#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012504.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012504_Fobs loop_ _publ_author_name 'Dubler, Erich' 'Schmalle, Helmut W.' 'Arod, Fr\'ed\'eric' 'Schneider, Alain' _publ_section_title ; Platinum complexes of oxopurines: cis-bis(theophyllinato-N^7^)bis(triphenylphosphine)platinum(II) and cis-chloro(theobrominato-N^1^)bis(triphenylphosphine)platinum(II) ethanol hemisolvate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m111 _journal_page_last m115 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.172 _cell_angle_gamma 90.000 _cell_length_a 9.7839 _cell_length_b 20.7991 _cell_length_c 22.0788 _exptl_crystal_F_000 2160.00 _reflns_d_resolution_high 0.7041 _[local]_cod_data_source_file jz1480Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' FRED6 Stoe IPDS measurement' _shelx_refln_list_code 4 _shelx_f_calc_maximum 424.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 55844.30 47307.48 790.50 o 3 0 0 179896.47 169001.14 1167.75 o 4 0 0 118533.75 111617.49 841.54 o 5 0 0 50502.87 50925.47 571.45 o 6 0 0 58167.08 56353.32 564.52 o 7 0 0 90294.19 85423.08 618.78 o 8 0 0 58155.30 57190.47 546.77 o 9 0 0 19265.70 20000.75 432.69 o 10 0 0 23466.63 23954.42 487.28 o 11 0 0 14192.60 14197.18 482.55 o 12 0 0 13875.76 13419.19 519.56 o 13 0 0 12093.13 12220.85 519.90 o 2 1 0 276.19 283.95 281.58 o 3 1 0 781.55 857.09 238.65 o 4 1 0 171.71 149.41 176.62 o 5 1 0 42.20 80.28 302.54 o 6 1 0 892.49 1052.98 297.81 o 7 1 0 2034.97 2177.63 276.01 o 8 1 0 5888.31 5697.26 333.47 o 9 1 0 911.30 902.05 369.98 o 10 1 0 350.76 103.61 388.40 o 11 1 0 916.11 928.25 400.91 o 12 1 0 159.23 64.23 438.60 o 13 1 0 2658.49 2498.76 558.60 o 1 2 0 31132.31 18558.35 697.37 o 2 2 0 319.67 146.54 218.54 o 3 2 0 13184.26 12081.41 400.57 o 4 2 0 1225.05 920.47 184.91 o 5 2 0 6852.72 6243.87 336.01 o 6 2 0 2958.82 2642.09 246.43 o 7 2 0 11963.29 11534.13 312.85 o 8 2 0 2430.98 2378.08 284.96 o 9 2 0 953.05 1167.41 373.36 o 10 2 0 2424.84 2286.98 423.22 o 11 2 0 1287.85 1384.43 485.25 o 12 2 0 1717.48 2383.49 488.29 o 13 2 0 732.11 471.22 535.79 o 1 3 0 22047.07 17859.29 622.83 o 2 3 0 230.32 269.75 233.92 o 3 3 0 4887.58 4268.55 305.42 o 4 3 0 3980.63 3451.35 222.93 o 5 3 0 1955.85 2632.79 344.46 o 6 3 0 129.82 -6.93 235.61 o 7 3 0 2817.39 2922.66 290.20 o 8 3 0 8484.18 8153.09 333.30 o 9 3 0 1788.50 2010.81 345.81 o 10 3 0 1702.19 2048.67 423.56 o 11 3 0 1545.97 1823.70 404.29 o 12 3 0 1770.34 1702.69 410.21 o 13 3 0 1145.33 735.23 499.62 o 0 4 0 6193.59 6088.03 518.89 o 1 4 0 59717.08 50556.68 939.40 o 2 4 0 29205.55 25347.47 565.03 o 3 4 0 70360.35 67159.66 751.45 o 4 4 0 46584.23 44380.93 542.89 o 5 4 0 23893.40 24746.44 442.83 o 6 4 0 26014.45 25690.41 426.09 o 7 4 0 21777.85 22974.46 400.57 o 8 4 0 4112.77 4282.07 321.47 o 9 4 0 19362.67 19988.92 441.14 o 10 4 0 11947.21 11553.06 383.67 o 11 4 0 9753.63 10066.04 476.46 o 12 4 0 7599.67 7467.89 503.84 o 13 4 0 4933.62 4650.02 584.13 o 1 5 0 45682.50 41496.80 806.89 o 2 5 0 19.67 75.21 242.37 o 3 5 0 2634.07 2633.47 236.29 o 4 5 0 640.33 625.54 173.92 o 5 5 0 1940.13 1893.85 276.85 o 6 5 0 694.56 834.61 260.29 o 7 5 0 94.24 -8.62 293.75 o 8 5 0 8.31 63.89 306.60 o 9 5 0 444.59 433.02 327.73 o 10 5 0 374.05 485.93 420.52 o 11 5 0 610.89 484.07 377.25 o 12 5 0 954.23 817.37 429.81 o 13 5 0 137.56 0.17 609.99 o 0 6 0 666.00 768.02 252.01 o 1 6 0 15900.56 13828.38 507.39 o 2 6 0 43982.41 40650.03 676.75 o 3 6 0 18769.02 17863.35 430.49 o 4 6 0 24319.87 23705.80 441.81 o 5 6 0 16009.81 15571.46 356.12 o 6 6 0 13147.70 12748.52 378.09 o 7 6 0 8197.25 8644.09 419.33 o 8 6 0 20575.89 20138.50 404.12 o 9 6 0 7123.73 7498.99 339.05 o 10 6 0 11127.21 10873.95 442.15 o 11 6 0 10018.03 9523.66 462.26 o 12 6 0 7615.62 7123.43 437.93 o 13 6 0 4449.32 4028.21 543.22 o 1 7 0 1128.29 1165.21 277.87 o 2 7 0 8.45 68.11 219.39 o 3 7 0 798.54 1064.48 199.78 o 4 7 0 2551.14 2628.23 305.92 o 5 7 0 16963.39 17782.39 423.39 o 6 7 0 3425.90 3297.37 298.32 o 7 7 0 6447.15 6329.90 322.82 o 8 7 0 111.85 246.60 274.32 o 9 7 0 2940.94 2902.38 378.60 o 10 7 0 3411.91 3098.10 364.74 o 11 7 0 4367.10 4167.99 478.66 o 12 7 0 3936.46 4120.49 530.72 o 13 7 0 3322.81 2570.26 619.96 o 0 8 0 524.11 578.55 283.27 o 1 8 0 11611.58 10837.44 390.77 o 2 8 0 12688.44 11918.82 373.53 o 3 8 0 7904.84 7158.25 280.91 o 4 8 0 12354.10 13022.17 387.90 o 5 8 0 5219.15 4877.35 320.46 o 6 8 0 8943.62 8425.72 318.09 o 7 8 0 3524.57 3579.46 309.81 o 8 8 0 8485.86 8592.71 353.75 o 9 8 0 4123.24 4117.62 370.15 o 10 8 0 2083.85 2080.44 381.14 o 11 8 0 2353.82 2291.38 435.73 o 12 8 0 1062.66 899.18 485.42 o 13 8 0 500.66 51.38 619.79 o 1 9 0 2103.92 2200.28 266.37 o 2 9 0 2274.68 2224.11 247.61 o 3 9 0 47.82 103.10 252.68 o 4 9 0 313.16 353.08 259.78 o 5 9 0 7.26 -10.31 258.60 o 6 9 0 1003.36 904.25 322.32 o 7 9 0 154.25 175.95 281.75 o 8 9 0 723.49 763.79 324.18 o 9 9 0 49.31 114.93 309.64 o 10 9 0 17.31 -7.61 333.30 o 11 9 0 120.73 197.24 483.22 o 12 9 0 54.29 275.84 475.28 o 13 9 0 151.60 27.89 599.17 o 0 10 0 32308.90 30243.92 569.59 o 1 10 0 63652.98 61221.04 772.58 o 2 10 0 36085.01 37911.26 606.27 o 3 10 0 47535.49 49973.56 645.48 o 4 10 0 47521.57 49159.92 591.90 o 5 10 0 32593.05 33032.89 498.43 o 6 10 0 21961.98 22782.79 439.95 o 7 10 0 32419.97 32589.89 474.26 o 8 10 0 33477.40 34546.45 506.21 o 9 10 0 14567.35 15041.42 463.45 o 10 10 0 12534.83 12885.94 485.25 o 11 10 0 13478.68 13810.46 524.13 o 12 10 0 6547.81 6095.30 647.00 o 1 11 0 1588.73 1584.88 343.11 o 2 11 0 2425.56 2740.46 314.71 o 3 11 0 6087.03 6063.69 333.81 o 4 11 0 607.94 400.91 262.99 o 5 11 0 1121.86 1010.73 319.11 o 6 11 0 3757.41 3523.35 346.15 o 7 11 0 3392.50 3383.40 346.66 o 8 11 0 2686.65 2797.25 399.73 o 9 11 0 3232.88 3265.43 405.81 o 10 11 0 6532.23 6371.81 450.94 o 11 11 0 4425.54 4470.36 476.46 o 12 11 0 3475.36 3490.05 535.96 o 0 12 0 113.02 397.02 287.84 o 1 12 0 1073.32 1384.93 306.26 o 2 12 0 7.33 132.00 285.47 o 3 12 0 6.91 155.83 269.41 o 4 12 0 97.95 403.28 326.20 o 5 12 0 1455.73 2272.45 405.64 o 6 12 0 76.39 136.74 328.40 o 7 12 0 129.23 536.29 355.11 o 8 12 0 2168.15 2257.07 376.91 o 9 12 0 64.63 76.90 478.83 o 10 12 0 34.95 104.12 452.97 o 11 12 0 149.14 1.52 570.10 o 12 12 0 625.88 301.53 637.87 o 1 13 0 259.29 161.92 311.33 o 2 13 0 4446.45 4744.34 357.47 o 3 13 0 282.84 203.16 269.25 o 4 13 0 1164.17 1348.93 371.67 o 5 13 0 3144.31 3269.65 329.59 o 6 13 0 2037.54 2206.19 347.67 o 7 13 0 4879.46 5193.08 421.87 o 8 13 0 3379.71 3551.24 511.28 o 9 13 0 4890.98 4854.03 398.21 o 10 13 0 5963.82 6604.04 470.21 o 11 13 0 5098.83 5215.05 528.52 o 12 13 0 5355.29 5230.43 734.55 o 0 14 0 32126.42 33608.73 587.17 o 1 14 0 27556.36 28633.01 512.63 o 2 14 0 30105.05 31029.52 525.14 o 3 14 0 22581.66 23889.01 489.65 o 4 14 0 24328.46 25786.24 518.04 o 5 14 0 21748.60 21980.80 443.17 o 6 14 0 16903.59 17819.24 536.46 o 7 14 0 17082.59 17454.66 437.93 o 8 14 0 16363.31 16642.70 475.79 o 9 14 0 13714.28 13979.82 504.18 o 10 14 0 11108.51 12036.28 600.86 o 11 14 0 9971.61 10460.19 586.66 o 12 14 0 6567.52 6492.83 588.86 o 1 15 0 2761.65 2658.32 325.02 o 2 15 0 788.13 697.03 375.05 o 3 15 0 136.41 203.50 359.67 o 4 15 0 2980.42 3093.88 406.32 o 5 15 0 1855.91 2080.61 299.84 o 6 15 0 430.53 275.50 374.21 o 7 15 0 61.22 151.61 333.64 o 8 15 0 115.76 195.05 353.42 o 9 15 0 560.60 772.58 538.83 o 10 15 0 154.43 194.88 468.35 o 11 15 0 174.53 579.73 670.49 o 0 16 0 4750.26 4864.00 432.18 o 1 16 0 2690.91 3094.21 334.32 o 2 16 0 2717.95 3042.49 425.93 o 3 16 0 4213.72 4325.00 352.74 o 4 16 0 3894.59 4203.48 329.42 o 5 16 0 529.68 660.52 373.87 o 6 16 0 1265.02 1276.93 402.43 o 7 16 0 2165.35 2429.97 443.33 o 8 16 0 963.85 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19 0 274.52 429.81 449.25 o 8 19 0 43.76 319.95 520.58 o 9 19 0 126.91 320.80 559.11 o 10 19 0 0.62 107.16 600.69 o 0 20 0 11726.99 13092.98 505.03 o 1 20 0 12999.17 13785.45 513.81 o 2 20 0 24144.63 24965.49 543.90 o 3 20 0 20581.98 22069.53 558.60 o 4 20 0 14639.35 16702.20 601.03 o 5 20 0 23094.53 24852.58 547.45 o 6 20 0 17297.69 18075.80 594.61 o 7 20 0 10514.14 10694.11 557.93 o 8 20 0 9963.85 7644.52 548.80 o 9 20 0 10783.94 10938.51 668.13 o 10 20 0 8341.31 6806.19 604.92 o 1 21 0 21.20 -29.24 367.28 o 2 21 0 1560.61 1616.49 353.42 o 3 21 0 291.26 210.77 497.76 o 4 21 0 274.38 320.97 391.28 o 5 21 0 277.22 312.85 452.12 o 6 21 0 880.27 855.06 511.45 o 7 21 0 2348.36 1659.08 515.67 o 8 21 0 2662.44 2257.57 548.63 o 9 21 0 3289.12 3321.04 762.44 o 0 22 0 4022.06 4390.75 515.17 o 1 22 0 1656.16 1875.42 451.28 o 2 22 0 1898.51 2118.30 454.49 o 3 22 0 4213.92 4078.91 470.88 o 4 22 0 2796.61 3012.92 493.03 o 5 22 0 1147.79 1554.12 559.28 o 6 22 0 1436.96 1409.27 518.72 o 7 22 0 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