#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2012520.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012520_Fobs loop_ _publ_author_name 'Wouters, Johan' 'Norberg, Bernadette' 'Guccione, Salvatore' _publ_section_title ; 4-Methyl-2-[N-(3,4-methylenedioxybenzylidene)hydrazino]thiazole and its reduction product, 4-methyl-2-[N-(3,4-methylenedioxybenzylidene)hydrazono]-4,5-dihydrothiazole ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o69 _journal_page_last o71 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.127 _cell_angle_gamma 90.000 _cell_length_a 6.2190 _cell_length_b 12.1630 _cell_length_c 15.8550 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high .8111 _[local]_cod_data_source_file sk1506Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sga25 P 21/n z=4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 184.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1736.30 1611.26 12.40 o 4 0 0 1027.88 1067.25 11.69 o 6 0 0 13.69 14.09 1.06 o 1 1 0 76.74 84.27 1.57 o 2 1 0 189.69 181.90 5.65 o 3 1 0 728.94 753.60 6.41 o 4 1 0 1.23 .03 .74 o 5 1 0 334.67 312.08 9.33 o 6 1 0 14.02 11.91 1.09 o 7 1 0 32.61 31.96 1.32 o 0 2 0 96.60 90.55 1.10 o 1 2 0 880.08 850.09 4.12 o 2 2 0 7.29 12.56 1.89 o 3 2 0 768.14 803.91 21.04 o 4 2 0 121.64 124.05 3.81 o 5 2 0 38.31 44.28 1.14 o 6 2 0 84.97 76.68 2.55 o 7 2 0 8.43 7.19 .85 o 1 3 0 8980.24 9838.60 80.24 o 2 3 0 407.39 419.21 5.52 o 3 3 0 1504.18 1578.72 22.61 o 4 3 0 19.05 20.64 .91 o 5 3 0 246.25 233.62 13.25 o 6 3 0 55.06 50.80 2.17 o 7 3 0 11.06 12.71 1.09 o 0 4 0 3169.47 3056.26 16.49 o 1 4 0 424.83 305.36 3.24 o 2 4 0 20.65 25.18 .48 o 3 4 0 18.73 13.62 .41 o 4 4 0 54.73 50.26 1.05 o 5 4 0 19.38 22.14 .80 o 6 4 0 56.38 49.07 2.00 o 7 4 0 4.65 4.02 1.06 o 1 5 0 225.34 219.70 4.77 o 2 5 0 1204.65 1165.28 23.73 o 3 5 0 .32 .32 .54 o 4 5 0 574.15 542.05 7.60 o 5 5 0 490.80 466.41 7.72 o 6 5 0 184.58 186.14 5.14 o 7 5 0 5.83 4.87 .88 o 0 6 0 19.22 18.37 .73 o 1 6 0 348.43 328.14 4.26 o 2 6 0 1614.89 1760.08 11.36 o 3 6 0 70.40 61.02 1.40 o 4 6 0 15.71 15.58 .66 o 5 6 0 53.19 47.83 1.73 o 6 6 0 19.73 21.98 1.14 o 7 6 0 4.10 3.52 .65 o 1 7 0 111.95 119.17 2.10 o 2 7 0 139.08 138.59 2.99 o 3 7 0 129.47 127.22 2.58 o 4 7 0 42.06 42.46 1.78 o 5 7 0 138.72 126.10 3.35 o 6 7 0 12.04 14.64 1.00 o 0 8 0 9.42 14.12 .46 o 1 8 0 463.29 448.45 6.25 o 2 8 0 2.07 2.35 .34 o 3 8 0 144.32 161.24 3.10 o 4 8 0 31.98 29.46 1.35 o 5 8 0 4.12 3.76 .82 o 6 8 0 .68 .12 .65 o 1 9 0 117.74 122.12 2.58 o 2 9 0 89.15 98.17 4.64 o 3 9 0 182.38 190.22 3.45 o 4 9 0 115.04 111.86 3.17 o 5 9 0 12.76 14.12 .97 o 6 9 0 35.07 31.96 1.23 o 0 10 0 124.23 129.35 2.84 o 1 10 0 15.40 16.34 .87 o 2 10 0 17.23 17.80 .68 o 3 10 0 48.20 49.01 1.67 o 4 10 0 .16 -.70 1.14 o 5 10 0 3.59 2.88 .62 o 1 11 0 28.30 29.02 1.44 o 2 11 0 47.10 52.62 1.79 o 3 11 0 .91 .47 .59 o 4 11 0 .10 -1.20 1.20 o 5 11 0 1.31 2.93 .53 o 0 12 0 199.41 215.10 5.19 o 1 12 0 36.89 36.09 1.35 o 2 12 0 5.91 3.90 .70 o 3 12 0 24.61 22.07 1.06 o 4 12 0 5.15 6.34 .76 o 1 13 0 4.42 5.05 .70 o 2 13 0 2.09 .97 1.44 o 3 13 0 38.60 42.61 1.38 o 0 14 0 107.69 109.19 3.23 o 1 14 0 2.66 1.38 .62 o 2 14 0 9.85 10.51 .79 o -7 0 1 14.73 11.97 .91 o -5 0 1 34.89 34.38 .98 o -3 0 1 1100.87 1100.45 7.71 o -1 0 1 11816.57 9304.75 102.49 o 1 0 1 538.95 591.68 3.03 o 3 0 1 240.27 222.63 3.38 o 5 0 1 .24 .00 .77 o 7 0 1 38.64 33.81 1.26 o -7 1 1 39.76 31.16 1.38 o -6 1 1 59.39 61.45 2.02 o -5 1 1 53.57 53.75 1.80 o -4 1 1 1054.19 1052.54 9.63 o -3 1 1 1607.71 1770.48 10.29 o -2 1 1 323.41 340.90 22.36 o -1 1 1 6.01 7.93 1.51 o 0 1 1 92.10 109.16 .94 o 1 1 1 2112.07 2064.64 16.01 o 2 1 1 12.24 19.96 .92 o 3 1 1 1.56 5.25 .32 o 4 1 1 653.59 640.18 7.24 o 5 1 1 323.07 304.87 8.60 o 6 1 1 55.20 48.10 1.73 o 7 1 1 218.84 197.67 4.49 o -7 2 1 19.51 17.37 1.09 o -6 2 1 218.30 202.01 5.72 o -5 2 1 195.62 202.31 5.05 o -4 2 1 1891.28 1988.45 104.23 o -3 2 1 86.25 76.52 1.54 o -2 2 1 4.44 5.50 2.49 o -1 2 1 1530.04 1431.90 15.82 o 0 2 1 4868.98 4701.85 21.99 o 1 2 1 1718.90 1596.83 17.18 o 2 2 1 353.90 336.04 3.43 o 3 2 1 160.01 174.86 5.85 o 4 2 1 386.06 419.09 6.51 o 5 2 1 251.50 255.03 5.00 o 6 2 1 241.17 215.63 5.52 o 7 2 1 5.43 6.34 .82 o -7 3 1 50.54 50.36 1.91 o -6 3 1 54.03 62.30 2.49 o -5 3 1 7.90 7.92 .65 o -4 3 1 49.31 47.30 .99 o -3 3 1 303.10 332.91 4.65 o -2 3 1 10.54 15.48 .44 o -1 3 1 3889.12 3920.40 13.45 o 0 3 1 184.41 214.93 1.57 o 1 3 1 34126.69 29125.60 216.07 o 2 3 1 2990.82 3056.88 11.05 o 3 3 1 1199.40 1291.20 16.95 o 4 3 1 205.77 193.01 9.32 o 5 3 1 187.20 191.38 3.71 o 6 3 1 118.27 119.35 3.61 o 7 3 1 18.42 16.73 1.29 o -7 4 1 .04 -.65 2.35 o -6 4 1 6.73 4.64 1.00 o -5 4 1 2.08 1.60 .55 o -4 4 1 1.47 .60 .42 o -3 4 1 11.06 6.99 .33 o -2 4 1 26.66 12.49 1.16 o -1 4 1 1229.45 1160.89 20.42 o 0 4 1 91.86 54.78 .67 o 1 4 1 3949.57 3918.00 29.76 o 2 4 1 679.62 659.94 5.59 o 3 4 1 131.28 158.73 4.50 o 4 4 1 6.14 6.04 .41 o 5 4 1 29.03 30.47 .94 o 6 4 1 12.56 10.83 1.09 o 7 4 1 1.05 -.62 1.03 o -7 5 1 2.82 2.55 .91 o -6 5 1 16.54 14.29 1.12 o -5 5 1 363.81 339.73 9.76 o -4 5 1 9.22 7.90 .47 o -3 5 1 497.44 514.52 13.73 o -2 5 1 32.43 42.95 .89 o -1 5 1 830.62 884.31 6.32 o 0 5 1 377.14 365.65 2.73 o 1 5 1 75.07 81.30 1.41 o 2 5 1 15.54 12.10 .43 o 3 5 1 1.39 2.40 .23 o 4 5 1 4.09 3.63 1.51 o 5 5 1 185.33 204.66 3.67 o 6 5 1 39.77 47.63 1.61 o 7 5 1 16.45 19.46 1.12 o -7 6 1 .05 .85 .67 o -6 6 1 .17 .00 .79 o -5 6 1 127.17 124.04 3.43 o -4 6 1 37.38 39.21 .90 o -3 6 1 202.63 194.00 3.02 o -2 6 1 401.77 416.41 5.37 o -1 6 1 3.01 8.35 .54 o 0 6 1 263.87 234.21 2.49 o 1 6 1 15.60 6.09 .29 o 2 6 1 1576.00 1537.52 29.37 o 3 6 1 503.90 523.31 6.87 o 4 6 1 57.44 56.81 1.30 o 5 6 1 51.12 50.65 1.70 o 6 6 1 8.55 9.80 .85 o 7 6 1 33.18 33.45 1.23 o -6 7 1 30.98 27.61 1.17 o -5 7 1 53.71 51.27 1.53 o -4 7 1 3.12 2.33 .98 o -3 7 1 11.64 11.29 .69 o -2 7 1 .09 1.97 1.45 o -1 7 1 40.86 43.32 .86 o 0 7 1 441.00 390.34 3.62 o 1 7 1 14.63 18.08 .46 o 2 7 1 52.99 63.08 1.39 o 3 7 1 153.72 140.17 2.74 o 4 7 1 230.24 237.01 10.58 o 5 7 1 4.34 2.29 .67 o 6 7 1 21.89 20.48 1.00 o -6 8 1 1.30 2.38 .67 o -5 8 1 10.09 7.48 .94 o -4 8 1 69.05 62.12 1.91 o -3 8 1 145.17 139.70 2.94 o -2 8 1 .74 1.67 .31 o -1 8 1 36.39 33.24 1.23 o 0 8 1 330.55 314.35 3.63 o 1 8 1 24.62 22.65 .60 o 2 8 1 636.43 605.52 7.72 o 3 8 1 .71 .08 .59 o 4 8 1 9.49 8.66 1.00 o 5 8 1 6.21 6.40 .82 o 6 8 1 19.76 22.54 1.14 o -6 9 1 3.19 5.60 .70 o -5 9 1 116.86 122.14 3.76 o -4 9 1 42.37 45.57 1.50 o -3 9 1 123.16 128.52 2.96 o -2 9 1 136.75 131.31 2.77 o -1 9 1 348.22 340.70 9.52 o 0 9 1 1.47 2.71 .84 o 1 9 1 110.38 112.60 6.02 o 2 9 1 29.42 30.05 .81 o 3 9 1 1.08 1.30 1.54 o 4 9 1 4.50 3.37 .67 o 5 9 1 3.69 2.88 .70 o 6 9 1 .88 2.05 .56 o -5 10 1 10.38 12.33 .76 o -4 10 1 15.30 10.62 .82 o -3 10 1 54.61 64.03 2.14 o -2 10 1 105.31 118.17 2.54 o -1 10 1 4.66 4.53 .70 o 0 10 1 2.39 3.32 .29 o 1 10 1 253.19 242.27 13.69 o 2 10 1 4.84 3.50 .45 o 3 10 1 1.81 1.47 .67 o 4 10 1 3.07 1.97 .70 o 5 10 1 .01 -.12 1.12 o -5 11 1 8.43 9.30 .82 o -4 11 1 8.05 7.01 .73 o -3 11 1 .04 .00 1.50 o -2 11 1 12.23 10.68 1.00 o -1 11 1 137.20 153.36 4.46 o 0 11 1 26.49 25.80 .79 o 1 11 1 84.40 86.39 2.76 o 2 11 1 55.95 54.88 1.79 o 3 11 1 2.72 -.23 1.61 o 4 11 1 32.20 30.34 1.20 o 5 11 1 29.43 34.22 1.20 o -4 12 1 2.65 .38 1.29 o -3 12 1 1.24 3.11 .59 o -2 12 1 29.59 32.60 1.38 o -1 12 1 32.50 39.88 1.38 o 0 12 1 .19 .23 .39 o 1 12 1 6.28 10.01 .91 o 2 12 1 1.70 9.80 .91 o 3 12 1 3.99 3.43 .59 o 4 12 1 12.53 11.59 .88 o -3 13 1 44.64 39.82 1.41 o -2 13 1 8.55 9.42 .73 o -1 13 1 8.30 8.86 .82 o 0 13 1 37.39 38.43 1.00 o 1 13 1 48.45 50.59 1.64 o 2 13 1 24.62 26.97 1.20 o 3 13 1 2.08 2.67 .65 o -2 14 1 .69 .65 1.06 o -1 14 1 19.85 20.28 1.00 o 0 14 1 18.02 20.43 .71 o 1 14 1 9.06 9.80 .88 o 2 14 1 4.88 5.49 .65 o -6 0 2 343.19 326.61 9.63 o -4 0 2 64.29 62.86 1.43 o -2 0 2 132.34 117.66 3.24 o 0 0 2 10098.50 7875.97 36.57 o 2 0 2 204.85 189.37 4.77 o 4 0 2 1727.71 1766.01 12.06 o 6 0 2 59.99 54.76 1.82 o -7 1 2 26.75 25.00 1.32 o -6 1 2 6.57 7.42 1.09 o -5 1 2 19.18 16.61 .87 o -4 1 2 731.08 749.86 17.61 o -3 1 2 1835.03 2117.60 25.84 o -2 1 2 36.13 39.45 2.24 o -1 1 2 1948.21 2025.08 33.84 o 0 1 2 772.50 728.22 9.17 o 1 1 2 5290.50 5367.24 105.78 o 2 1 2 1031.13 1021.47 44.33 o 3 1 2 18.97 17.73 1.03 o 4 1 2 168.09 147.51 2.51 o 5 1 2 9.34 9.79 .54 o 6 1 2 154.57 149.95 4.46 o 7 1 2 .51 -1.41 1.41 o -7 2 2 .15 2.17 .67 o -6 2 2 78.62 71.66 2.41 o -5 2 2 268.72 268.68 4.50 o -4 2 2 82.96 83.72 4.96 o -3 2 2 1115.43 1170.98 28.24 o -2 2 2 709.58 747.51 34.04 o -1 2 2 5342.62 5592.47 106.99 o 0 2 2 3446.68 3652.97 35.91 o 1 2 2 2321.83 2386.70 7.55 o 2 2 2 306.00 293.11 8.22 o 3 2 2 128.69 124.51 5.27 o 4 2 2 3.04 4.90 .87 o 5 2 2 76.75 67.98 3.02 o 6 2 2 3.67 2.32 .70 o 7 2 2 22.67 21.13 1.03 o -7 3 2 155.76 157.41 5.05 o -6 3 2 26.30 24.62 1.53 o -5 3 2 71.83 69.62 1.59 o -4 3 2 208.81 208.15 10.31 o -3 3 2 147.58 130.28 4.50 o -2 3 2 133.67 164.57 4.86 o -1 3 2 118.02 120.03 1.90 o 0 3 2 7366.08 7373.80 59.92 o 1 3 2 17093.48 14911.78 89.79 o 2 3 2 178.81 169.51 2.69 o 3 3 2 6.21 1.24 .23 o 4 3 2 .20 .16 .37 o 5 3 2 695.90 712.85 9.35 o 6 3 2 72.49 64.53 2.11 o 7 3 2 4.45 4.26 .70 o -7 4 2 .30 -.59 1.73 o -6 4 2 2.87 2.41 .85 o -5 4 2 13.17 13.13 .91 o -4 4 2 197.65 208.80 3.35 o -3 4 2 154.54 182.77 3.90 o -2 4 2 3074.61 3449.39 66.26 o -1 4 2 10.88 18.29 .37 o 0 4 2 312.21 303.01 3.79 o 1 4 2 8.31 4.44 .23 o 2 4 2 53.93 56.60 1.23 o 3 4 2 71.90 73.09 1.66 o 4 4 2 43.06 51.62 2.01 o 5 4 2 3.97 6.19 1.54 o 6 4 2 140.98 131.88 4.23 o 7 4 2 .46 -.56 1.88 o -7 5 2 47.51 53.50 1.67 o -6 5 2 81.88 75.62 2.52 o -5 5 2 126.35 114.20 2.38 o -4 5 2 33.31 33.54 .80 o -3 5 2 281.89 305.17 5.01 o -2 5 2 34.64 32.44 .68 o -1 5 2 6.14 12.27 .35 o 0 5 2 76.43 68.28 .87 o 1 5 2 31.99 35.17 1.23 o 2 5 2 1047.51 943.63 10.86 o 3 5 2 124.57 115.15 6.35 o 4 5 2 252.85 242.58 3.67 o 5 5 2 34.39 32.64 1.61 o 6 5 2 .26 .82 1.67 o 7 5 2 2.73 4.11 .73 o -6 6 2 73.83 80.00 2.08 o -5 6 2 12.22 14.56 1.23 o -4 6 2 471.54 502.77 28.55 o -3 6 2 98.46 105.41 2.24 o -2 6 2 1286.87 1303.32 25.25 o -1 6 2 154.77 151.30 3.01 o 0 6 2 637.52 575.67 5.90 o 1 6 2 921.62 894.40 11.28 o 2 6 2 7920.88 7940.20 50.37 o 3 6 2 122.41 128.27 2.49 o 4 6 2 114.75 104.13 3.01 o 5 6 2 55.82 52.35 1.79 o 6 6 2 .21 1.44 .73 o -6 7 2 10.58 12.62 .94 o -5 7 2 4.46 8.51 .85 o -4 7 2 20.89 19.99 .78 o -3 7 2 69.45 72.13 3.68 o -2 7 2 49.42 49.95 3.62 o -1 7 2 747.82 782.30 7.58 o 0 7 2 14.37 14.62 2.98 o 1 7 2 269.45 250.18 4.32 o 2 7 2 1.59 5.38 .44 o 3 7 2 130.47 117.15 2.55 o 4 7 2 8.48 9.06 .61 o 5 7 2 23.03 29.35 1.26 o 6 7 2 1.19 .50 .62 o -6 8 2 9.12 8.80 .82 o -5 8 2 2.37 3.64 .73 o -4 8 2 148.15 139.10 4.37 o -3 8 2 286.67 292.96 16.52 o -2 8 2 44.75 40.00 .90 o -1 8 2 288.45 274.51 4.98 o 0 8 2 86.46 92.39 1.43 o 1 8 2 .42 .27 .71 o 2 8 2 59.33 55.36 1.14 o 3 8 2 26.02 23.78 1.29 o 4 8 2 2.00 2.23 .67 o 5 8 2 4.91 6.87 .82 o 6 8 2 8.87 6.22 .79 o -6 9 2 13.92 12.30 .88 o -5 9 2 12.47 11.00 .88 o -4 9 2 29.33 27.97 1.26 o -3 9 2 26.77 25.58 .80 o -2 9 2 33.40 34.78 1.69 o -1 9 2 83.47 87.10 1.79 o 0 9 2 36.38 31.44 .51 o 1 9 2 91.11 94.39 2.71 o 2 9 2 5.86 6.53 .49 o 3 9 2 414.57 390.65 7.02 o 4 9 2 84.40 83.60 2.73 o 5 9 2 .62 .59 .59 o 6 9 2 5.14 3.08 .56 o -5 10 2 2.06 .26 .53 o -4 10 2 56.93 55.55 1.79 o -3 10 2 32.45 36.18 1.47 o -2 10 2 323.84 343.15 12.65 o -1 10 2 5.01 4.18 .65 o 0 10 2 2.17 1.69 .38 o 1 10 2 1.36 1.52 .78 o 2 10 2 430.32 459.48 7.65 o 3 10 2 122.09 127.74 3.49 o 4 10 2 9.94 10.83 .94 o 5 10 2 2.96 4.02 .76 o -5 11 2 7.82 5.40 .70 o -4 11 2 .74 1.23 .62 o -3 11 2 79.88 76.91 2.20 o -2 11 2 6.35 3.87 .79 o -1 11 2 9.36 10.09 1.00 o 0 11 2 12.88 15.21 .64 o 1 11 2 48.76 51.94 1.67 o 2 11 2 45.69 55.20 1.79 o 3 11 2 28.81 27.91 1.26 o 4 11 2 64.17 68.02 1.94 o 5 11 2 11.64 11.77 .82 o -4 12 2 .04 -1.17 1.17 o -3 12 2 53.73 56.84 1.58 o -2 12 2 10.84 14.50 1.06 o -1 12 2 37.56 38.53 1.50 o 0 12 2 100.61 93.40 4.24 o 1 12 2 109.61 108.20 3.08 o 2 12 2 5.66 7.19 .70 o 3 12 2 1.27 1.56 .59 o 4 12 2 34.95 30.78 1.17 o -3 13 2 .76 -.38 1.29 o -2 13 2 6.64 6.37 .73 o -1 13 2 1.19 2.26 .59 o 0 13 2 11.94 13.51 1.32 o 1 13 2 290.24 285.50 7.98 o 2 13 2 67.31 64.33 2.20 o 3 13 2 .43 .38 .91 o -2 14 2 1.23 1.58 .53 o -1 14 2 1.27 .76 .65 o 0 14 2 19.60 23.43 .84 o 1 14 2 .42 .26 .65 o 2 14 2 1.27 2.11 .53 o -7 0 3 .24 .59 .59 o -5 0 3 418.29 383.18 12.72 o -3 0 3 1983.85 1997.01 11.64 o -1 0 3 160.71 164.55 2.55 o 1 0 3 10731.96 10670.81 121.59 o 3 0 3 2.53 4.47 .25 o 5 0 3 11.08 8.93 .90 o 7 0 3 210.57 200.52 4.46 o -7 1 3 92.89 87.57 2.73 o -6 1 3 50.27 46.25 1.76 o -5 1 3 26.65 24.93 .87 o -4 1 3 9.21 12.33 1.31 o -3 1 3 25.50 47.45 16.77 o -2 1 3 118.09 108.77 2.74 o -1 1 3 2.63 4.26 .28 o 0 1 3 5058.40 5055.28 61.12 o 1 1 3 2183.65 2204.57 9.26 o 2 1 3 1389.83 1493.63 49.30 o 3 1 3 358.61 359.17 5.96 o 4 1 3 2.41 4.34 .60 o 5 1 3 43.08 38.17 1.00 o 6 1 3 27.59 25.53 1.17 o 7 1 3 22.72 23.42 1.06 o -7 2 3 6.82 5.58 .91 o -6 2 3 222.93 234.82 6.72 o -5 2 3 30.19 33.41 1.79 o -4 2 3 80.56 67.98 4.21 o -3 2 3 13.11 14.24 .60 o -2 2 3 18.38 7.26 .82 o -1 2 3 955.32 838.57 5.08 o 0 2 3 903.95 839.97 3.17 o 1 2 3 2034.38 1901.35 8.50 o 2 2 3 188.81 179.14 6.22 o 3 2 3 3.36 3.42 1.25 o 4 2 3 43.15 47.13 .99 o 5 2 3 138.13 133.61 3.00 o 6 2 3 44.09 43.84 1.44 o 7 2 3 .02 -.26 .53 o -7 3 3 51.83 46.25 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