#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/25/2012567.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012567_Fobs loop_ _publ_author_name 'Bore, Lothar' 'Honda, Tadashi' 'Gribble, Gordon W.' 'Lork, Enno' 'Jasinski, Jerry P.' _publ_section_title ; The anti-inflammatory triterpenoid methyl 2-cyano-3,12-dioxooleana-1,9(11)-dien-28-oate methanol solvate hydrate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o199 _journal_page_last o200 _journal_volume 58 _journal_year 2002 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.5370 _cell_length_b 8.9500 _cell_length_c 51.1280 _exptl_crystal_F_000 1208.00 _reflns_d_resolution_high 0.7694 _[local]_cod_data_source_file fr1352Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' TP-155B in P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 185.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 380.27 389.39 13.00 o 4 0 0 3010.96 2547.74 127.13 o 6 0 0 110.76 114.92 15.78 o 8 0 0 1.55 -9.00 13.87 o 1 1 0 34552.33 35419.41 913.98 o 2 1 0 8201.05 8205.21 30.10 o 3 1 0 4078.09 3710.98 68.80 o 4 1 0 131.02 102.42 14.65 o 5 1 0 756.10 795.34 38.56 o 6 1 0 0.46 15.56 10.95 o 7 1 0 4.53 15.69 10.06 o 8 1 0 14.03 26.89 13.15 o 0 2 0 81.27 97.11 4.46 o 1 2 0 70.32 62.71 4.76 o 2 2 0 420.80 799.78 35.41 o 3 2 0 754.12 1060.15 61.09 o 4 2 0 1417.05 1496.31 36.46 o 5 2 0 173.85 204.18 18.49 o 6 2 0 1149.77 997.66 73.24 o 7 2 0 8.55 7.87 13.27 o 8 2 0 1.10 0.12 11.61 o 1 3 0 278.74 350.97 10.10 o 2 3 0 10.57 11.70 7.46 o 3 3 0 203.85 345.87 26.23 o 4 3 0 24.81 110.58 26.78 o 5 3 0 320.92 375.03 30.83 o 6 3 0 22.26 45.57 22.01 o 7 3 0 86.32 125.34 36.25 o 8 3 0 4.00 16.97 22.26 o 0 4 0 5793.35 6168.12 31.75 o 1 4 0 752.70 766.69 21.84 o 2 4 0 2157.82 2221.87 64.84 o 3 4 0 149.13 297.83 50.61 o 4 4 0 92.18 114.07 19.96 o 5 4 0 1215.07 1286.93 96.61 o 6 4 0 747.62 710.22 24.21 o 7 4 0 18.51 49.56 16.55 o 1 5 0 105.45 79.06 8.22 o 2 5 0 280.91 277.31 13.98 o 3 5 0 85.58 100.02 12.64 o 4 5 0 397.27 497.42 19.96 o 5 5 0 198.68 190.09 23.28 o 6 5 0 74.73 87.28 15.21 o 7 5 0 63.24 56.65 16.96 o 0 6 0 608.85 609.77 19.38 o 1 6 0 78.81 76.64 9.21 o 2 6 0 36.14 43.02 11.13 o 3 6 0 0.10 7.33 9.61 o 4 6 0 12.89 29.15 21.72 o 5 6 0 94.42 97.01 15.63 o 6 6 0 13.72 22.39 15.43 o 7 6 0 31.30 97.31 20.82 o 1 7 0 27.26 34.78 11.14 o 2 7 0 0.21 -3.77 12.13 o 3 7 0 272.74 286.44 25.37 o 4 7 0 453.08 391.58 21.44 o 5 7 0 7.19 41.42 14.22 o 6 7 0 8.67 5.09 13.79 o 0 8 0 147.88 163.06 15.34 o 1 8 0 8.28 13.03 12.57 o 2 8 0 822.51 726.42 43.43 o 3 8 0 56.39 52.14 16.34 o 4 8 0 322.11 313.57 20.76 o 5 8 0 7.31 25.48 24.00 o 6 8 0 38.95 51.78 18.81 o 1 9 0 989.78 902.22 24.30 o 2 9 0 142.94 147.61 17.61 o 3 9 0 11.21 12.38 12.75 o 4 9 0 10.11 17.74 15.36 o 5 9 0 0.30 -11.45 13.79 o 0 10 0 890.27 812.14 31.31 o 1 10 0 288.84 309.51 19.55 o 2 10 0 374.56 334.93 35.98 o 3 10 0 7.32 -1.98 12.14 o 4 10 0 11.20 11.12 13.74 o 1 11 0 56.03 44.67 16.41 o 2 11 0 52.09 59.34 18.80 o 1 0 1 301.80 259.45 6.38 o 2 0 1 12755.71 12596.51 260.86 o 3 0 1 140.48 149.48 7.71 o 4 0 1 258.66 281.50 14.46 o 5 0 1 28.41 16.52 8.81 o 6 0 1 163.53 161.08 12.79 o 7 0 1 0.44 2.93 10.53 o 8 0 1 160.52 104.41 17.84 o 1 1 1 13254.77 16956.57 1047.53 o 2 1 1 1554.05 1429.04 23.64 o 3 1 1 1313.37 1472.57 25.44 o 4 1 1 1230.85 1269.04 31.48 o 5 1 1 222.73 242.59 11.15 o 6 1 1 620.13 562.44 21.27 o 7 1 1 65.97 61.43 11.35 o 8 1 1 23.90 12.81 11.08 o 0 2 1 1867.38 1872.70 50.91 o 1 2 1 4515.18 4541.81 71.24 o 2 2 1 2525.51 3700.90 69.62 o 3 2 1 2419.21 2614.23 51.81 o 4 2 1 131.87 123.85 10.40 o 5 2 1 1367.83 1273.46 55.68 o 6 2 1 816.15 741.21 29.44 o 7 2 1 199.81 176.59 15.62 o 8 2 1 43.59 38.10 14.59 o 0 3 1 63.73 88.08 5.86 o 1 3 1 1768.63 1905.77 40.92 o 2 3 1 655.03 697.70 16.21 o 3 3 1 259.83 586.66 13.75 o 4 3 1 315.49 459.77 14.26 o 5 3 1 852.20 762.95 27.79 o 6 3 1 612.96 600.46 22.32 o 7 3 1 208.95 170.27 25.59 o 8 3 1 57.19 75.77 15.89 o 0 4 1 92.56 75.09 7.40 o 1 4 1 1583.68 1738.14 32.08 o 2 4 1 254.04 301.87 12.88 o 3 4 1 1408.62 1454.52 37.46 o 4 4 1 77.28 170.70 12.40 o 5 4 1 1077.99 1196.54 59.63 o 6 4 1 303.52 419.14 29.09 o 7 4 1 140.72 164.56 32.61 o 0 5 1 41.34 85.77 9.98 o 1 5 1 240.69 252.49 10.23 o 2 5 1 1.23 13.73 8.89 o 3 5 1 934.09 909.42 21.64 o 4 5 1 561.10 612.55 23.83 o 5 5 1 66.49 116.07 12.96 o 6 5 1 86.50 94.63 13.98 o 7 5 1 1.98 30.55 11.62 o 0 6 1 325.93 336.59 13.50 o 1 6 1 116.53 112.38 8.34 o 2 6 1 33.64 32.89 10.21 o 3 6 1 238.94 234.63 13.82 o 4 6 1 187.55 168.84 13.55 o 5 6 1 77.49 86.04 16.98 o 6 6 1 50.82 50.76 14.10 o 7 6 1 174.08 167.36 22.39 o 0 7 1 53.94 52.28 11.36 o 1 7 1 23.13 37.62 11.97 o 2 7 1 28.16 0.08 16.57 o 3 7 1 20.21 -6.42 12.81 o 4 7 1 502.99 479.69 18.71 o 5 7 1 186.89 196.37 20.52 o 6 7 1 64.42 97.96 17.77 o 0 8 1 25.35 37.75 11.12 o 1 8 1 112.72 120.73 10.21 o 2 8 1 69.59 82.41 13.17 o 3 8 1 58.10 55.83 12.03 o 4 8 1 49.30 59.03 14.76 o 5 8 1 199.02 190.63 18.26 o 6 8 1 30.49 15.90 19.05 o 0 9 1 76.77 89.47 23.91 o 1 9 1 501.99 481.03 16.28 o 2 9 1 45.63 31.64 13.79 o 3 9 1 4.48 12.92 12.13 o 4 9 1 22.16 7.30 13.31 o 5 9 1 37.71 27.77 14.25 o 0 10 1 246.07 250.07 17.86 o 1 10 1 347.06 346.31 16.25 o 2 10 1 75.17 67.79 16.24 o 3 10 1 33.60 37.67 13.91 o 4 10 1 60.89 55.78 15.82 o 0 11 1 23.52 23.51 14.63 o 1 11 1 33.07 34.66 12.69 o 2 11 1 2.13 12.36 13.86 o 1 0 2 32593.02 28562.90 158.34 o 2 0 2 9947.50 9297.36 307.79 o 3 0 2 2142.52 1747.49 42.86 o 4 0 2 102.89 146.63 11.49 o 5 0 2 26.84 50.12 11.87 o 6 0 2 492.30 493.58 19.38 o 7 0 2 4.01 -10.93 11.57 o 8 0 2 21.41 0.73 18.51 o 1 1 2 8934.95 10371.87 409.98 o 2 1 2 4612.54 4885.64 92.28 o 3 1 2 3177.07 3080.28 92.01 o 4 1 2 563.18 506.06 17.71 o 5 1 2 469.32 437.56 14.54 o 6 1 2 107.08 110.45 12.70 o 7 1 2 116.18 123.50 13.97 o 8 1 2 90.72 72.01 23.08 o 0 2 2 301.17 349.80 16.34 o 1 2 2 3100.51 3133.42 128.66 o 2 2 2 6318.26 6799.03 237.31 o 3 2 2 1344.06 1512.58 48.31 o 4 2 2 885.09 924.32 27.85 o 5 2 2 509.21 447.87 35.63 o 6 2 2 505.30 464.94 30.12 o 7 2 2 133.04 102.01 18.42 o 8 2 2 71.90 79.26 31.05 o 0 3 2 22.62 17.34 7.36 o 1 3 2 110.85 134.61 6.61 o 2 3 2 569.07 599.14 20.77 o 3 3 2 1554.02 1898.50 61.94 o 4 3 2 592.88 610.15 21.28 o 5 3 2 43.16 108.95 14.75 o 6 3 2 61.55 100.42 16.29 o 7 3 2 50.68 20.25 15.10 o 8 3 2 72.91 56.37 17.55 o 0 4 2 113.90 165.48 9.69 o 1 4 2 937.58 1064.32 22.37 o 2 4 2 833.31 833.12 28.27 o 3 4 2 60.50 102.23 11.52 o 4 4 2 271.55 278.65 16.31 o 5 4 2 397.91 534.34 80.04 o 6 4 2 415.86 387.53 40.82 o 7 4 2 189.13 164.56 24.74 o 0 5 2 742.07 904.90 35.98 o 1 5 2 323.39 358.15 15.47 o 2 5 2 1339.49 1331.12 77.25 o 3 5 2 869.20 871.75 43.11 o 4 5 2 228.90 264.35 35.94 o 5 5 2 200.03 315.98 26.68 o 6 5 2 49.76 66.36 15.79 o 7 5 2 4.74 5.85 17.80 o 0 6 2 1024.87 992.76 26.38 o 1 6 2 335.92 326.22 12.47 o 2 6 2 1024.41 1012.54 56.95 o 3 6 2 231.92 210.20 14.32 o 4 6 2 74.09 105.01 14.61 o 5 6 2 39.65 49.15 13.90 o 6 6 2 10.07 28.11 14.43 o 7 6 2 42.79 80.04 19.51 o 0 7 2 94.04 144.12 15.66 o 1 7 2 220.78 214.53 16.90 o 2 7 2 200.55 226.13 31.28 o 3 7 2 273.68 277.23 17.00 o 4 7 2 9.61 4.37 15.01 o 5 7 2 67.97 97.15 18.53 o 6 7 2 225.19 267.21 21.03 o 0 8 2 6.52 15.51 12.21 o 1 8 2 136.09 117.37 16.44 o 2 8 2 791.41 729.67 23.64 o 3 8 2 103.91 118.96 15.53 o 4 8 2 117.76 137.21 16.52 o 5 8 2 132.11 143.45 23.00 o 6 8 2 154.32 214.72 20.93 o 0 9 2 2001.79 1739.06 41.20 o 1 9 2 5.27 17.21 16.91 o 2 9 2 83.68 73.36 16.81 o 3 9 2 45.68 39.56 17.72 o 4 9 2 224.16 179.46 20.56 o 5 9 2 56.34 45.68 19.78 o 0 10 2 1226.91 1174.72 56.36 o 1 10 2 68.71 74.24 15.54 o 2 10 2 156.49 167.44 24.64 o 3 10 2 95.62 78.38 18.91 o 4 10 2 7.03 13.81 12.66 o 0 11 2 0.70 -14.16 14.16 o 1 11 2 126.51 123.92 16.44 o 2 11 2 55.38 76.10 17.56 o 1 0 3 7550.11 7065.31 74.22 o 2 0 3 5380.02 5180.37 146.81 o 3 0 3 1446.19 1362.91 63.08 o 4 0 3 839.58 937.34 23.94 o 5 0 3 1304.53 1219.03 33.06 o 6 0 3 13.55 24.60 13.06 o 7 0 3 29.14 41.75 14.12 o 8 0 3 3.22 -3.78 11.17 o 0 1 3 11010.30 11367.55 178.57 o 1 1 3 132.17 197.87 10.57 o 2 1 3 5248.27 5094.41 203.69 o 3 1 3 633.51 729.87 18.84 o 4 1 3 616.32 594.23 20.54 o 5 1 3 86.59 85.16 11.97 o 6 1 3 133.45 175.28 13.50 o 7 1 3 5.92 9.24 10.54 o 8 1 3 93.95 86.33 17.17 o 0 2 3 1730.14 1796.20 37.76 o 1 2 3 263.88 330.41 14.69 o 2 2 3 24.58 29.82 13.34 o 3 2 3 774.63 879.70 35.35 o 4 2 3 1525.42 1599.49 96.08 o 5 2 3 192.57 225.95 21.60 o 6 2 3 110.85 99.19 16.59 o 7 2 3 117.95 89.84 15.39 o 8 2 3 61.09 66.17 14.66 o 0 3 3 1.87 -4.74 5.44 o 1 3 3 2498.71 2841.16 100.28 o 2 3 3 5496.55 5939.11 143.68 o 3 3 3 1518.59 1960.28 45.18 o 4 3 3 42.34 141.15 13.07 o 5 3 3 542.50 526.36 34.67 o 6 3 3 853.92 774.07 24.77 o 7 3 3 4.55 18.48 13.10 o 8 3 3 22.80 25.29 12.60 o 0 4 3 966.65 889.28 31.86 o 1 4 3 1117.95 1260.64 47.88 o 2 4 3 780.23 871.28 47.13 o 3 4 3 508.68 547.60 16.17 o 4 4 3 192.45 265.09 29.99 o 5 4 3 61.02 196.52 32.28 o 6 4 3 2.18 21.98 17.06 o 7 4 3 14.07 18.63 13.78 o 0 5 3 1130.49 1190.91 31.24 o 1 5 3 1475.33 1460.51 31.59 o 2 5 3 132.65 128.74 11.57 o 3 5 3 124.68 124.86 14.92 o 4 5 3 166.75 276.57 20.94 o 5 5 3 699.84 689.00 22.84 o 6 5 3 40.11 69.89 16.54 o 7 5 3 19.71 30.63 14.07 o 0 6 3 199.83 213.78 13.18 o 1 6 3 718.78 734.74 22.27 o 2 6 3 11.22 35.18 23.61 o 3 6 3 18.39 9.24 13.29 o 4 6 3 812.55 760.05 23.29 o 5 6 3 240.76 224.09 21.01 o 6 6 3 2.90 4.48 12.46 o 7 6 3 226.76 247.77 32.91 o 0 7 3 62.84 54.73 12.36 o 1 7 3 120.83 147.48 11.97 o 2 7 3 175.89 194.01 15.38 o 3 7 3 574.35 555.05 39.13 o 4 7 3 162.29 147.86 16.50 o 5 7 3 243.64 268.35 19.65 o 6 7 3 470.66 539.35 25.08 o 0 8 3 116.90 128.16 14.16 o 1 8 3 199.71 170.63 14.42 o 2 8 3 34.13 51.15 14.57 o 3 8 3 2.49 -2.88 11.92 o 4 8 3 325.60 286.82 20.80 o 5 8 3 7.38 9.18 15.61 o 6 8 3 386.95 367.56 25.43 o 0 9 3 88.74 94.57 16.32 o 1 9 3 250.13 248.94 18.10 o 2 9 3 198.45 206.86 32.81 o 3 9 3 50.38 34.20 16.46 o 4 9 3 18.67 31.12 16.57 o 5 9 3 128.02 149.00 21.58 o 0 10 3 169.33 163.42 20.35 o 1 10 3 166.01 138.50 20.70 o 2 10 3 59.07 58.95 16.25 o 3 10 3 72.11 49.83 20.21 o 4 10 3 33.69 2.01 17.18 o 0 11 3 2.28 24.39 16.13 o 1 11 3 96.20 85.26 17.19 o 2 11 3 200.01 195.28 19.31 o 1 0 4 2707.38 2497.12 62.49 o 2 0 4 1762.18 1935.05 43.67 o 3 0 4 1572.50 1400.86 34.44 o 4 0 4 132.10 125.13 10.19 o 5 0 4 134.64 150.47 14.21 o 6 0 4 1.75 -6.67 11.99 o 7 0 4 194.74 216.92 18.15 o 8 0 4 101.42 64.79 19.77 o 0 1 4 14553.74 14385.02 252.11 o 1 1 4 447.49 526.02 16.59 o 2 1 4 278.71 325.77 12.90 o 3 1 4 42.90 35.40 6.38 o 4 1 4 1484.18 1430.77 31.91 o 5 1 4 740.05 732.36 28.46 o 6 1 4 94.70 107.20 11.78 o 7 1 4 0.42 4.24 10.31 o 8 1 4 121.17 99.22 17.35 o 0 2 4 160.93 235.01 17.38 o 1 2 4 2336.60 2433.21 53.59 o 2 2 4 3424.56 3639.10 77.31 o 3 2 4 1504.82 1485.94 36.31 o 4 2 4 206.80 232.90 19.67 o 5 2 4 404.02 320.63 17.09 o 6 2 4 399.30 358.24 22.02 o 7 2 4 68.69 36.25 24.75 o 8 2 4 20.97 7.96 15.74 o 0 3 4 1411.02 1598.69 45.11 o 1 3 4 5907.26 6023.76 161.57 o 2 3 4 1789.83 2036.20 47.33 o 3 3 4 802.18 1130.51 52.62 o 4 3 4 232.59 267.01 14.24 o 5 3 4 101.36 95.76 12.93 o 6 3 4 21.10 16.70 13.15 o 7 3 4 20.23 30.47 14.75 o 8 3 4 8.33 9.68 14.92 o 0 4 4 510.24 499.63 18.20 o 1 4 4 736.47 874.65 27.82 o 2 4 4 1317.20 1394.91 32.32 o 3 4 4 848.25 965.53 21.44 o 4 4 4 345.10 368.10 18.70 o 5 4 4 455.56 557.38 21.39 o 6 4 4 244.98 236.10 18.33 o 7 4 4 13.34 21.73 12.95 o 0 5 4 396.78 471.11 21.91 o 1 5 4 936.69 1007.11 21.41 o 2 5 4 346.71 345.35 14.37 o 3 5 4 785.49 823.00 22.01 o 4 5 4 1345.59 1366.66 37.62 o 5 5 4 182.97 319.66 48.16 o 6 5 4 191.08 156.19 17.81 o 7 5 4 95.61 107.27 18.75 o 0 6 4 349.09 403.45 21.97 o 1 6 4 33.56 55.56 8.51 o 2 6 4 69.90 95.63 21.22 o 3 6 4 35.02 21.87 12.52 o 4 6 4 199.35 225.84 23.72 o 5 6 4 9.00 41.25 16.05 o 6 6 4 31.99 52.63 17.36 o 7 6 4 43.38 121.87 19.08 o 0 7 4 54.70 55.98 17.49 o 1 7 4 708.37 723.04 36.72 o 2 7 4 82.89 67.12 12.83 o 3 7 4 169.77 186.55 17.11 o 4 7 4 168.88 170.19 16.68 o 5 7 4 46.35 92.36 17.47 o 6 7 4 114.64 193.95 20.73 o 0 8 4 198.44 197.48 16.41 o 1 8 4 94.64 96.47 13.17 o 2 8 4 624.03 588.43 21.74 o 3 8 4 131.97 141.89 25.18 o 4 8 4 150.66 153.24 24.02 o 5 8 4 77.99 96.89 25.91 o 6 8 4 44.82 164.57 64.91 o 0 9 4 533.71 529.72 39.44 o 1 9 4 973.78 886.77 23.17 o 2 9 4 2.12 6.79 11.81 o 3 9 4 230.43 233.27 18.59 o 4 9 4 114.92 86.30 17.36 o 5 9 4 172.37 202.41 21.40 o 0 10 4 6.24 7.23 15.21 o 1 10 4 345.87 379.30 33.71 o 2 10 4 342.62 321.46 22.77 o 3 10 4 28.23 -2.50 17.31 o 4 10 4 19.26 26.10 14.60 o 0 11 4 51.87 37.47 19.87 o 1 11 4 45.08 16.05 15.60 o 2 11 4 40.83 6.54 17.92 o 1 0 5 3123.19 3050.62 124.77 o 2 0 5 880.21 820.42 22.01 o 3 0 5 3691.59 3692.27 77.42 o 4 0 5 5631.75 5134.34 304.00 o 5 0 5 24.20 10.87 14.30 o 6 0 5 0.61 1.12 13.57 o 7 0 5 5.00 -8.47 12.67 o 8 0 5 78.72 104.79 28.45 o 0 1 5 3517.51 3391.05 50.84 o 1 1 5 6860.30 6588.71 335.00 o 2 1 5 4887.62 4692.23 179.56 o 3 1 5 120.39 136.91 13.85 o 4 1 5 397.06 346.93 11.52 o 5 1 5 710.61 707.86 18.77 o 6 1 5 239.43 217.43 15.28 o 7 1 5 204.65 162.58 16.17 o 8 1 5 30.13 80.28 21.62 o 0 2 5 1034.05 965.81 26.14 o 1 2 5 2330.73 2341.04 47.31 o 2 2 5 1161.02 2498.77 79.45 o 3 2 5 1165.59 1210.22 29.31 o 4 2 5 757.31 752.32 29.39 o 5 2 5 299.02 249.55 15.22 o 6 2 5 100.39 120.39 14.13 o 7 2 5 265.04 234.05 23.49 o 8 2 5 1.01 9.11 13.62 o 0 3 5 27.37 20.76 6.42 o 1 3 5 751.63 921.76 19.05 o 2 3 5 3486.63 3738.29 77.08 o 3 3 5 884.77 1261.59 68.00 o 4 3 5 327.43 310.81 14.59 o 5 3 5 101.40 149.29 20.12 o 6 3 5 274.11 212.05 18.00 o 7 3 5 239.50 194.39 19.98 o 8 3 5 24.07 8.03 13.71 o 0 4 5 110.23 135.06 9.37 o 1 4 5 772.32 784.24 14.64 o 2 4 5 1138.75 1340.98 36.00 o 3 4 5 123.03 139.78 11.77 o 4 4 5 55.88 165.31 14.23 o 5 4 5 877.27 898.06 66.13 o 6 4 5 197.94 217.50 28.01 o 7 4 5 46.37 34.95 20.91 o 0 5 5 490.95 448.61 13.40 o 1 5 5 285.60 303.09 10.89 o 2 5 5 716.31 710.82 25.19 o 3 5 5 402.43 411.60 23.39 o 4 5 5 693.50 813.08 30.36 o 5 5 5 61.07 101.40 23.71 o 6 5 5 29.82 68.15 15.01 o 7 5 5 138.82 172.17 19.08 o 0 6 5 89.68 91.69 12.56 o 1 6 5 364.18 406.90 20.41 o 2 6 5 84.17 87.24 11.57 o 3 6 5 468.62 505.99 18.65 o 4 6 5 230.96 238.90 17.10 o 5 6 5 46.61 79.87 16.64 o 6 6 5 82.71 126.00 23.84 o 7 6 5 36.20 33.48 29.67 o 0 7 5 177.13 195.41 14.59 o 1 7 5 111.17 125.70 20.45 o 2 7 5 247.04 261.51 16.79 o 3 7 5 997.57 905.23 38.56 o 4 7 5 203.63 205.50 26.77 o 5 7 5 151.02 252.44 22.47 o 6 7 5 44.31 125.21 31.94 o 0 8 5 27.17 31.73 13.24 o 1 8 5 35.04 34.77 11.22 o 2 8 5 802.55 727.50 27.55 o 3 8 5 67.89 51.28 15.56 o 4 8 5 28.45 21.08 13.79 o 5 8 5 100.26 145.73 34.02 o 6 8 5 28.21 18.80 23.06 o 0 9 5 73.54 61.01 18.09 o 1 9 5 818.18 764.88 40.99 o 2 9 5 0.91 9.81 12.34 o 3 9 5 36.23 18.71 15.31 o 4 9 5 9.93 4.45 12.77 o 5 9 5 11.80 -2.62 13.86 o 0 10 5 0.68 -14.09 14.60 o 1 10 5 162.55 147.09 16.75 o 2 10 5 128.53 155.46 30.38 o 3 10 5 188.04 163.67 20.43 o 4 10 5 32.92 28.90 15.46 o 0 11 5 225.03 256.33 22.49 o 1 11 5 80.89 82.00 24.44 o 2 11 5 26.21 30.70 19.25 o 1 0 6 2479.47 2478.76 125.22 o 2 0 6 5.68 5.84 5.57 o 3 0 6 231.01 244.01 10.53 o 4 0 6 29.45 25.17 8.67 o 5 0 6 1.74 2.01 9.65 o 6 0 6 1655.40 1583.01 40.50 o 7 0 6 44.01 62.24 17.19 o 8 0 6 292.54 279.18 21.56 o 0 1 6 380.47 349.83 14.55 o 1 1 6 3913.55 3533.97 1184.10 o 2 1 6 145.22 141.44 6.36 o 3 1 6 83.28 100.54 7.71 o 4 1 6 198.29 224.10 9.95 o 5 1 6 1217.24 1133.90 27.01 o 6 1 6 33.87 46.94 11.65 o 7 1 6 496.73 486.54 26.51 o 8 1 6 67.65 58.14 13.97 o 0 2 6 1916.58 2014.03 45.28 o 1 2 6 13566.68 13835.85 462.35 o 2 2 6 3469.39 4684.22 118.06 o 3 2 6 878.04 879.28 31.28 o 4 2 6 404.21 377.67 15.75 o 5 2 6 108.95 99.78 12.91 o 6 2 6 283.02 296.45 17.75 o 7 2 6 1.51 -6.39 11.85 o 8 2 6 0.68 18.63 12.98 o 0 3 6 1720.27 1774.48 37.91 o 1 3 6 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526.48 32.23 o 2 4 30 153.80 140.98 14.26 o 3 4 30 169.30 137.29 13.84 o 4 4 30 492.79 408.63 24.64 o 5 4 30 137.88 178.65 29.37 o 6 4 30 32.32 58.93 21.15 o 0 5 30 170.55 175.89 15.25 o 1 5 30 457.88 451.91 16.38 o 2 5 30 1436.37 1576.42 38.55 o 3 5 30 210.54 158.04 14.51 o 4 5 30 57.46 41.03 13.04 o 5 5 30 79.15 93.52 25.13 o 6 5 30 84.20 117.90 26.44 o 0 6 30 607.15 658.25 21.86 o 1 6 30 118.35 122.18 13.90 o 2 6 30 14.47 13.02 13.84 o 3 6 30 42.28 16.47 21.74 o 4 6 30 37.88 33.37 27.90 o 5 6 30 5.24 17.83 22.51 o 6 6 30 31.70 -20.29 24.41 o 0 7 30 60.34 88.93 15.94 o 1 7 30 130.78 141.73 14.34 o 2 7 30 0.56 -14.02 19.77 o 3 7 30 42.85 -0.09 22.59 o 4 7 30 27.14 61.68 29.80 o 5 7 30 291.80 304.72 42.57 o 0 8 30 71.20 51.73 16.27 o 1 8 30 158.11 186.74 16.96 o 2 8 30 185.42 173.14 33.15 o 3 8 30 115.35 117.99 32.94 o 4 8 30 52.10 52.31 30.56 o 0 9 30 34.83 11.50 20.24 o 1 9 30 288.34 293.93 40.44 o 2 9 30 204.10 177.37 39.91 o 3 9 30 37.75 21.40 29.56 o 0 10 30 71.09 92.65 17.60 o 1 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1 6 52 75.17 47.19 32.29 o 2 6 52 0.68 3.75 18.63 o 0 7 52 490.91 668.02 50.71 o 1 7 52 1.42 -11.39 19.22 o 1 0 53 189.33 224.56 17.23 o 2 0 53 11.30 -22.95 22.95 o 3 0 53 14.39 -10.05 23.06 o 4 0 53 27.58 8.13 20.89 o 5 0 53 18.69 30.71 24.73 o 0 1 53 107.33 90.42 23.66 o 1 1 53 11.65 -0.84 11.30 o 2 1 53 79.63 35.00 39.07 o 3 1 53 170.56 377.31 38.31 o 4 1 53 18.44 29.34 24.76 o 5 1 53 29.13 18.93 25.48 o 0 2 53 75.46 58.17 16.19 o 1 2 53 62.81 30.91 17.24 o 2 2 53 103.20 60.46 37.86 o 3 2 53 250.29 238.94 40.13 o 4 2 53 3.52 12.43 16.14 o 0 3 53 21.34 21.20 20.52 o 1 3 53 148.51 89.02 49.12 o 2 3 53 44.64 3.76 27.04 o 3 3 53 106.62 83.04 20.60 o 4 3 53 79.62 260.37 37.39 o 0 4 53 46.34 36.09 25.65 o 1 4 53 121.30 119.58 45.70 o 2 4 53 3.37 7.66 17.09 o 3 4 53 12.46 4.96 10.99 o 4 4 53 118.12 134.41 21.86 o 0 5 53 47.00 21.78 27.60 o 1 5 53 71.38 71.01 24.35 o 2 5 53 24.24 0.81 22.52 o 3 5 53 107.55 143.08 18.97 o 0 6 53 10.37 10.87 19.73 o 1 6 53 5.45 57.37 25.09 o 2 6 53 93.66 98.73 35.39 o 0 7 53 37.15 3.08 24.90 o 0 0 54 201.85 242.60 19.75 o 1 0 54 16.01 -15.95 15.95 o 2 0 54 41.09 15.69 30.02 o 3 0 54 0.67 -1.88 21.74 o 4 0 54 4.28 2.06 22.89 o 0 1 54 75.85 46.67 15.25 o 1 1 54 88.83 92.30 41.03 o 2 1 54 124.97 21.04 29.62 o 3 1 54 292.82 433.82 42.85 o 4 1 54 115.32 193.41 36.66 o 0 2 54 248.10 340.55 22.04 o 1 2 54 5.90 29.22 14.77 o 2 2 54 329.27 310.41 43.88 o 3 2 54 56.34 25.82 36.98 o 4 2 54 70.89 124.43 18.05 o 0 3 54 175.55 198.79 31.41 o 1 3 54 42.39 42.44 28.14 o 2 3 54 22.66 -8.91 20.67 o 3 3 54 87.62 58.94 22.15 o 4 3 54 140.53 159.42 21.51 o 0 4 54 0.01 -8.10 18.45 o 1 4 54 9.69 5.84 11.33 o 2 4 54 200.60 243.53 36.74 o 3 4 54 6.90 9.71 12.16 o 0 5 54 0.46 6.02 20.07 o 1 5 54 14.97 27.13 21.10 o 2 5 54 25.03 8.74 21.32 o 3 5 54 19.37 10.35 11.76 o 0 6 54 21.89 88.89 26.06 o 1 6 54 57.50 35.47 32.99 o 2 6 54 95.97 137.03 30.09 o 1 0 55 141.01 177.42 22.93 o 2 0 55 132.09 175.61 34.42 o 3 0 55 97.97 101.24 32.82 o 4 0 55 115.72 94.74 31.61 o 0 1 55 12.28 0.46 10.93 o 1 1 55 252.46 167.11 29.47 o 2 1 55 55.42 44.28 33.15 o 3 1 55 73.98 186.17 37.51 o 4 1 55 10.60 1.74 20.66 o 0 2 55 19.55 17.10 29.10 o 1 2 55 34.92 32.34 16.17 o 2 2 55 200.52 106.63 42.33 o 3 2 55 11.73 -27.53 27.53 o 4 2 55 345.52 536.58 27.60 o 0 3 55 238.27 260.76 36.72 o 1 3 55 64.80 52.96 18.96 o 2 3 55 37.76 25.40 24.34 o 3 3 55 190.45 141.95 23.40 o 4 3 55 24.80 186.47 28.90 o 0 4 55 157.53 185.72 38.55 o 1 4 55 10.83 14.30 13.16 o 2 4 55 74.62 71.57 33.20 o 3 4 55 66.98 66.92 16.87 o 0 5 55 64.76 7.12 27.46 o 1 5 55 101.47 100.66 29.78 o 2 5 55 30.64 66.08 24.01 o 3 5 55 68.64 99.21 33.48 o 0 6 55 83.64 119.62 33.74 o 1 6 55 9.32 35.21 20.30 o 0 0 56 46.68 25.33 15.66 o 1 0 56 2.19 -15.19 15.19 o 2 0 56 44.56 -34.44 34.44 o 3 0 56 112.09 145.61 30.33 o 4 0 56 9.64 45.94 21.80 o 0 1 56 29.23 39.60 22.94 o 1 1 56 217.34 169.69 21.48 o 2 1 56 20.71 -27.03 27.03 o 3 1 56 47.92 85.89 36.49 o 4 1 56 326.02 474.68 44.61 o 0 2 56 2.64 5.01 15.36 o 1 2 56 29.08 9.57 18.22 o 2 2 56 244.65 132.48 40.46 o 3 2 56 66.02 99.61 52.48 o 4 2 56 32.12 62.92 31.67 o 0 3 56 16.27 3.70 18.88 o 1 3 56 29.10 47.41 15.72 o 2 3 56 27.65 27.39 27.05 o 3 3 56 66.15 46.05 20.06 o 4 3 56 213.69 371.39 32.22 o 0 4 56 351.01 487.20 46.62 o 1 4 56 16.22 23.07 19.55 o 2 4 56 0.52 -2.76 19.30 o 3 4 56 24.90 28.29 16.89 o 0 5 56 55.80 9.33 23.50 o 1 5 56 238.50 252.17 41.11 o 2 5 56 2.95 -15.01 15.01 o 0 6 56 41.20 22.89 20.89 o 1 6 56 2.42 6.54 22.38 o 1 0 57 5.78 -7.82 13.40 o 2 0 57 88.57 77.60 36.82 o 3 0 57 41.42 119.38 31.11 o 4 0 57 0.03 10.64 17.97 o 0 1 57 20.49 10.75 13.77 o 1 1 57 43.80 33.46 19.23 o 2 1 57 36.39 34.04 23.62 o 3 1 57 12.62 4.69 34.35 o 4 1 57 28.33 69.53 26.05 o 0 2 57 37.93 6.55 22.53 o 1 2 57 28.66 16.49 14.27 o 2 2 57 2.52 -32.66 32.66 o 3 2 57 287.86 213.86 53.29 o 4 2 57 125.87 179.97 20.48 o 0 3 57 141.99 236.20 33.90 o 1 3 57 4.79 15.62 12.06 o 2 3 57 128.56 159.76 37.02 o 3 3 57 2.13 -15.38 15.38 o 0 4 57 151.82 197.18 34.67 o 1 4 57 111.53 186.74 34.73 o 2 4 57 62.02 53.72 29.83 o 3 4 57 95.88 54.38 20.39 o 0 5 57 12.33 -5.55 21.16 o 1 5 57 72.56 81.17 28.61 o 2 5 57 56.72 71.77 25.15 o 0 0 58 0.25 -5.91 9.91 o 1 0 58 0.08 -12.64 12.64 o 2 0 58 28.98 -29.08 29.08 o 3 0 58 135.85 265.63 37.78 o 4 0 58 75.62 131.83 31.16 o 0 1 58 40.78 31.66 13.63 o 1 1 58 63.32 55.90 33.69 o 2 1 58 56.70 34.12 30.52 o 3 1 58 58.58 81.71 33.33 o 4 1 58 3.73 -18.66 18.66 o 0 2 58 116.65 180.25 32.30 o 1 2 58 73.92 90.42 21.80 o 2 2 58 50.84 99.34 27.61 o 3 2 58 241.56 204.76 60.24 o 0 3 58 1.35 27.80 20.91 o 1 3 58 18.60 23.15 16.08 o 2 3 58 79.39 123.45 33.87 o 3 3 58 112.92 106.37 32.53 o 0 4 58 0.59 14.83 20.00 o 1 4 58 14.84 -8.31 18.44 o 2 4 58 46.99 26.12 29.05 o 0 5 58 199.39 274.88 37.99 o 1 5 58 40.06 67.34 31.88 o 1 0 59 62.82 84.90 23.73 o 2 0 59 122.47 144.92 38.05 o 3 0 59 185.08 301.51 48.94 o 0 1 59 66.73 101.54 22.87 o 1 1 59 24.36 27.12 14.72 o 2 1 59 16.59 -23.44 23.44 o 3 1 59 4.34 -21.91 21.91 o 0 2 59 4.35 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61 6.45 36.34 26.05 o 3 1 61 9.73 14.08 26.35 o 0 2 61 23.53 17.50 22.76 o 1 2 61 5.36 17.19 14.80 o 2 2 61 53.67 50.22 29.35 o 3 2 61 5.42 2.73 21.54 o 0 3 61 68.01 103.60 30.32 o 1 3 61 162.12 244.07 40.53 o 2 3 61 1.21 -19.72 19.72 o 0 4 61 1.43 34.15 22.79 o 1 4 61 100.76 114.63 33.30 o 0 0 62 434.67 654.81 50.62 o 1 0 62 22.11 54.32 19.83 o 2 0 62 20.55 -23.33 26.65 o 3 0 62 105.78 242.79 45.24 o 0 1 62 83.95 136.99 40.46 o 1 1 62 65.06 59.34 23.22 o 2 1 62 41.19 56.96 35.75 o 0 2 62 18.37 -3.72 25.22 o 1 2 62 1.52 -2.15 14.28 o 2 2 62 25.81 -24.01 28.55 o 0 3 62 13.37 8.24 25.35 o 1 3 62 102.03 80.11 32.59 o 2 3 62 179.54 212.81 43.75 o 0 4 62 207.33 321.47 39.93 o 1 0 63 56.06 24.71 23.26 o 2 0 63 14.60 -14.37 25.56 o 0 1 63 1.64 -3.58 16.62 o 1 1 63 41.14 43.43 19.79 o 2 1 63 28.72 -11.26 32.39 o 0 2 63 0.26 5.43 17.17 o 1 2 63 44.18 15.44 27.14 o 2 2 63 126.52 185.35 34.15 o 0 3 63 21.79 40.40 25.61 o 1 3 63 11.28 9.94 26.02 o 0 0 64 104.45 303.27 42.62 o 1 0 64 7.78 -18.41 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