#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/24/2012429.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012429_Fobs loop_ _publ_author_name 'Coles, Simon J.' 'Hall, Christopher W.' 'Hursthouse, Michael B.' _publ_section_title ; 2,4-Dihydroxy-1,3-bis(methoxycarbonylmethoxy)calix[4]arene and 1,3-bis(ethoxycarbonylmethoxy)-2,4-dihydroxycalix[4]arene chloroform solvate ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o29 _journal_page_last o31 _journal_volume 58 _journal_year 2002 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.392 _cell_angle_gamma 90.000 _cell_length_a 10.0274 _cell_length_b 10.2433 _cell_length_c 16.8525 _exptl_crystal_F_000 748.00 _reflns_d_resolution_high 0.7703 _[local]_cod_data_source_file fr1354IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 01AWE002 in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 130.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -13 0 32.04 25.28 17.99 o 2 -13 0 104.16 103.01 35.10 o 0 -12 0 297.24 265.96 51.85 o 1 -12 0 40.90 52.68 35.68 o 2 -12 0 136.72 170.78 27.11 o 3 -12 0 28.54 12.54 17.25 o 4 -12 0 5.17 -2.62 15.38 o 5 -12 0 16.07 21.11 21.60 o 1 -11 0 498.17 482.46 43.93 o 2 -11 0 107.67 102.43 18.86 o 3 -11 0 20.65 15.25 14.08 o 4 -11 0 62.41 62.95 18.59 o 5 -11 0 82.36 92.16 23.86 o 6 -11 0 68.43 40.33 19.80 o 7 -11 0 13.82 28.61 23.46 o 0 -10 0 1429.29 1646.19 137.98 o 1 -10 0 198.24 187.89 16.39 o 2 -10 0 28.48 34.54 9.71 o 3 -10 0 22.75 45.78 14.00 o 4 -10 0 362.17 356.44 25.13 o 5 -10 0 117.41 99.23 21.90 o 6 -10 0 80.63 91.90 23.11 o 7 -10 0 86.08 42.65 20.33 o 8 -10 0 42.33 46.74 25.31 o 1 -9 0 656.67 638.56 27.47 o 2 -9 0 309.67 316.87 19.71 o 3 -9 0 36.73 32.09 6.90 o 4 -9 0 272.81 275.49 16.04 o 5 -9 0 133.62 145.93 27.23 o 6 -9 0 289.84 340.31 35.05 o 7 -9 0 25.51 23.19 15.56 o 8 -9 0 46.62 57.85 18.38 o 9 -9 0 12.85 22.47 35.68 o 0 -8 0 663.61 736.49 40.32 o 1 -8 0 922.27 948.87 36.34 o 2 -8 0 127.48 118.21 10.66 o 3 -8 0 200.36 182.58 12.79 o 4 -8 0 9.29 10.72 4.18 o 5 -8 0 954.74 1020.38 51.28 o 6 -8 0 398.52 446.00 24.87 o 7 -8 0 114.28 100.68 12.98 o 8 -8 0 86.75 70.98 18.63 o 9 -8 0 45.85 58.46 32.20 o 10 -8 0 48.56 38.50 19.90 o 1 -7 0 221.81 206.70 10.41 o 2 -7 0 228.71 232.55 10.98 o 3 -7 0 305.11 282.13 13.60 o 4 -7 0 122.05 112.02 6.86 o 5 -7 0 17.92 19.89 6.56 o 6 -7 0 281.08 264.85 13.12 o 7 -7 0 38.92 48.73 10.95 o 8 -7 0 607.00 630.53 51.16 o 9 -7 0 123.61 103.09 24.16 o 10 -7 0 50.08 53.92 16.68 o 0 -6 0 1841.55 1916.14 76.33 o 1 -6 0 1377.13 1526.40 50.29 o 2 -6 0 2160.20 2281.64 59.41 o 3 -6 0 166.85 160.40 9.37 o 4 -6 0 262.00 288.64 10.04 o 5 -6 0 120.33 128.02 8.42 o 6 -6 0 693.01 705.60 30.68 o 7 -6 0 36.02 32.04 10.13 o 8 -6 0 69.22 60.56 14.03 o 9 -6 0 112.24 112.78 17.01 o 10 -6 0 93.65 71.44 23.44 o 11 -6 0 23.17 28.62 26.81 o 1 -5 0 2926.61 3094.97 77.88 o 2 -5 0 44.88 63.75 4.89 o 3 -5 0 682.39 647.63 16.04 o 4 -5 0 802.22 800.22 23.40 o 5 -5 0 480.75 453.01 14.74 o 6 -5 0 172.15 165.08 10.95 o 7 -5 0 1019.40 1197.40 48.98 o 8 -5 0 302.78 312.40 19.53 o 9 -5 0 6.69 4.22 8.88 o 10 -5 0 43.74 34.14 22.32 o 11 -5 0 100.61 95.04 20.65 o 0 -4 0 5316.03 5317.46 181.76 o 1 -4 0 5296.16 5369.45 144.24 o 2 -4 0 392.73 384.20 11.60 o 3 -4 0 1403.12 1414.73 32.49 o 4 -4 0 308.87 341.15 11.50 o 5 -4 0 910.95 956.16 29.49 o 6 -4 0 49.77 28.82 6.37 o 7 -4 0 806.55 838.22 33.92 o 8 -4 0 688.90 729.04 35.99 o 9 -4 0 14.58 -1.68 7.17 o 10 -4 0 20.74 36.23 12.49 o 11 -4 0 82.42 89.68 18.73 o 12 -4 0 64.57 82.00 30.44 o 1 -3 0 2263.21 2160.99 51.05 o 2 -3 0 372.69 356.47 10.12 o 3 -3 0 773.87 781.52 29.90 o 4 -3 0 1916.17 2003.37 56.35 o 5 -3 0 407.00 436.74 16.16 o 6 -3 0 1458.83 1570.69 42.43 o 7 -3 0 79.74 86.64 7.37 o 8 -3 0 56.61 47.68 9.37 o 9 -3 0 334.47 357.63 24.20 o 10 -3 0 22.14 16.80 11.48 o 11 -3 0 80.00 59.02 25.68 o 12 -3 0 1.16 -7.43 16.13 o 0 -2 0 3915.04 3795.94 127.46 o 1 -2 0 5702.55 5685.15 152.17 o 2 -2 0 1333.30 1279.87 31.70 o 3 -2 0 2146.55 2057.72 51.77 o 4 -2 0 15.46 21.53 5.35 o 5 -2 0 533.78 561.16 21.35 o 6 -2 0 158.92 154.70 7.70 o 7 -2 0 784.70 814.30 24.62 o 8 -2 0 464.12 487.85 20.44 o 9 -2 0 637.50 642.60 35.39 o 10 -2 0 195.02 173.36 18.75 o 11 -2 0 10.54 12.54 15.14 o 12 -2 0 5.94 18.65 29.79 o 1 -1 0 1676.29 1465.66 36.24 o 2 -1 0 3549.26 3564.54 106.63 o 3 -1 0 33.39 28.66 3.35 o 4 -1 0 4.83 5.31 3.25 o 5 -1 0 1275.66 1247.66 32.27 o 6 -1 0 1534.31 1599.85 44.81 o 7 -1 0 104.27 98.75 8.16 o 8 -1 0 20.39 25.49 6.45 o 9 -1 0 523.91 536.18 29.75 o 10 -1 0 114.46 88.28 17.21 o 11 -1 0 71.98 81.08 16.53 o 12 -1 0 26.39 24.27 26.17 o 2 0 0 46.98 50.92 14.18 o 3 0 0 3.84 4.53 2.45 o 4 0 0 1857.67 1731.80 44.90 o 5 0 0 231.32 257.63 9.66 o 6 0 0 133.03 120.39 8.11 o 7 0 0 67.38 63.58 7.14 o 8 0 0 516.97 550.86 31.82 o 9 0 0 466.52 482.58 24.99 o 10 0 0 52.47 64.77 11.72 o 11 0 0 147.01 151.39 17.29 o 12 0 0 70.13 72.82 27.08 o 1 1 0 1608.04 1374.97 41.29 o 2 1 0 3485.36 3533.04 81.98 o 3 1 0 38.87 38.51 2.58 o 4 1 0 7.02 2.04 3.13 o 5 1 0 1273.71 1271.07 32.48 o 6 1 0 1526.05 1611.68 40.96 o 7 1 0 114.55 131.55 8.22 o 8 1 0 18.46 19.04 7.06 o 9 1 0 529.22 623.11 26.99 o 10 1 0 115.19 110.28 12.01 o 11 1 0 72.66 65.37 13.07 o 12 1 0 26.07 21.58 20.50 o 0 2 0 3830.70 3714.33 128.16 o 1 2 0 5691.76 5631.01 138.70 o 2 2 0 1346.47 1284.66 34.70 o 3 2 0 2159.19 2047.88 46.01 o 4 2 0 14.60 6.24 3.25 o 5 2 0 534.90 569.55 17.62 o 6 2 0 153.18 161.20 6.56 o 7 2 0 774.58 807.69 23.54 o 8 2 0 451.06 477.61 19.34 o 9 2 0 641.73 684.40 31.12 o 10 2 0 184.99 187.48 26.06 o 11 2 0 11.62 21.05 14.78 o 12 2 0 5.51 27.56 18.77 o 1 3 0 2273.10 2173.70 53.68 o 2 3 0 362.44 344.56 11.16 o 3 3 0 772.83 750.46 21.22 o 4 3 0 1896.02 1936.07 47.01 o 5 3 0 413.36 441.62 11.54 o 6 3 0 1458.17 1611.19 43.99 o 7 3 0 72.53 52.67 6.96 o 8 3 0 58.31 51.80 7.45 o 9 3 0 338.29 341.06 21.11 o 10 3 0 20.26 19.76 9.93 o 11 3 0 80.36 119.79 29.12 o 12 3 0 1.13 -9.09 18.69 o 0 4 0 5524.68 5528.22 164.85 o 1 4 0 5229.29 5233.06 123.39 o 2 4 0 400.70 381.06 13.23 o 3 4 0 1394.69 1422.41 44.30 o 4 4 0 313.83 328.58 10.66 o 5 4 0 893.17 944.51 26.22 o 6 4 0 51.86 41.33 6.20 o 7 4 0 800.94 844.78 32.67 o 8 4 0 662.61 701.80 32.24 o 9 4 0 12.40 13.71 8.86 o 10 4 0 21.45 -2.54 9.77 o 11 4 0 83.41 98.75 20.44 o 12 4 0 64.05 38.26 27.87 o 1 5 0 2935.34 3068.95 75.47 o 2 5 0 42.67 59.70 5.49 o 3 5 0 698.23 641.65 18.06 o 4 5 0 785.86 761.09 22.60 o 5 5 0 494.89 514.04 19.86 o 6 5 0 174.59 163.42 9.92 o 7 5 0 1035.57 1221.51 51.80 o 8 5 0 306.46 314.16 19.18 o 9 5 0 7.08 1.57 9.42 o 10 5 0 43.94 53.60 31.79 o 11 5 0 100.38 71.15 21.29 o 0 6 0 1778.99 1854.40 61.72 o 1 6 0 1366.89 1537.46 39.11 o 2 6 0 2195.03 2249.47 53.90 o 3 6 0 159.66 153.24 8.64 o 4 6 0 255.98 276.19 12.44 o 5 6 0 122.92 125.09 8.96 o 6 6 0 695.75 730.66 31.18 o 7 6 0 38.49 48.27 9.52 o 8 6 0 69.35 59.11 10.80 o 9 6 0 109.09 111.73 13.74 o 10 6 0 91.75 71.96 22.44 o 11 6 0 25.21 59.41 44.60 o 1 7 0 212.23 181.32 9.77 o 2 7 0 221.57 236.04 11.74 o 3 7 0 304.16 307.68 15.02 o 4 7 0 115.71 96.94 9.73 o 5 7 0 17.38 13.38 6.37 o 6 7 0 284.52 260.39 17.58 o 7 7 0 36.06 29.24 11.83 o 8 7 0 601.17 640.23 46.97 o 9 7 0 132.63 133.04 23.86 o 10 7 0 47.80 41.27 19.46 o 0 8 0 665.35 768.67 37.43 o 1 8 0 924.44 929.05 39.36 o 2 8 0 132.98 144.38 10.42 o 3 8 0 202.88 188.59 12.83 o 4 8 0 8.12 5.18 6.60 o 5 8 0 966.74 1069.93 53.12 o 6 8 0 396.55 403.56 26.59 o 7 8 0 116.52 121.36 16.59 o 8 8 0 81.87 84.16 18.29 o 9 8 0 48.27 59.43 20.67 o 10 8 0 48.26 17.32 22.84 o 1 9 0 671.82 679.58 31.68 o 2 9 0 310.15 316.61 19.08 o 3 9 0 35.46 25.14 8.45 o 4 9 0 278.07 273.33 19.84 o 5 9 0 129.45 144.68 16.67 o 6 9 0 292.44 302.58 29.09 o 7 9 0 28.29 21.33 16.43 o 8 9 0 47.49 58.39 24.86 o 9 9 0 12.94 -17.14 20.87 o 0 10 0 1421.10 1652.96 151.37 o 1 10 0 205.00 224.11 17.53 o 2 10 0 25.15 13.47 8.14 o 3 10 0 25.59 14.51 8.85 o 4 10 0 364.92 367.77 34.24 o 5 10 0 113.36 91.68 16.85 o 6 10 0 82.80 88.09 20.45 o 7 10 0 85.31 74.93 18.42 o 8 10 0 41.47 40.01 34.60 o 1 11 0 495.88 514.36 37.79 o 2 11 0 108.36 87.27 28.35 o 3 11 0 21.69 25.66 14.75 o 4 11 0 60.52 45.99 17.64 o 5 11 0 85.66 90.69 41.35 o 6 11 0 68.27 58.49 20.94 o 7 11 0 14.10 9.24 26.89 o 0 12 0 294.04 289.08 50.04 o 1 12 0 40.40 6.68 23.14 o 2 12 0 137.48 125.12 25.33 o 3 12 0 28.14 45.03 20.90 o 4 12 0 5.34 -2.96 17.64 o 5 12 0 17.19 -26.48 29.16 o 1 13 0 30.32 5.07 18.31 o 2 13 0 104.99 127.13 28.45 o -2 -13 1 14.08 6.53 19.77 o -1 -13 1 19.94 6.24 19.02 o 0 -13 1 139.31 142.70 28.33 o 1 -13 1 155.62 147.35 32.67 o 2 -13 1 35.19 19.72 20.58 o -5 -12 1 59.98 57.56 32.33 o -4 -12 1 10.26 30.47 19.97 o -3 -12 1 53.62 55.57 20.97 o -2 -12 1 83.63 81.41 21.88 o -1 -12 1 132.01 154.94 24.51 o 0 -12 1 26.54 26.54 13.40 o 1 -12 1 104.98 49.10 35.24 o 2 -12 1 135.09 153.56 24.87 o 3 -12 1 64.36 58.19 25.90 o 4 -12 1 97.07 101.68 44.07 o 5 -12 1 26.70 18.83 26.54 o -7 -11 1 4.55 -0.91 23.18 o -6 -11 1 10.88 6.62 14.72 o -5 -11 1 120.05 120.33 23.47 o -4 -11 1 362.15 390.22 48.47 o -3 -11 1 47.64 27.29 20.47 o -2 -11 1 24.29 21.98 16.42 o -1 -11 1 50.30 41.21 13.77 o 0 -11 1 12.79 14.09 11.29 o 1 -11 1 16.41 3.26 12.18 o 2 -11 1 29.20 21.42 13.44 o 3 -11 1 65.68 60.41 25.54 o 4 -11 1 70.42 70.46 18.35 o 5 -11 1 4.91 17.56 22.84 o 6 -11 1 72.31 66.82 23.75 o 7 -11 1 40.21 19.25 22.43 o -8 -10 1 18.46 8.58 21.17 o -7 -10 1 50.60 15.83 17.32 o -6 -10 1 156.24 188.88 61.97 o -5 -10 1 285.11 308.63 36.62 o -4 -10 1 101.65 90.41 11.09 o -3 -10 1 52.44 40.13 14.68 o -2 -10 1 128.40 136.87 14.37 o -1 -10 1 452.51 514.24 26.16 o 0 -10 1 95.05 105.01 12.47 o 1 -10 1 292.30 279.47 20.17 o 2 -10 1 175.60 158.56 16.37 o 3 -10 1 260.59 294.47 25.00 o 4 -10 1 4.54 -0.44 6.90 o 5 -10 1 17.36 32.82 15.11 o 6 -10 1 29.24 37.71 16.36 o 7 -10 1 38.01 28.34 23.68 o 8 -10 1 80.11 70.15 28.69 o -9 -9 1 20.85 23.42 21.19 o -8 -9 1 24.98 27.00 23.05 o -7 -9 1 202.98 209.72 31.10 o -6 -9 1 239.33 268.82 30.89 o -5 -9 1 220.64 190.51 23.52 o -4 -9 1 120.14 100.34 8.78 o -3 -9 1 3.18 -2.19 6.94 o -2 -9 1 153.50 154.02 15.17 o -1 -9 1 100.50 91.87 9.91 o 0 -9 1 1226.12 1261.90 52.34 o 1 -9 1 196.27 197.23 14.79 o 2 -9 1 269.66 270.70 16.66 o 3 -9 1 28.58 14.18 8.08 o 4 -9 1 13.60 14.25 5.38 o 5 -9 1 91.40 87.67 14.05 o 6 -9 1 16.68 15.57 12.66 o 7 -9 1 107.76 91.71 16.23 o 8 -9 1 23.12 17.05 17.51 o 9 -9 1 37.37 32.51 24.45 o -10 -8 1 106.88 78.74 24.95 o -9 -8 1 5.92 -6.29 14.49 o -8 -8 1 68.03 54.74 17.93 o -7 -8 1 58.13 50.33 7.42 o -6 -8 1 67.32 88.46 12.06 o -5 -8 1 23.04 20.72 8.59 o -4 -8 1 317.55 321.32 13.42 o -3 -8 1 87.09 71.30 9.47 o -2 -8 1 296.58 325.05 16.41 o -1 -8 1 671.61 712.18 27.00 o 0 -8 1 1170.80 1266.99 42.12 o 1 -8 1 477.96 498.96 20.91 o 2 -8 1 351.94 362.00 19.00 o 3 -8 1 91.28 95.80 8.96 o 4 -8 1 471.48 500.94 19.39 o 5 -8 1 89.99 88.56 13.46 o 6 -8 1 191.40 212.39 16.40 o 7 -8 1 78.05 60.94 9.90 o 8 -8 1 63.00 52.28 15.27 o 9 -8 1 141.97 175.57 30.67 o 10 -8 1 74.65 63.18 22.68 o -10 -7 1 44.15 41.20 20.62 o -9 -7 1 38.06 45.69 29.43 o -8 -7 1 106.10 110.70 24.82 o -7 -7 1 138.25 142.55 26.40 o -6 -7 1 19.20 10.81 4.38 o -5 -7 1 78.15 66.14 8.49 o -4 -7 1 228.05 235.82 9.70 o -3 -7 1 733.13 787.70 27.85 o -2 -7 1 652.25 692.85 27.07 o -1 -7 1 71.23 72.88 6.57 o 0 -7 1 477.10 476.17 17.05 o 1 -7 1 56.83 45.28 8.43 o 2 -7 1 182.08 181.88 9.94 o 3 -7 1 207.87 210.80 9.26 o 4 -7 1 443.59 489.52 18.34 o 5 -7 1 323.92 321.13 18.28 o 6 -7 1 229.37 217.08 12.27 o 7 -7 1 361.95 383.04 24.04 o 8 -7 1 165.97 167.33 20.19 o 9 -7 1 345.36 390.06 42.51 o 10 -7 1 33.70 42.31 19.24 o -11 -6 1 144.69 135.34 31.63 o -10 -6 1 76.97 75.44 18.63 o -9 -6 1 107.40 91.72 15.65 o -8 -6 1 135.07 131.51 14.86 o -7 -6 1 1080.98 1232.94 57.96 o -6 -6 1 2.93 -0.27 11.25 o -5 -6 1 780.92 843.41 30.98 o -4 -6 1 285.92 310.86 10.07 o -3 -6 1 935.03 995.66 29.40 o -2 -6 1 495.61 489.34 16.79 o -1 -6 1 1901.96 2013.45 51.99 o 0 -6 1 234.09 243.31 9.94 o 1 -6 1 1085.48 1195.40 35.81 o 2 -6 1 296.81 309.30 11.09 o 3 -6 1 193.05 215.15 8.78 o 4 -6 1 74.93 75.73 4.68 o 5 -6 1 164.63 164.35 10.60 o 6 -6 1 14.43 15.91 4.34 o 7 -6 1 326.89 333.47 23.09 o 8 -6 1 22.06 12.25 11.77 o 9 -6 1 4.29 13.64 12.21 o 10 -6 1 212.92 204.83 31.88 o 11 -6 1 2.05 -8.33 25.81 o -11 -5 1 20.16 -0.81 16.70 o -10 -5 1 42.33 24.70 13.05 o -9 -5 1 137.64 141.24 37.60 o -8 -5 1 285.98 300.04 17.59 o -7 -5 1 182.99 189.38 11.63 o -6 -5 1 1132.71 1115.35 41.96 o -5 -5 1 127.60 129.70 6.14 o -4 -5 1 203.60 178.11 9.58 o -3 -5 1 619.23 650.70 19.07 o -2 -5 1 165.06 146.70 6.65 o -1 -5 1 17.48 13.83 3.60 o 0 -5 1 1959.67 2160.43 60.75 o 1 -5 1 2424.53 2421.49 60.30 o 2 -5 1 813.60 761.10 24.95 o 3 -5 1 1669.05 1766.62 42.86 o 4 -5 1 340.30 320.11 11.75 o 5 -5 1 570.98 579.75 18.94 o 6 -5 1 823.21 831.78 32.53 o 7 -5 1 381.25 393.53 26.43 o 8 -5 1 33.45 8.38 8.63 o 9 -5 1 39.29 53.34 12.19 o 10 -5 1 26.58 25.22 14.07 o 11 -5 1 20.31 52.19 17.34 o -12 -4 1 188.86 184.81 55.14 o -11 -4 1 6.22 -18.11 13.75 o -10 -4 1 10.73 -0.17 13.05 o -9 -4 1 79.49 72.00 10.57 o -8 -4 1 1155.17 1155.01 50.98 o -7 -4 1 885.96 924.66 35.42 o -6 -4 1 75.44 47.77 7.63 o -5 -4 1 198.34 203.09 14.47 o -4 -4 1 963.52 924.16 25.18 o -3 -4 1 2112.31 2191.72 55.62 o -2 -4 1 1320.42 1209.43 31.00 o -1 -4 1 709.18 661.96 18.87 o 0 -4 1 1615.04 1516.16 38.12 o 1 -4 1 1051.90 1002.80 24.74 o 2 -4 1 877.81 905.82 23.64 o 3 -4 1 201.22 223.28 7.43 o 4 -4 1 44.59 43.55 4.25 o 5 -4 1 64.46 74.74 5.14 o 6 -4 1 93.94 105.36 8.13 o 7 -4 1 338.93 335.27 15.66 o 8 -4 1 142.91 125.93 12.08 o 9 -4 1 133.80 116.94 15.05 o 10 -4 1 3.63 3.87 12.76 o 11 -4 1 89.68 102.95 21.35 o 12 -4 1 65.81 67.71 30.58 o -12 -3 1 7.06 0.01 14.56 o -11 -3 1 22.31 20.99 22.78 o -10 -3 1 61.19 84.40 26.76 o -9 -3 1 279.35 293.80 19.30 o -8 -3 1 17.41 11.25 6.13 o -7 -3 1 352.02 328.83 16.11 o -6 -3 1 351.81 351.82 21.05 o -5 -3 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2565.69 64.04 o 4 -2 1 57.01 51.06 6.48 o 5 -2 1 1496.96 1566.45 38.04 o 6 -2 1 68.41 65.97 5.79 o 7 -2 1 123.37 133.81 8.27 o 8 -2 1 35.30 30.96 7.23 o 9 -2 1 86.93 104.74 14.21 o 10 -2 1 227.05 234.67 21.61 o 11 -2 1 280.03 306.21 36.23 o 12 -2 1 119.25 174.38 43.84 o -12 -1 1 58.55 54.16 33.60 o -11 -1 1 22.34 28.89 18.66 o -10 -1 1 65.35 69.51 22.64 o -9 -1 1 404.15 405.45 21.21 o -8 -1 1 232.83 219.33 12.52 o -7 -1 1 1230.76 1182.79 41.24 o -6 -1 1 947.20 1049.20 28.85 o -5 -1 1 1381.10 1451.45 39.97 o -4 -1 1 1896.35 1879.68 44.48 o -3 -1 1 2635.53 2452.23 68.48 o -2 -1 1 2968.76 2933.78 86.99 o -1 -1 1 1907.96 1661.85 44.16 o 1 -1 1 1447.12 1291.85 32.97 o 2 -1 1 12981.91 13517.23 361.14 o 3 -1 1 12.61 20.75 6.82 o 4 -1 1 1414.19 1424.32 39.52 o 5 -1 1 178.48 189.63 8.56 o 6 -1 1 363.90 365.74 16.19 o 7 -1 1 164.50 158.37 9.25 o 8 -1 1 528.64 524.06 23.50 o 9 -1 1 348.10 368.79 20.88 o 10 -1 1 31.54 15.78 12.83 o 11 -1 1 51.32 26.89 13.84 o 12 -1 1 56.42 71.91 31.79 o -12 0 1 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228.66 228.77 14.31 o -5 -6 2 1669.87 1723.98 61.21 o -4 -6 2 726.77 771.80 19.52 o -3 -6 2 250.86 270.44 10.25 o -2 -6 2 736.65 753.45 21.81 o -1 -6 2 62.54 67.50 5.54 o 0 -6 2 496.83 506.23 17.75 o 1 -6 2 852.19 894.19 26.00 o 2 -6 2 692.97 701.56 21.92 o 3 -6 2 855.68 896.89 24.85 o 4 -6 2 240.54 258.66 11.53 o 5 -6 2 2.43 1.10 4.85 o 6 -6 2 61.12 47.21 5.95 o 7 -6 2 52.16 78.19 14.05 o 8 -6 2 225.69 258.78 23.54 o 9 -6 2 156.99 140.26 21.27 o 10 -6 2 288.92 318.54 46.81 o 11 -6 2 7.77 24.08 25.30 o -12 -5 2 3.12 28.04 24.13 o -11 -5 2 39.49 35.54 13.70 o -10 -5 2 56.86 55.27 17.77 o -9 -5 2 48.55 39.79 13.10 o -8 -5 2 156.58 144.05 11.93 o -7 -5 2 379.11 384.99 20.29 o -6 -5 2 865.23 888.03 38.64 o -5 -5 2 1612.08 1780.31 49.99 o -4 -5 2 1180.99 1253.72 33.91 o -3 -5 2 920.46 952.73 25.56 o -2 -5 2 531.80 562.74 16.76 o -1 -5 2 160.37 182.68 7.13 o 0 -5 2 342.67 288.88 9.98 o 1 -5 2 1995.13 2025.39 48.36 o 2 -5 2 2405.82 2313.29 62.88 o 3 -5 2 660.29 713.81 18.19 o 4 -5 2 285.81 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