#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:38:10 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180793 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/24/2012440.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012440_Fobs loop_ _publ_author_name 'Janczak, Jan' 'Idemori, Ynara Marina' _publ_section_title ; Tetrakis[phthalocyaninato(2--)antimony(III)] hexadecaiodotetraantimony(III) ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m23 _journal_page_last m25 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 88.590 _cell_angle_beta 62.540 _cell_angle_gamma 69.160 _cell_length_a 15.9630 _cell_length_b 16.0510 _cell_length_c 16.5520 _exptl_crystal_F_000 2312.00 _reflns_d_resolution_high 0.7774 _cod_data_source_file na1539Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' (SbPc)SbI4 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 830.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 6721.21 7200.52 120.67 o 4 0 0 6535.37 6604.43 196.02 o 5 0 0 57775.13 56185.68 271.20 o 6 0 0 3101.89 2959.07 193.44 o 7 0 0 1880.93 1996.51 81.06 o 8 0 0 43894.04 43157.13 215.78 o 9 0 0 106537.01 107049.77 303.97 o 10 0 0 6496.02 6483.66 273.99 o 11 0 0 69.39 61.17 150.64 o 12 0 0 408.75 148.72 205.53 o 13 0 0 10120.99 10175.46 289.37 o 14 0 0 967.12 1218.94 231.59 o 15 0 0 77.06 40.77 274.03 o 16 0 0 596.63 547.35 222.29 o -16 1 0 2106.26 2544.72 320.65 o -14 1 0 3500.55 2885.83 308.67 o -13 1 0 4057.71 4461.89 329.53 o -12 1 0 9551.47 9563.23 456.02 o -11 1 0 1790.49 1618.30 194.10 o -10 1 0 2039.61 2000.22 110.24 o -9 1 0 12593.08 12971.27 175.25 o -8 1 0 46053.56 49597.32 283.81 o -7 1 0 9021.10 8468.22 140.33 o -6 1 0 1070.34 1145.35 70.69 o -5 1 0 13092.89 12760.11 150.73 o -4 1 0 66436.49 71966.01 867.87 o -3 1 0 497.50 575.90 61.72 o -2 1 0 8667.62 9060.45 107.86 o 4 1 0 2345.42 2191.83 217.28 o 5 1 0 2718.95 2728.83 404.95 o 6 1 0 4142.44 4492.20 341.46 o 7 1 0 782.45 744.63 111.98 o 8 1 0 3552.20 3383.33 89.60 o 9 1 0 32394.74 32211.83 238.03 o 10 1 0 753.90 899.40 168.36 o 11 1 0 25334.50 25336.61 609.51 o 12 1 0 69.82 295.64 162.60 o 14 1 0 232.10 97.76 205.12 o 15 1 0 1500.29 1573.78 263.25 o 16 1 0 1.95 323.20 236.23 o 17 1 0 708.93 995.01 277.13 o -16 2 0 115.05 226.97 356.16 o -15 2 0 58.44 148.54 192.33 o -14 2 0 874.30 673.34 185.31 o -13 2 0 946.38 996.63 238.14 o -12 2 0 4989.98 5251.75 333.34 o -11 2 0 15539.87 17460.99 519.76 o -10 2 0 898.63 645.42 100.74 o -9 2 0 40.25 33.26 303.44 o -8 2 0 8032.07 7876.32 244.89 o -7 2 0 12560.61 13165.60 169.14 o -6 2 0 6620.78 6982.55 106.63 o -5 2 0 3820.70 3993.89 76.74 o -4 2 0 7212.77 7033.05 95.74 o -3 2 0 6482.50 6826.46 145.83 o -2 2 0 2518.20 2546.26 80.65 o -1 2 0 7802.14 8576.56 110.49 o 0 2 0 878.35 819.31 45.86 o 4 2 0 38499.41 38081.10 367.52 o 5 2 0 8519.21 8785.20 710.91 o 6 2 0 3988.62 3783.73 281.47 o 7 2 0 3305.73 3194.99 170.16 o 8 2 0 104.46 240.23 106.98 o 9 2 0 3624.90 3653.19 201.81 o 10 2 0 4268.22 4512.39 255.11 o 11 2 0 8834.34 9151.51 360.65 o 12 2 0 3034.15 3325.55 272.77 o 13 2 0 11881.15 12404.03 462.14 o 14 2 0 481.10 382.30 200.50 o 15 2 0 241.18 35.42 269.50 o 16 2 0 36.49 165.34 190.67 o 17 2 0 1122.79 810.97 264.98 o -15 3 0 975.00 1039.82 247.13 o -14 3 0 199.57 63.30 272.26 o -13 3 0 0.70 158.30 265.32 o -12 3 0 515.31 364.56 181.31 o -11 3 0 17585.81 17655.34 554.52 o -9 3 0 6495.94 6603.81 178.44 o -8 3 0 5120.37 5506.04 186.25 o -7 3 0 2533.38 2427.24 114.63 o -6 3 0 854.66 735.44 53.01 o -5 3 0 2756.08 2803.13 100.78 o -4 3 0 2710.04 2850.56 72.18 o -3 3 0 0.31 112.86 49.62 o -2 3 0 202764.36 201269.91 363.90 o -1 3 0 2805.29 2831.78 88.25 o 0 3 0 8938.41 9155.46 284.95 o 1 3 0 571.30 625.43 48.11 o 2 3 0 23645.33 25480.14 207.38 o 4 3 0 1735.96 1815.34 84.82 o 5 3 0 14355.21 14261.73 185.57 o 6 3 0 56.15 182.54 76.07 o 7 3 0 19284.07 18360.13 267.35 o 8 3 0 59340.33 59211.40 206.97 o 9 3 0 5092.25 4942.97 115.97 o 10 3 0 2618.72 2402.14 244.90 o 11 3 0 14416.38 14335.91 462.66 o 12 3 0 94.73 156.55 163.15 o 13 3 0 21102.13 22418.39 290.96 o 14 3 0 3650.34 3764.42 327.06 o 15 3 0 27.27 151.09 165.15 o 16 3 0 612.71 673.10 245.00 o 17 3 0 1159.67 1301.91 266.02 o -15 4 0 45.32 338.73 250.38 o -14 4 0 272.48 176.67 270.23 o -11 4 0 750.09 923.81 221.57 o -10 4 0 7211.48 7420.12 409.35 o -9 4 0 3441.23 3616.49 166.50 o -8 4 0 11223.32 12028.32 421.38 o -7 4 0 13010.19 12931.61 277.76 o -6 4 0 711.13 734.91 59.22 o -5 4 0 35797.61 38244.69 239.56 o -4 4 0 39.92 93.54 50.52 o -3 4 0 2962.81 3151.92 71.44 o -2 4 0 17049.83 18011.67 214.41 o -1 4 0 46549.18 49377.20 430.34 o 0 4 0 28840.23 30332.75 374.70 o 1 4 0 125222.76 128257.77 423.49 o 2 4 0 200882.64 201947.34 461.80 o 3 4 0 8931.14 9040.18 215.69 o 4 4 0 1941.83 2082.65 57.86 o 5 4 0 16975.32 17041.88 140.59 o 6 4 0 36834.90 36161.17 314.08 o 7 4 0 2.87 11.56 87.23 o 8 4 0 1416.60 1317.34 70.20 o 9 4 0 2580.63 2459.64 77.62 o 10 4 0 18076.78 17878.76 304.47 o 11 4 0 24245.61 25149.04 389.40 o 12 4 0 881.37 825.13 200.89 o 13 4 0 1364.29 1384.26 202.20 o 14 4 0 6420.81 7091.58 392.15 o 15 4 0 6049.00 6603.32 396.50 o 16 4 0 637.36 509.46 215.21 o 17 4 0 653.73 523.44 292.04 o -14 5 0 20.44 37.51 427.77 o -13 5 0 161.69 242.14 205.53 o -12 5 0 3619.42 3804.25 329.33 o -11 5 0 4652.18 4762.06 241.20 o -10 5 0 10285.28 10991.79 284.65 o -9 5 0 10688.74 11555.72 256.11 o -8 5 0 4238.82 4317.17 123.02 o -7 5 0 74391.05 76053.12 490.00 o -6 5 0 51991.32 55176.67 376.99 o -5 5 0 32764.06 35461.71 287.31 o -4 5 0 4345.71 4324.29 100.36 o -3 5 0 76836.59 79745.97 220.26 o -2 5 0 187.10 220.57 57.82 o -1 5 0 11191.08 11567.74 167.80 o 0 5 0 93.62 68.80 79.34 o 1 5 0 131023.63 135915.59 213.85 o 2 5 0 598608.38 600890.50 407.98 o 3 5 0 53161.46 56791.05 183.28 o 4 5 0 12273.58 12690.86 336.28 o 5 5 0 32.67 99.11 34.54 o 6 5 0 0.05 87.39 40.06 o 7 5 0 12502.09 12140.64 711.59 o 8 5 0 80.69 126.95 57.35 o 9 5 0 1043.94 925.31 59.63 o 10 5 0 33570.85 34509.64 195.44 o 11 5 0 57568.73 60214.56 290.69 o 12 5 0 77.70 182.60 113.34 o 13 5 0 6119.02 6118.67 955.05 o 14 5 0 119.42 57.76 379.79 o 15 5 0 3023.72 2949.85 297.54 o 16 5 0 322.19 756.30 242.64 o 18 5 0 195.15 210.18 318.75 o -13 6 0 1409.81 942.51 232.35 o -12 6 0 1358.72 1569.42 262.31 o -11 6 0 5480.75 5549.21 244.22 o -10 6 0 7873.23 9099.31 468.14 o -9 6 0 1832.11 1903.86 120.27 o -8 6 0 4842.21 4832.90 136.71 o -7 6 0 25.34 98.50 86.48 o -6 6 0 43244.66 45669.45 1145.76 o -5 6 0 4441.69 4585.17 96.35 o -4 6 0 10303.68 9564.95 179.19 o -3 6 0 21965.20 21447.49 179.17 o -2 6 0 21525.79 22277.88 237.91 o -1 6 0 4970.77 4930.25 130.04 o 0 6 0 7861.01 8252.39 164.29 o 1 6 0 16359.57 17580.77 222.33 o 2 6 0 30711.00 31849.24 173.36 o 3 6 0 32633.00 32498.24 175.55 o 4 6 0 45848.14 45705.42 212.00 o 5 6 0 22748.73 22736.20 135.93 o 6 6 0 68360.56 68950.08 174.92 o 7 6 0 625.20 498.02 52.37 o 8 6 0 8429.78 8210.19 137.86 o 9 6 0 696.17 738.59 71.28 o 10 6 0 701.35 687.76 107.09 o 11 6 0 15708.44 15074.02 1274.59 o 12 6 0 1339.68 1470.10 132.63 o 13 6 0 10845.54 10655.42 663.75 o 14 6 0 1145.39 1212.29 151.28 o 16 6 0 47.20 139.61 175.59 o 17 6 0 27.63 24.02 269.40 o 18 6 0 566.79 942.30 271.85 o -10 7 0 7218.85 7027.79 531.97 o -9 7 0 718.50 584.56 245.21 o -8 7 0 9353.21 9359.25 289.25 o -7 7 0 1553.26 1500.22 87.08 o -6 7 0 2047.41 1951.21 107.78 o -5 7 0 8394.36 8858.73 149.89 o -4 7 0 3818.61 3810.90 86.01 o -3 7 0 1912.65 2111.44 78.14 o -2 7 0 1858.31 1751.65 71.49 o -1 7 0 35.56 27.21 60.71 o 0 7 0 2520.52 2264.36 109.63 o 1 7 0 65.08 111.34 49.79 o 2 7 0 25260.45 26269.05 212.37 o 3 7 0 25607.50 25556.72 209.62 o 4 7 0 2893.40 2876.33 72.65 o 5 7 0 566.78 507.17 57.33 o 6 7 0 2172.76 2323.30 54.67 o 7 7 0 13.38 122.34 52.54 o 8 7 0 23681.24 24193.20 297.12 o 9 7 0 5499.26 5697.61 300.14 o 10 7 0 81.08 168.77 102.82 o 11 7 0 3685.80 3814.46 347.88 o 12 7 0 1909.97 2095.55 151.04 o 13 7 0 252.22 117.99 120.02 o 14 7 0 5798.51 5749.79 312.59 o 15 7 0 2298.76 2304.51 183.80 o 16 7 0 614.00 542.62 227.53 o 17 7 0 1997.21 1805.16 212.07 o 18 7 0 0.81 138.37 207.43 o -11 8 0 271.85 242.06 106.87 o -10 8 0 8.86 181.27 110.41 o -9 8 0 9821.49 10735.47 430.29 o -8 8 0 14.85 82.70 211.87 o -7 8 0 176.99 176.50 88.20 o -6 8 0 2854.30 2773.50 212.98 o -5 8 0 648.80 579.12 82.11 o -4 8 0 413.39 391.51 82.65 o -3 8 0 1261.74 1290.52 82.85 o -2 8 0 1585.88 1497.77 76.66 o -1 8 0 15771.99 17020.26 162.00 o 0 8 0 100429.03 105171.78 1234.66 o 1 8 0 41227.55 44866.31 594.56 o 2 8 0 15318.25 16688.01 242.32 o 3 8 0 41541.82 44852.29 614.72 o 4 8 0 37407.54 39741.84 325.72 o 5 8 0 2044.39 2264.11 99.03 o 6 8 0 20295.40 20189.35 156.26 o 7 8 0 27627.93 29306.19 983.84 o 8 8 0 1877.44 2026.55 106.57 o 9 8 0 14223.55 14465.07 552.97 o 10 8 0 37436.02 37508.39 436.73 o 11 8 0 24.84 85.06 116.10 o 12 8 0 2468.89 2725.98 462.87 o 13 8 0 13992.38 14638.17 1402.98 o 14 8 0 51.07 259.54 217.66 o 15 8 0 8867.89 9348.07 588.90 o 16 8 0 1832.31 1641.29 159.83 o 17 8 0 783.39 690.84 235.04 o 18 8 0 209.97 382.57 219.51 o -11 9 0 913.82 901.63 147.93 o -10 9 0 82.33 5.24 234.95 o -9 9 0 456.42 326.43 142.75 o -8 9 0 14138.28 15149.96 355.70 o -7 9 0 1133.60 1037.01 115.44 o -6 9 0 10710.50 11130.04 472.12 o -5 9 0 5796.60 5426.86 204.38 o -4 9 0 1959.50 1874.19 94.21 o -3 9 0 10374.03 10188.24 527.24 o -2 9 0 3191.21 2932.90 102.13 o -1 9 0 1940.62 1807.73 101.70 o 0 9 0 10057.58 10729.14 146.18 o 1 9 0 19138.49 19484.22 209.34 o 2 9 0 4756.27 5086.42 207.12 o 3 9 0 40385.34 43352.18 587.20 o 4 9 0 17586.90 18563.97 289.90 o 5 9 0 12244.22 12264.16 158.13 o 6 9 0 687.92 743.87 47.74 o 7 9 0 3670.24 3546.42 77.86 o 8 9 0 4437.76 4319.54 209.95 o 9 9 0 1909.85 1543.90 164.81 o 10 9 0 8.34 67.40 86.76 o 11 9 0 60.38 134.43 218.23 o 12 9 0 2601.47 2621.19 150.33 o 13 9 0 2954.33 3375.16 400.10 o 14 9 0 2767.13 2633.49 181.26 o 15 9 0 2406.49 2313.92 170.81 o 16 9 0 3111.74 3068.95 227.00 o 17 9 0 87.36 121.87 169.87 o 18 9 0 2.75 61.19 248.73 o -11 10 0 261.81 490.99 204.78 o -10 10 0 2520.95 2017.21 197.97 o -9 10 0 2121.79 2165.63 199.37 o -8 10 0 9593.76 9742.21 707.64 o -7 10 0 11690.12 11644.79 335.74 o -5 10 0 32197.41 33720.49 289.12 o -4 10 0 23956.95 24038.69 266.43 o -3 10 0 9114.38 8896.01 416.71 o -2 10 0 3289.86 3163.94 148.48 o -1 10 0 20292.30 19494.24 223.10 o 0 10 0 2162.16 2339.76 133.96 o 1 10 0 13328.25 13337.62 196.81 o 2 10 0 147.00 137.99 62.53 o 3 10 0 9713.08 9362.50 320.17 o 4 10 0 77254.35 83209.63 534.30 o 5 10 0 7669.14 7808.96 306.50 o 6 10 0 3241.01 3230.57 83.03 o 7 10 0 14273.37 15379.61 221.60 o 8 10 0 4039.43 3675.90 336.53 o 9 10 0 2745.24 2630.65 213.11 o 10 10 0 4123.76 4128.60 260.18 o 11 10 0 92.59 64.17 265.47 o 12 10 0 4990.52 5243.84 212.33 o 13 10 0 4056.29 3933.56 194.43 o 14 10 0 99.11 163.44 120.99 o 15 10 0 4318.51 3791.79 434.51 o 16 10 0 397.25 296.23 147.36 o 17 10 0 796.86 1005.35 242.58 o 18 10 0 0.14 163.11 190.06 o -10 11 0 482.46 286.48 317.22 o -9 11 0 4193.14 4095.33 249.06 o -8 11 0 2719.36 2326.60 203.35 o -7 11 0 159.51 260.17 104.15 o -6 11 0 3752.80 4166.73 152.42 o -5 11 0 617.58 649.73 108.86 o -4 11 0 17093.85 17480.97 1063.62 o -3 11 0 70.71 146.28 89.67 o -2 11 0 10293.90 10162.25 359.92 o -1 11 0 32941.43 35650.32 432.96 o 0 11 0 6155.14 5398.46 223.29 o 1 11 0 1299.47 1222.57 113.78 o 2 11 0 41.05 30.16 89.49 o 3 11 0 35318.86 35284.45 342.09 o 4 11 0 6600.86 6989.62 207.14 o 5 11 0 13889.16 13937.10 209.12 o 6 11 0 13291.47 13346.36 195.96 o 7 11 0 30475.17 32306.79 421.32 o 8 11 0 57347.05 60595.85 551.92 o 9 11 0 3553.49 3582.32 213.28 o 10 11 0 1353.84 1325.00 201.22 o 11 11 0 56.06 143.84 114.72 o 12 11 0 321.86 94.25 285.93 o 13 11 0 5220.95 4936.28 328.08 o 14 11 0 39.73 62.94 239.49 o 15 11 0 590.89 760.12 226.96 o 16 11 0 2630.01 2095.13 321.58 o 17 11 0 83.29 187.32 306.85 o -9 12 0 48.65 252.47 222.29 o -8 12 0 1964.75 1835.07 128.52 o -7 12 0 46.37 142.17 150.98 o -6 12 0 2032.05 1768.95 112.41 o -5 12 0 799.78 565.80 103.33 o -4 12 0 1610.06 1449.26 106.27 o -3 12 0 5066.72 5320.87 192.74 o -2 12 0 211.59 240.30 80.65 o -1 12 0 20.17 138.57 99.98 o 0 12 0 3585.05 3672.72 250.37 o 1 12 0 30.68 28.72 140.78 o 2 12 0 12.55 73.11 88.46 o 3 12 0 509.69 534.24 63.14 o 4 12 0 1571.53 1403.31 82.56 o 5 12 0 38468.45 39962.81 348.70 o 6 12 0 2706.32 2688.66 102.21 o 7 12 0 702.64 719.38 109.48 o 8 12 0 2292.51 2205.27 150.87 o 9 12 0 1383.29 990.76 176.65 o 10 12 0 17376.72 17851.28 508.06 o 11 12 0 854.28 1102.91 226.93 o 12 12 0 2.63 78.28 289.87 o 13 12 0 114.79 160.57 139.97 o 14 12 0 5787.74 5576.58 370.13 o 15 12 0 87.92 108.78 180.73 o 16 12 0 1001.39 793.57 273.71 o -8 13 0 159.30 106.59 211.59 o -7 13 0 4555.23 4288.15 376.68 o -6 13 0 2120.54 1804.71 141.10 o -5 13 0 2534.53 2326.34 156.20 o -4 13 0 969.40 811.97 145.14 o -3 13 0 2646.29 2422.23 126.56 o -2 13 0 2569.21 2543.60 129.81 o -1 13 0 550.99 491.95 87.11 o 0 13 0 35.24 144.01 106.54 o 1 13 0 4734.94 5133.39 211.90 o 2 13 0 15586.90 16453.32 243.05 o 3 13 0 21519.12 21464.04 293.22 o 4 13 0 23039.98 22480.21 295.15 o 5 13 0 13279.47 14241.11 219.72 o 6 13 0 12506.42 12964.24 185.26 o 7 13 0 947.64 898.90 108.50 o 8 13 0 3426.27 3685.28 299.95 o 9 13 0 2214.94 1769.59 194.81 o 10 13 0 184.06 204.23 177.65 o 11 13 0 2383.80 2458.42 261.04 o 12 13 0 12585.67 12405.52 479.79 o 13 13 0 67.56 33.64 282.08 o 14 13 0 4010.28 3816.22 321.25 o 15 13 0 1520.99 1679.66 286.21 o 16 13 0 499.30 640.09 278.07 o 17 13 0 2922.56 2228.01 334.93 o -7 14 0 1093.49 865.67 212.34 o -6 14 0 6280.70 6178.56 236.01 o -5 14 0 1015.59 801.09 111.41 o -4 14 0 3957.31 3631.98 156.75 o -3 14 0 644.72 630.55 111.79 o -2 14 0 2263.26 2561.70 139.88 o -1 14 0 375.25 282.84 72.21 o 0 14 0 848.37 721.08 90.04 o 1 14 0 3108.56 2840.00 146.57 o 2 14 0 1211.12 1032.90 106.58 o 3 14 0 4670.09 4981.21 232.23 o 4 14 0 5221.30 5760.03 248.53 o 5 14 0 56.24 64.39 113.75 o 7 14 0 28.05 116.15 142.97 o 8 14 0 833.69 628.63 136.98 o 9 14 0 12.73 104.81 244.37 o 10 14 0 158.10 146.04 151.48 o 12 14 0 382.17 212.77 194.67 o 13 14 0 1001.67 948.92 232.33 o 14 14 0 671.52 560.44 247.37 o 15 14 0 39.36 226.00 256.83 o 16 14 0 3146.12 2703.93 312.38 o 17 14 0 714.67 399.21 253.80 o -6 15 0 2569.74 2578.00 221.67 o -5 15 0 784.78 498.72 157.38 o -4 15 0 83.92 173.64 142.28 o -3 15 0 4446.82 4184.19 171.69 o -2 15 0 619.91 501.61 107.60 o -1 15 0 1323.32 1278.78 107.45 o 0 15 0 4109.26 3986.20 303.98 o 1 15 0 2615.85 2399.24 131.72 o 2 15 0 579.71 475.58 99.56 o 3 15 0 4587.59 4594.19 221.39 o 4 15 0 544.72 680.43 87.69 o 5 15 0 6.66 44.16 88.14 o 6 15 0 3780.22 3726.56 157.66 o 7 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10 18 263.14 134.48 208.42 o 14 10 18 104.29 321.25 274.82 o 15 10 18 228.87 410.72 253.44 o 10 11 18 603.55 682.55 205.10 o 11 11 18 250.82 75.82 235.84 o 12 11 18 160.57 83.62 281.19 o 14 11 18 580.15 473.29 243.95 o 3 -8 19 414.66 422.51 174.83 o 4 -8 19 5279.44 5482.58 307.80 o 5 -8 19 4171.87 3389.69 355.45 o 3 -7 19 225.62 510.22 349.05 o 4 -7 19 1270.90 1081.28 160.32 o 5 -7 19 3955.01 4140.84 233.21 o 1 -6 19 396.11 477.98 165.68 o 2 -6 19 399.40 386.47 158.68 o 3 -6 19 37.96 324.63 223.81 o 4 -6 19 284.99 180.46 162.24 o 5 -6 19 199.80 310.68 149.46 o 6 -6 19 431.14 502.67 243.36 o 7 -6 19 77.63 209.57 280.94 o 9 -6 19 484.87 296.33 312.37 o 2 -5 19 1929.52 2103.32 239.72 o 3 -5 19 318.15 388.90 198.57 o 4 -5 19 49.67 97.88 240.34 o 5 -5 19 799.05 769.64 158.38 o 6 -5 19 289.93 290.28 241.60 o 7 -5 19 311.15 534.95 252.65 o 8 -5 19 121.02 194.07 267.02 o 9 -5 19 415.28 422.45 208.43 o 10 -5 19 220.58 498.29 265.73 o 1 -4 19 49.62 122.02 222.58 o 2 -4 19 229.54 223.62 150.53 o 3 -4 19 2472.47 2748.31 230.95 o 4 -4 19 62.42 112.37 317.47 o 5 -4 19 2427.31 2954.36 243.01 o 6 -4 19 3382.42 3202.94 287.82 o 7 -4 19 588.01 678.53 284.90 o 8 -4 19 220.94 262.64 280.49 o 9 -4 19 20.28 200.07 328.33 o 10 -4 19 1336.53 1476.38 262.05 o 12 -4 19 609.26 544.78 257.00 o 1 -3 19 369.06 491.22 157.98 o 2 -3 19 631.10 653.62 167.50 o 3 -3 19 428.39 639.66 186.18 o 4 -3 19 809.07 852.03 158.60 o 5 -3 19 262.38 358.27 220.22 o 6 -3 19 7027.51 7165.60 153.23 o 7 -3 19 4714.57 4708.06 224.35 o 8 -3 19 313.71 487.40 226.71 o 10 -3 19 1.69 36.20 253.15 o 12 -3 19 112.24 71.39 286.28 o 13 -3 19 19.84 164.74 301.77 o 14 -3 19 268.39 458.78 252.45 o 1 -2 19 290.65 17.42 337.46 o 2 -2 19 814.18 740.53 157.28 o 3 -2 19 446.71 318.06 164.42 o 5 -2 19 38.61 197.94 221.14 o 6 -2 19 562.29 491.79 158.06 o 7 -2 19 4702.47 4965.62 254.58 o 8 -2 19 473.76 386.42 209.84 o 9 -2 19 319.62 192.07 214.76 o 12 -2 19 5.65 43.17 222.56 o 13 -2 19 224.84 25.04 227.81 o 1 -1 19 566.89 480.99 156.40 o 2 -1 19 59.93 274.42 226.95 o 3 -1 19 492.86 387.84 150.10 o 4 -1 19 121.75 149.55 157.74 o 5 -1 19 9.59 38.89 143.74 o 6 -1 19 17.84 67.65 322.95 o 7 -1 19 226.05 249.66 247.98 o 8 -1 19 1609.61 1198.11 225.66 o 9 -1 19 396.19 248.68 221.18 o 10 -1 19 327.36 341.66 195.05 o 12 -1 19 0.66 247.50 224.74 o 13 -1 19 65.36 258.94 275.95 o 14 -1 19 114.51 422.54 263.71 o 15 -1 19 22.15 169.22 328.56 o 1 0 19 88.03 181.55 195.22 o 2 0 19 12.64 126.07 189.00 o 3 0 19 137.76 276.65 191.71 o 4 0 19 2064.75 2235.85 181.54 o 5 0 19 633.57 507.94 127.60 o 6 0 19 427.27 334.91 123.40 o 7 0 19 1474.28 1854.75 227.04 o 8 0 19 741.22 461.60 265.57 o 9 0 19 933.97 742.11 228.57 o 10 0 19 398.12 186.91 238.40 o 12 0 19 230.59 370.87 256.30 o 13 0 19 878.63 817.51 227.52 o 14 0 19 236.38 288.71 281.58 o 15 0 19 362.01 304.54 320.07 o 2 1 19 450.10 540.91 217.49 o 3 1 19 3.24 148.79 225.79 o 4 1 19 340.95 327.99 142.57 o 5 1 19 2270.47 2426.38 122.54 o 6 1 19 398.87 476.26 130.27 o 7 1 19 2534.69 2687.62 156.83 o 8 1 19 2881.86 3012.91 213.44 o 9 1 19 903.08 934.84 206.75 o 10 1 19 34.26 20.00 201.72 o 11 1 19 176.70 14.45 226.41 o 12 1 19 1215.35 1476.74 216.06 o 13 1 19 53.08 151.08 217.50 o 14 1 19 519.21 364.82 219.87 o 15 1 19 97.92 84.80 224.17 o 16 1 19 1000.83 1299.36 211.54 o 2 2 19 24.00 35.05 226.88 o 3 2 19 1224.04 1086.57 149.55 o 4 2 19 87.49 84.32 71.79 o 5 2 19 605.99 469.14 130.39 o 6 2 19 103.87 228.50 115.96 o 7 2 19 39.82 68.04 143.31 o 8 2 19 4063.12 4187.99 158.58 o 9 2 19 1462.37 1915.60 285.54 o 10 2 19 208.61 177.85 117.42 o 11 2 19 587.71 420.27 198.16 o 12 2 19 60.75 73.99 114.38 o 13 2 19 989.73 990.90 229.23 o 14 2 19 272.14 189.20 169.38 o 15 2 19 42.79 524.30 261.11 o 16 2 19 148.21 645.75 262.57 o 3 3 19 563.67 550.35 157.21 o 4 3 19 1855.83 2216.89 225.28 o 5 3 19 128.92 71.80 172.67 o 7 3 19 322.02 433.64 157.46 o 8 3 19 26.17 137.62 185.60 o 9 3 19 3363.49 3874.85 472.84 o 10 3 19 176.43 44.25 158.33 o 11 3 19 270.63 269.06 135.63 o 12 3 19 1192.93 1321.22 378.10 o 13 3 19 0.00 114.44 307.64 o 14 3 19 85.38 6.96 290.26 o 15 3 19 148.05 238.01 283.09 o 16 3 19 132.39 433.92 295.49 o 3 4 19 941.41 890.12 156.44 o 4 4 19 175.70 127.27 180.30 o 5 4 19 943.11 1143.22 129.67 o 6 4 19 1.47 75.51 222.07 o 7 4 19 0.59 100.87 117.29 o 8 4 19 14.68 194.93 299.50 o 9 4 19 206.89 210.17 148.75 o 10 4 19 1895.72 2031.57 222.97 o 12 4 19 215.43 257.76 142.66 o 13 4 19 75.74 75.02 155.35 o 4 5 19 200.28 62.42 304.15 o 5 5 19 26.46 194.72 211.69 o 6 5 19 1875.66 1927.16 180.57 o 7 5 19 382.03 473.50 140.29 o 8 5 19 1266.12 1316.20 185.25 o 9 5 19 597.70 688.20 210.20 o 10 5 19 750.17 736.83 190.98 o 11 5 19 1057.45 1118.12 139.80 o 12 5 19 73.54 154.02 129.86 o 13 5 19 243.60 282.29 178.11 o 15 5 19 214.92 231.64 264.52 o 16 5 19 202.60 25.82 313.21 o 5 6 19 8.00 76.70 160.21 o 6 6 19 154.19 24.76 226.58 o 7 6 19 1531.16 2089.66 228.33 o 8 6 19 500.24 313.81 209.92 o 9 6 19 2167.71 2735.59 367.84 o 10 6 19 459.93 340.94 150.85 o 11 6 19 588.47 522.12 156.89 o 12 6 19 2.41 150.15 157.17 o 13 6 19 476.04 457.46 142.54 o 14 6 19 596.08 359.10 157.76 o 15 6 19 0.43 23.89 232.76 o 16 6 19 156.32 296.37 324.62 o 6 7 19 0.06 57.95 308.92 o 7 7 19 166.98 223.28 138.55 o 8 7 19 19.11 86.82 218.49 o 9 7 19 26.89 111.36 158.16 o 10 7 19 716.58 1174.25 249.34 o 11 7 19 62.93 93.41 221.22 o 12 7 19 50.30 188.98 224.77 o 13 7 19 1199.40 946.16 151.93 o 14 7 19 101.27 51.84 299.99 o 15 7 19 504.56 166.97 143.85 o 16 7 19 78.66 158.93 158.75 o 8 8 19 27.73 171.08 207.86 o 9 8 19 149.58 84.50 226.46 o 11 8 19 438.83 446.83 299.45 o 13 8 19 125.06 56.27 347.86 o 14 8 19 1390.19 1444.35 192.85 o 9 9 19 209.60 348.35 253.19 o 10 9 19 13.67 286.83 232.65 o 11 9 19 577.96 294.27 269.38 o 12 9 19 814.36 681.89 301.84 o 14 9 19 54.85 144.72 211.21 o 5 -6 20 19.16 64.90 308.50 o 4 -5 20 0.28 78.51 207.92 o 5 -5 20 57.84 229.26 214.29 o 6 -5 20 135.65 299.69 155.87 o 3 -4 20 75.30 172.18 164.49 o 4 -4 20 262.38 693.29 224.02 o 5 -4 20 98.79 528.18 237.92 o 6 -4 20 474.76 234.47 152.44 o 7 -4 20 440.75 278.96 228.13 o 10 -4 20 116.31 546.46 217.09 o 3 -3 20 223.61 193.81 150.36 o 4 -3 20 109.59 285.04 159.13 o 5 -3 20 1.98 119.36 251.04 o 6 -3 20 165.40 237.51 194.21 o 7 -3 20 863.04 357.24 248.16 o 3 -2 20 118.48 232.62 202.04 o 4 -2 20 170.57 379.49 152.96 o 5 -2 20 113.85 81.31 189.12 o 6 -2 20 164.83 401.04 222.49 o 7 -2 20 141.63 254.42 219.23 o 8 -2 20 512.80 333.15 212.97 o 9 -2 20 394.71 71.44 224.36 o 13 -2 20 61.37 176.91 208.92 o 3 -1 20 0.15 274.04 150.51 o 4 -1 20 201.63 137.43 155.42 o 5 -1 20 235.00 543.58 144.58 o 6 -1 20 0.32 75.96 150.72 o 7 -1 20 197.86 309.33 156.56 o 9 -1 20 606.80 620.39 210.27 o 10 -1 20 550.84 346.54 274.26 o 13 -1 20 4.62 100.70 241.99 o 14 -1 20 8.30 360.65 251.09 o 3 0 20 2.85 126.47 159.71 o 4 0 20 69.34 74.33 164.98 o 5 0 20 469.96 590.64 204.13 o 6 0 20 11.77 147.41 158.55 o 7 0 20 292.22 341.66 150.85 o 8 0 20 40.25 185.04 223.10 o 9 0 20 415.97 423.49 220.92 o 10 0 20 365.27 319.81 225.06 o 14 0 20 0.57 135.43 223.31 o 4 1 20 358.43 429.57 178.76 o 5 1 20 52.63 163.94 159.17 o 6 1 20 203.78 316.38 139.74 o 7 1 20 24.66 175.33 150.50 o 8 1 20 8.06 313.78 319.22 o 10 1 20 138.57 114.70 342.01 o 11 1 20 584.97 486.00 217.23 o 13 1 20 836.11 511.36 247.21 o 14 1 20 3.00 276.19 307.48 o 4 2 20 146.26 149.43 145.75 o 5 2 20 590.34 268.80 158.43 o 6 2 20 68.52 81.83 159.26 o 7 2 20 87.39 190.02 129.10 o 8 2 20 569.95 572.82 208.25 o 9 2 20 65.54 240.54 137.26 o 10 2 20 107.80 11.15 214.79 o 11 2 20 358.09 193.69 212.68 o 12 2 20 2365.19 1808.85 285.90 o 14 2 20 246.16 418.75 232.99 o 15 2 20 0.09 290.53 265.58 o 5 3 20 67.25 126.96 216.38 o 6 3 20 402.56 448.60 157.78 o 7 3 20 51.20 165.37 201.81 o 8 3 20 262.93 206.75 158.97 o 9 3 20 135.07 15.48 296.20 o 10 3 20 53.51 146.56 293.65 o 11 3 20 331.21 308.96 289.58 o 12 3 20 1508.89 1264.49 289.88 o 13 3 20 929.96 1014.31 193.10 o 14 3 20 124.61 194.87 271.84 o 15 3 20 25.77 178.26 313.35 o 6 4 20 2.75 125.11 143.79 o 7 4 20 343.67 496.07 151.25 o 8 4 20 11.14 352.78 159.02 o 9 4 20 114.50 32.28 339.32 o 11 4 20 524.79 404.32 262.43 o 12 4 20 184.76 154.29 373.39 o 13 4 20 131.55 238.48 177.49 o 14 4 20 2.14 185.48 220.60 o 15 4 20 264.71 213.53 219.84 o 7 5 20 1.18 235.11 313.03 o 8 5 20 121.14 325.08 158.49 o 9 5 20 53.63 123.01 159.20 o 10 5 20 328.65 593.82 276.82 o 11 5 20 325.81 268.41 275.47 o 12 5 20 26.01 10.22 151.17 o 13 5 20 466.12 271.75 225.63 o 14 5 20 78.93 310.30 187.66 o 8 6 20 44.23 122.30 228.99 o 9 6 20 163.10 369.85 158.75 o 10 6 20 186.18 407.99 361.08 o 11 6 20 965.31 1254.53 335.18 o 13 6 20 1216.37 1330.45 155.97 o 14 6 20 431.81 379.57 159.41 o 9 7 20 216.83 174.03 150.61 o 10 7 20 130.23 330.60 241.90 o 11 7 20 153.85 74.94 342.39 o 12 7 20 299.22 295.61 293.17 o 13 7 20 183.15 270.00 277.15 o 7 -2 21 254.49 329.22 170.15 o 8 -2 21 188.53 132.92 319.84 o 9 -2 21 39.60 68.13 285.89 o 7 -1 21 34.63 109.31 236.61 o 8 -1 21 398.67 283.55 336.02 o 9 -1 21 0.06 66.83 227.03 o 7 0 21 4.83 71.00 335.68 o 8 0 21 25.21 321.82 271.81 o 9 0 21 743.31 635.41 258.93 o 7 1 21 2.28 311.82 157.76 o 8 1 21 64.09 210.41 158.02 o 9 1 21 678.94 343.56 254.33 o 10 1 21 1268.56 870.11 280.35 o 11 1 21 343.00 462.87 287.95 o 8 2 21 23.95 107.43 160.35 o 9 2 21 139.98 78.21 217.80 o 10 2 21 224.04 344.88 225.40 o 11 2 21 732.31 327.64 220.39 o 12 2 21 1219.90 725.06 224.50 o 9 3 21 151.57 190.63 154.73 o