2 1 14.01 12.80 0.87 o -8 2 1 0.03 0.34 0.36 o -7 2 1 221.48 252.29 3.51 o -6 2 1 424.84 442.97 4.78 o -5 2 1 84.01 67.25 1.24 o -4 2 1 1244.23 1401.08 6.13 o -3 2 1 629.42 613.82 5.86 o -2 2 1 691.06 649.85 4.59 o -1 2 1 1934.76 2057.64 29.15 o 0 2 1 8769.59 9830.62 143.06 o 1 2 1 1237.99 1404.07 10.32 o 2 2 1 34.22 32.92 0.81 o 3 2 1 27.33 24.86 0.53 o 4 2 1 8.10 8.29 0.36 o 5 2 1 21.25 17.59 1.07 o 6 2 1 42.29 48.95 0.93 o 7 2 1 0.52 1.58 0.37 o 8 2 1 479.93 468.91 5.97 o 9 2 1 318.31 296.30 4.22 o 10 2 1 1.08 0.44 0.70 o 11 2 1 55.54 59.87 2.92 o 12 2 1 6.21 9.04 1.58 o 13 2 1 51.11 60.24 3.55 o -13 3 1 171.40 174.46 4.82 o -12 3 1 264.90 282.51 4.76 o -11 3 1 311.33 287.09 4.41 o -10 3 1 6.58 10.48 1.23 o -9 3 1 371.54 362.95 3.97 o -8 3 1 9.72 9.35 0.64 o -7 3 1 1435.38 1401.60 8.22 o -6 3 1 1477.48 1508.58 11.12 o -5 3 1 2014.73 1986.37 7.76 o -4 3 1 3877.88 3960.85 41.57 o -3 3 1 1686.54 1787.91 29.98 o -2 3 1 1853.56 1963.23 21.27 o -1 3 1 154.79 172.07 2.74 o 0 3 1 2086.02 2386.98 13.72 o 1 3 1 381.30 437.78 3.81 o 2 3 1 2595.55 2807.08 18.63 o 3 3 1 1686.00 1656.22 8.08 o 4 3 1 637.65 556.93 3.40 o 5 3 1 2261.21 2340.68 10.85 o 6 3 1 1836.40 1772.59 10.96 o 7 3 1 336.36 324.57 4.94 o 8 3 1 1449.24 1467.56 29.64 o 9 3 1 26.72 26.99 1.20 o 10 3 1 152.22 154.11 3.19 o 11 3 1 24.01 28.78 1.68 o 12 3 1 197.42 204.07 44.40 o 13 3 1 92.93 111.46 9.47 o -13 4 1 61.08 72.19 4.33 o -12 4 1 13.80 14.58 1.70 o -11 4 1 57.74 55.37 2.05 o -10 4 1 330.97 331.95 6.91 o -9 4 1 61.31 61.04 1.57 o -8 4 1 329.46 292.39 3.41 o -7 4 1 1203.31 1180.02 16.00 o -6 4 1 238.74 246.46 5.13 o -5 4 1 1019.16 1063.39 8.78 o -4 4 1 63.66 64.87 1.18 o -3 4 1 0.06 0.11 0.29 o -2 4 1 85.50 90.27 1.54 o -1 4 1 198.40 212.92 3.15 o 0 4 1 1562.06 1761.31 13.83 o 1 4 1 6413.43 7221.21 63.52 o 2 4 1 545.09 560.67 4.92 o 3 4 1 170.13 227.53 2.23 o 4 4 1 2040.44 2154.91 10.59 o 5 4 1 2145.60 2224.49 14.60 o 6 4 1 148.24 147.20 2.26 o 7 4 1 87.66 75.28 2.85 o 8 4 1 181.51 184.96 2.67 o 9 4 1 63.79 67.69 1.97 o 10 4 1 6.53 6.21 1.11 o 11 4 1 32.89 30.07 1.75 o 12 4 1 13.26 14.60 2.48 o -13 5 1 48.62 48.39 2.39 o -12 5 1 64.63 70.98 4.71 o -11 5 1 169.16 163.27 3.22 o -10 5 1 265.54 247.68 3.57 o -9 5 1 235.92 237.56 4.07 o -8 5 1 478.22 481.20 5.86 o -7 5 1 3402.49 3476.45 48.18 o -6 5 1 1265.24 1310.45 17.62 o -5 5 1 1623.53 1608.89 16.84 o -4 5 1 319.13 341.54 5.56 o -3 5 1 398.12 494.10 7.85 o -2 5 1 38.35 24.37 0.74 o -1 5 1 546.71 514.47 3.75 o 0 5 1 1403.66 1444.29 5.82 o 1 5 1 4113.74 4371.72 58.44 o 2 5 1 2073.37 2208.76 20.22 o 3 5 1 5788.28 6469.15 36.36 o 4 5 1 1676.03 1637.88 11.46 o 5 5 1 2280.60 2283.82 14.61 o 6 5 1 153.23 130.32 2.83 o 7 5 1 94.82 91.51 2.14 o 8 5 1 2.02 2.29 0.75 o 9 5 1 150.79 142.54 2.88 o 10 5 1 186.63 185.07 4.71 o 11 5 1 106.59 103.42 2.92 o 12 5 1 404.43 406.98 6.47 o -12 6 1 0.82 0.44 0.86 o -11 6 1 73.24 66.06 2.11 o -10 6 1 7.63 5.77 1.11 o -9 6 1 5.76 6.37 1.06 o -8 6 1 148.38 139.55 3.14 o -7 6 1 76.00 64.69 2.26 o -6 6 1 90.71 83.46 2.52 o -5 6 1 84.78 86.78 1.92 o -4 6 1 1.61 0.11 0.34 o -3 6 1 264.46 253.03 3.31 o -2 6 1 1522.99 1861.66 13.05 o -1 6 1 115.36 120.20 1.95 o 0 6 1 370.87 399.74 2.95 o 1 6 1 22.65 28.44 0.81 o 2 6 1 4.22 5.54 0.37 o 3 6 1 206.38 247.65 2.82 o 4 6 1 49.01 64.23 1.34 o 5 6 1 17.13 15.71 0.74 o 6 6 1 10.05 12.67 0.92 o 7 6 1 57.47 57.75 2.00 o 8 6 1 2.04 1.83 0.78 o 9 6 1 0.76 1.39 0.72 o 10 6 1 108.93 108.79 2.72 o 11 6 1 71.28 73.79 2.54 o 12 6 1 0.12 0.06 0.84 o -12 7 1 132.18 135.71 3.47 o -11 7 1 220.17 222.10 6.47 o -10 7 1 264.42 251.61 4.28 o -9 7 1 975.64 961.04 9.26 o -8 7 1 552.37 522.58 5.25 o -7 7 1 53.97 51.26 1.38 o -6 7 1 142.78 140.16 6.21 o -5 7 1 49.59 45.88 1.57 o -4 7 1 382.20 359.23 6.04 o -3 7 1 2040.01 2207.72 14.58 o -2 7 1 1540.53 1618.42 12.13 o -1 7 1 1376.13 1358.59 10.86 o 0 7 1 1955.63 2013.24 13.54 o 1 7 1 860.39 857.12 4.62 o 2 7 1 1892.67 1970.82 15.73 o 3 7 1 390.09 376.07 3.16 o 4 7 1 531.24 553.73 6.40 o 5 7 1 115.46 125.84 4.68 o 6 7 1 584.64 480.65 17.39 o 7 7 1 413.49 405.69 4.72 o 8 7 1 991.33 983.57 12.10 o 9 7 1 170.25 158.83 4.53 o 10 7 1 169.11 175.22 3.65 o 11 7 1 76.22 74.86 2.24 o 12 7 1 12.91 14.36 1.32 o -12 8 1 3.17 2.65 0.96 o -11 8 1 1.63 2.07 0.82 o -10 8 1 49.10 49.28 1.86 o -9 8 1 13.44 13.20 1.17 o -8 8 1 2.93 2.73 0.72 o -7 8 1 647.48 607.03 6.91 o -6 8 1 30.28 28.33 1.27 o -5 8 1 122.87 122.17 2.50 o -4 8 1 582.64 553.50 7.67 o -3 8 1 477.73 460.78 3.79 o -2 8 1 36.09 47.54 1.14 o -1 8 1 249.88 256.35 2.40 o 0 8 1 283.69 309.27 3.07 o 1 8 1 0.29 1.20 0.31 o 2 8 1 230.25 242.06 2.89 o 3 8 1 4.60 7.29 0.62 o 4 8 1 177.22 156.03 7.97 o 5 8 1 23.84 13.17 1.08 o 6 8 1 373.44 307.43 5.87 o 7 8 1 85.44 81.20 2.05 o 8 8 1 125.69 120.40 2.64 o 9 8 1 1.08 0.58 0.70 o 10 8 1 71.08 74.40 3.03 o 11 8 1 43.23 42.71 1.88 o -11 9 1 89.90 88.75 4.12 o -10 9 1 263.86 255.86 3.84 o -9 9 1 100.92 103.21 2.48 o -8 9 1 565.49 547.48 12.49 o -7 9 1 44.92 41.76 2.30 o -6 9 1 427.35 425.84 6.76 o -5 9 1 711.69 689.77 12.38 o -4 9 1 254.67 274.08 6.67 o -3 9 1 676.85 703.32 9.38 o -2 9 1 519.55 506.99 4.02 o -1 9 1 790.64 769.65 4.82 o 0 9 1 573.44 577.38 5.19 o 1 9 1 1871.56 1901.04 16.71 o 2 9 1 389.22 374.56 3.34 o 3 9 1 368.27 353.07 8.38 o 4 9 1 945.79 926.66 6.61 o 5 9 1 252.84 271.16 3.59 o 6 9 1 381.03 351.90 3.94 o 7 9 1 371.75 348.64 4.36 o 8 9 1 9.64 8.31 0.94 o 9 9 1 168.67 168.57 3.22 o 10 9 1 254.01 243.31 4.13 o 11 9 1 260.45 281.89 7.30 o -11 10 1 2.13 5.00 1.06 o -10 10 1 11.55 15.28 1.40 o -9 10 1 14.48 13.00 1.09 o -8 10 1 74.59 66.63 2.06 o -7 10 1 15.24 14.96 1.17 o -6 10 1 13.29 10.29 1.00 o -5 10 1 31.03 28.59 1.17 o -4 10 1 113.99 97.53 1.89 o -3 10 1 50.93 50.47 3.21 o -2 10 1 25.64 26.59 1.23 o -1 10 1 20.04 17.34 0.66 o 0 10 1 1058.84 1125.55 10.54 o 1 10 1 29.05 26.49 0.82 o 2 10 1 18.42 15.99 0.78 o 3 10 1 53.54 50.82 1.55 o 4 10 1 9.86 8.09 0.76 o 5 10 1 0.59 1.10 0.66 o 6 10 1 3.75 1.96 0.70 o 7 10 1 1.46 2.81 0.85 o 8 10 1 241.08 231.52 4.20 o 9 10 1 37.48 38.97 1.88 o 10 10 1 0.05 -0.39 1.06 o -10 11 1 66.73 79.05 2.69 o -9 11 1 131.96 128.93 3.75 o -8 11 1 527.22 499.17 6.56 o -7 11 1 356.96 355.12 6.48 o -6 11 1 198.38 192.97 3.84 o -5 11 1 84.27 85.20 1.99 o -4 11 1 438.78 442.95 5.18 o -3 11 1 745.58 740.30 6.18 o -2 11 1 620.40 625.31 9.40 o -1 11 1 453.59 439.16 6.62 o 0 11 1 76.53 76.67 2.24 o 1 11 1 223.89 207.54 3.98 o 2 11 1 846.83 828.30 10.30 o 3 11 1 1372.47 1365.09 20.79 o 4 11 1 648.39 638.24 9.26 o 5 11 1 219.91 211.44 3.67 o 6 11 1 2.64 4.55 1.00 o 7 11 1 39.94 38.64 1.67 o 8 11 1 111.09 107.81 2.51 o 9 11 1 392.11 367.83 7.62 o 10 11 1 109.53 109.59 3.56 o -9 12 1 13.18 13.25 1.75 o -8 12 1 15.81 19.42 1.76 o -7 12 1 9.65 8.17 1.26 o -6 12 1 0.86 0.84 0.89 o -5 12 1 2.00 1.10 0.70 o -4 12 1 4.61 4.82 0.82 o -3 12 1 45.43 44.27 1.51 o -2 12 1 178.49 175.33 3.69 o -1 12 1 20.24 22.97 0.95 o 0 12 1 117.69 125.61 2.54 o 1 12 1 186.15 178.86 3.30 o 2 12 1 123.82 113.19 3.27 o 3 12 1 65.25 61.98 1.59 o 4 12 1 0.00 0.45 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