#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:38:10 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180793 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/24/2012483.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012483_Fobs loop_ _publ_author_name 'Nesterov, Vladimir N.' 'Montoya, Nicole G.' 'Antipin, Mikhail Yu.' 'Sanghadasa, Mohan' 'Clark, Ronald D.' 'Timofeeva, Tatiana V.' _publ_section_title ; Three polar derivatives of N-ethylcarbazole: materials for optical applications ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o72 _journal_page_last o75 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.637 _cell_angle_gamma 90.000 _cell_length_a 19.3841 _cell_length_b 16.4557 _cell_length_c 6.5323 _exptl_crystal_F_000 848.00 _reflns_d_resolution_high 0.7810 _cod_data_source_file bm1472Vsup4.hkl _cod_data_source_block V #BEGIN Tags that were not found in dictionaries: _shelx_title ' p2c in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 218.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 21160.53 17457.33 100.76 o 4 0 0 11133.03 9074.23 91.16 o 6 0 0 108.66 80.75 5.14 o 7 0 0 2029.66 1819.12 31.68 o 8 0 0 5404.02 4663.50 72.12 o 9 0 0 4630.82 4163.98 76.14 o 10 0 0 3818.07 3669.41 128.03 o 11 0 0 1236.89 1207.96 28.96 o 12 0 0 3217.70 2975.21 74.69 o 13 0 0 1116.15 939.55 22.71 o 14 0 0 46.78 38.47 7.91 o 15 0 0 1515.23 1303.14 24.60 o 16 0 0 1640.99 1371.46 27.78 o 17 0 0 95.88 73.30 10.67 o 18 0 0 46.22 35.49 8.27 o 19 0 0 119.98 81.17 9.16 o 20 0 0 271.97 215.39 11.65 o 21 0 0 18.66 12.78 13.34 o 22 0 0 8.72 3.47 41.63 o 23 0 0 332.19 301.73 17.10 o 24 0 0 12.90 10.00 18.08 o 1 1 0 473.37 530.89 11.36 o 2 1 0 1238.99 1361.70 62.37 o 3 1 0 202.61 197.84 11.02 o 4 1 0 2141.69 2071.92 79.52 o 5 1 0 61.65 65.87 9.14 o 6 1 0 627.30 583.81 55.55 o 7 1 0 146.30 138.74 34.53 o 9 1 0 5047.95 4780.03 503.87 o 10 1 0 137.13 110.08 21.70 o 11 1 0 57.57 29.64 13.18 o 12 1 0 106.05 103.98 20.85 o 13 1 0 1089.92 903.08 44.82 o 14 1 0 49.91 26.56 7.50 o 15 1 0 36.86 35.86 6.82 o 16 1 0 11.23 8.08 7.11 o 17 1 0 89.34 57.66 8.52 o 18 1 0 2.97 4.42 22.27 o 19 1 0 64.91 44.42 8.39 o 20 1 0 6.72 11.91 31.50 o 21 1 0 180.69 157.36 12.38 o 22 1 0 20.58 25.37 37.44 o 23 1 0 163.46 138.50 12.93 o 24 1 0 94.69 85.78 12.17 o 0 2 0 1521.06 1662.77 31.47 o 1 2 0 2467.74 2655.04 28.19 o 2 2 0 164.74 183.71 5.94 o 3 2 0 5954.77 6170.99 203.51 o 4 2 0 2171.01 2281.83 113.09 o 5 2 0 1055.61 1040.40 37.89 o 6 2 0 1793.51 1833.18 58.33 o 7 2 0 442.66 539.78 19.03 o 8 2 0 974.25 927.42 18.55 o 9 2 0 1189.30 1381.18 90.03 o 10 2 0 264.35 238.19 25.05 o 11 2 0 357.45 339.75 39.14 o 12 2 0 1.55 6.50 5.86 o 13 2 0 465.56 435.76 40.84 o 14 2 0 165.70 135.58 37.89 o 15 2 0 402.33 356.61 42.37 o 16 2 0 24.29 12.52 7.75 o 17 2 0 531.73 483.45 47.88 o 18 2 0 0.40 -2.80 27.90 o 19 2 0 121.18 101.03 27.09 o 20 2 0 37.14 29.79 13.86 o 21 2 0 11.09 27.63 35.39 o 22 2 0 107.03 105.73 25.05 o 23 2 0 74.65 84.71 22.72 o 24 2 0 18.37 -26.93 46.78 o 1 3 0 654.71 612.95 14.62 o 2 3 0 1125.62 1225.80 57.82 o 3 3 0 55.52 49.29 4.43 o 4 3 0 166.95 192.95 10.56 o 5 3 0 133.55 152.98 6.00 o 6 3 0 356.77 418.32 24.03 o 7 3 0 0.66 5.12 6.43 o 8 3 0 472.85 524.90 20.39 o 10 3 0 0.08 6.57 19.94 o 11 3 0 85.14 86.91 14.82 o 12 3 0 190.53 238.49 14.88 o 13 3 0 3.61 7.73 24.07 o 14 3 0 94.60 88.97 11.59 o 15 3 0 32.95 29.02 8.02 o 16 3 0 26.49 14.32 7.67 o 17 3 0 85.01 73.87 25.67 o 18 3 0 210.39 152.25 31.35 o 19 3 0 112.71 92.45 17.72 o 20 3 0 64.90 61.48 11.47 o 21 3 0 0.06 -0.51 16.19 o 22 3 0 0.68 22.19 34.25 o 23 3 0 1.02 -21.18 42.67 o 24 3 0 1.72 37.83 46.86 o 0 4 0 45263.71 45056.43 216.64 o 1 4 0 1686.73 1808.10 34.90 o 2 4 0 19.13 31.17 4.58 o 3 4 0 84.80 96.52 5.38 o 4 4 0 2.30 5.90 4.54 o 5 4 0 771.49 856.00 32.26 o 6 4 0 240.25 255.93 7.46 o 7 4 0 12.06 17.42 4.67 o 8 4 0 2905.79 3173.55 100.48 o 9 4 0 50.28 73.46 5.68 o 10 4 0 72.76 69.11 16.64 o 11 4 0 1557.26 1846.94 82.81 o 12 4 0 94.88 105.78 14.88 o 13 4 0 48.49 58.30 6.87 o 14 4 0 88.42 85.20 15.90 o 15 4 0 434.34 440.69 12.52 o 16 4 0 1182.60 1299.74 84.01 o 17 4 0 96.44 93.69 13.97 o 18 4 0 0.97 8.52 31.31 o 19 4 0 7.76 3.29 13.12 o 20 4 0 104.04 105.27 28.00 o 21 4 0 21.78 16.47 32.34 o 22 4 0 0.55 -4.47 14.49 o 23 4 0 44.07 20.59 32.21 o 24 4 0 5.09 -3.41 19.26 o 1 5 0 852.14 922.75 19.43 o 2 5 0 64.03 74.13 5.05 o 4 5 0 2.78 5.35 4.56 o 5 5 0 167.78 211.35 6.66 o 6 5 0 62.19 69.47 5.09 o 7 5 0 891.34 1042.47 21.29 o 8 5 0 43.98 50.48 5.48 o 9 5 0 27.94 17.15 5.27 o 11 5 0 3.05 6.87 9.87 o 12 5 0 118.36 135.28 17.95 o 13 5 0 0.44 -4.94 29.47 o 14 5 0 0.33 -3.48 7.64 o 15 5 0 520.06 539.96 15.56 o 16 5 0 11.68 -3.48 11.75 o 17 5 0 12.58 20.86 11.36 o 18 5 0 25.74 21.94 14.77 o 19 5 0 132.51 120.51 10.55 o 20 5 0 70.82 66.02 10.82 o 21 5 0 91.79 65.68 19.77 o 22 5 0 13.31 2.97 30.43 o 23 5 0 77.99 90.12 24.94 o 0 6 0 2941.05 2897.94 73.61 o 1 6 0 7.70 14.85 4.69 o 2 6 0 1888.10 2003.79 37.48 o 3 6 0 28.71 47.18 4.81 o 4 6 0 349.53 350.19 8.66 o 5 6 0 1553.04 1623.24 30.77 o 6 6 0 280.73 306.18 8.14 o 7 6 0 742.34 736.17 27.32 o 8 6 0 737.86 790.41 17.90 o 9 6 0 26.86 25.03 8.41 o 10 6 0 1856.72 2062.75 76.74 o 11 6 0 386.68 431.03 14.54 o 12 6 0 36.87 42.89 7.37 o 13 6 0 1144.46 1242.62 48.56 o 14 6 0 0.16 -0.67 7.63 o 15 6 0 482.21 500.41 14.23 o 16 6 0 0.03 5.54 31.24 o 17 6 0 349.82 373.31 12.10 o 18 6 0 6.75 7.99 14.00 o 19 6 0 15.69 22.55 10.96 o 20 6 0 9.96 38.95 39.00 o 21 6 0 57.12 54.48 10.37 o 22 6 0 31.57 46.22 11.69 o 23 6 0 294.23 389.36 53.90 o 1 7 0 155.37 138.63 11.59 o 2 7 0 1.51 -1.59 4.75 o 3 7 0 259.96 261.67 7.97 o 4 7 0 2440.58 2413.99 44.68 o 5 7 0 35.44 30.69 5.27 o 6 7 0 204.79 204.73 13.29 o 7 7 0 358.00 375.42 9.46 o 8 7 0 89.89 88.13 6.32 o 9 7 0 151.94 142.77 8.63 o 10 7 0 58.78 60.36 6.50 o 11 7 0 197.49 191.96 8.39 o 12 7 0 55.45 49.28 7.66 o 13 7 0 771.52 834.32 31.92 o 14 7 0 514.20 573.19 15.46 o 15 7 0 4.85 3.18 12.70 o 16 7 0 163.45 200.08 20.96 o 17 7 0 6.93 2.96 9.17 o 18 7 0 83.98 79.83 9.74 o 19 7 0 30.25 41.70 13.33 o 20 7 0 0.22 3.04 34.69 o 21 7 0 17.38 35.16 38.42 o 22 7 0 1.86 13.93 42.97 o 23 7 0 74.22 114.56 14.77 o 0 8 0 34.39 21.13 7.16 o 1 8 0 162.56 175.44 11.59 o 2 8 0 487.94 497.84 11.87 o 3 8 0 1497.75 1352.69 27.91 o 4 8 0 3242.49 3282.53 56.23 o 5 8 0 2951.22 2949.18 52.97 o 6 8 0 498.22 497.26 11.68 o 7 8 0 232.06 237.94 7.64 o 8 8 0 4.52 8.78 6.16 o 9 8 0 63.05 66.83 6.68 o 10 8 0 1191.16 1163.59 25.56 o 11 8 0 826.69 857.85 18.60 o 12 8 0 306.58 327.45 10.74 o 13 8 0 427.71 464.35 13.81 o 14 8 0 2175.90 2303.31 47.94 o 15 8 0 199.25 245.74 10.80 o 16 8 0 1141.48 1236.18 59.75 o 17 8 0 2935.37 3067.52 160.80 o 18 8 0 22.58 38.80 10.19 o 19 8 0 287.28 297.27 14.77 o 20 8 0 35.07 23.90 9.90 o 21 8 0 4.15 -1.33 36.71 o 22 8 0 74.06 81.65 19.82 o 1 9 0 427.29 385.90 9.73 o 2 9 0 335.28 348.86 16.98 o 3 9 0 2.39 -1.58 12.27 o 4 9 0 423.43 393.28 10.88 o 5 9 0 125.90 145.32 7.90 o 6 9 0 19.65 15.61 6.40 o 7 9 0 600.75 591.73 28.29 o 8 9 0 405.36 447.32 11.40 o 9 9 0 1598.70 1615.03 65.26 o 10 9 0 87.35 107.08 7.94 o 11 9 0 158.98 160.58 9.12 o 12 9 0 632.52 649.02 28.40 o 13 9 0 642.46 671.45 45.04 o 14 9 0 1.58 11.07 13.25 o 15 9 0 397.93 392.54 12.77 o 16 9 0 2.89 7.83 9.96 o 17 9 0 1.85 16.79 15.17 o 18 9 0 14.53 21.61 10.24 o 19 9 0 147.05 176.63 11.60 o 20 9 0 46.86 49.21 10.15 o 21 9 0 40.22 72.72 11.63 o 22 9 0 56.86 47.43 12.63 o 0 10 0 3589.68 3486.84 88.95 o 1 10 0 527.00 523.92 13.01 o 2 10 0 339.67 358.11 9.69 o 3 10 0 416.57 430.65 11.36 o 4 10 0 288.05 318.77 12.21 o 5 10 0 64.53 89.93 6.91 o 6 10 0 6.71 0.50 8.66 o 7 10 0 780.74 831.98 17.73 o 8 10 0 26.70 38.27 6.96 o 9 10 0 0.02 -10.05 26.63 o 10 10 0 87.88 81.98 8.65 o 11 10 0 251.71 282.97 11.53 o 12 10 0 1031.71 1099.72 22.32 o 13 10 0 384.69 428.78 26.13 o 14 10 0 6.02 -9.15 17.27 o 15 10 0 17.22 24.20 22.83 o 16 10 0 905.40 987.27 22.90 o 17 10 0 169.36 179.35 11.82 o 18 10 0 153.85 159.12 13.46 o 19 10 0 47.42 54.54 11.06 o 20 10 0 60.82 81.08 38.62 o 21 10 0 33.08 31.21 18.93 o 1 11 0 47.21 52.28 7.51 o 2 11 0 106.75 114.28 7.34 o 3 11 0 16.37 14.73 6.74 o 4 11 0 1.05 6.72 9.57 o 5 11 0 201.75 231.99 8.59 o 6 11 0 8.46 24.82 12.38 o 7 11 0 148.78 163.07 8.90 o 8 11 0 0.33 6.27 11.05 o 9 11 0 213.74 218.02 9.41 o 10 11 0 48.16 47.46 8.21 o 11 11 0 268.15 297.87 23.00 o 12 11 0 89.26 104.02 10.26 o 13 11 0 214.11 225.97 14.03 o 14 11 0 162.61 188.23 11.20 o 15 11 0 129.91 143.73 11.16 o 16 11 0 0.00 -3.20 9.99 o 17 11 0 17.17 23.36 10.89 o 18 11 0 46.91 42.88 11.42 o 19 11 0 0.02 -12.85 25.50 o 20 11 0 0.70 38.78 39.27 o 21 11 0 21.04 28.50 40.66 o 0 12 0 46.25 34.76 10.11 o 1 12 0 300.48 312.28 13.58 o 2 12 0 22.08 13.86 7.38 o 3 12 0 1053.02 1034.17 22.12 o 4 12 0 25.24 24.66 7.68 o 5 12 0 195.54 195.65 9.02 o 6 12 0 1121.09 1087.37 24.08 o 7 12 0 3.33 9.40 7.93 o 8 12 0 11.79 15.10 27.94 o 9 12 0 87.18 84.31 9.28 o 10 12 0 234.60 232.85 10.45 o 11 12 0 151.59 159.44 10.30 o 12 12 0 86.10 111.54 9.88 o 13 12 0 714.38 754.92 45.61 o 14 12 0 18.49 23.93 11.87 o 15 12 0 250.25 287.41 13.55 o 16 12 0 99.36 103.93 12.26 o 17 12 0 386.24 414.82 14.78 o 18 12 0 33.77 39.09 10.80 o 19 12 0 1.92 2.01 16.97 o 20 12 0 16.49 41.07 49.20 o 1 13 0 215.67 220.01 9.75 o 2 13 0 852.50 864.27 19.52 o 3 13 0 70.08 82.69 9.27 o 4 13 0 677.97 696.50 16.23 o 5 13 0 82.66 92.91 9.06 o 6 13 0 53.90 69.27 8.94 o 7 13 0 1380.92 1304.94 27.39 o 8 13 0 3.41 9.81 8.71 o 9 13 0 902.06 948.82 20.96 o 10 13 0 125.98 142.30 10.04 o 11 13 0 660.62 667.10 16.69 o 12 13 0 936.56 959.80 56.46 o 13 13 0 808.30 946.13 24.25 o 14 13 0 300.07 296.59 13.87 o 15 13 0 79.65 84.81 20.50 o 16 13 0 298.17 365.07 14.45 o 17 13 0 113.19 125.53 12.18 o 18 13 0 75.35 103.75 12.88 o 19 13 0 107.85 139.55 13.27 o 0 14 0 1977.87 1937.68 50.55 o 1 14 0 146.91 159.47 9.97 o 2 14 0 772.29 735.64 19.40 o 3 14 0 60.05 65.76 9.12 o 4 14 0 644.90 627.47 34.48 o 5 14 0 1.10 -6.68 33.92 o 6 14 0 277.44 303.03 11.24 o 7 14 0 90.64 109.45 9.82 o 8 14 0 91.40 95.44 10.11 o 9 14 0 134.63 147.00 10.36 o 10 14 0 295.94 325.79 12.46 o 11 14 0 47.30 45.21 10.21 o 12 14 0 300.09 327.68 13.94 o 13 14 0 0.04 -4.64 10.91 o 14 14 0 69.89 69.10 12.02 o 15 14 0 25.47 17.03 16.59 o 16 14 0 114.18 151.24 13.05 o 17 14 0 8.02 7.43 18.16 o 18 14 0 52.35 62.52 12.98 o 1 15 0 203.37 212.79 10.12 o 2 15 0 40.36 36.82 9.56 o 3 15 0 525.15 508.42 29.71 o 4 15 0 98.97 99.64 10.04 o 5 15 0 127.00 140.99 17.15 o 6 15 0 190.60 200.06 10.63 o 7 15 0 8.47 4.67 35.30 o 8 15 0 109.01 115.46 10.23 o 9 15 0 13.53 4.41 14.45 o 10 15 0 36.84 40.44 9.90 o 11 15 0 83.59 112.89 10.96 o 12 15 0 168.09 184.34 12.50 o 13 15 0 190.02 203.12 13.80 o 14 15 0 13.25 18.68 15.46 o 15 15 0 202.08 227.26 13.99 o 16 15 0 73.34 64.08 12.39 o 17 15 0 0.25 10.22 39.87 o 0 16 0 1760.33 1689.80 46.69 o 1 16 0 366.62 371.34 12.56 o 2 16 0 408.91 384.28 15.45 o 3 16 0 340.26 353.46 24.59 o 4 16 0 197.78 210.37 11.36 o 5 16 0 447.69 420.64 21.98 o 6 16 0 9.52 8.41 8.88 o 7 16 0 36.30 40.20 9.27 o 8 16 0 110.70 127.56 10.38 o 9 16 0 17.10 15.71 10.15 o 10 16 0 253.05 288.22 12.66 o 11 16 0 0.33 1.76 13.55 o 12 16 0 765.55 792.56 19.96 o 13 16 0 153.98 159.96 14.71 o 14 16 0 379.20 395.53 25.22 o 15 16 0 318.25 354.72 15.62 o 16 16 0 5.62 -8.46 18.23 o 1 17 0 18.09 24.02 25.84 o 2 17 0 56.38 59.76 10.56 o 3 17 0 12.56 10.19 10.72 o 4 17 0 4.73 18.67 16.24 o 5 17 0 0.12 4.39 34.40 o 6 17 0 31.54 29.27 10.11 o 7 17 0 16.48 28.35 31.98 o 8 17 0 69.06 69.41 10.90 o 9 17 0 148.31 160.56 11.98 o 10 17 0 0.16 -9.86 15.51 o 11 17 0 0.41 4.76 16.83 o 12 17 0 4.85 8.49 15.55 o 13 17 0 70.64 78.22 13.48 o 14 17 0 2.93 4.62 53.62 o 0 18 0 33.91 45.33 62.48 o 1 18 0 48.10 53.74 10.35 o 2 18 0 23.66 17.00 13.97 o 3 18 0 2.39 20.31 36.32 o 4 18 0 71.29 77.70 11.40 o 5 18 0 241.42 252.25 13.33 o 6 18 0 1.03 40.29 43.72 o 7 18 0 0.17 2.29 43.00 o 8 18 0 2.32 0.44 15.75 o 9 18 0 163.22 164.75 12.63 o 10 18 0 9.59 22.21 21.07 o 11 18 0 289.09 342.61 15.38 o 12 18 0 170.53 179.48 14.52 o 1 19 0 54.17 59.07 18.23 o 2 19 0 16.66 17.07 14.58 o 3 19 0 5.77 26.85 36.97 o 4 19 0 14.28 -18.31 52.04 o 5 19 0 77.46 55.57 12.29 o 6 19 0 16.87 11.26 15.60 o 7 19 0 29.40 31.69 16.13 o 8 19 0 1.51 22.34 42.19 o 9 19 0 0.01 -29.77 44.84 o 10 19 0 106.92 124.60 13.27 o 0 20 0 56.28 52.14 17.49 o 1 20 0 10.08 28.37 38.12 o 2 20 0 11.13 -18.84 41.97 o 3 20 0 164.46 171.30 13.18 o 4 20 0 75.92 86.10 20.56 o 5 20 0 199.22 188.96 13.81 o 6 20 0 4.93 7.06 17.50 o 7 20 0 100.95 112.73 13.81 o 1 21 0 69.82 84.75 23.97 o -24 1 1 101.12 118.03 18.97 o -23 1 1 1.50 26.70 54.98 o -22 1 1 0.44 7.27 45.55 o -21 1 1 187.61 150.63 16.70 o -20 1 1 397.65 299.79 19.65 o -19 1 1 166.86 127.35 15.90 o -18 1 1 47.23 47.60 13.75 o -17 1 1 9.99 14.31 30.56 o -16 1 1 163.82 170.17 14.31 o -15 1 1 391.28 371.13 16.24 o -14 1 1 119.54 101.90 11.81 o -13 1 1 186.53 170.40 12.50 o -12 1 1 480.05 429.18 17.49 o -11 1 1 101.71 124.16 10.56 o -10 1 1 1128.89 1124.30 30.90 o -9 1 1 142.16 152.22 9.32 o -8 1 1 1340.74 1422.73 35.78 o -7 1 1 1272.37 1140.77 31.81 o -6 1 1 120.54 115.53 8.18 o -5 1 1 113.13 96.22 8.41 o -4 1 1 1703.72 1545.64 49.19 o -3 1 1 767.65 819.06 23.86 o -2 1 1 1027.71 971.28 27.26 o -1 1 1 967.92 1072.84 25.67 o 0 1 1 3480.06 3402.55 49.87 o 1 1 1 12589.22 12353.45 96.33 o 2 1 1 894.83 824.96 22.61 o 3 1 1 2086.18 1815.44 46.12 o 4 1 1 522.60 465.76 14.09 o 5 1 1 4.71 8.75 5.91 o 6 1 1 525.08 456.79 15.22 o 8 1 1 0.50 12.50 6.36 o 9 1 1 566.34 475.42 16.13 o 10 1 1 585.74 614.58 18.86 o 11 1 1 61.79 40.44 7.72 o 12 1 1 423.44 374.09 15.11 o 13 1 1 496.67 427.93 15.00 o 14 1 1 131.02 108.03 10.68 o 15 1 1 331.27 335.23 15.34 o 16 1 1 386.05 398.62 15.56 o 17 1 1 653.29 620.71 23.29 o 18 1 1 236.56 166.88 15.90 o 19 1 1 0.80 17.15 42.37 o 20 1 1 35.13 23.17 11.70 o 21 1 1 9.37 -26.81 52.26 o 22 1 1 5.18 -35.78 37.94 o 23 1 1 3.76 16.70 48.05 o 24 1 1 47.41 50.55 16.70 o -24 2 1 109.76 92.81 19.65 o -23 2 1 0.28 2.73 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