#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:38:41 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180794 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/25/2012545.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012545_Fobs loop_ _publ_author_name 'Otieno, Tom' 'Blanton, Jaime R.' 'Hatfield, M. Jason' 'Asher, Sherry L.' 'Parkin, Sean' _publ_section_title ; A copper(II)--pyrazole complex cation with f̱ \/overline 3 imposed symmetry ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m182 _journal_page_last m185 _journal_volume 58 _journal_year 2002 _space_group_IT_number 147 _symmetry_space_group_name_Hall '-P 3' _symmetry_space_group_name_H-M 'P -3' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 120.000 _cell_length_a 9.9950 _cell_length_b 9.9950 _cell_length_c 8.0520 _exptl_crystal_F_000 383.00 _reflns_d_resolution_high .7696 _cod_data_source_file bj1038IIsup3.hkl _cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' k01129 in P3bar' _shelx_refln_list_code 4 _shelx_f_calc_maximum 82.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 1 0 593.77 503.71 6.01 o -1 2 0 2560.56 2610.41 26.99 o 0 2 0 912.27 997.75 12.02 o -2 3 0 163.24 179.58 2.16 o -1 3 0 509.98 532.32 6.49 o 0 3 0 1005.38 969.86 11.35 o -3 4 0 319.47 277.65 3.06 o -2 4 0 464.07 592.34 6.28 o -1 4 0 843.26 717.07 8.59 o 0 4 0 120.84 100.57 1.32 o -4 5 0 813.67 826.00 14.41 o -3 5 0 489.35 514.09 7.55 o -2 5 0 60.09 58.81 1.55 o -1 5 0 268.23 241.24 3.33 o 0 5 0 190.56 165.14 3.14 o -5 6 0 2.12 3.04 .62 o -4 6 0 602.07 666.31 8.27 o -3 6 0 958.03 970.43 13.03 o -2 6 0 260.81 255.70 10.36 o -1 6 0 165.18 163.47 7.91 o 0 6 0 731.22 727.65 10.75 o -6 7 0 82.53 78.60 2.16 o -5 7 0 913.25 900.45 12.57 o -4 7 0 601.19 595.34 9.18 o -3 7 0 348.57 378.76 5.12 o -2 7 0 447.56 476.84 6.89 o -1 7 0 38.77 36.45 2.54 o 0 7 0 7.71 4.29 1.06 o -7 8 0 898.25 950.99 17.11 o -6 8 0 28.29 29.20 1.25 o -5 8 0 10.15 11.66 .94 o -4 8 0 865.37 904.80 13.41 o -3 8 0 25.97 17.97 1.21 o -2 8 0 115.05 116.53 2.15 o -1 8 0 698.57 742.53 12.50 o 0 8 0 27.55 28.67 1.49 o -8 9 0 5.42 9.01 1.42 o -7 9 0 11.19 9.71 1.21 o -6 9 0 317.02 333.28 7.33 o -5 9 0 .85 3.70 5.92 o -4 9 0 11.06 13.71 4.08 o -3 9 0 200.88 203.27 3.82 o -2 9 0 135.74 130.94 2.75 o -1 9 0 5.91 6.20 1.11 o 0 9 0 182.08 167.17 4.73 o -9 10 0 37.28 33.04 2.17 o -8 10 0 497.13 532.04 13.85 o -7 10 0 32.33 32.11 1.65 o -6 10 0 2.36 2.42 1.23 o -5 10 0 120.72 119.26 4.01 o -4 10 0 29.93 33.73 2.14 o -3 10 0 37.12 35.37 1.60 o -2 10 0 78.77 67.83 2.66 o -1 10 0 1.71 1.69 1.16 o 0 10 0 46.69 47.52 2.93 o -10 11 0 76.80 78.29 5.11 o -9 11 0 12.68 14.46 1.84 o -8 11 0 42.66 43.40 2.41 o -7 11 0 76.51 83.44 3.43 o -6 11 0 13.23 11.42 1.52 o -5 11 0 125.12 116.50 4.56 o -4 11 0 73.68 70.70 3.19 o -3 11 0 .64 .70 1.12 o -2 11 0 4.98 3.90 1.44 o -1 11 0 93.37 96.21 6.22 o 0 11 0 33.75 41.49 4.67 o -10 12 0 6.99 16.61 4.42 o -9 12 0 41.96 31.87 4.01 o -8 12 0 2.49 -.53 2.81 o -7 12 0 .34 2.13 3.11 o -6 12 0 69.59 55.73 4.05 o -5 12 0 21.68 18.38 2.00 o -4 12 0 4.60 2.85 1.73 o -3 12 0 55.52 51.78 3.76 o -2 12 0 9.95 10.67 2.66 o -1 1 1 1854.65 1808.60 19.45 o 0 1 1 67.22 75.08 .88 o 1 1 1 6756.84 6271.07 65.73 o -3 2 1 6.11 6.20 .53 o -2 2 1 3851.25 4167.11 47.36 o -1 2 1 895.01 924.02 10.83 o 1 2 1 2.52 6.14 .48 o 2 2 1 494.49 407.76 4.27 o -5 3 1 618.91 664.56 8.13 o -4 3 1 1389.72 1254.77 21.00 o -3 3 1 250.69 261.79 3.17 o -2 3 1 141.10 143.83 1.87 o -1 3 1 1.48 2.16 .29 o 0 3 1 3497.95 3404.84 40.16 o 1 3 1 250.38 240.33 2.64 o 2 3 1 649.46 715.23 8.00 o 3 3 1 254.20 229.67 3.15 o -7 4 1 274.06 275.05 4.90 o -6 4 1 1453.85 1450.44 27.47 o -5 4 1 161.52 146.96 1.92 o -4 4 1 40.50 48.59 1.37 o -3 4 1 133.78 114.08 1.41 o -2 4 1 974.31 989.19 11.56 o -1 4 1 2816.02 2804.20 43.07 o 0 4 1 727.55 709.17 10.71 o 1 4 1 411.80 389.08 4.46 o 2 4 1 836.18 864.73 11.96 o 3 4 1 44.17 44.01 3.14 o 4 4 1 269.24 261.99 4.65 o -9 5 1 65.52 69.87 2.00 o -8 5 1 1.84 2.05 .81 o -7 5 1 975.40 983.66 13.74 o -6 5 1 541.22 603.45 10.12 o -5 5 1 11.94 11.89 .51 o -4 5 1 62.99 57.34 .88 o -3 5 1 364.07 355.11 4.08 o -2 5 1 1.28 2.53 .45 o -1 5 1 657.26 685.49 8.96 o 0 5 1 361.93 318.24 5.24 o 1 5 1 41.60 27.44 1.03 o 2 5 1 733.15 727.83 10.73 o 3 5 1 259.88 286.66 4.86 o 4 5 1 9.22 9.15 1.03 o 5 5 1 282.34 300.36 7.09 o -11 6 1 160.05 151.23 5.69 o -10 6 1 6.61 3.19 1.04 o -9 6 1 40.86 34.79 1.51 o -8 6 1 249.48 254.16 5.00 o -7 6 1 15.67 14.62 .84 o -6 6 1 457.26 459.47 6.40 o -5 6 1 184.44 175.40 2.99 o -4 6 1 15.30 12.41 1.01 o -3 6 1 1313.05 1274.75 15.05 o -2 6 1 373.98 365.18 5.15 o -1 6 1 330.95 369.46 6.46 o 0 6 1 334.63 311.68 6.09 o 1 6 1 118.42 134.13 2.73 o 2 6 1 248.51 236.11 5.98 o 3 6 1 323.37 336.79 9.42 o 4 6 1 252.34 253.96 5.87 o 5 6 1 5.59 6.25 1.51 o 6 6 1 83.33 82.97 4.81 o -12 7 1 3.67 2.36 1.48 o -11 7 1 125.64 121.59 4.29 o -10 7 1 91.23 89.30 4.32 o -9 7 1 64.23 50.50 3.66 o -8 7 1 244.83 244.95 4.14 o -7 7 1 266.55 292.71 4.30 o -6 7 1 18.93 16.28 1.06 o -5 7 1 1034.83 1027.46 17.12 o -4 7 1 962.25 981.21 13.58 o -3 7 1 39.39 41.55 .97 o -2 7 1 163.79 166.21 2.85 o -1 7 1 501.21 516.06 9.46 o 0 7 1 .56 .76 2.29 o 1 7 1 248.14 252.12 5.53 o 2 7 1 57.34 54.92 1.89 o 3 7 1 .96 -.22 1.11 o 4 7 1 31.47 34.78 2.10 o 5 7 1 16.96 16.92 1.99 o -12 8 1 8.50 5.18 2.17 o -11 8 1 3.46 2.57 2.78 o -10 8 1 41.44 35.02 2.64 o -9 8 1 150.51 162.67 3.99 o -8 8 1 5.60 5.97 1.38 o -7 8 1 477.42 523.97 8.45 o -6 8 1 421.01 429.51 10.75 o -5 8 1 1.11 1.05 .65 o -4 8 1 435.63 469.87 6.75 o -3 8 1 291.28 310.57 4.61 o -2 8 1 21.37 18.78 .97 o -1 8 1 467.33 491.31 10.58 o 0 8 1 131.24 140.11 3.61 o 1 8 1 6.45 5.18 1.96 o 2 8 1 257.30 277.76 8.06 o 3 8 1 51.07 48.70 2.56 o 4 8 1 .68 4.09 2.76 o -12 9 1 7.11 5.81 1.98 o -11 9 1 26.67 21.62 1.97 o -10 9 1 2.43 3.69 1.11 o -9 9 1 259.55 250.43 6.38 o -8 9 1 114.83 120.71 3.11 o -7 9 1 38.73 35.57 1.34 o -6 9 1 182.42 213.72 4.22 o -5 9 1 32.17 30.94 1.39 o -4 9 1 188.74 188.50 4.22 o -3 9 1 202.95 199.17 3.93 o -2 9 1 24.79 19.92 2.53 o -1 9 1 1.43 2.23 .88 o 0 9 1 129.30 130.32 5.68 o 1 9 1 118.57 112.31 7.18 o 2 9 1 9.30 9.90 1.60 o 3 9 1 21.50 15.96 3.24 o -12 10 1 20.66 22.53 2.87 o -11 10 1 81.13 68.47 5.20 o -10 10 1 84.52 86.12 4.96 o -9 10 1 3.44 3.57 1.47 o -8 10 1 131.03 135.01 4.51 o -7 10 1 73.06 80.37 2.64 o -6 10 1 35.94 30.40 1.79 o -5 10 1 13.94 15.29 1.24 o -4 10 1 126.56 138.08 3.24 o -3 10 1 24.83 26.93 2.40 o -2 10 1 75.22 69.15 3.12 o -1 10 1 97.10 90.64 4.41 o 0 10 1 2.38 2.32 1.43 o 1 10 1 52.89 46.56 3.49 o 2 10 1 44.77 37.28 4.71 o -11 11 1 10.89 13.15 2.97 o -10 11 1 54.25 53.87 3.95 o -9 11 1 76.92 71.18 4.39 o -8 11 1 4.05 3.11 2.63 o -7 11 1 88.48 92.08 5.11 o -6 11 1 12.59 3.76 2.15 o -5 11 1 13.06 10.95 2.05 o -4 11 1 44.74 41.23 2.31 o -3 11 1 43.94 45.60 3.31 o -2 11 1 25.92 22.83 1.90 o -1 11 1 36.59 33.83 3.18 o 0 11 1 30.78 33.36 3.60 o -10 12 1 2.75 6.87 18.91 o -9 12 1 23.34 20.24 3.67 o -8 12 1 43.74 42.03 4.34 o -7 12 1 5.77 6.56 2.47 o -6 12 1 24.44 23.64 2.81 o -5 12 1 58.85 58.73 6.04 o -4 12 1 26.02 19.42 2.58 o -3 12 1 53.35 43.72 3.94 o -2 12 1 19.01 16.66 3.33 o 0 0 2 2879.20 3018.61 94.84 o -1 1 2 2204.48 2211.77 23.23 o 0 1 2 703.72 639.32 6.84 o 1 1 2 3422.31 3089.75 33.06 o -3 2 2 656.45 687.39 8.48 o -2 2 2 654.56 576.23 6.66 o -1 2 2 30.59 31.77 .78 o 0 2 2 2487.16 2524.80 26.50 o 1 2 2 5121.81 4686.43 48.17 o 2 2 2 277.31 290.91 3.01 o -5 3 2 118.61 126.35 1.68 o -4 3 2 560.31 525.58 6.03 o -3 3 2 18.19 35.88 .56 o -2 3 2 1172.56 1242.59 14.38 o -1 3 2 399.51 404.28 6.02 o 0 3 2 1171.00 1273.96 14.37 o 1 3 2 1285.18 1279.62 14.25 o 2 3 2 3.75 2.38 .45 o 3 3 2 208.69 219.95 3.46 o -7 4 2 371.70 344.70 5.47 o -6 4 2 952.82 932.41 13.52 o -5 4 2 419.49 406.68 4.83 o -4 4 2 6.82 10.46 .55 o -3 4 2 9.76 11.41 .53 o -2 4 2 419.27 383.83 4.62 o -1 4 2 4549.23 4717.79 80.60 o 0 4 2 694.18 704.10 11.31 o 1 4 2 3.02 5.15 .76 o 2 4 2 17.02 14.14 2.06 o 3 4 2 87.64 100.38 1.94 o 4 4 2 53.35 49.75 2.00 o -9 5 2 536.69 587.63 10.26 o -8 5 2 13.92 9.61 1.28 o -7 5 2 22.78 19.11 1.88 o -6 5 2 165.74 173.64 2.69 o -5 5 2 73.18 79.43 1.55 o -4 5 2 4.14 2.14 .68 o -3 5 2 2215.10 2176.94 26.74 o -2 5 2 17.50 16.38 .68 o -1 5 2 62.80 52.85 1.91 o 0 5 2 2363.13 2309.00 44.08 o 1 5 2 85.36 106.66 2.30 o 2 5 2 193.33 196.56 10.22 o 3 5 2 566.19 580.22 10.84 o 4 5 2 21.43 17.79 1.90 o 5 5 2 107.29 116.34 5.45 o -11 6 2 116.85 120.25 4.75 o -10 6 2 7.44 8.23 1.11 o -9 6 2 2.75 3.96 1.00 o -8 6 2 211.96 237.47 5.51 o -7 6 2 59.95 58.50 1.44 o -6 6 2 334.44 351.90 4.67 o -5 6 2 551.62 573.23 8.20 o -4 6 2 38.77 38.04 .89 o -3 6 2 46.95 32.74 1.33 o -2 6 2 909.43 868.15 12.88 o -1 6 2 40.31 37.93 1.25 o 0 6 2 124.93 112.06 2.34 o 1 6 2 330.43 341.68 6.17 o 2 6 2 .55 .98 .91 o 3 6 2 210.49 216.70 5.21 o 4 6 2 459.58 495.40 12.19 o 5 6 2 15.60 16.14 2.99 o 6 6 2 9.10 13.46 3.39 o -12 7 2 .83 .03 2.31 o -11 7 2 .59 -1.04 1.57 o -10 7 2 199.62 207.92 6.88 o -9 7 2 41.00 29.24 2.45 o -8 7 2 82.75 74.39 3.65 o -7 7 2 1214.07 1297.49 17.05 o -6 7 2 158.68 178.67 3.00 o -5 7 2 163.06 165.24 3.26 o -4 7 2 658.90 652.47 10.03 o -3 7 2 .66 .93 .47 o -2 7 2 146.82 144.91 2.96 o -1 7 2 470.45 483.94 11.65 o 0 7 2 52.42 46.60 3.45 o 1 7 2 .63 2.59 1.46 o 2 7 2 149.20 157.09 4.46 o 3 7 2 3.70 7.44 1.36 o 4 7 2 35.77 38.32 2.31 o 5 7 2 68.23 56.88 4.48 o -12 8 2 83.56 62.26 4.11 o -11 8 2 2.90 2.86 1.28 o -10 8 2 38.66 35.53 1.88 o -9 8 2 209.96 240.81 5.49 o -8 8 2 29.87 29.79 1.35 o -7 8 2 248.41 262.15 4.55 o -6 8 2 602.27 674.35 11.13 o -5 8 2 .95 1.02 .74 o -4 8 2 20.74 20.97 1.38 o -3 8 2 595.79 644.84 9.10 o -2 8 2 117.81 122.42 2.41 o -1 8 2 29.38 24.69 1.34 o 0 8 2 271.62 274.03 6.11 o 1 8 2 5.71 3.21 1.22 o 2 8 2 3.53 6.06 1.87 o 3 8 2 49.74 45.46 3.12 o 4 8 2 25.46 25.62 3.03 o -12 9 2 12.72 16.52 2.27 o -11 9 2 139.60 131.04 6.72 o -10 9 2 8.48 9.45 1.73 o -9 9 2 2.22 3.46 1.15 o -8 9 2 215.69 227.68 7.13 o -7 9 2 8.73 9.56 1.25 o -6 9 2 39.22 44.85 1.51 o -5 9 2 93.38 97.03 2.70 o -4 9 2 61.11 58.45 1.73 o -3 9 2 64.44 56.32 1.95 o -2 9 2 30.79 27.42 1.38 o -1 9 2 62.49 56.33 3.12 o 0 9 2 175.77 183.24 8.68 o 1 9 2 84.66 82.09 4.10 o 2 9 2 .85 2.34 1.78 o 3 9 2 13.84 14.84 3.20 o -11 10 2 8.68 7.10 1.76 o -10 10 2 22.68 17.72 2.38 o -9 10 2 3.57 5.35 1.83 o -8 10 2 20.44 15.02 1.32 o -7 10 2 30.67 31.31 2.12 o -6 10 2 6.35 5.89 1.46 o -5 10 2 36.40 33.65 2.02 o -4 10 2 73.98 62.91 3.29 o -3 10 2 81.24 79.88 4.01 o -2 10 2 28.57 22.96 2.68 o -1 10 2 160.15 157.28 8.47 o 0 10 2 .38 2.98 1.84 o 1 10 2 .75 2.71 2.02 o -11 11 2 13.89 8.24 2.74 o -10 11 2 36.98 33.97 3.04 o -9 11 2 119.35 114.88 7.42 o -8 11 2 5.25 9.33 2.54 o -7 11 2 4.53 3.67 2.75 o -6 11 2 100.57 118.47 7.04 o -5 11 2 16.93 16.34 1.99 o -4 11 2 67.81 61.66 4.17 o -3 11 2 118.45 132.18 6.45 o -2 11 2 1.08 4.31 1.79 o -1 11 2 11.93 16.66 2.47 o 0 11 2 76.25 79.79 6.77 o -9 12 2 12.17 12.32 4.54 o -8 12 2 129.15 122.52 9.06 o -7 12 2 25.08 19.77 3.00 o -6 12 2 8.20 3.73 2.30 o -5 12 2 31.84 41.72 3.82 o -4 12 2 24.45 22.20 2.65 o -3 12 2 9.42 11.67 2.81 o 0 0 3 383.78 335.75 12.18 o -1 1 3 113.23 115.15 2.06 o 0 1 3 26.22 32.83 .51 o 1 1 3 435.77 383.80 4.01 o -3 2 3 1314.05 1369.88 14.65 o -2 2 3 284.87 271.87 3.19 o -1 2 3 75.79 59.82 .79 o 0 2 3 907.55 944.35 9.73 o 1 2 3 2530.13 2550.57 28.70 o 2 2 3 973.75 915.17 9.75 o -5 3 3 63.19 67.74 1.00 o -4 3 3 130.76 126.14 1.84 o -3 3 3 123.92 94.79 1.25 o -2 3 3 947.60 890.19 9.86 o -1 3 3 239.81 259.68 3.34 o 0 3 3 172.15 171.92 2.41 o 1 3 3 1774.48 1728.01 27.59 o 2 3 3 753.90 707.18 10.17 o 3 3 3 .79 1.02 .44 o -7 4 3 239.54 263.87 5.30 o -6 4 3 65.07 60.12 1.12 o -5 4 3 27.96 18.42 1.17 o -4 4 3 704.19 703.27 8.41 o -3 4 3 467.52 519.36 6.03 o -2 4 3 1.78 2.27 .49 o -1 4 3 1400.91 1421.41 21.63 o 0 4 3 30.86 30.16 .81 o 1 4 3 320.90 303.46 4.33 o 2 4 3 220.82 213.13 3.90 o 3 4 3 22.64 28.14 2.00 o 4 4 3 2.88 3.03 .91 o -9 5 3 311.97 345.45 8.55 o -8 5 3 7.63 6.45 .82 o -7 5 3 9.59 10.48 .75 o -6 5 3 291.88 280.90 6.12 o -5 5 3 665.21 700.12 9.98 o -4 5 3 106.40 107.31 1.65 o -3 5 3 2413.76 2394.39 31.82 o -2 5 3 479.16 500.20 6.21 o -1 5 3 178.77 180.70 3.21 o 0 5 3 2117.86 2137.07 32.62 o 1 5 3 702.18 738.96 22.53 o 2 5 3 32.39 25.10 2.69 o 3 5 3 296.93 295.67 6.79 o 4 5 3 131.40 120.54 4.45 o 5 5 3 11.95 8.26 1.73 o -11 6 3 96.01 108.43 6.21 o -10 6 3 24.60 26.15 2.03 o -9 6 3 1.77 1.58 .95 o -8 6 3 314.88 368.37 6.64 o -7 6 3 110.75 110.56 2.20 o -6 6 3 97.86 94.99 1.82 o -5 6 3 669.94 660.91 9.25 o -4 6 3 43.98 46.91 1.20 o -3 6 3 450.87 477.17 10.47 o -2 6 3 1148.02 1152.59 19.81 o -1 6 3 395.58 444.77 8.66 o 0 6 3 95.14 84.33 1.88 o 1 6 3 158.81 159.69 3.30 o 2 6 3 85.99 91.06 3.21 o 3 6 3 185.43 178.93 4.93 o 4 6 3 208.44 240.13 11.92 o 5 6 3 45.40 37.25 2.81 o 6 6 3 1.16 1.34 3.67 o -12 7 3 6.98 2.64 3.01 o -11 7 3 18.28 10.50 1.77 o -10 7 3 391.55 424.54 10.23 o -9 7 3 250.58 264.66 6.04 o -8 7 3 5.51 4.55 .88 o -7 7 3 190.68 195.85 4.63 o -6 7 3 402.28 432.75 6.63 o -5 7 3 28.17 31.76 1.25 o -4 7 3 95.98 89.24 2.27 o -3 7 3 10.11 10.84 1.83 o -2 7 3 39.04 30.23 1.17 o -1 7 3 59.19 56.99 2.38 o 0 7 3 16.94 18.97 1.22 o 1 7 3 45.07 43.91 2.06 o 2 7 3 161.69 149.95 4.73 o 3 7 3 75.99 72.51 5.73 o 4 7 3 11.25 10.26 1.97 o 5 7 3 72.67 67.60 5.77 o -12 8 3 81.81 71.20 5.48 o -11 8 3 46.01 39.71 2.64 o -10 8 3 9.23 9.19 1.38 o -9 8 3 134.36 152.85 4.85 o -8 8 3 27.63 35.73 1.64 o -7 8 3 190.09 175.89 3.73 o -6 8 3 297.35 318.51 6.76 o -5 8 3 25.59 25.13 .90 o -4 8 3 .50 1.23 .48 o -3 8 3 337.63 335.00 6.17 o -2 8 3 150.73 154.02 3.88 o -1 8 3 9.90 7.98 1.57 o 0 8 3 62.57 54.66 2.38 o 1 8 3 14.28 17.48 1.94 o 2 8 3 1.27 .29 1.36 o 3 8 3 48.04 43.09 3.24 o 4 8 3 47.86 40.44 4.43 o -11 9 3 51.72 46.57 3.03 o -10 9 3 11.08 13.25 2.02 o -9 9 3 .61 .34 1.22 o -8 9 3 106.08 109.16 3.51 o -7 9 3 133.88 133.30 4.16 o -6 9 3 5.24 4.86 2.03 o -5 9 3 55.60 49.66 2.25 o -4 9 3 96.53 86.60 5.67 o -3 9 3 94.39 93.70 2.42 o -2 9 3 302.07 314.78 7.14 o -1 9 3 117.15 101.71 3.47 o 0 9 3 8.61 13.07 2.34 o 1 9 3 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12.36 13.87 3.21 o 4 4 8 34.52 42.63 8.58 o -8 5 8 1.25 3.34 2.93 o -7 5 8 53.03 50.80 11.20 o -6 5 8 125.64 112.14 9.68 o -5 5 8 9.13 10.18 1.90 o -4 5 8 16.05 17.04 2.34 o -3 5 8 62.91 57.38 4.69 o -2 5 8 6.28 9.39 1.90 o -1 5 8 11.27 10.21 2.75 o 0 5 8 86.75 82.78 4.61 o 1 5 8 4.55 4.93 2.92 o 2 5 8 60.47 65.61 6.67 o 3 5 8 36.39 29.59 4.69 o -8 6 8 13.68 12.51 6.88 o -7 6 8 2.81 .72 2.66 o -6 6 8 83.71 84.14 5.55 o -5 6 8 30.27 29.38 2.86 o -4 6 8 19.95 16.98 2.03 o -3 6 8 24.11 27.89 3.14 o -2 6 8 1.92 .14 1.88 o -1 6 8 4.54 4.55 2.26 o 0 6 8 45.15 46.91 5.39 o 1 6 8 11.17 8.44 3.47 o 2 6 8 1.70 -1.76 4.40 o -7 7 8 34.44 28.08 6.68 o -6 7 8 .78 -.75 2.16 o -5 7 8 46.06 42.61 4.07 o -4 7 8 106.71 106.51 7.61 o -3 7 8 25.41 27.91 3.97 o -2 7 8 19.87 18.05 2.74 o -1 7 8 31.43 26.51 4.30 o 0 7 8 1.95 1.01 3.17 o -6 8 8 45.24 32.02 4.12 o -5 8 8 5.76 5.03 3.84 o -4 8 8 97.46 106.28 10.13 o -3 8 8 35.48 30.35 6.26 o -2 8 8 7.10 5.14 2.60 o 0 0 9 18.23 10.70 2.55 o -1 1 9 47.06 40.88 2.27 o 0 1 9 1.93 1.98 1.66 o 1 1 9 121.94 143.85 6.04 o -3 2 9 113.39 108.30 7.08 o -2 2 9 .54 -.18 1.59 o -1 2 9 14.62 16.43 2.25 o 0 2 9 260.73 264.82 12.65 o 1 2 9 111.97 109.64 8.83 o 2 2 9 29.79 32.99 4.09 o -5 3 9 25.62 21.85 4.08 o -4 3 9 37.88 35.11 5.00 o -3 3 9 25.61 30.69 2.86 o -2 3 9 61.04 57.14 3.70 o -1 3 9 10.92 8.56 2.98 o 0 3 9 27.92 30.59 3.89 o 1 3 9 53.27 44.50 6.68 o 2 3 9 10.18 10.09 4.85 o 3 3 9 2.37 2.87 6.42 o -6 4 9 11.90 10.58 3.84 o -5 4 9 10.15 10.85 2.58 o -4 4 9 46.13 42.66 4.08 o -3 4 9 27.96 23.56 2.30 o -2 4 9 30.64 29.54 4.80 o -1 4 9 70.06 73.03 5.03 o 0 4 9 36.10 29.51 3.77 o 1 4 9 17.88 32.42 5.37 o 2 4 9 17.93 11.99 4.03 o -6 5 9 31.53 30.41 5.07 o -5 5 9 5.96 5.29 2.58 o -4 5 9 .39 -.29 1.61 o -3 5 9 19.12 19.19 2.56 o -2 5 9 51.46 43.54 4.99 o -1 5 9 47.49 45.24 6.03 o 0 5 9 90.08 66.75 8.46 o 1 5 9 9.32 1.11 3.24 o -5 6 9 52.33 46.54 5.29 o -4 6 9 2.18 -.14 2.69 o -3 6 9 3.27 5.23 2.20 o -2 6 9 41.71 55.85 9.74 o -1 6 9 5.66 5.00 3.74 o -1 1 10 59.63 56.20 8.65 o 0 1 10 1.77 3.32 2.57 o 1 1 10 12.87 18.19 3.77 o -3 2 10 44.68 41.09 6.07 o -2 2 10 85.07 69.18 8.37 o -1 2 10 9.71 15.74 3.37 o 0 2 10 25.12 22.72 3.82 o 1 2 10 53.90 56.37 7.31 o -3 3 10 11.89 14.73 4.01 o -2 3 10 41.90 44.28 4.72 o -1 3 10 2.55 1.82 2.57 o 0 3 10 3.55 3.78 2.95 o