#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:38:41 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180794 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/25/2012550.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012550_Fobs loop_ _publ_author_name 'Harrity, Joseph P. A.' 'Adams, Harry' 'Davies, Mark W.' 'Wybrow, Robert A. J.' 'Johnson, Christopher N.' _publ_section_title ; 5-Butyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3-(2,4,6-trimethylphenyl)isoxazole ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o168 _journal_page_last o169 _journal_volume 58 _journal_year 2002 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.331 _cell_angle_gamma 90.000 _cell_length_a 33.1325 _cell_length_b 9.9664 _cell_length_c 27.5051 _exptl_crystal_F_000 3200.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file bm1469Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ohj18m in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 736.99 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 143236.16 136183.16 3692.56 o 6 0 0 39220.97 36731.04 831.83 o 8 0 0 38053.36 38821.25 1310.00 o 10 0 0 13121.79 14417.02 821.86 o 12 0 0 513.82 379.59 180.07 o 14 0 0 7238.25 6873.13 428.36 o 16 0 0 1487.95 1546.24 242.95 o 18 0 0 14769.76 16262.41 668.89 o 20 0 0 3319.00 2833.58 328.97 o 22 0 0 5037.14 4094.36 620.96 o 24 0 0 468.27 471.53 501.42 o 26 0 0 6954.54 6823.94 866.69 o 28 0 0 2708.91 2769.42 677.41 o 30 0 0 155.70 19.92 498.10 o 32 0 0 599.81 501.42 561.19 o 34 0 0 68.20 19.92 654.17 o 36 0 0 113.12 534.62 604.36 o 38 0 0 48.48 26.57 694.02 o 1 1 0 488.06 694.61 87.84 o 3 1 0 737.22 689.19 449.95 o 5 1 0 6331.07 6148.70 215.20 o 7 1 0 156.30 213.90 82.02 o 9 1 0 20342.28 18108.49 396.27 o 11 1 0 10.28 -22.75 110.34 o 13 1 0 49252.96 51968.79 914.45 o 15 1 0 15056.58 14979.42 423.35 o 17 1 0 46.62 -17.35 144.04 o 19 1 0 318.17 106.86 157.85 o 21 1 0 10.36 244.10 224.74 o 23 1 0 1307.54 1174.96 250.17 o 25 1 0 17.59 183.91 318.10 o 27 1 0 1099.00 795.03 341.97 o 29 1 0 1.98 -109.22 363.57 o 31 1 0 419.55 584.88 388.47 o 33 1 0 21.64 -94.31 416.74 o 35 1 0 4.20 331.53 423.70 o 37 1 0 141.68 349.03 479.83 o 0 2 0 10050.75 6777.45 441.65 o 2 2 0 3107.91 3990.67 245.71 o 4 2 0 4141.64 2876.40 1238.82 o 6 2 0 9033.66 11041.33 576.64 o 8 2 0 23029.82 25429.39 505.31 o 10 2 0 1974.14 1751.53 140.38 o 12 2 0 204.94 203.93 116.29 o 14 2 0 2596.73 2664.65 185.68 o 16 2 0 78.82 2.64 137.52 o 18 2 0 3152.75 2696.36 211.37 o 20 2 0 178.10 464.69 247.26 o 22 2 0 253.19 190.15 215.22 o 24 2 0 247.11 246.63 239.62 o 26 2 0 2.58 50.55 393.50 o 28 2 0 286.60 241.83 371.60 o 30 2 0 25.31 110.98 366.52 o 32 2 0 130.78 214.18 414.62 o 34 2 0 115.39 -115.73 426.28 o 36 2 0 544.33 870.01 541.27 o 1 3 0 7010.23 8224.87 309.83 o 3 3 0 247.77 178.83 123.54 o 5 3 0 2145.72 1784.59 163.92 o 7 3 0 1022.34 965.60 140.07 o 9 3 0 4160.32 3452.38 245.08 o 11 3 0 2173.24 2939.73 183.38 o 13 3 0 10513.58 11643.14 514.56 o 15 3 0 99.13 83.40 135.77 o 17 3 0 244.39 225.74 211.65 o 19 3 0 71.32 178.82 206.14 o 21 3 0 864.91 542.57 246.23 o 23 3 0 13576.79 13600.67 652.21 o 25 3 0 356.24 434.05 265.29 o 27 3 0 776.91 771.98 395.16 o 29 3 0 31.94 -421.75 358.64 o 31 3 0 423.38 248.38 411.49 o 33 3 0 0.51 91.99 423.29 o 35 3 0 18.64 -167.35 434.27 o 0 4 0 67916.72 67021.38 1576.20 o 2 4 0 2011.19 2396.75 209.55 o 4 4 0 2026.85 1868.41 196.90 o 6 4 0 397.97 310.90 107.23 o 8 4 0 1207.69 1192.10 163.28 o 10 4 0 1481.04 1157.62 156.41 o 12 4 0 145.36 318.11 145.00 o 14 4 0 14535.74 15308.21 451.14 o 16 4 0 766.02 791.76 230.27 o 18 4 0 16008.46 16099.64 754.77 o 20 4 0 469.26 479.09 265.11 o 22 4 0 654.39 611.37 271.56 o 24 4 0 47.56 -17.27 254.13 o 26 4 0 28.00 -119.32 292.45 o 28 4 0 68.27 451.09 310.73 o 30 4 0 3.72 409.78 395.60 o 32 4 0 199.64 294.75 452.91 o 34 4 0 3.52 -146.67 516.36 o 1 5 0 3162.35 3574.97 232.46 o 3 5 0 235.20 -16.93 165.89 o 5 5 0 1140.17 1070.37 189.28 o 7 5 0 888.12 849.85 163.63 o 9 5 0 3710.50 2807.03 678.68 o 11 5 0 939.34 902.14 171.29 o 13 5 0 6117.95 6074.06 356.12 o 15 5 0 292.74 299.21 236.61 o 17 5 0 727.48 368.59 245.61 o 19 5 0 607.53 382.87 268.10 o 21 5 0 3354.09 2650.85 354.80 o 23 5 0 850.78 897.47 298.35 o 25 5 0 519.06 137.80 303.22 o 27 5 0 7390.48 8100.56 591.52 o 29 5 0 124.94 367.36 329.98 o 31 5 0 1.74 -123.48 437.22 o 33 5 0 82.64 -81.50 452.56 o 0 6 0 4089.44 4776.11 399.66 o 2 6 0 1060.73 1294.24 196.95 o 4 6 0 2100.70 2311.53 258.87 o 6 6 0 451.77 705.89 172.12 o 8 6 0 9012.56 10115.80 474.91 o 10 6 0 430.80 393.58 178.34 o 12 6 0 1476.75 1346.39 203.76 o 14 6 0 15.98 232.26 228.76 o 16 6 0 38.05 29.98 245.67 o 18 6 0 177.75 141.69 247.10 o 20 6 0 144.36 328.56 303.16 o 22 6 0 2075.65 1961.81 354.32 o 24 6 0 957.68 1223.35 376.15 o 26 6 0 4.15 -136.50 301.06 o 28 6 0 905.12 1066.36 379.52 o 30 6 0 2.01 -111.56 350.84 o 32 6 0 41.54 -308.76 474.08 o 1 7 0 1297.01 1435.13 308.67 o 3 7 0 1376.64 1656.07 240.81 o 5 7 0 7479.73 8587.16 446.70 o 7 7 0 569.04 448.14 213.04 o 9 7 0 5000.43 4385.97 352.27 o 11 7 0 20.48 95.41 178.33 o 13 7 0 379.71 487.21 245.96 o 15 7 0 19.30 313.27 241.50 o 17 7 0 49.65 322.53 256.17 o 19 7 0 304.77 291.13 273.96 o 21 7 0 1343.46 1110.96 315.09 o 23 7 0 2487.03 2615.91 404.05 o 25 7 0 95.01 -33.69 351.85 o 27 7 0 0.51 160.97 401.29 o 29 7 0 550.71 414.93 434.81 o 0 8 0 4194.64 4205.42 480.22 o 2 8 0 138.74 309.70 258.49 o 4 8 0 277.58 370.18 239.01 o 6 8 0 795.84 899.96 223.35 o 8 8 0 548.02 533.85 208.24 o 10 8 0 2046.67 2083.48 400.29 o 12 8 0 624.85 825.84 330.91 o 14 8 0 256.07 -77.80 278.93 o 16 8 0 8.09 -54.40 306.50 o 18 8 0 186.81 654.17 340.94 o 20 8 0 203.19 206.50 354.15 o 22 8 0 226.40 82.67 365.23 o 24 8 0 7.13 53.43 376.03 o 26 8 0 189.65 478.43 424.36 o 28 8 0 125.71 -164.77 434.90 o 1 9 0 894.34 684.54 389.59 o 3 9 0 713.82 983.81 308.09 o 5 9 0 1813.19 2336.93 358.75 o 7 9 0 25.69 313.17 275.31 o 9 9 0 4554.58 4350.83 346.02 o 11 9 0 1140.86 1417.94 295.55 o 13 9 0 5971.94 5873.20 558.59 o 15 9 0 2746.24 1948.22 402.22 o 17 9 0 248.71 458.15 339.14 o 19 9 0 79.41 65.42 341.98 o 21 9 0 19.77 -169.70 371.80 o 23 9 0 487.80 665.56 410.29 o 0 10 0 2312.05 2795.99 796.96 o 2 10 0 221.91 536.75 419.08 o 4 10 0 45.85 -119.71 390.82 o 6 10 0 933.48 1189.78 480.14 o 8 10 0 629.85 747.63 376.15 o 10 10 0 615.93 514.55 401.85 o 12 10 0 1026.64 1101.77 423.75 o 14 10 0 189.33 258.83 386.26 o 16 10 0 99.61 111.34 355.38 o 18 10 0 1071.41 1303.66 448.33 o 20 10 0 58.74 3.32 547.91 o 1 11 0 169.52 275.67 483.00 o 3 11 0 90.17 -294.18 457.84 o 5 11 0 11.08 110.22 509.38 o 7 11 0 264.66 -112.90 687.37 o 9 11 0 940.06 1205.40 694.02 o 11 11 0 496.41 320.75 429.10 o 13 11 0 148.30 65.67 424.16 o -37 1 1 224.22 128.39 478.99 o -35 1 1 11.64 -376.57 391.84 o -33 1 1 8.07 69.97 375.49 o -31 1 1 1150.04 1359.73 438.92 o -29 1 1 699.55 936.36 387.24 o -27 1 1 16.27 475.47 355.31 o -25 1 1 347.95 297.85 329.14 o -23 1 1 0.32 -71.84 218.51 o -21 1 1 701.99 520.36 207.16 o -19 1 1 2537.22 2389.24 212.54 o -17 1 1 12533.02 13407.91 417.83 o -15 1 1 1404.10 1740.14 180.07 o -13 1 1 411.22 528.13 138.65 o -11 1 1 1296.47 1370.87 142.12 o -9 1 1 150560.11 149399.53 2087.11 o -7 1 1 8293.59 7459.05 306.27 o -5 1 1 31271.08 30952.04 709.86 o -3 1 1 9942.91 10279.16 303.18 o -1 1 1 12857.71 12085.56 340.08 o 1 1 1 35685.24 22859.49 6236.18 o 3 1 1 1745.90 1375.31 126.18 o 5 1 1 3426.07 3501.96 186.37 o 7 1 1 514.91 558.81 87.45 o 9 1 1 36272.44 36752.10 644.83 o 11 1 1 35006.06 36933.39 678.95 o 13 1 1 56676.38 59756.02 1010.17 o 15 1 1 43895.39 43139.55 1192.20 o 17 1 1 1444.97 1458.51 190.44 o 19 1 1 395.74 365.03 167.37 o 21 1 1 1165.31 1054.51 242.48 o 23 1 1 787.35 614.93 332.53 o 25 1 1 1441.51 1916.01 393.95 o 27 1 1 9.23 33.99 368.59 o 29 1 1 3.77 89.13 355.03 o 31 1 1 3.52 -187.03 385.29 o 33 1 1 0.05 178.25 435.33 o 35 1 1 59.06 -192.87 475.13 o 37 1 1 0.60 297.33 503.16 o -36 2 1 295.70 959.23 507.31 o -34 2 1 1.41 -302.55 404.99 o -32 2 1 1.11 -308.03 356.85 o -30 2 1 21.89 -233.89 357.80 o -28 2 1 694.22 760.17 375.14 o -26 2 1 1127.85 1071.12 300.97 o -24 2 1 726.12 701.02 251.63 o -22 2 1 64.41 -65.01 225.28 o -20 2 1 425.82 370.09 214.47 o -18 2 1 765.74 820.16 177.95 o -16 2 1 2488.23 2623.94 203.32 o -14 2 1 1192.54 1513.29 171.59 o -12 2 1 283.71 314.16 164.02 o -10 2 1 1307.82 1208.90 134.32 o -8 2 1 206.58 277.05 104.49 o -6 2 1 5068.17 4866.98 189.87 o -4 2 1 255531.94 255788.30 4859.25 o -2 2 1 10463.90 10680.25 406.25 o 0 2 1 18115.75 17910.52 545.46 o 2 2 1 86804.04 87223.52 2500.45 o 4 2 1 24103.15 23984.60 573.81 o 6 2 1 1368.19 907.72 125.10 o 8 2 1 5082.44 5220.79 187.04 o 10 2 1 8311.23 7879.76 310.10 o 12 2 1 10482.67 11171.08 317.81 o 14 2 1 122.73 90.67 120.74 o 16 2 1 194.49 49.22 128.59 o 18 2 1 14203.59 13700.67 564.38 o 20 2 1 70.91 10.24 209.53 o 22 2 1 1921.72 2106.53 299.55 o 24 2 1 107.43 270.34 246.32 o 26 2 1 24.81 34.80 325.46 o 28 2 1 2416.46 2089.23 597.72 o 30 2 1 2.43 -235.97 356.96 o 32 2 1 38.39 -90.76 414.88 o 34 2 1 94.46 349.86 436.44 o 36 2 1 266.93 118.78 487.97 o -37 3 1 55.41 117.47 465.79 o -35 3 1 16.40 268.92 493.04 o -33 3 1 41.22 720.74 453.03 o -31 3 1 929.24 618.50 426.72 o -29 3 1 10.87 183.55 372.58 o -27 3 1 135.52 399.49 287.25 o -25 3 1 3091.76 3186.91 369.47 o -23 3 1 2417.54 2497.99 328.53 o -21 3 1 310.30 233.50 252.05 o -19 3 1 1380.71 1313.32 254.11 o -17 3 1 1104.05 974.62 179.79 o -15 3 1 13.71 79.67 140.55 o -13 3 1 15668.22 18565.35 479.43 o -11 3 1 38.63 125.71 115.70 o -9 3 1 342.80 424.21 129.71 o -7 3 1 66.33 76.69 105.42 o -5 3 1 13250.37 10443.57 2418.01 o -3 3 1 14569.78 14586.56 425.38 o -1 3 1 3758.85 3999.62 229.42 o 1 3 1 100556.35 99330.95 1730.55 o 3 3 1 2231.52 1762.12 150.02 o 5 3 1 5191.64 4740.18 1098.08 o 7 3 1 66.48 -39.69 112.44 o 9 3 1 252.31 242.07 125.58 o 11 3 1 2750.89 2989.10 178.46 o 13 3 1 2121.70 2098.91 165.14 o 15 3 1 7048.13 7309.55 294.29 o 17 3 1 960.19 764.28 225.17 o 19 3 1 566.55 469.15 235.19 o 21 3 1 567.47 600.86 263.05 o 23 3 1 11899.63 11604.52 602.36 o 25 3 1 22.68 165.59 271.38 o 27 3 1 42.30 413.03 349.34 o 29 3 1 31.16 -15.44 385.64 o 31 3 1 7.10 53.92 400.78 o 33 3 1 89.32 142.03 417.88 o 35 3 1 59.97 115.69 485.35 o -36 4 1 220.75 728.14 490.98 o -34 4 1 48.98 177.27 441.70 o -32 4 1 21.09 -260.28 420.94 o -30 4 1 80.28 265.04 366.19 o -28 4 1 1313.34 1265.89 339.94 o -26 4 1 1188.87 877.51 299.00 o -24 4 1 0.53 -230.41 281.29 o -22 4 1 1339.52 1121.39 286.53 o -20 4 1 877.70 716.78 275.31 o -18 4 1 2596.59 2350.64 308.06 o -16 4 1 51.21 61.46 148.40 o -14 4 1 4899.46 4561.67 257.53 o -12 4 1 2387.20 2406.56 199.38 o -10 4 1 23.74 -101.08 125.69 o -8 4 1 423.32 363.99 130.51 o -6 4 1 406.44 361.08 135.16 o -4 4 1 4265.69 5174.60 276.02 o -2 4 1 2564.01 2768.14 235.27 o 0 4 1 19740.00 22599.25 523.93 o 2 4 1 4888.77 4710.10 230.70 o 4 4 1 7563.22 7026.57 354.64 o 6 4 1 642.92 312.27 105.93 o 8 4 1 24.13 17.04 138.52 o 10 4 1 297.50 357.03 191.41 o 12 4 1 642.79 644.61 148.46 o 14 4 1 1790.80 1936.09 190.25 o 16 4 1 1316.77 1481.30 357.75 o 18 4 1 20.88 16.09 221.59 o 20 4 1 17.25 -91.55 237.56 o 22 4 1 372.82 406.48 274.43 o 24 4 1 2248.84 2333.24 354.47 o 26 4 1 0.53 452.47 304.34 o 28 4 1 26.00 -413.39 354.10 o 30 4 1 11.22 144.21 394.96 o 32 4 1 105.83 65.86 423.06 o 34 4 1 23.41 338.09 488.35 o -33 5 1 100.45 -403.79 419.97 o -31 5 1 129.31 346.06 448.19 o -29 5 1 13.22 -116.15 322.47 o -27 5 1 4169.16 4166.98 470.96 o -25 5 1 409.25 296.25 424.38 o -23 5 1 295.00 333.91 276.37 o -21 5 1 2831.25 2633.45 347.68 o -19 5 1 148.62 134.55 234.48 o -17 5 1 2130.25 2153.88 288.72 o -15 5 1 303.83 546.65 230.38 o -13 5 1 242.54 285.48 155.66 o -11 5 1 429.02 282.64 154.17 o -9 5 1 11268.29 8547.78 1674.05 o -7 5 1 7287.14 6632.01 1130.15 o -5 5 1 7178.87 8527.27 510.27 o -3 5 1 3372.53 4249.64 297.56 o -1 5 1 411.33 444.07 147.52 o 1 5 1 1109.89 1170.38 169.19 o 3 5 1 172.92 336.67 148.29 o 5 5 1 1254.25 1404.35 168.32 o 7 5 1 0.61 -47.02 143.81 o 9 5 1 487.54 575.82 171.46 o 11 5 1 10.66 -8.44 149.51 o 13 5 1 7875.29 7483.24 543.56 o 15 5 1 3633.08 3929.90 356.70 o 17 5 1 329.65 303.22 253.15 o 19 5 1 1449.86 1644.13 306.27 o 21 5 1 391.20 433.00 288.76 o 23 5 1 464.52 330.52 284.72 o 25 5 1 537.24 539.26 309.21 o 27 5 1 196.97 269.88 319.41 o 29 5 1 106.43 313.13 451.54 o 31 5 1 39.43 -85.58 432.20 o 33 5 1 48.38 512.32 468.46 o -32 6 1 111.15 534.62 604.36 o -30 6 1 30.90 375.66 365.44 o -28 6 1 173.41 683.40 363.20 o -26 6 1 625.69 622.84 322.88 o -24 6 1 335.75 -51.62 294.29 o -22 6 1 1043.12 1191.05 330.22 o -20 6 1 15.44 -153.20 240.80 o -18 6 1 87.48 155.30 247.32 o -16 6 1 32.65 380.37 254.23 o -14 6 1 447.22 383.99 245.21 o -12 6 1 313.74 261.64 168.62 o -10 6 1 21.09 -3.50 160.31 o -8 6 1 2165.61 2289.16 269.45 o -6 6 1 0.88 21.88 200.54 o -4 6 1 356.85 36.30 194.24 o -2 6 1 1311.33 1489.30 203.22 o 0 6 1 311.09 169.46 164.58 o 2 6 1 206.96 249.46 159.85 o 4 6 1 3263.86 3729.37 255.40 o 6 6 1 111.12 65.20 152.32 o 8 6 1 2295.74 2088.71 218.93 o 10 6 1 736.03 926.78 209.52 o 12 6 1 594.53 701.29 181.03 o 14 6 1 1819.42 1612.20 288.46 o 16 6 1 0.01 189.46 252.02 o 18 6 1 689.03 391.98 284.08 o 20 6 1 288.89 293.16 280.02 o 22 6 1 1296.42 1241.41 329.39 o 24 6 1 18.46 119.16 297.55 o 26 6 1 48.07 223.68 324.91 o 28 6 1 55.57 -2.95 361.43 o 30 6 1 327.35 206.99 386.90 o 32 6 1 102.59 -222.66 472.65 o -29 7 1 0.77 219.56 417.02 o -27 7 1 0.05 98.13 362.92 o -25 7 1 1015.15 994.95 408.44 o -23 7 1 1367.76 1885.94 408.48 o -21 7 1 1282.27 1556.71 377.67 o -19 7 1 797.08 712.04 293.21 o -17 7 1 435.50 513.33 271.12 o -15 7 1 168.93 299.00 230.36 o -13 7 1 475.17 274.79 218.66 o -11 7 1 742.24 609.66 217.05 o -9 7 1 309.18 368.50 202.89 o -7 7 1 371.02 622.26 231.54 o -5 7 1 837.94 1147.09 250.83 o -3 7 1 22.27 49.93 176.74 o -1 7 1 3.57 -2.43 183.29 o 1 7 1 36.01 197.29 178.40 o 3 7 1 3774.09 3880.50 283.01 o 5 7 1 4243.66 4412.18 295.75 o 7 7 1 1548.01 1562.42 218.21 o 9 7 1 2722.50 2421.13 293.81 o 11 7 1 559.61 874.00 216.36 o 13 7 1 2084.61 1749.61 288.39 o 15 7 1 386.71 312.83 243.63 o 17 7 1 2.96 24.55 248.67 o 19 7 1 38.61 203.07 280.34 o 21 7 1 3.65 -195.06 302.77 o 23 7 1 1029.58 593.09 330.19 o 25 7 1 11.02 55.75 326.31 o 27 7 1 240.17 495.80 377.25 o 29 7 1 264.00 469.85 455.23 o -28 8 1 1.72 230.85 425.51 o -26 8 1 168.17 244.39 399.44 o -24 8 1 28.58 -33.93 336.45 o -22 8 1 232.97 186.55 372.25 o -20 8 1 165.66 250.37 344.57 o -18 8 1 2.03 -148.08 322.29 o -16 8 1 1408.31 1682.67 375.99 o -14 8 1 0.02 156.07 295.35 o -12 8 1 1.01 -6.79 279.34 o -10 8 1 974.95 1086.69 276.86 o -8 8 1 4091.27 3815.63 353.17 o -6 8 1 1444.45 1689.95 321.80 o -4 8 1 228.85 -2.52 242.14 o -2 8 1 1197.16 1032.38 221.41 o 0 8 1 7641.14 7413.48 406.59 o 2 8 1 806.76 799.13 280.51 o 4 8 1 748.46 982.61 251.63 o 6 8 1 1602.72 1298.16 223.99 o 8 8 1 68.45 36.96 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