#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/25/2012551.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012551_Fobs loop_ _publ_author_name 'van Albada, Gerard A.' 'Mutikainen, Ilpo' 'Turpeinen, Urho' 'Reedijk, Jan' _publ_section_title ; Aqua[bis(pyrimidin-2-yl-\kN)amine](carbonato-\k^2^O,O')copper(II) dihydrate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m179 _journal_page_last m181 _journal_volume 58 _journal_year 2002 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.870 _cell_angle_gamma 90.000 _cell_length_a 5.8520 _cell_length_b 12.8970 _cell_length_c 16.8010 _exptl_crystal_F_000 716.00 _reflns_d_resolution_high 0.8507 _[local]_cod_data_source_file bm1478Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' bmp25a in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 138.57 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6447.47 7169.44 17.53 o 2 0 0 2190.83 2364.21 12.47 o 3 0 0 10931.09 10868.79 32.19 o 4 0 0 1706.21 1619.12 15.30 o 5 0 0 446.13 482.49 10.19 o 6 0 0 271.37 270.74 7.95 o 1 1 0 6645.71 7990.95 19.23 o 2 1 0 29.75 37.54 1.31 o 3 1 0 2.40 -2.30 2.84 o 4 1 0 1390.37 1390.03 15.66 o 5 1 0 348.08 328.08 9.28 o 6 1 0 1862.93 1795.07 19.10 o 0 2 0 664.91 722.93 5.61 o 1 2 0 1315.92 1468.81 9.20 o 2 2 0 6110.82 6427.58 24.19 o 3 2 0 1106.38 1121.62 12.62 o 4 2 0 148.57 144.78 4.36 o 5 2 0 178.97 174.31 5.11 o 6 2 0 222.57 206.15 6.22 o 1 3 0 260.35 264.00 3.47 o 2 3 0 1698.54 1594.06 10.13 o 3 3 0 3425.28 3523.45 16.45 o 4 3 0 199.73 229.48 6.35 o 5 3 0 1141.74 1179.25 16.48 o 6 3 0 805.85 822.99 13.30 o 0 4 0 4780.78 4380.65 74.79 o 1 4 0 985.08 1011.66 6.74 o 2 4 0 236.65 262.59 4.30 o 3 4 0 3876.98 3853.78 24.51 o 4 4 0 2939.50 2879.55 21.46 o 5 4 0 258.65 260.09 7.42 o 6 4 0 1412.67 1431.13 17.15 o 1 5 0 2281.86 1955.62 10.22 o 2 5 0 5141.19 5360.82 22.71 o 3 5 0 176.43 181.29 5.46 o 4 5 0 504.99 519.37 8.67 o 5 5 0 669.03 691.03 13.33 o 6 5 0 525.37 552.84 10.64 o 0 6 0 734.96 663.17 10.92 o 1 6 0 444.37 384.35 5.28 o 2 6 0 1675.64 1757.19 12.23 o 3 6 0 65.29 67.47 2.36 o 4 6 0 196.00 198.22 4.26 o 5 6 0 3.56 5.83 2.09 o 6 6 0 108.94 105.75 3.35 o 1 7 0 3483.82 3310.17 70.35 o 2 7 0 1548.94 1559.30 16.81 o 3 7 0 19.87 25.54 1.63 o 4 7 0 72.78 68.87 2.87 o 5 7 0 620.03 642.30 12.56 o 6 7 0 180.17 167.00 4.94 o 0 8 0 3475.01 3155.21 23.03 o 1 8 0 946.66 835.36 12.71 o 2 8 0 4.16 8.48 1.70 o 3 8 0 400.76 392.51 6.74 o 4 8 0 1211.24 1238.85 18.01 o 5 8 0 151.91 154.39 4.70 o 1 9 0 31.91 26.14 2.08 o 2 9 0 932.59 985.35 11.78 o 3 9 0 40.87 44.81 2.69 o 4 9 0 680.41 625.94 12.76 o 5 9 0 416.72 407.65 8.94 o 0 10 0 2.26 7.24 1.33 o 1 10 0 22.02 48.90 6.14 o 2 10 0 573.63 531.08 12.45 o 3 10 0 245.98 245.43 7.04 o 4 10 0 0.24 2.36 2.15 o 5 10 0 29.93 23.66 2.00 o 1 11 0 639.59 582.02 13.60 o 2 11 0 885.90 821.91 15.78 o 3 11 0 443.95 425.85 11.42 o 4 11 0 515.35 499.43 10.29 o 0 12 0 235.85 221.47 6.36 o 1 12 0 36.00 34.28 2.96 o 2 12 0 4.19 8.87 2.56 o 3 12 0 793.48 739.77 13.69 o 4 12 0 732.77 628.54 10.06 o 1 13 0 161.76 174.39 5.13 o 2 13 0 322.21 297.08 8.46 o 3 13 0 32.48 31.70 2.34 o 0 14 0 759.34 825.94 14.62 o 1 14 0 62.20 63.89 3.14 o 2 14 0 112.70 111.16 3.48 o -6 1 1 443.33 417.21 9.53 o -5 1 1 24.60 24.97 2.18 o -4 1 1 0.16 5.91 1.64 o -3 1 1 1127.21 1300.13 13.53 o -2 1 1 634.01 679.25 7.81 o -1 1 1 24.69 40.53 1.18 o 0 1 1 7851.83 9617.31 1210.04 o 1 1 1 1840.64 2354.46 10.90 o 2 1 1 7832.88 9111.64 26.74 o 3 1 1 1420.99 1753.20 14.45 o 4 1 1 1619.83 1578.85 16.33 o 5 1 1 590.46 600.48 11.77 o 6 1 1 300.69 315.04 8.43 o -6 2 1 666.31 643.31 11.72 o -5 2 1 1200.52 1204.19 16.80 o -4 2 1 5106.17 5275.61 32.26 o -3 2 1 764.72 812.43 11.08 o -2 2 1 14.30 7.66 1.02 o -1 2 1 3593.94 3563.57 13.64 o 0 2 1 16744.39 31649.54 2664.88 o 1 2 1 167.58 243.44 4.30 o 2 2 1 1503.93 1484.49 11.61 o 3 2 1 6295.12 6442.40 29.07 o 4 2 1 6.45 30.36 1.91 o 5 2 1 1129.90 1093.70 16.08 o 6 2 1 488.64 468.88 10.12 o -6 3 1 1689.18 1688.71 18.65 o -5 3 1 62.92 64.85 2.87 o -4 3 1 55.32 70.03 2.54 o -3 3 1 2990.91 3227.20 143.97 o -2 3 1 4839.03 5343.00 152.05 o -1 3 1 1022.62 986.48 9.57 o 0 3 1 3146.96 3240.53 102.66 o 2 3 1 7315.56 7636.56 224.32 o 3 3 1 240.90 270.49 4.82 o 4 3 1 1849.50 1916.32 19.07 o 5 3 1 500.38 470.05 10.86 o 6 3 1 631.39 580.57 11.11 o -6 4 1 17.95 27.13 2.34 o -5 4 1 26.55 24.53 2.39 o -4 4 1 102.69 114.82 3.87 o -3 4 1 592.60 717.59 11.00 o -2 4 1 881.04 1083.56 22.02 o -1 4 1 4273.55 4310.46 33.71 o 0 4 1 1336.01 1358.39 47.02 o 1 4 1 624.99 720.00 5.78 o 2 4 1 2327.16 2520.74 35.66 o 3 4 1 27.23 27.01 1.73 o 4 4 1 26.83 34.74 6.62 o 5 4 1 332.06 321.24 9.44 o 6 4 1 136.47 133.89 3.95 o -6 5 1 1014.94 1027.89 14.32 o -5 5 1 944.56 1008.42 15.99 o -4 5 1 755.74 780.53 10.68 o -3 5 1 2.23 16.11 1.67 o -2 5 1 8477.65 8773.05 25.23 o -1 5 1 4186.70 3938.40 38.88 o 0 5 1 393.00 327.47 6.87 o 1 5 1 3760.20 3318.81 40.39 o 2 5 1 2215.15 2115.07 47.16 o 3 5 1 487.86 550.26 9.93 o 4 5 1 335.97 309.13 5.91 o 5 5 1 422.09 435.18 11.03 o 6 5 1 64.45 67.78 2.88 o -6 6 1 100.19 108.12 3.24 o -5 6 1 76.65 81.54 3.02 o -4 6 1 2429.38 2495.63 18.47 o -3 6 1 2094.67 2308.58 21.27 o -2 6 1 1972.97 2043.67 13.37 o -1 6 1 4541.32 4175.11 104.52 o 0 6 1 4816.31 4304.00 53.28 o 1 6 1 11.78 27.63 1.07 o 2 6 1 1419.89 1427.76 11.10 o 3 6 1 3748.78 3695.34 26.91 o 4 6 1 1964.40 1915.22 20.88 o 5 6 1 639.39 627.53 12.78 o 6 6 1 478.88 478.74 9.75 o -6 7 1 238.95 267.51 6.93 o -5 7 1 131.27 123.81 3.71 o -4 7 1 159.72 164.18 5.16 o -3 7 1 832.27 800.24 10.49 o -2 7 1 388.43 378.67 8.64 o -1 7 1 2314.54 2323.03 35.17 o 0 7 1 902.96 869.47 14.95 o 1 7 1 497.14 494.54 6.59 o 2 7 1 202.39 187.00 5.79 o 3 7 1 8.96 12.16 1.50 o 4 7 1 708.76 741.45 14.15 o 5 7 1 637.59 623.38 12.55 o 6 7 1 104.79 95.38 5.70 o -5 8 1 21.43 24.97 2.27 o -4 8 1 68.67 56.84 2.91 o -3 8 1 25.53 24.66 3.76 o -2 8 1 34.19 44.85 2.24 o -1 8 1 232.65 210.26 5.93 o 0 8 1 293.29 283.36 5.21 o 1 8 1 964.01 987.74 13.65 o 2 8 1 1161.78 1060.41 15.23 o 3 8 1 132.07 133.04 2.70 o 4 8 1 12.99 5.34 2.21 o 5 8 1 250.68 247.58 7.09 o -5 9 1 459.34 446.53 9.54 o -4 9 1 38.02 30.59 2.38 o -3 9 1 859.17 828.75 15.18 o -2 9 1 3485.75 3722.86 39.49 o -1 9 1 449.44 429.04 10.44 o 0 9 1 3.10 8.44 1.24 o 1 9 1 790.72 710.61 12.76 o 2 9 1 937.51 1004.88 11.95 o 3 9 1 1.98 1.01 2.22 o 4 9 1 651.26 692.15 13.50 o 5 9 1 593.93 580.60 10.76 o -5 10 1 98.32 96.06 3.02 o -4 10 1 1432.19 1348.85 17.36 o -3 10 1 1024.15 972.60 16.48 o -2 10 1 6.54 14.52 2.26 o -1 10 1 2045.61 2097.75 34.84 o 0 10 1 1392.49 1346.20 26.25 o 1 10 1 298.45 332.71 7.57 o 2 10 1 197.07 176.44 5.36 o 3 10 1 547.83 579.90 13.07 o 4 10 1 419.28 414.23 10.68 o 5 10 1 29.76 24.72 2.18 o -4 11 1 99.47 90.00 3.08 o -3 11 1 27.74 31.26 2.82 o -2 11 1 232.29 228.04 7.01 o -1 11 1 0.08 18.13 2.58 o 0 11 1 14.80 17.16 1.64 o 1 11 1 0.64 4.24 2.23 o 2 11 1 59.76 59.85 3.07 o 3 11 1 7.65 13.03 2.21 o 4 11 1 31.28 33.43 2.47 o -4 12 1 127.89 118.04 3.55 o -3 12 1 162.77 172.58 5.10 o -2 12 1 0.88 -2.56 2.56 o -1 12 1 654.99 649.94 14.38 o 0 12 1 23.53 28.63 4.48 o 1 12 1 304.97 324.71 9.06 o 2 12 1 198.47 174.41 5.07 o 3 12 1 412.38 411.38 10.59 o 4 12 1 54.54 54.55 2.52 o -3 13 1 676.11 676.89 11.79 o -2 13 1 103.95 119.19 3.80 o -1 13 1 5.60 11.05 2.49 o 0 13 1 519.69 525.91 10.17 o 1 13 1 213.47 236.94 7.16 o 2 13 1 615.99 574.92 12.68 o 3 13 1 29.39 31.87 2.46 o -2 14 1 86.50 84.64 3.30 o -1 14 1 241.67 275.94 8.01 o 0 14 1 171.53 177.76 4.42 o 1 14 1 5.13 -0.64 4.35 o 2 14 1 78.15 89.01 3.18 o 0 15 1 52.47 45.95 2.17 o -6 0 2 0.26 3.36 1.73 o -5 0 2 2011.83 2042.14 21.74 o -4 0 2 4957.05 4984.17 28.22 o -3 0 2 93.14 86.43 2.63 o -2 0 2 4621.18 4794.43 18.16 o -1 0 2 1352.21 1792.17 8.60 o 0 0 2 3703.47 3700.93 102.96 o 1 0 2 3345.17 4088.59 12.89 o 2 0 2 498.32 624.05 6.68 o 3 0 2 5458.47 5366.51 23.28 o 4 0 2 1095.14 1197.70 13.72 o 5 0 2 2225.33 2407.88 22.29 o 6 0 2 1904.90 2024.20 19.99 o -6 1 2 664.93 684.49 12.24 o -5 1 2 28.08 34.89 2.46 o -4 1 2 4.15 1.64 3.46 o -3 1 2 4224.28 4144.27 21.53 o -2 1 2 1758.26 1655.11 10.75 o -1 1 2 1013.09 1087.65 6.88 o 0 1 2 2077.56 2301.68 223.04 o 1 1 2 5551.21 6444.56 18.11 o 2 1 2 316.68 357.66 5.69 o 3 1 2 2100.90 2209.59 16.12 o 4 1 2 3282.50 3460.51 23.94 o 5 1 2 231.68 242.45 7.08 o 6 1 2 34.57 39.52 2.33 o -6 2 2 233.79 228.05 6.60 o -5 2 2 251.79 265.71 7.73 o -4 2 2 226.58 321.81 8.74 o -3 2 2 118.63 146.07 4.31 o -2 2 2 202.54 288.38 5.23 o -1 2 2 143.30 130.62 3.18 o 0 2 2 651.49 669.25 63.27 o 1 2 2 7165.15 8170.91 22.20 o 2 2 2 445.64 508.72 7.20 o 3 2 2 172.53 222.87 6.08 o 4 2 2 787.24 816.46 12.54 o 5 2 2 66.51 70.48 2.83 o 6 2 2 99.82 90.14 2.83 o -6 3 2 501.49 497.60 10.78 o -5 3 2 3.53 -2.67 4.19 o -4 3 2 1188.49 1305.23 16.89 o -3 3 2 1120.70 1088.75 87.41 o -2 3 2 7952.35 8336.31 447.57 o -1 3 2 1874.05 1720.92 12.04 o 0 3 2 2313.05 2168.99 129.96 o 2 3 2 260.31 258.05 10.53 o 3 3 2 4102.91 4048.90 116.35 o 4 3 2 1328.36 1204.27 40.87 o 5 3 2 24.63 34.36 2.44 o 6 3 2 75.51 75.50 2.71 o -6 4 2 221.45 210.96 6.28 o -5 4 2 798.72 856.28 14.79 o -4 4 2 646.86 670.45 38.92 o -3 4 2 1400.65 1661.10 16.50 o -2 4 2 1863.23 1889.63 41.19 o -1 4 2 95.90 59.16 2.26 o 0 4 2 9147.49 8753.57 411.89 o 1 4 2 16660.44 15617.58 70.77 o 2 4 2 10535.31 10661.39 182.49 o 3 4 2 5610.65 5711.18 29.73 o 4 4 2 98.20 110.72 2.27 o 5 4 2 902.86 889.12 14.83 o 6 4 2 644.34 644.95 11.58 o -6 5 2 537.03 558.70 10.69 o -5 5 2 349.25 397.07 10.38 o -4 5 2 492.67 555.99 19.93 o -3 5 2 5975.25 6462.19 33.75 o -2 5 2 236.86 214.37 6.86 o -1 5 2 117.91 123.11 8.65 o 0 5 2 940.92 912.18 29.16 o 1 5 2 172.75 140.12 2.76 o 2 5 2 1074.16 1033.89 10.79 o 3 5 2 328.35 308.03 8.07 o 4 5 2 9.48 26.21 5.70 o 5 5 2 31.96 28.72 2.33 o 6 5 2 4.84 6.71 1.92 o -6 6 2 27.37 36.24 2.35 o -5 6 2 886.86 957.73 15.26 o -4 6 2 7.67 15.07 1.70 o -3 6 2 83.36 98.42 3.34 o -2 6 2 0.49 5.27 1.38 o -1 6 2 185.61 146.49 5.87 o 0 6 2 555.53 586.68 16.34 o 1 6 2 4891.20 4872.02 65.88 o 2 6 2 4.50 6.80 1.44 o 3 6 2 713.10 769.40 12.85 o 4 6 2 87.86 94.54 3.97 o 5 6 2 20.23 21.12 2.34 o 6 6 2 18.77 14.70 2.04 o -6 7 2 493.19 408.89 34.84 o -5 7 2 1495.04 1442.77 17.76 o -4 7 2 10.03 15.66 2.25 o -3 7 2 990.28 971.70 11.38 o -2 7 2 1208.44 1150.44 14.63 o -1 7 2 372.63 369.48 6.47 o 0 7 2 1569.42 1342.19 31.66 o 1 7 2 1985.95 1755.84 16.68 o 2 7 2 256.24 273.86 7.71 o 3 7 2 521.52 504.86 8.25 o 4 7 2 1838.25 1949.20 22.41 o 5 7 2 499.22 532.47 11.59 o 6 7 2 2.62 4.78 1.51 o -5 8 2 914.24 917.74 13.62 o -4 8 2 4144.26 3977.75 30.95 o -3 8 2 1397.56 1369.40 44.89 o -2 8 2 1208.13 1173.84 16.16 o -1 8 2 4854.19 4096.35 27.50 o 0 8 2 3213.16 2893.41 95.04 o 1 8 2 214.86 193.83 5.37 o 2 8 2 259.62 218.59 6.68 o 3 8 2 560.39 558.27 9.14 o 4 8 2 35.89 38.75 2.58 o 5 8 2 838.59 823.51 13.81 o -5 9 2 59.07 50.34 2.38 o -4 9 2 27.56 26.97 2.34 o -3 9 2 23.20 26.74 2.69 o -2 9 2 318.53 381.68 6.76 o -1 9 2 1803.33 1741.12 19.81 o 0 9 2 265.85 276.46 5.43 o 1 9 2 236.05 228.18 6.84 o 2 9 2 28.39 28.56 1.71 o 3 9 2 80.22 93.99 3.31 o 4 9 2 338.39 333.98 9.89 o 5 9 2 1026.56 985.28 13.71 o -5 10 2 59.28 52.26 2.26 o -4 10 2 6.22 9.55 1.99 o -3 10 2 332.99 329.70 8.76 o -2 10 2 468.53 477.86 12.22 o -1 10 2 8.16 12.51 1.69 o 0 10 2 6.54 14.59 1.04 o 1 10 2 24.21 29.03 4.55 o 2 10 2 560.85 521.71 12.71 o 3 10 2 260.74 262.33 8.05 o 4 10 2 0.29 1.07 3.60 o 5 10 2 1.94 4.04 1.87 o -4 11 2 509.09 478.15 9.71 o -3 11 2 1346.52 1394.40 18.89 o -2 11 2 861.75 827.94 15.97 o -1 11 2 6.61 9.91 2.48 o 0 11 2 376.17 349.99 20.41 o 1 11 2 1826.05 1794.77 22.70 o 2 11 2 39.51 41.50 2.93 o 3 11 2 13.33 12.21 2.48 o 4 11 2 582.23 577.47 11.20 o -4 12 2 397.71 338.01 7.38 o -3 12 2 406.06 364.51 9.73 o -2 12 2 618.88 616.59 13.85 o -1 12 2 1516.98 1479.12 21.35 o 0 12 2 552.26 549.60 9.54 o 1 12 2 39.90 45.48 2.82 o 2 12 2 1765.19 1774.99 22.77 o 3 12 2 529.49 525.80 11.62 o 4 12 2 239.58 213.82 6.33 o -3 13 2 200.10 191.34 5.91 o -2 13 2 392.64 352.15 10.35 o -1 13 2 0.06 1.04 4.78 o 0 13 2 198.42 199.63 8.93 o 1 13 2 40.01 42.22 2.95 o 2 13 2 649.82 626.03 13.14 o 3 13 2 114.82 95.17 3.05 o -2 14 2 284.93 271.26 8.09 o -1 14 2 618.96 658.06 13.32 o 0 14 2 307.82 346.87 6.42 o 1 14 2 1.79 -4.40 4.40 o 2 14 2 245.07 223.36 6.38 o 0 15 2 105.77 116.70 6.56 o -6 1 3 1364.12 1318.33 16.13 o -5 1 3 3167.35 3070.66 24.61 o -4 1 3 890.55 767.84 11.12 o -3 1 3 1338.82 1151.78 11.11 o -2 1 3 1333.18 1432.23 10.14 o -1 1 3 75.11 95.76 2.71 o 0 1 3 6905.53 7342.97 187.48 o 1 1 3 2507.93 2896.31 12.58 o 2 1 3 1119.58 1245.04 10.28 o 3 1 3 7863.92 8582.34 32.16 o 4 1 3 1932.69 2104.43 19.00 o 5 1 3 348.37 373.88 9.71 o 6 1 3 109.42 120.87 3.74 o -6 2 3 367.90 377.53 9.25 o -5 2 3 723.84 749.88 13.42 o -4 2 3 1356.80 1373.97 15.84 o -3 2 3 889.08 921.25 10.70 o -2 2 3 6744.60 6032.59 21.66 o -1 2 3 6253.33 5600.63 17.31 o 0 2 3 1147.49 1239.76 113.37 o 2 2 3 1374.80 1265.49 11.13 o 3 2 3 5659.36 5813.97 28.13 o 4 2 3 2126.95 2199.88 20.17 o 5 2 3 1295.10 1275.70 17.27 o 6 2 3 44.45 49.10 2.33 o -6 3 3 536.98 564.10 11.03 o -5 3 3 87.00 95.36 3.12 o -4 3 3 154.82 214.29 21.61 o -3 3 3 2519.84 2630.45 19.36 o -2 3 3 209.06 246.22 17.54 o -1 3 3 1866.67 1780.22 23.11 o 0 3 3 10.63 -0.08 0.99 o 1 3 3 6268.44 6836.87 166.55 o 2 3 3 356.74 368.93 12.89 o 3 3 3 1231.22 1266.41 13.85 o 4 3 3 595.73 566.17 20.42 o 5 3 3 68.59 73.82 2.83 o 6 3 3 482.74 464.52 9.90 o -6 4 3 0.62 -0.17 3.29 o -5 4 3 733.39 723.07 13.81 o -4 4 3 104.09 141.31 16.77 o -3 4 3 430.16 466.20 8.94 o -2 4 3 134.95 148.41 12.30 o -1 4 3 6.45 0.21 1.59 o 0 4 3 193.84 214.32 8.57 o 1 4 3 134.82 169.93 3.31 o 2 4 3 580.77 501.66 6.48 o 3 4 3 31.84 39.94 1.93 o 4 4 3 272.89 259.99 9.22 o 5 4 3 386.70 381.08 9.96 o 6 4 3 23.64 19.46 2.17 o -6 5 3 1179.81 1254.01 15.31 o -5 5 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