#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:40:40 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180798 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/29/2012983.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2012983_Fobs loop_ _publ_author_name 'Huang, Xinjiang' 'Kuhn, Genevieve H.' 'Nesterov, Vladimir N.' 'Averkiev, Boris B.' 'Penn, Benjamin' 'Antipin, Mikhail Yu.' 'Timofeeva, Tatiana V.' _publ_section_title ; (E)-(4-Hydroxyphenyl)(4-nitrophenyl)diazene, (E)-(4-methoxyphenyl)(4-nitrophenyl)diazene and (E)-[4-(6-bromohexyloxy)phenyl](4-cyanophenyl)diazene ; _journal_issue 10 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o624 _journal_page_last o628 _journal_volume 58 _journal_year 2002 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 86.502 _cell_angle_beta 80.511 _cell_angle_gamma 87.604 _cell_length_a 7.4279 _cell_length_b 12.0094 _cell_length_c 19.5524 _exptl_crystal_F_000 792.00 _reflns_d_resolution_high 0.7093 _cod_data_source_file gg1133IIIcsup4.hkl _cod_data_source_block IIIc #BEGIN Tags that were not found in dictionaries: _shelx_title ' v2m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 146.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ 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400.93 408.77 100.17 o 8 5 0 625.97 742.22 186.90 o 9 5 0 453.18 411.52 252.73 o -9 6 0 43.57 -115.78 263.98 o -8 6 0 771.76 749.53 181.15 o -7 6 0 788.50 871.99 168.37 o -6 6 0 2055.15 2033.02 185.01 o -5 6 0 1050.34 1174.94 98.28 o -4 6 0 1801.49 1672.99 93.66 o -3 6 0 885.05 778.31 73.56 o -2 6 0 113.05 28.03 38.30 o -1 6 0 142.86 96.96 38.35 o 0 6 0 1901.51 1916.36 109.27 o 1 6 0 4648.09 4847.33 166.21 o 3 6 0 1775.28 1680.63 88.73 o 4 6 0 234.69 192.65 64.08 o 5 6 0 31.34 -22.17 66.52 o 6 6 0 362.15 375.91 96.44 o 7 6 0 343.89 237.86 101.09 o 8 6 0 160.41 104.96 129.22 o -9 7 0 3.41 541.19 338.74 o -8 7 0 23.29 39.76 153.62 o -7 7 0 20.26 71.66 116.10 o -6 7 0 427.51 380.94 124.64 o -5 7 0 79.41 66.72 61.32 o -4 7 0 19.32 -3.03 50.75 o -3 7 0 145.91 115.75 51.08 o -2 7 0 884.28 772.74 73.76 o -1 7 0 1796.30 1754.70 80.64 o 0 7 0 2581.75 2536.92 135.16 o 1 7 0 282.32 250.48 74.32 o 2 7 0 190.92 154.30 77.74 o 3 7 0 350.51 310.74 63.85 o 4 7 0 3043.11 3015.49 130.48 o 5 7 0 746.99 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485.72 609.53 162.44 o 7 9 0 741.13 606.55 170.51 o 8 9 0 440.73 317.57 264.64 o -8 10 0 32.10 56.90 247.44 o -7 10 0 143.64 104.17 147.99 o -6 10 0 264.82 286.63 131.63 o -5 10 0 242.36 167.06 111.15 o -4 10 0 5.69 -27.32 62.85 o -3 10 0 78.54 69.27 77.09 o -2 10 0 202.24 145.10 81.24 o -1 10 0 744.52 760.93 123.17 o 0 10 0 481.73 372.74 103.24 o 1 10 0 399.64 292.89 106.56 o 2 10 0 360.62 337.54 114.42 o 3 10 0 2.54 -29.83 92.10 o 4 10 0 68.47 61.04 112.17 o 5 10 0 23.79 34.53 113.98 o 6 10 0 0.61 45.66 132.57 o 7 10 0 7.24 10.83 150.24 o 8 10 0 38.41 39.70 230.24 o -7 11 0 24.45 -56.24 224.28 o -6 11 0 6.54 31.10 204.44 o -5 11 0 16.09 29.11 154.82 o -4 11 0 776.36 721.19 133.92 o -3 11 0 490.88 482.63 111.63 o -2 11 0 660.17 661.97 122.72 o -1 11 0 1135.11 1082.99 143.36 o 0 11 0 83.14 27.90 90.05 o 1 11 0 5.89 -43.35 87.58 o 2 11 0 304.82 271.02 117.14 o 3 11 0 1507.68 1647.73 194.38 o 4 11 0 1368.36 1474.41 193.42 o 5 11 0 1015.09 1333.38 203.30 o 6 11 0 25.47 70.71 157.25 o 7 11 0 0.12 37.13 170.04 o 8 11 0 59.71 -58.88 250.09 o -7 12 0 33.62 -127.69 224.28 o -6 12 0 513.50 533.25 240.82 o -5 12 0 361.83 354.62 195.17 o -4 12 0 889.21 751.86 143.98 o -3 12 0 403.45 438.48 122.40 o -2 12 0 36.55 -11.37 98.65 o -1 12 0 12.22 -17.43 86.17 o 0 12 0 688.46 607.54 141.02 o 1 12 0 49.37 41.96 107.13 o 2 12 0 271.46 182.14 120.01 o 3 12 0 57.37 6.03 114.90 o 4 12 0 19.51 -24.37 117.91 o 5 12 0 2.83 -4.08 137.23 o 6 12 0 7.01 -116.93 158.47 o 7 12 0 0.36 16.54 261.33 o -6 13 0 129.54 62.85 231.56 o -5 13 0 217.41 144.23 203.11 o -4 13 0 117.82 184.35 121.54 o -3 13 0 1.43 71.09 107.80 o -2 13 0 156.14 84.54 118.43 o -1 13 0 135.17 92.29 109.37 o 0 13 0 1681.11 1643.55 197.43 o 1 13 0 874.92 866.23 162.70 o 2 13 0 394.03 437.98 149.24 o 3 13 0 7.74 20.71 128.74 o 4 13 0 47.06 102.34 142.26 o 5 13 0 429.67 537.36 182.86 o 6 13 0 261.84 457.79 196.91 o -5 14 0 0.31 322.86 252.07 o -4 14 0 182.25 159.45 218.99 o -3 14 0 1.41 -9.47 112.54 o -2 14 0 57.13 -53.63 114.01 o -1 14 0 17.53 -90.81 107.99 o 0 14 0 100.22 54.03 116.43 o 1 14 0 12.55 42.52 138.61 o 2 14 0 521.27 679.03 171.25 o 3 14 0 0.12 -116.06 132.45 o 4 14 0 272.55 231.95 165.91 o 5 14 0 43.47 -64.01 165.84 o 6 14 0 38.56 -81.99 187.36 o -4 15 0 185.43 183.93 246.78 o -3 15 0 256.11 306.61 149.38 o -2 15 0 53.91 96.58 131.22 o -1 15 0 95.76 96.35 125.45 o 0 15 0 69.33 -17.32 126.99 o 1 15 0 356.58 410.97 168.02 o 2 15 0 238.53 345.12 157.09 o 3 15 0 489.51 690.72 197.86 o 4 15 0 44.14 -13.46 168.77 o 5 15 0 96.44 -66.16 275.89 o -2 16 0 13.38 78.72 143.46 o -1 16 0 0.50 57.63 151.75 o 0 16 0 0.11 -29.47 140.50 o 1 16 0 0.12 -37.40 139.41 o 2 16 0 68.15 124.01 161.23 o 3 16 0 0.58 -117.77 164.21 o -3 -16 1 3.10 -44.44 190.14 o -2 -16 1 4.44 16.35 157.30 o -1 -16 1 4.60 -56.88 159.45 o 0 -16 1 23.12 -16.26 138.42 o 1 -16 1 6.97 -43.41 138.94 o 2 -16 1 14.88 -86.40 139.15 o -4 -15 1 314.83 295.08 189.77 o -3 -15 1 264.03 409.46 187.34 o -2 -15 1 229.06 198.54 158.69 o -1 -15 1 109.05 86.89 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538.40 114.24 o -2 -8 1 854.09 950.45 127.65 o -1 -8 1 18.68 6.74 65.32 o 0 -8 1 1835.26 1802.37 126.86 o 1 -8 1 3376.42 3506.47 164.54 o 2 -8 1 2168.68 2024.39 97.14 o 3 -8 1 1424.87 1282.91 107.77 o 4 -8 1 34.54 14.80 53.22 o 5 -8 1 78.80 73.79 66.76 o 6 -8 1 146.54 45.19 104.43 o 7 -8 1 938.50 741.16 159.38 o 8 -8 1 148.34 134.31 228.91 o -8 -7 1 148.89 128.35 199.80 o -7 -7 1 1131.85 1199.04 151.35 o -6 -7 1 2042.28 2172.17 156.75 o -5 -7 1 266.02 258.60 83.62 o -4 -7 1 503.89 503.75 82.66 o -3 -7 1 4.45 -12.92 48.19 o -2 -7 1 1216.91 1217.46 127.81 o -1 -7 1 2238.40 2111.66 127.28 o 0 -7 1 2236.79 2414.86 134.23 o 1 -7 1 893.64 761.54 62.42 o 2 -7 1 246.64 143.31 48.44 o 3 -7 1 0.52 30.73 46.68 o 4 -7 1 47.33 45.32 52.71 o 5 -7 1 6.23 -10.27 58.14 o 6 -7 1 2.36 -20.63 69.69 o 7 -7 1 56.68 85.74 127.76 o 8 -7 1 0.30 -93.29 199.14 o 9 -7 1 0.48 -161.43 255.38 o -9 -6 1 81.57 136.29 205.76 o -7 -6 1 168.56 56.17 89.12 o -6 -6 1 249.23 191.64 82.74 o -5 -6 1 120.56 63.07 73.47 o -4 -6 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