#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:38:41 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180794 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/25/2012571.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012571_Fobs loop_ _publ_author_name 'Lu, Tong-Bu' 'Luck, Rudy L.' _publ_section_title ; Interpenetrating nets in cis-bis(pyridine-4-carboxylate)nickel(II) ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m152 _journal_page_last m154 _journal_volume 58 _journal_year 2002 _space_group_IT_number 96 _symmetry_space_group_name_Hall 'P 4nw 2abw' _symmetry_space_group_name_H-M 'P 43 21 2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.6780 _cell_length_b 11.6780 _cell_length_c 8.6610 _exptl_crystal_F_000 616.00 _reflns_d_resolution_high 0.8422 _cod_data_source_file fr1362Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' nickel in P 43 21 2' _shelx_refln_list_code 4 _shelx_f_calc_maximum 165.15 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/4' '-x+1/2, y+1/2, -z+3/4' '-y, -x, -z+1/2' 'y, x, -z' 'y+1/2, -x+1/2, z+1/4' '-y+1/2, x+1/2, z+3/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 883.83 865.88 3.87 o 0 2 0 14974.36 14691.48 208.08 o 1 2 0 1418.24 1526.93 32.91 o 2 2 0 281.59 256.93 3.25 o 1 3 0 602.48 592.90 15.99 o 2 3 0 1092.50 1022.42 13.95 o 3 3 0 2349.89 2376.00 11.36 o 0 4 0 357.54 429.55 4.56 o 1 4 0 1868.45 1771.96 54.53 o 2 4 0 2218.13 2208.30 36.55 o 3 4 0 263.55 240.20 4.45 o 4 4 0 4789.66 4889.01 19.14 o 1 5 0 119.34 127.96 4.63 o 2 5 0 96.55 85.47 1.88 o 3 5 0 211.31 198.50 4.99 o 4 5 0 91.09 76.02 2.80 o 5 5 0 4612.17 4399.01 20.80 o 0 6 0 458.19 460.94 27.57 o 1 6 0 1869.67 1765.49 81.99 o 2 6 0 1684.81 1705.87 40.50 o 3 6 0 5102.01 4934.73 106.12 o 4 6 0 400.79 369.12 4.85 o 5 6 0 4383.10 4459.70 15.84 o 6 6 0 237.14 277.60 6.85 o 1 7 0 1.03 2.54 0.87 o 2 7 0 47.15 50.96 2.75 o 3 7 0 19.07 13.32 1.17 o 4 7 0 23.40 38.29 1.16 o 5 7 0 3260.51 3213.91 14.42 o 6 7 0 33.81 34.83 1.32 o 7 7 0 2823.77 2852.47 21.25 o 0 8 0 3332.17 3328.46 115.07 o 1 8 0 6347.99 6126.86 271.17 o 2 8 0 370.58 384.26 7.81 o 3 8 0 3187.77 3011.70 72.61 o 4 8 0 59.15 57.82 2.34 o 5 8 0 1205.23 1204.89 24.47 o 6 8 0 144.60 149.67 3.27 o 7 8 0 188.25 187.93 4.04 o 8 8 0 83.26 82.05 2.80 o 1 9 0 763.50 733.83 11.08 o 2 9 0 353.12 344.75 16.59 o 3 9 0 143.40 140.96 5.56 o 4 9 0 49.37 46.72 1.87 o 5 9 0 830.43 804.45 8.81 o 6 9 0 0.02 7.61 8.24 o 7 9 0 1251.68 1245.95 11.37 o 8 9 0 4.75 -1.41 4.22 o 9 9 0 1923.73 1811.17 21.13 o 0 10 0 4.33 7.99 1.32 o 1 10 0 2273.91 2137.12 134.60 o 2 10 0 614.32 619.77 8.84 o 3 10 0 614.44 610.39 8.14 o 4 10 0 135.75 140.33 3.09 o 5 10 0 239.87 234.96 9.43 o 6 10 0 11.39 13.06 1.66 o 7 10 0 467.57 447.58 13.53 o 8 10 0 202.88 192.50 7.49 o 9 10 0 14.15 15.33 2.11 o 1 11 0 1384.13 1376.55 34.80 o 2 11 0 696.05 640.51 24.71 o 3 11 0 784.20 789.87 9.50 o 4 11 0 5.21 9.03 2.20 o 5 11 0 180.81 178.68 4.26 o 6 11 0 5.71 6.22 4.12 o 7 11 0 49.03 52.22 3.61 o 8 11 0 128.23 125.65 2.67 o 0 12 0 289.55 320.44 5.29 o 1 12 0 667.37 643.50 26.57 o 2 12 0 120.34 123.75 2.64 o 3 12 0 32.22 32.69 1.55 o 4 12 0 9.06 6.55 2.13 o 5 12 0 24.37 27.67 1.66 o 6 12 0 65.03 72.36 2.02 o 1 13 0 12.29 13.75 1.61 o 2 13 0 92.11 88.18 4.33 o 3 13 0 53.61 57.79 2.90 o 4 13 0 117.49 121.56 2.74 o 0 1 1 5094.89 5698.45 51.61 o 1 1 1 406.29 466.15 10.58 o -1 2 1 27202.25 26670.80 373.03 o 0 2 1 2942.89 2823.12 71.29 o 1 2 1 27275.81 27237.29 270.70 o 2 2 1 810.24 901.82 4.27 o -2 3 1 189.02 188.13 2.38 o -1 3 1 1072.43 1065.02 4.89 o 0 3 1 1200.44 1264.27 21.46 o 1 3 1 999.94 1014.44 16.04 o 2 3 1 202.12 195.89 4.84 o 3 3 1 250.69 221.02 2.79 o -3 4 1 2590.72 2583.65 37.43 o -2 4 1 1676.69 1661.41 13.05 o -1 4 1 1116.88 1066.98 31.84 o 0 4 1 384.05 360.30 9.75 o 1 4 1 1022.37 1008.02 43.80 o 2 4 1 1531.69 1538.88 22.77 o 3 4 1 2559.29 2535.21 53.35 o 4 4 1 7476.30 7639.86 79.11 o -4 5 1 1246.15 1171.26 7.46 o -3 5 1 1011.56 1039.28 6.67 o -2 5 1 187.07 182.12 4.85 o -1 5 1 967.00 886.88 10.72 o 0 5 1 666.17 654.72 15.28 o 1 5 1 840.59 822.47 25.68 o 2 5 1 133.98 205.22 55.95 o 3 5 1 1156.87 1233.41 8.90 o 4 5 1 1282.65 1214.64 7.63 o 5 5 1 133.17 108.21 6.57 o -5 6 1 1498.13 1462.57 9.34 o -4 6 1 1500.44 1533.51 9.04 o -3 6 1 1829.91 1871.48 35.50 o -2 6 1 1480.14 1400.76 48.55 o -1 6 1 877.54 903.92 39.39 o 0 6 1 1723.12 1698.77 25.31 o 1 6 1 928.34 971.54 54.68 o 2 6 1 1365.54 1295.46 30.59 o 3 6 1 1886.24 1939.75 39.92 o 4 6 1 1545.28 1594.06 12.19 o 5 6 1 1450.49 1422.84 9.23 o 6 6 1 214.29 201.06 6.91 o -6 7 1 1551.28 1522.79 12.83 o -5 7 1 1260.37 1253.64 13.57 o -4 7 1 376.08 352.40 5.19 o -3 7 1 3404.24 3416.89 89.50 o -2 7 1 724.61 704.93 35.89 o -1 7 1 2607.86 2518.15 106.40 o 0 7 1 1372.85 1396.26 25.60 o 1 7 1 2682.20 2684.09 79.08 o 2 7 1 644.02 630.64 10.51 o 3 7 1 3517.29 3593.12 50.38 o 4 7 1 412.43 403.88 9.62 o 5 7 1 1244.75 1241.22 29.33 o 6 7 1 1627.10 1589.14 18.62 o 7 7 1 311.50 321.34 6.45 o -7 8 1 1220.58 1195.04 10.65 o -6 8 1 298.92 292.58 17.53 o -5 8 1 567.82 564.17 7.05 o -4 8 1 676.69 669.41 14.31 o -3 8 1 363.32 352.87 13.44 o -2 8 1 1147.65 1089.84 52.59 o -1 8 1 139.77 135.84 5.60 o 0 8 1 1361.69 1327.63 17.95 o 1 8 1 157.64 156.77 6.29 o 2 8 1 1183.02 1152.09 21.16 o 3 8 1 333.95 325.27 12.20 o 4 8 1 609.41 596.06 6.94 o 5 8 1 500.19 495.51 18.30 o 6 8 1 275.07 277.74 5.64 o 7 8 1 1187.56 1161.88 10.51 o 8 8 1 42.91 47.23 1.78 o -8 9 1 550.22 529.83 8.37 o -7 9 1 46.73 43.78 1.79 o -6 9 1 340.38 342.43 6.59 o -5 9 1 857.34 831.51 27.80 o -4 9 1 248.25 235.11 14.58 o -3 9 1 1345.48 1322.80 58.38 o -2 9 1 830.07 803.95 36.19 o -1 9 1 1797.16 1696.67 84.00 o 0 9 1 126.57 129.43 3.23 o 1 9 1 1915.46 1837.17 56.69 o 2 9 1 795.89 775.37 45.80 o 3 9 1 1386.91 1392.98 28.39 o 4 9 1 281.31 278.21 5.63 o 5 9 1 802.07 759.82 15.98 o 6 9 1 295.12 311.61 6.32 o 7 9 1 46.23 48.00 1.83 o 8 9 1 492.94 492.68 12.55 o 9 9 1 31.64 31.09 1.99 o -9 10 1 200.52 204.26 4.41 o -8 10 1 46.07 47.52 2.12 o -7 10 1 293.86 298.08 28.03 o -6 10 1 73.92 74.34 3.41 o -5 10 1 176.49 175.08 3.69 o -4 10 1 125.04 130.04 2.75 o -3 10 1 748.01 706.34 21.59 o -2 10 1 897.40 858.35 28.26 o -1 10 1 53.82 52.95 1.59 o 0 10 1 2197.29 2132.60 30.25 o 1 10 1 50.47 49.83 3.29 o 2 10 1 979.40 940.60 20.30 o 3 10 1 784.09 766.73 22.96 o 4 10 1 85.08 86.09 4.36 o 5 10 1 148.96 148.54 7.57 o 6 10 1 73.75 74.54 5.30 o 7 10 1 265.74 255.64 5.48 o 8 10 1 51.15 57.10 3.32 o 9 10 1 226.98 233.13 4.89 o -8 11 1 799.79 773.15 19.13 o -7 11 1 10.17 14.99 3.17 o -6 11 1 545.47 543.79 8.94 o -5 11 1 88.36 82.33 3.57 o -4 11 1 105.11 102.37 3.01 o -3 11 1 227.14 217.91 14.63 o -2 11 1 209.30 207.43 15.07 o -1 11 1 526.59 496.16 15.08 o 0 11 1 613.79 582.18 14.90 o 1 11 1 647.09 624.35 21.03 o 2 11 1 181.02 174.69 15.57 o 3 11 1 298.79 291.36 13.19 o 4 11 1 89.89 86.28 3.35 o 5 11 1 51.32 51.30 3.08 o 6 11 1 467.97 473.90 24.83 o 7 11 1 13.11 17.17 2.02 o 8 11 1 796.64 777.14 10.99 o -6 12 1 403.47 390.55 6.26 o -5 12 1 447.97 461.84 7.65 o -4 12 1 218.83 220.88 6.52 o -3 12 1 667.88 652.14 7.74 o -2 12 1 253.41 243.91 7.54 o -1 12 1 239.52 245.86 5.13 o 0 12 1 644.08 636.61 11.84 o 1 12 1 224.22 220.01 3.88 o 2 12 1 296.94 280.20 4.86 o 3 12 1 680.96 645.29 7.91 o 4 12 1 251.90 256.97 4.45 o 5 12 1 406.62 412.15 7.01 o 6 12 1 438.06 433.78 6.85 o -4 13 1 132.86 139.25 2.44 o -3 13 1 432.48 420.96 6.89 o -2 13 1 245.48 249.05 9.91 o -1 13 1 227.98 222.56 3.79 o 0 13 1 99.49 90.62 3.27 o 1 13 1 266.99 266.05 6.05 o 2 13 1 217.90 220.28 10.29 o 3 13 1 477.40 479.05 11.44 o 4 13 1 139.19 138.86 7.79 o 0 1 2 461.64 455.77 3.01 o 1 1 2 35.85 34.66 1.09 o -1 2 2 314.57 337.54 4.15 o 0 2 2 215.87 273.72 5.35 o 1 2 2 335.34 365.08 4.22 o 2 2 2 1049.96 1164.82 7.71 o -2 3 2 3096.03 3168.61 13.64 o -1 3 2 16584.26 17468.71 123.78 o 0 3 2 517.66 474.80 9.60 o 1 3 2 16345.62 18226.88 116.47 o 2 3 2 3130.91 3082.92 13.63 o 3 3 2 3137.03 3193.60 14.49 o -3 4 2 2917.30 2892.79 15.44 o -2 4 2 1711.11 1800.23 11.66 o -1 4 2 249.28 273.04 4.73 o 0 4 2 8641.70 9656.22 455.17 o 1 4 2 215.76 242.10 4.32 o 2 4 2 1863.58 2061.19 11.76 o 3 4 2 2776.49 2667.80 15.03 o 4 4 2 1126.76 1118.64 10.03 o -4 5 2 1454.33 1452.17 12.05 o -3 5 2 837.14 818.28 8.96 o -2 5 2 4940.61 4987.77 20.69 o -1 5 2 4600.88 4404.80 20.11 o 0 5 2 3426.60 3169.28 29.66 o 1 5 2 4409.08 4509.34 18.30 o 2 5 2 5199.05 4949.53 20.54 o 3 5 2 658.64 636.16 7.73 o 4 5 2 1462.72 1421.10 11.95 o 5 5 2 374.63 410.18 7.31 o -5 6 2 496.31 505.69 8.39 o -4 6 2 1781.50 1805.18 14.37 o -3 6 2 686.79 761.82 9.30 o -2 6 2 1615.34 1625.45 12.83 o -1 6 2 362.71 416.99 6.88 o 0 6 2 527.99 528.25 5.25 o 1 6 2 383.08 404.31 6.68 o 2 6 2 1569.46 1559.04 12.14 o 3 6 2 626.18 672.16 8.63 o 4 6 2 1811.41 1824.81 14.24 o 5 6 2 492.50 486.88 8.36 o 6 6 2 814.39 783.17 10.70 o -6 7 2 305.48 294.18 7.83 o -5 7 2 416.94 410.12 8.43 o -4 7 2 914.63 907.30 11.32 o -3 7 2 295.46 292.41 6.81 o -2 7 2 2535.68 2627.27 17.61 o -1 7 2 14.93 17.44 1.44 o 0 7 2 2922.50 2728.95 86.12 o 1 7 2 11.34 11.79 1.36 o 2 7 2 2605.19 2507.78 16.90 o 3 7 2 325.73 306.66 6.77 o 4 7 2 862.40 837.50 10.66 o 5 7 2 396.87 391.71 8.07 o 6 7 2 275.60 252.86 7.32 o 7 7 2 53.34 51.65 2.20 o -7 8 2 100.78 102.79 3.25 o -6 8 2 815.19 775.59 12.07 o -5 8 2 414.93 428.82 9.08 o -4 8 2 1470.02 1488.72 15.32 o -3 8 2 313.65 347.48 7.89 o -2 8 2 494.73 504.79 9.07 o -1 8 2 68.54 73.77 1.98 o 0 8 2 106.72 98.58 4.20 o 1 8 2 71.16 73.13 1.99 o 2 8 2 545.21 539.41 8.96 o 3 8 2 330.00 318.72 7.58 o 4 8 2 1491.25 1497.36 14.84 o 5 8 2 440.60 425.03 9.16 o 6 8 2 763.85 708.93 11.66 o 7 8 2 106.34 118.42 3.37 o 8 8 2 582.52 575.31 12.00 o -8 9 2 39.14 41.03 2.70 o -7 9 2 311.39 303.68 8.33 o -6 9 2 316.12 317.89 9.21 o -5 9 2 50.31 53.26 2.39 o -4 9 2 1299.02 1321.92 15.43 o -3 9 2 279.17 296.41 8.16 o -2 9 2 1806.53 1855.77 17.31 o -1 9 2 262.30 280.66 7.53 o 0 9 2 1827.54 1745.84 49.74 o 1 9 2 267.96 266.91 7.57 o 2 9 2 1954.34 1882.52 17.01 o 3 9 2 271.75 285.58 7.58 o 4 9 2 1278.89 1159.24 14.66 o 5 9 2 51.90 46.06 2.32 o 6 9 2 241.50 238.34 7.29 o 7 9 2 304.23 299.91 7.99 o 8 9 2 47.68 47.60 2.78 o 9 9 2 98.25 99.84 3.37 o -9 10 2 12.47 20.92 3.05 o -8 10 2 1076.85 1079.43 17.14 o -7 10 2 90.71 87.57 3.18 o -6 10 2 1761.96 1768.40 19.96 o -5 10 2 155.17 157.49 4.83 o -4 10 2 1373.08 1403.25 16.87 o -3 10 2 20.54 17.56 2.32 o -2 10 2 24.58 30.42 2.26 o -1 10 2 193.54 199.17 6.47 o 0 10 2 7.74 9.30 1.37 o 1 10 2 196.29 185.59 5.60 o 2 10 2 45.69 43.82 2.31 o 3 10 2 17.09 19.66 2.20 o 4 10 2 1233.50 1223.46 15.47 o 5 10 2 172.15 166.80 4.75 o 6 10 2 1649.59 1597.69 18.39 o 7 10 2 102.17 100.71 3.20 o 8 10 2 1014.90 985.87 16.54 o 9 10 2 18.20 19.72 3.00 o -8 11 2 9.28 9.01 3.18 o -7 11 2 66.14 66.41 3.28 o -6 11 2 255.07 261.82 8.49 o -5 11 2 396.30 386.34 11.05 o -4 11 2 1162.49 1181.33 17.12 o -3 11 2 220.18 235.26 6.85 o -2 11 2 1550.41 1558.69 18.61 o -1 11 2 199.69 205.90 6.02 o 0 11 2 1057.94 1003.07 40.33 o 1 11 2 218.58 212.72 6.27 o 2 11 2 1739.51 1605.54 19.11 o 3 11 2 190.92 184.57 5.35 o 4 11 2 1224.91 1170.83 16.77 o 5 11 2 435.69 423.33 10.82 o 6 11 2 230.56 237.16 7.28 o 7 11 2 65.17 65.05 3.18 o 8 11 2 10.41 10.77 3.13 o -6 12 2 552.82 547.01 9.91 o -5 12 2 445.96 422.20 8.77 o -4 12 2 283.21 265.98 20.89 o -3 12 2 136.27 134.65 2.91 o -2 12 2 9.84 13.88 2.41 o -1 12 2 87.72 81.82 3.16 o 0 12 2 3.61 24.28 6.16 o 1 12 2 98.19 81.12 3.05 o 2 12 2 22.09 19.77 2.55 o 3 12 2 134.36 117.28 3.44 o 4 12 2 267.87 265.79 7.90 o 5 12 2 456.89 405.31 11.87 o 6 12 2 562.35 546.09 13.77 o -4 13 2 168.16 177.99 3.67 o -3 13 2 561.25 563.13 21.06 o -2 13 2 406.52 434.03 8.90 o -1 13 2 369.90 331.95 11.17 o 0 13 2 172.42 162.25 3.26 o 1 13 2 370.19 351.00 9.80 o 2 13 2 412.56 362.43 10.75 o 3 13 2 558.93 558.03 13.77 o 4 13 2 145.93 124.37 4.07 o 0 1 3 17.94 30.47 3.78 o 1 1 3 742.70 873.46 7.05 o -1 2 3 334.72 301.28 4.60 o 0 2 3 514.04 481.56 67.99 o 1 2 3 299.41 256.45 4.31 o 2 2 3 503.21 532.51 6.10 o -2 3 3 3267.51 3162.96 15.76 o -1 3 3 2220.38 1817.79 14.05 o 0 3 3 5131.15 4901.03 239.77 o 1 3 3 2387.85 2637.65 13.13 o 2 3 3 3338.72 3201.81 15.50 o 3 3 3 3217.42 3297.41 16.20 o -3 4 3 1437.99 1383.76 12.39 o -2 4 3 1234.83 1149.28 10.61 o -1 4 3 8494.01 8143.29 26.68 o 0 4 3 4854.78 4464.26 1521.88 o 1 4 3 8344.64 8353.90 25.20 o 2 4 3 1201.44 1194.73 9.89 o 3 4 3 1345.88 1365.47 11.54 o 4 4 3 1237.37 1306.82 11.42 o -4 5 3 523.23 535.25 8.27 o -3 5 3 1398.07 1410.88 12.30 o -2 5 3 2905.28 2907.66 17.02 o -1 5 3 3943.25 2187.11 22.93 o 0 5 3 5481.39 5066.42 320.82 o 1 5 3 4157.19 4398.12 19.54 o 2 5 3 2819.69 2835.58 16.14 o 3 5 3 1395.91 1411.63 11.99 o 4 5 3 445.09 462.96 7.75 o 5 5 3 543.40 509.60 8.24 o -5 6 3 589.92 615.02 9.65 o -4 6 3 1010.98 1040.45 11.59 o -3 6 3 702.25 722.34 9.53 o -2 6 3 636.14 623.85 8.76 o -1 6 3 241.17 269.60 6.11 o 0 6 3 3081.04 3171.64 18.07 o 1 6 3 328.33 355.11 6.80 o 2 6 3 652.28 619.75 8.48 o 3 6 3 775.75 769.90 9.79 o 4 6 3 931.98 926.64 10.79 o 5 6 3 531.44 526.14 9.21 o 6 6 3 1454.32 1439.04 14.68 o -6 7 3 216.06 224.78 6.26 o -5 7 3 96.88 108.20 3.22 o -4 7 3 919.61 915.88 11.72 o -3 7 3 457.90 472.21 8.59 o -2 7 3 1536.70 1559.02 14.29 o -1 7 3 1329.44 1350.10 13.41 o 0 7 3 103.39 111.58 2.36 o 1 7 3 1446.95 1455.74 13.29 o 2 7 3 1425.97 1334.04 13.39 o 3 7 3 483.43 486.15 8.48 o 4 7 3 1004.47 933.51 12.06 o 5 7 3 94.66 97.01 2.94 o 6 7 3 341.56 339.82 8.52 o 7 7 3 3.43 2.47 5.15 o -7 8 3 243.06 236.67 7.46 o -6 8 3 63.85 66.28 2.52 o -5 8 3 2415.73 2319.26 20.29 o -4 8 3 166.80 164.14 4.69 o -3 8 3 528.46 552.62 9.77 o -2 8 3 669.03 632.40 10.63 o -1 8 3 85.83 87.82 2.82 o 0 8 3 1709.53 1714.11 37.60 o 1 8 3 99.43 88.76 2.42 o 2 8 3 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737.06 323.24 10.17 o -1 4 9 419.51 230.31 7.64 o 0 4 9 515.78 354.34 212.14 o 1 4 9 417.19 465.23 12.33 o 2 4 9 829.16 889.91 16.79 o 3 4 9 317.17 313.90 9.23 o 4 4 9 208.59 211.29 6.61 o -4 5 9 104.08 89.61 3.91 o -3 5 9 73.99 59.64 3.61 o -2 5 9 352.19 245.02 7.29 o -1 5 9 437.98 241.56 8.17 o 0 5 9 49.61 37.22 8.38 o 1 5 9 393.78 448.15 12.46 o 2 5 9 320.64 342.27 10.05 o 3 5 9 71.69 82.36 3.41 o 4 5 9 98.72 97.24 3.75 o -3 6 9 482.02 513.43 14.15 o -2 6 9 322.56 354.73 10.24 o -1 6 9 267.60 290.08 8.63 o 0 6 9 510.49 573.40 16.36 o 1 6 9 262.48 260.93 7.69 o 2 6 9 391.94 402.26 10.91 o 3 6 9 490.01 514.78 14.31 o 0 1 10 32.68 34.49 5.34 o 1 1 10 743.48 718.06 17.17 o -1 2 10 17.28 10.98 3.00 o 0 2 10 162.35 162.02 13.00 o 1 2 10 22.93 22.80 3.03 o 2 2 10 154.60 167.71 5.11 o -1 3 10 363.08 307.81 9.77 o 0 3 10 426.86 421.48 67.65 o 1 3 10 351.42 401.16 11.01 o