#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/25/2012505.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012505_Fobs loop_ _publ_author_name 'Dubler, Erich' 'Schmalle, Helmut W.' 'Arod, Fr\'ed\'eric' 'Schneider, Alain' _publ_section_title ; Platinum complexes of oxopurines: cis-bis(theophyllinato-N^7^)bis(triphenylphosphine)platinum(II) and cis-chloro(theobrominato-N^1^)bis(triphenylphosphine)platinum(II) ethanol hemisolvate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m111 _journal_page_last m115 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 62.565 _cell_angle_beta 81.354 _cell_angle_gamma 89.019 _cell_length_a 11.4777 _cell_length_b 19.3276 _cell_length_c 20.5946 _exptl_crystal_F_000 1908.00 _reflns_d_resolution_high 0.7262 _[local]_cod_data_source_file jz1480IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' FRED5 Stoe IPDS measurement' _shelx_refln_list_code 4 _shelx_f_calc_maximum 418.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 41746.91 37723.89 1225.28 o 3 0 0 16597.21 14854.16 881.20 o 4 0 0 2353.93 2605.47 677.42 o 5 0 0 1077.08 1178.26 589.13 o 6 0 0 30259.12 31598.43 739.98 o 7 0 0 15755.90 17060.22 634.66 o 8 0 0 2930.36 2967.87 652.06 o 9 0 0 41165.52 43218.02 760.89 o 10 0 0 4.90 -185.64 587.65 o 11 0 0 4289.73 4936.46 705.00 o 12 0 0 410.99 -72.55 664.09 o 13 0 0 3438.81 3541.64 797.54 o 14 0 0 283.98 677.97 882.31 o 15 0 0 5451.11 4782.46 798.28 o -15 1 0 220.25 -5.18 988.55 o -14 1 0 11270.23 9683.57 953.57 o -13 1 0 31.60 -351.67 777.00 o -12 1 0 348.60 419.04 660.58 o -11 1 0 1104.41 1353.73 689.08 o -10 1 0 10257.99 10304.35 656.13 o -9 1 0 319.11 393.50 622.82 o -8 1 0 38595.54 41625.71 844.18 o -7 1 0 20943.50 22587.84 667.61 o -6 1 0 4470.13 3755.60 573.96 o -5 1 0 48407.52 54661.95 906.56 o -4 1 0 2447.93 3126.86 680.75 o -3 1 0 6486.82 7191.93 811.05 o -2 1 0 4059.02 4006.76 888.23 o 2 1 0 41588.35 42533.38 1184.00 o 3 1 0 32994.29 34498.75 1077.95 o 4 1 0 33514.04 39023.57 966.71 o 5 1 0 1668.19 1449.42 585.62 o 6 1 0 1388.44 1395.56 556.93 o 7 1 0 35.63 163.62 636.88 o 8 1 0 40294.67 44905.82 856.03 o 9 1 0 3342.53 3766.15 624.67 o 10 1 0 16155.71 15877.51 599.50 o 11 1 0 2300.56 2071.49 698.15 o 12 1 0 75.30 -219.70 719.06 o 13 1 0 2690.42 2325.80 781.62 o 14 1 0 2709.14 2282.12 885.27 o 15 1 0 141.55 -424.40 995.77 o -15 2 0 4426.04 3287.52 998.36 o -14 2 0 215.72 108.65 876.57 o -13 2 0 6233.55 6493.59 806.05 o -12 2 0 3753.63 3564.04 686.67 o -11 2 0 0.87 -546.93 689.08 o -10 2 0 12568.74 12616.09 666.13 o -9 2 0 11364.92 11299.38 678.71 o -8 2 0 3854.91 4365.65 674.27 o -7 2 0 2755.75 3583.66 669.46 o -6 2 0 73344.44 78553.17 958.01 o -5 2 0 7193.07 8495.13 641.51 o -4 2 0 40501.21 43798.82 947.46 o -3 2 0 9728.37 9758.90 828.26 o -2 2 0 4703.44 4159.83 892.86 o -1 2 0 9257.90 6670.72 960.60 o 1 2 0 1433.99 849.73 998.54 o 2 2 0 3129.45 2894.76 1015.57 o 3 2 0 31502.83 31531.62 989.11 o 4 2 0 9033.33 10702.10 718.69 o 5 2 0 30201.65 31288.97 788.66 o 6 2 0 3197.17 3596.80 548.97 o 7 2 0 7361.89 7589.68 686.49 o 8 2 0 1715.58 1860.13 643.55 o 9 2 0 24554.10 25394.13 666.31 o 10 2 0 1064.51 783.66 651.88 o 11 2 0 3616.50 4078.58 698.89 o 12 2 0 6318.77 6998.51 808.65 o 13 2 0 77.97 210.07 749.60 o 14 2 0 1792.39 1578.98 878.79 o 15 2 0 93.55 -215.44 840.67 o -15 3 0 155.13 -358.14 971.15 o -14 3 0 1777.42 1460.52 872.13 o -13 3 0 1532.87 1068.51 766.63 o -12 3 0 581.79 1051.48 675.57 o -11 3 0 17599.68 17820.74 791.62 o -10 3 0 13.69 70.15 456.61 o -9 3 0 4008.74 4452.08 650.21 o -8 3 0 35.57 554.34 637.44 o -7 3 0 6051.29 6185.98 683.90 o -6 3 0 4068.73 4345.10 568.40 o -5 3 0 27541.68 32245.87 787.55 o -4 3 0 8187.26 9874.21 716.29 o -3 3 0 11691.57 11107.26 815.49 o -2 3 0 175164.53 185068.56 1996.16 o -1 3 0 12325.99 9960.46 984.85 o 0 3 0 250.37 464.94 1144.76 o 1 3 0 4566.89 3798.91 1081.46 o 2 3 0 78700.13 78031.41 1501.98 o 3 3 0 371.10 260.05 696.48 o 4 3 0 111170.38 120199.79 1304.49 o 5 3 0 10716.15 10637.51 640.40 o 6 3 0 542.62 909.33 525.65 o 7 3 0 16614.14 17486.47 732.57 o 8 3 0 3869.01 4258.48 641.33 o 9 3 0 4235.15 4363.06 625.78 o 10 3 0 1991.11 2117.95 702.59 o 11 3 0 3122.57 4220.73 690.19 o 12 3 0 16.53 -19.25 751.64 o 13 3 0 6900.12 6361.44 787.92 o 14 3 0 74.72 70.15 843.81 o 15 3 0 332.66 -398.12 986.14 o -15 4 0 496.28 121.97 966.15 o -14 4 0 111.39 -513.62 750.16 o -13 4 0 203.33 65.34 747.57 o -12 4 0 4926.33 5721.04 763.48 o -11 4 0 262.06 557.30 683.71 o -10 4 0 28480.78 30215.46 856.03 o -9 4 0 75.20 148.44 606.72 o -8 4 0 1110.84 696.30 634.66 o -7 4 0 8482.43 9405.01 690.74 o -6 4 0 9080.71 9645.81 527.50 o -5 4 0 5659.23 6485.82 547.49 o -4 4 0 19601.94 20046.59 760.52 o -3 4 0 39864.23 44046.28 1033.34 o -2 4 0 1070.50 801.43 807.53 o -1 4 0 69279.94 70269.23 1537.52 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5 0 449.67 489.00 1002.43 o 1 5 0 5816.03 4900.18 958.57 o 2 5 0 1799.77 1961.37 912.85 o 3 5 0 68194.55 66916.75 1165.12 o 4 5 0 5872.10 6214.85 629.11 o 5 5 0 116.42 331.49 528.05 o 6 5 0 32.93 169.35 569.70 o 7 5 0 15741.25 15929.70 716.66 o 8 5 0 76.36 -390.35 595.98 o 9 5 0 5201.62 5146.72 610.42 o 10 5 0 3001.23 2826.09 686.49 o 11 5 0 3003.30 2874.40 672.98 o 12 5 0 1925.10 1437.57 755.16 o 13 5 0 2328.87 2457.22 847.14 o 14 5 0 398.85 -283.18 944.87 o -15 6 0 14.32 -298.92 1025.20 o -14 6 0 1281.20 1011.32 831.60 o -13 6 0 2417.31 2423.53 641.14 o -12 6 0 995.82 972.82 752.75 o -11 6 0 3863.04 3593.10 676.68 o -10 6 0 3692.53 3427.63 701.67 o -9 6 0 1126.76 828.26 591.91 o -8 6 0 18.76 -82.18 608.20 o -7 6 0 25338.96 26740.64 760.52 o -6 6 0 1746.85 2070.20 518.06 o -5 6 0 13775.55 13855.99 625.22 o -4 6 0 15173.23 14595.97 671.50 o -3 6 0 28523.58 31263.61 836.59 o -2 6 0 21751.98 23637.10 841.78 o -1 6 0 19515.40 19317.54 1005.39 o 0 6 0 7576.98 8000.02 900.63 o 1 6 0 7119.96 8165.67 1008.91 o 2 6 0 78828.04 77275.70 1375.38 o 3 6 0 2804.00 2623.24 761.26 o 4 6 0 1410.74 1153.09 681.68 o 5 6 0 47.98 89.58 510.47 o 6 6 0 2458.35 2694.13 639.11 o 7 6 0 73.66 282.81 605.23 o 8 6 0 8275.49 9004.30 647.43 o 9 6 0 2636.32 3169.80 583.76 o 10 6 0 13.82 -2.22 658.17 o 11 6 0 11012.98 10842.21 709.81 o 12 6 0 1383.79 1741.85 733.69 o 13 6 0 706.36 195.82 839.55 o 14 6 0 82.51 71.63 934.32 o -15 7 0 2034.83 481.41 1033.53 o -14 7 0 843.88 888.60 872.50 o -13 7 0 5.24 108.28 707.96 o -12 7 0 10004.37 10218.29 778.29 o -11 7 0 56.36 1.67 631.52 o -10 7 0 1467.48 587.65 675.57 o -9 7 0 2963.36 2336.17 582.28 o -8 7 0 8981.25 8789.79 647.99 o -7 7 0 373.78 647.99 613.38 o -6 7 0 24767.81 26656.80 771.63 o -5 7 0 4461.29 4960.89 545.82 o -4 7 0 171.76 403.30 528.24 o -3 7 0 50557.73 51831.41 917.66 o -2 7 0 10683.95 10297.50 712.77 o -1 7 0 331.50 490.11 617.08 o 0 7 0 207.23 175.83 668.72 o 1 7 0 17355.78 16491.81 988.92 o 2 7 0 1571.44 1791.64 701.11 o 3 7 0 30692.40 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