#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/25/2012590.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2012590_Fobs
loop_
_publ_author_name
'Kato, Masako'
'Ogawa, Yuki'
'Kozakai, Mikiko'
'Sugimoto, Yukihiro'
_publ_section_title
;
 Bis(8-quinolinolato-<i>N</i>,<i>O</i>)platinum(II) and its synthetic
 intermediate, 8-hydroxyquinolinium
 dichloro(8-quinolinolato-<i>N</i>,<i>O</i>)platinate(II) tetrahydrate
;
_journal_issue                   3
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              m147
_journal_page_last               m149
_journal_volume                  58
_journal_year                    2002
_space_group_IT_number           14
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_[local]_cod_data_source_file    oa1121Isup2.hkl
_[local]_cod_data_source_block   I
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_F_squared_calc
_refln_observed_status
1 0 -1 27849.39 624.39 30286.96 o
1 0 1 41247.21 915.16 40249.76 o
0 0 2 28323.97 631.87 28170.36 o
2 0 0 17694.92 400.28 17681.98 o
2 0 -2 4165.56 113.73 4292.13 o
1 0 -3 7537.81 179.62 7982.12 o
0 -1 1 8433.65 198.47 8417.77 o
1 -1 0 10236.47 239.12 10049.00 o
1 -1 -1 121.15 12.23 99.83 o
1 -1 1 9.05 17.46 7.57 o
0 -1 2 177.83 14.00 154.19 o
1 -1 -2 41435.55 930.45 40737.07 o
3 0 -1 22587.72 514.49 22789.18 o
1 0 3 12182.23 283.09 12613.84 o
2 0 2 5549.86 137.29 5765.23 o
2 -1 -1 23483.75 536.16 22824.98 o
2 -1 0 315.59 25.05 284.50 o
1 -1 2 22335.60 507.79 22186.64 o
2 -1 -2 13460.97 327.83 12279.77 o
0 0 4 20945.03 478.21 21197.82 o
3 0 -3 13442.18 326.36 13581.91 o
2 -1 1 17992.33 413.28 17711.87 o
3 0 1 13042.31 304.61 13171.96 o
1 -1 -3 6347.83 159.11 5965.05 o
2 0 -4 20112.91 463.67 20349.06 o
0 -1 3 15349.50 355.52 15533.60 o
2 -1 -3 33599.41 766.91 33220.51 o
3 -1 -1 -20.82 23.28 0.92 o
1 -1 3 66.65 7.25 64.69 o
2 -1 2 3.55 19.74 5.91 o
3 -1 -2 15183.72 362.37 14947.18 o
3 -1 0 10825.78 259.00 10737.50 o
4 0 -2 10566.18 258.75 10558.81 o
1 -1 -4 17124.22 398.81 17354.06 o
1 0 -5 17408.04 404.83 17793.25 o
4 0 0 11445.70 274.06 11673.81 o
0 -1 4 659.76 33.76 640.50 o
3 -1 -3 366.43 31.16 322.87 o
3 -1 1 99.21 10.06 89.12 o
2 -1 -4 234.34 21.85 230.67 o
2 -1 3 9995.27 242.05 10177.79 o
2 0 4 11599.95 277.42 11449.00 o
3 0 -5 8449.90 216.08 8674.41 o
1 -1 4 11619.81 278.40 11701.25 o
3 0 3 20374.13 471.22 19735.04 o
4 0 -4 6484.02 179.15 6508.40 o
3 -1 -4 9947.54 256.40 10221.82 o
3 -1 2 8392.59 207.65 8447.35 o
4 -1 -1 12672.38 305.11 12357.15 o
4 -1 -2 20.11 26.47 0.23 o
1 0 5 3781.14 106.05 3992.71 o
1 -1 -5 280.23 20.75 251.94 o
4 -1 0 1733.22 63.25 1627.62 o
0 -2 0 7803.68 195.99 7510.76 o
2 -1 -5 17219.79 406.84 17410.26 o
4 -1 -3 11048.36 281.52 11092.07 o
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1 -2 0 228.15 19.35 205.40 o
0 -1 5 10907.52 264.87 11307.97 o
4 0 2 14262.84 338.81 14194.04 o
1 -2 -1 13086.00 327.97 12286.86 o
2 0 -6 10493.72 258.29 11238.95 o
5 0 -1 14552.28 348.32 14531.86 o
1 -2 1 8178.40 204.86 8233.12 o
4 -1 1 20811.74 484.17 20028.43 o
2 -1 4 55.94 7.88 56.07 o
0 -2 2 12393.08 298.13 12122.63 o
5 0 -3 13638.89 336.55 13645.54 o
1 -2 -2 890.52 48.84 708.83 o
3 -1 -5 2217.99 82.13 2059.31 o
0 0 6 9311.04 230.94 9480.74 o
3 -1 3 1036.53 47.23 1014.75 o
4 -1 -4 -50.35 35.54 2.57 o
2 -2 -1 73.57 9.57 67.72 o
2 -2 0 12391.02 300.48 11977.70 o
1 -1 5 66.42 8.22 54.22 o
1 -2 2 199.35 16.53 209.26 o
2 -2 -2 8375.13 233.42 8035.85 o
2 -2 1 -6.76 23.24 8.12 o
1 -2 -3 15084.19 363.17 14692.90 o
0 -2 3 580.41 37.61 565.28 o
4 -1 2 241.81 20.00 219.13 o
5 0 1 13901.31 334.65 14065.13 o
1 -1 -6 12875.17 312.38 13043.83 o
2 -1 -6 536.19 39.71 501.18 o
5 -1 -2 8625.04 223.29 8886.15 o
5 -1 -1 45.78 9.39 50.22 o
2 -2 -3 1054.84 61.05 925.51 o
4 -1 -5 8709.35 237.09 8799.27 o
4 0 -6 9294.68 245.58 9602.41 o
5 -1 -3 112.76 11.89 103.77 o
3 -2 -1 11711.90 290.66 11263.13 o
0 -1 6 130.03 12.34 136.19 o
1 -2 3 12501.71 303.34 12356.10 o
2 -2 2 15718.73 374.55 15397.38 o
3 -2 -2 -32.57 31.71 8.01 o
5 -1 0 17590.54 417.81 17151.41 o
5 0 -5 8130.50 222.70 7990.70 o
3 -2 0 173.22 16.52 159.78 o
3 -1 -6 14611.17 358.10 14757.08 o
3 -1 4 6741.99 176.87 7011.62 o
2 -1 5 13242.59 320.38 13274.53 o
1 0 -7 12347.67 302.14 12747.35 o
1 -2 -4 733.08 42.31 555.77 o
5 -1 -4 9849.82 263.56 10036.75 o
0 -2 4 14237.38 343.56 14247.55 o
3 -2 -3 10567.31 284.08 10614.34 o
3 -2 1 10647.22 264.64 10458.90 o
2 -2 -4 9823.47 253.90 9870.39 o
3 0 -7 12416.35 308.54 12699.41 o
3 0 5 12365.90 302.04 12391.35 o
4 -1 3 9075.25 229.71 9260.91 o
6 0 -2 26501.58 619.66 25713.78 o
5 -1 1 58.12 9.45 52.91 o
1 -1 6 12456.29 304.65 12198.96 o
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2 -2 3 107.62 10.99 103.80 o
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1 -2 4 45.73 9.02 46.52 o
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3 -2 2 237.54 20.50 220.66 o
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1 -2 -5 10426.85 263.41 10159.64 o
4 -2 0 5928.84 163.64 5900.62 o
1 0 7 6286.08 170.90 6496.33 o
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0 -2 5 -0.45 25.41 0.36 o
6 -1 -2 30.35 28.40 51.13 o
0 -1 7 6175.21 168.42 6523.18 o
6 -1 -3 8077.65 219.69 8088.35 o
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2 -1 6 51.55 8.97 49.50 o
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4 -2 1 36.60 24.52 30.87 o
2 -2 4 10725.08 269.37 10824.44 o
2 0 -8 11262.12 284.06 11519.41 o
3 -2 -5 16985.74 421.32 16867.13 o
3 -2 3 16230.10 391.19 15592.10 o
4 -2 -4 16707.47 423.39 16305.43 o
5 -1 -6 7437.67 213.75 7620.30 o
6 -1 -4 115.26 14.18 123.98 o
6 -1 0 31.15 9.58 24.61 o
4 -1 -7 6792.87 194.29 6991.72 o
1 -2 5 8206.49 214.24 8294.13 o
5 0 -7 11420.46 303.97 11232.40 o
1 -1 7 71.56 9.81 77.81 o
5 -1 3 -3.43 25.64 0.21 o
0 0 8 10141.78 258.68 10111.06 o
6 0 -6 6291.87 187.42 6340.39 o
4 -2 2 7661.27 203.81 7691.72 o
1 -2 -6 217.38 20.24 229.49 o
6 0 2 12713.85 315.92 12808.26 o
2 -2 -6 6845.58 189.61 6916.36 o
6 -1 -5 7983.92 227.87 8241.68 o
5 -2 -2 177.12 17.68 174.40 o
4 0 -8 17832.74 437.35 17906.28 o
5 -2 -1 8391.65 223.52 8337.52 o
6 -1 1 9089.39 236.95 9262.13 o
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7 0 -3 9954.96 264.45 10010.42 o
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2 -1 -8 4.64 29.24 22.32 o
0 -2 6 8165.67 215.59 8292.04 o
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5 -2 0 158.43 14.08 150.98 o
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3 -2 -6 1446.16 71.32 1275.34 o
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3 -2 4 243.36 19.15 217.48 o
2 -2 5 16.01 27.35 16.29 o
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4 -1 -8 99.85 12.60 73.57 o
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2 -3 0 25.19 20.33 17.79 o
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