#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013034.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013034_Fobs loop_ _publ_author_name 'Baum, Gerhard' 'Blake, Alexander J.' 'Fenske, Dieter' 'Hubberstey, Peter' 'Julio, Carine' 'Withersby, Matthew A.' _publ_section_title ; (Acetonitrile)[2,6-bis(pyrazol-1-yl)pyridine](isonicotinamide)copper(II)--tetrafluoroborate--acetonitrile (1/2/2) ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m542 _journal_page_last m544 _journal_volume 58 _journal_year 2002 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.1790 _cell_length_b 22.7470 _cell_length_c 31.7520 _exptl_crystal_F_000 2808.00 _reflns_d_resolution_high 0.7551 _[local]_cod_data_source_file gg1141Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CUINAM #900 for CJ/PH in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 247.54 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 2 0 5993.25 4341.67 184.14 o 4 2 0 6633.87 5984.93 296.80 o 2 3 0 5856.73 6313.04 142.57 o 4 3 0 98.46 81.73 153.20 o 2 4 0 477.02 341.47 104.19 o 4 4 0 2773.28 2596.61 130.67 o 2 5 0 14622.71 12475.16 219.84 o 4 5 0 6030.79 7625.66 121.65 o 6 5 0 256.46 140.12 186.36 o 2 6 0 294.15 161.47 81.20 o 4 6 0 5396.12 4619.76 105.99 o 6 6 0 533.36 421.28 140.24 o 2 7 0 9560.64 7641.00 103.22 o 4 7 0 8988.62 8747.01 105.39 o 6 7 0 11767.51 14058.64 782.37 o 0 8 0 35844.84 33130.77 180.84 o 2 8 0 31821.99 27011.37 208.10 o 4 8 0 1117.24 633.11 76.16 o 6 8 0 2419.69 2290.03 113.06 o 2 9 0 10266.78 8539.84 102.98 o 4 9 0 14016.44 12916.93 764.08 o 6 9 0 11729.59 11666.84 335.10 o 8 9 0 5527.64 6909.83 191.88 o 2 10 0 46594.08 44381.99 376.86 o 4 10 0 19166.02 17615.86 104.39 o 6 10 0 3677.42 4412.86 101.37 o 8 10 0 51.09 144.26 134.59 o 2 11 0 1822.01 1443.27 71.62 o 4 11 0 1533.07 1309.16 67.35 o 6 11 0 555.65 317.09 89.48 o 8 11 0 340.64 443.12 142.88 o 0 12 0 1738.11 1662.06 95.25 o 2 12 0 535.66 528.83 63.67 o 4 12 0 617.29 324.88 63.94 o 6 12 0 309.78 522.97 82.24 o 8 12 0 547.34 674.14 111.34 o 2 13 0 0.39 -34.02 59.00 o 4 13 0 12371.13 12934.78 89.20 o 6 13 0 713.03 835.05 80.77 o 8 13 0 723.30 868.87 94.52 o 0 14 0 4364.17 4319.42 88.35 o 2 14 0 3195.91 2696.44 69.71 o 4 14 0 2650.91 3103.25 82.97 o 6 14 0 68.77 64.91 70.84 o 8 14 0 261.58 249.81 86.63 o 2 15 0 216.53 120.44 51.25 o 4 15 0 38.81 65.21 76.38 o 6 15 0 1036.99 1245.13 66.86 o 8 15 0 1548.49 1948.74 86.54 o 0 16 0 2383.63 2251.51 93.87 o 2 16 0 22162.28 21974.35 332.00 o 4 16 0 1087.72 882.76 99.74 o 6 16 0 2040.13 2230.30 76.38 o 8 16 0 33.25 15.21 78.36 o 2 17 0 16.93 75.23 100.08 o 4 17 0 5185.11 4985.06 77.84 o 6 17 0 2016.35 2231.33 65.89 o 8 17 0 1632.17 2008.03 81.45 o 0 18 0 7409.50 7201.11 102.15 o 2 18 0 4942.69 4435.05 68.08 o 4 18 0 2877.12 2889.32 102.84 o 6 18 0 2948.35 2942.05 278.16 o 8 18 0 249.90 253.69 69.32 o 2 19 0 1072.98 984.50 67.99 o 4 19 0 69.02 49.33 65.15 o 6 19 0 1477.35 1671.58 78.91 o 8 19 0 1106.25 1305.03 80.19 o 0 20 0 2613.24 2754.69 88.35 o 2 20 0 2429.97 2405.03 71.74 o 4 20 0 2503.92 2684.65 77.31 o 6 20 0 216.58 208.03 73.02 o 8 20 0 313.01 223.81 80.28 o 2 21 0 431.74 324.42 65.64 o 4 21 0 46.15 -20.23 56.25 o 6 21 0 134.25 84.22 65.39 o 0 22 0 1653.33 1861.53 94.56 o 2 22 0 2934.50 2520.87 90.76 o 4 22 0 1.64 134.70 57.83 o 6 22 0 44.75 85.59 63.94 o 2 23 0 335.14 284.08 54.37 o 4 23 0 3500.96 4196.00 75.89 o 6 23 0 357.93 320.68 51.73 o 0 24 0 504.44 403.78 84.21 o 2 24 0 4575.96 4364.37 60.12 o 4 24 0 1907.56 2093.03 92.14 o 6 24 0 326.25 318.69 77.31 o 2 25 0 197.45 186.15 61.68 o 4 25 0 902.46 807.86 65.64 o 6 25 0 97.64 205.69 93.87 o 0 26 0 2032.95 2094.14 82.83 o 2 26 0 3677.18 4358.72 66.71 o 4 26 0 635.97 531.87 62.95 o 2 27 0 991.50 831.81 109.06 o 4 27 0 2050.73 2110.03 75.89 o 0 28 0 619.97 559.77 73.16 o 2 28 0 1452.38 1195.89 58.01 o 2 29 0 210.12 381.08 74.89 o 0 30 0 798.33 932.49 83.52 o 3 1 1 230.28 88.35 281.61 o 1 2 1 999.49 1097.41 114.83 o 2 2 1 3236.42 2848.62 139.71 o 3 2 1 2782.57 2211.06 113.37 o 4 2 1 1908.26 2557.59 204.31 o 2 3 1 2560.14 2359.50 141.54 o 3 3 1 4379.60 3846.59 105.60 o 4 3 1 5917.57 6870.26 251.49 o 5 3 1 9861.72 9024.20 192.63 o 0 4 1 795.65 658.51 130.80 o 1 4 1 1518.71 1071.21 94.58 o 2 4 1 722.44 425.94 114.98 o 3 4 1 18045.43 17446.50 429.29 o 4 4 1 928.43 1160.74 88.49 o 5 4 1 571.81 153.65 100.74 o 6 4 1 772.70 915.24 245.03 o 1 5 1 11607.83 10552.79 146.17 o 2 5 1 8314.61 8284.68 117.86 o 3 5 1 78.61 152.20 71.63 o 4 5 1 712.57 757.24 73.70 o 5 5 1 673.87 252.03 70.74 o 6 5 1 294.49 261.61 139.34 o 0 6 1 29506.67 29881.88 210.52 o 1 6 1 21005.68 21411.25 136.19 o 2 6 1 28.30 -2.40 73.55 o 3 6 1 10701.02 11446.38 146.45 o 4 6 1 1360.06 1621.10 63.74 o 5 6 1 5096.89 5067.12 123.39 o 6 6 1 751.59 945.11 107.60 o 7 6 1 83.95 77.31 231.23 o 1 7 1 6052.43 5942.61 204.31 o 2 7 1 1083.22 1296.69 64.25 o 3 7 1 41967.72 41721.89 892.64 o 4 7 1 51.72 113.86 55.30 o 5 7 1 852.28 812.70 58.39 o 6 7 1 3249.79 3810.73 103.51 o 7 7 1 1718.90 2209.08 120.55 o 0 8 1 31906.06 32958.90 182.22 o 1 8 1 2.01 -0.85 79.58 o 2 8 1 137.68 119.90 56.48 o 3 8 1 6919.15 6390.16 165.28 o 4 8 1 31.89 19.34 52.45 o 5 8 1 3369.12 2643.52 61.17 o 6 8 1 75.18 44.70 77.04 o 7 8 1 38.25 79.50 90.35 o 1 9 1 1845.61 1330.43 60.70 o 2 9 1 23.12 109.69 55.72 o 3 9 1 5615.88 5386.97 62.44 o 4 9 1 214.02 116.38 49.21 o 5 9 1 252.21 260.17 52.54 o 6 9 1 48.04 65.85 68.11 o 7 9 1 334.18 503.63 71.03 o 8 9 1 49.27 76.46 101.12 o 0 10 1 15476.03 16082.85 104.52 o 1 10 1 29630.83 29511.59 230.43 o 2 10 1 5965.73 5869.15 108.54 o 3 10 1 826.65 644.09 46.63 o 4 10 1 747.55 482.52 48.53 o 5 10 1 4913.48 5930.57 60.02 o 6 10 1 289.60 393.11 65.44 o 7 10 1 39.65 73.79 66.06 o 8 10 1 79.00 26.93 87.12 o 1 11 1 28964.06 27380.34 169.26 o 2 11 1 1842.18 1599.69 53.16 o 3 11 1 9851.44 9114.56 101.82 o 4 11 1 3050.27 2615.28 50.89 o 5 11 1 5244.62 5366.63 68.87 o 6 11 1 2613.69 2674.64 65.19 o 7 11 1 1044.06 1173.57 58.94 o 8 11 1 751.02 821.70 88.38 o 0 12 1 17878.32 18131.68 91.98 o 1 12 1 354.30 292.25 50.78 o 2 12 1 31.39 19.61 44.03 o 3 12 1 1637.89 1328.32 68.04 o 4 12 1 1817.55 1353.52 46.85 o 5 12 1 8156.98 7966.32 64.87 o 6 12 1 472.63 460.32 57.48 o 7 12 1 1361.59 1427.62 60.48 o 8 12 1 244.73 237.89 74.72 o 9 12 1 1015.82 1250.46 108.90 o 1 13 1 7593.13 6541.43 107.40 o 2 13 1 979.70 791.03 42.96 o 3 13 1 16116.38 15584.26 104.61 o 4 13 1 3298.82 3323.00 46.92 o 5 13 1 9063.69 9040.14 66.08 o 6 13 1 4723.64 5330.57 65.95 o 7 13 1 11.70 -12.15 50.82 o 8 13 1 2240.11 2473.12 84.68 o 9 13 1 100.31 79.81 95.48 o 0 14 1 3600.20 2901.29 64.86 o 1 14 1 2216.00 2544.85 46.69 o 2 14 1 3232.74 2539.02 42.26 o 3 14 1 4787.07 4411.03 50.12 o 4 14 1 1578.55 1777.67 57.11 o 5 14 1 1410.18 1075.22 55.05 o 6 14 1 28.56 -22.09 48.38 o 7 14 1 5044.41 5268.62 79.60 o 8 14 1 6.48 12.80 62.72 o 9 14 1 1396.48 1444.22 92.76 o 1 15 1 4040.17 3754.19 65.25 o 2 15 1 513.24 432.97 40.20 o 3 15 1 62.60 32.15 40.95 o 4 15 1 2614.12 2854.69 53.96 o 5 15 1 918.69 946.21 51.15 o 6 15 1 149.63 162.55 47.21 o 7 15 1 5.68 0.42 46.92 o 8 15 1 239.04 275.40 60.29 o 9 15 1 16.29 -19.12 87.14 o 0 16 1 1819.32 1648.45 54.66 o 1 16 1 36.70 51.28 37.40 o 2 16 1 2312.13 2309.09 46.50 o 3 16 1 8096.74 7761.90 77.81 o 4 16 1 1382.37 1176.89 74.12 o 5 16 1 262.22 363.53 48.31 o 6 16 1 113.22 81.39 43.16 o 7 16 1 19.13 -10.34 53.57 o 8 16 1 40.25 37.61 55.35 o 9 16 1 47.16 30.76 68.18 o 1 17 1 1522.77 1174.24 37.26 o 2 17 1 2276.73 2545.87 47.10 o 3 17 1 1726.15 1688.89 51.87 o 4 17 1 1.82 7.34 46.99 o 5 17 1 2078.31 1979.75 46.18 o 6 17 1 1.53 13.94 44.22 o 7 17 1 673.97 686.31 54.32 o 8 17 1 8.46 -1.32 51.82 o 0 18 1 1873.88 1859.77 70.72 o 1 18 1 352.27 238.90 48.28 o 2 18 1 46.30 66.13 49.99 o 3 18 1 2403.99 2383.00 50.67 o 4 18 1 19.17 12.45 47.71 o 5 18 1 19.23 44.93 44.78 o 6 18 1 10.21 -42.84 42.84 o 7 18 1 307.85 297.51 48.78 o 8 18 1 18.24 59.53 49.15 o 1 19 1 2013.15 1988.91 44.69 o 2 19 1 1855.37 2047.68 50.27 o 3 19 1 1137.98 1213.69 49.69 o 4 19 1 2197.68 2557.64 49.71 o 5 19 1 803.04 841.73 41.92 o 6 19 1 1024.04 977.84 51.33 o 7 19 1 47.19 30.34 48.85 o 8 19 1 262.22 175.02 55.30 o 0 20 1 2362.33 3050.01 67.76 o 1 20 1 508.17 486.91 47.59 o 2 20 1 5984.12 6664.90 168.27 o 3 20 1 3232.88 3087.25 48.65 o 4 20 1 898.25 985.74 43.04 o 5 20 1 1200.35 1188.47 43.83 o 6 20 1 892.63 898.26 49.17 o 7 20 1 2372.51 2457.90 123.54 o 8 20 1 1.44 -50.92 53.86 o 1 21 1 2421.77 2552.47 41.58 o 2 21 1 160.27 58.27 46.24 o 3 21 1 4236.99 4691.78 52.99 o 4 21 1 93.42 117.98 42.53 o 5 21 1 1725.50 2051.56 49.70 o 6 21 1 813.86 831.14 45.22 o 7 21 1 96.22 127.07 44.65 o 0 22 1 235.16 261.28 53.19 o 1 22 1 1318.15 1272.30 41.83 o 2 22 1 2391.80 2671.87 45.82 o 3 22 1 356.34 381.38 40.66 o 4 22 1 1631.04 1548.30 43.34 o 5 22 1 1782.19 1899.20 50.38 o 6 22 1 578.35 611.27 45.90 o 7 22 1 242.80 282.36 50.04 o 1 23 1 5131.70 5049.28 41.67 o 2 23 1 521.97 618.97 43.14 o 3 23 1 2623.04 2566.42 41.79 o 4 23 1 572.49 685.63 40.81 o 5 23 1 912.44 1009.99 46.48 o 6 23 1 127.28 172.59 43.66 o 0 24 1 187.03 142.33 53.06 o 1 24 1 222.93 282.17 35.97 o 2 24 1 540.12 430.82 37.10 o 3 24 1 268.74 370.34 42.49 o 4 24 1 191.99 213.68 44.46 o 5 24 1 100.31 122.18 47.12 o 6 24 1 75.01 88.27 50.04 o 1 25 1 78.78 111.51 49.78 o 2 25 1 2.29 12.42 43.03 o 3 25 1 258.41 286.81 42.32 o 4 25 1 0.05 -28.91 45.12 o 5 25 1 14.08 63.54 40.38 o 6 25 1 27.22 202.93 93.18 o 0 26 1 133.82 199.27 54.91 o 1 26 1 58.62 89.20 38.57 o 2 26 1 474.11 553.92 40.31 o 3 26 1 198.38 171.84 40.63 o 4 26 1 284.00 271.65 44.00 o 5 26 1 1.59 10.54 44.01 o 1 27 1 117.80 116.89 41.02 o 2 27 1 72.25 64.35 40.20 o 3 27 1 367.08 342.00 59.37 o 4 27 1 156.69 148.60 45.42 o 0 28 1 28.68 33.42 62.23 o 1 28 1 7.38 27.52 38.93 o 2 28 1 323.83 300.13 37.41 o 3 28 1 171.93 155.24 47.62 o 1 29 1 639.20 535.19 44.05 o 2 29 1 12.46 73.85 43.44 o 3 0 2 14612.09 14039.85 360.99 o 3 1 2 8284.66 10132.70 1061.57 o 1 2 2 1333.24 1397.79 112.38 o 2 2 2 913.43 838.71 108.77 o 3 2 2 1617.31 1709.66 148.05 o 4 2 2 835.39 519.05 217.42 o 1 3 2 22.73 102.34 101.84 o 2 3 2 1915.25 1800.38 92.88 o 3 3 2 1883.78 1789.48 105.07 o 4 3 2 2231.75 2122.51 115.52 o 5 3 2 674.72 141.50 186.36 o 0 4 2 23344.94 24814.92 172.29 o 1 4 2 725.96 851.23 105.55 o 2 4 2 5274.51 6073.64 167.07 o 3 4 2 1358.68 1327.82 112.97 o 4 4 2 2401.42 1728.26 82.47 o 5 4 2 25.77 16.67 93.24 o 6 4 2 410.23 414.13 216.04 o 1 5 2 20289.23 22089.77 228.09 o 2 5 2 1373.18 1139.97 69.94 o 3 5 2 3091.30 3463.17 103.71 o 4 5 2 198.34 85.42 69.96 o 5 5 2 3954.75 4576.31 196.86 o 6 5 2 996.95 1004.02 135.17 o 0 6 2 3355.01 2889.23 112.21 o 1 6 2 2806.15 2196.84 78.33 o 2 6 2 3656.88 3480.19 98.28 o 3 6 2 770.66 777.47 101.81 o 4 6 2 455.64 221.12 64.92 o 5 6 2 821.86 592.54 63.01 o 6 6 2 2.97 16.70 102.95 o 7 6 2 727.07 722.66 216.73 o 1 7 2 16789.90 16420.09 276.26 o 2 7 2 2228.74 2256.55 95.90 o 3 7 2 563.87 421.46 72.82 o 4 7 2 140.83 48.07 56.13 o 5 7 2 5483.72 5699.30 140.57 o 6 7 2 870.71 880.52 79.67 o 7 7 2 105.32 181.22 108.44 o 0 8 2 992.96 989.09 109.75 o 1 8 2 3026.59 2402.54 79.55 o 2 8 2 758.82 519.45 92.73 o 3 8 2 140.39 107.51 60.53 o 4 8 2 476.28 313.01 54.32 o 5 8 2 1721.10 1113.44 55.12 o 6 8 2 1187.79 1203.77 75.35 o 7 8 2 1836.92 1965.41 95.78 o 8 8 2 715.12 749.58 196.71 o 1 9 2 36744.09 35800.76 798.24 o 2 9 2 14.56 50.07 90.53 o 3 9 2 7284.61 5853.08 106.60 o 4 9 2 530.34 287.09 49.40 o 5 9 2 9008.13 8187.68 84.98 o 6 9 2 813.03 823.86 70.17 o 7 9 2 1435.61 1320.96 73.42 o 8 9 2 247.51 311.41 104.19 o 0 10 2 4168.85 3782.43 137.35 o 1 10 2 105.50 -21.74 75.16 o 2 10 2 4759.83 4723.14 70.45 o 3 10 2 2465.30 1715.30 55.59 o 4 10 2 4757.93 4168.56 54.21 o 5 10 2 4042.71 4317.77 74.12 o 6 10 2 439.97 433.72 65.54 o 7 10 2 1666.25 2209.63 70.42 o 8 10 2 326.82 246.66 91.13 o 1 11 2 17552.14 16034.97 107.86 o 2 11 2 5335.80 4285.77 88.57 o 3 11 2 4178.21 3728.93 53.28 o 4 11 2 253.05 221.20 45.27 o 5 11 2 3709.63 3734.60 65.95 o 6 11 2 335.97 351.59 61.73 o 7 11 2 498.96 426.76 58.19 o 8 11 2 0.80 -6.42 86.10 o 9 11 2 45.31 96.63 189.12 o 0 12 2 2368.60 2215.54 81.92 o 1 12 2 2861.78 3141.34 52.25 o 2 12 2 2248.43 2071.33 55.59 o 3 12 2 101.20 41.02 42.90 o 4 12 2 170.16 161.71 44.75 o 5 12 2 1.66 18.73 54.68 o 6 12 2 119.03 94.64 55.22 o 7 12 2 2221.35 2341.91 65.65 o 8 12 2 241.01 320.45 80.99 o 9 12 2 74.30 39.34 141.50 o 1 13 2 1316.37 1468.96 43.99 o 2 13 2 2624.55 2174.93 44.63 o 3 13 2 0.65 22.11 42.14 o 4 13 2 1804.35 1778.43 46.74 o 5 13 2 2486.53 2224.72 56.42 o 6 13 2 56.73 80.49 53.87 o 7 13 2 351.48 314.94 50.40 o 8 13 2 164.12 242.60 67.71 o 9 13 2 15.86 5.94 89.96 o 0 14 2 11226.20 10983.82 251.93 o 1 14 2 2899.48 2846.98 60.57 o 2 14 2 2.73 30.39 39.75 o 3 14 2 20.56 1.31 44.04 o 4 14 2 267.68 262.05 52.21 o 5 14 2 50.04 55.36 53.25 o 6 14 2 249.56 297.53 50.31 o 7 14 2 7.41 45.13 50.53 o 8 14 2 56.15 56.72 60.60 o 9 14 2 1199.93 1247.79 89.66 o 1 15 2 5634.75 4710.94 65.45 o 2 15 2 1120.83 1021.44 42.97 o 3 15 2 6953.63 6185.78 105.00 o 4 15 2 440.15 525.31 48.62 o 5 15 2 6657.64 6520.32 71.23 o 6 15 2 263.02 302.67 46.09 o 7 15 2 593.23 503.00 45.02 o 8 15 2 73.29 60.89 56.75 o 9 15 2 0.32 8.46 84.37 o 0 16 2 1539.37 1274.23 53.66 o 1 16 2 1043.75 930.43 42.27 o 2 16 2 4275.28 3852.35 52.24 o 3 16 2 4464.64 5159.52 75.09 o 4 16 2 149.49 199.03 52.35 o 5 16 2 82.49 -16.70 47.88 o 6 16 2 1.53 -43.74 43.74 o 7 16 2 3625.71 3849.90 69.19 o 8 16 2 0.99 9.03 55.38 o 9 16 2 861.20 859.46 70.23 o 1 17 2 7792.89 7614.23 88.27 o 2 17 2 40.42 23.57 48.22 o 3 17 2 5802.02 6388.93 79.66 o 4 17 2 880.08 967.86 45.44 o 5 17 2 3309.33 3508.75 50.55 o 6 17 2 327.79 374.84 44.56 o 7 17 2 385.02 463.16 52.10 o 8 17 2 275.50 178.01 52.00 o 0 18 2 966.61 1118.25 90.07 o 1 18 2 1127.96 1061.74 51.33 o 2 18 2 122.36 108.48 47.16 o 3 18 2 1351.99 1450.71 47.22 o 4 18 2 1399.87 1749.26 46.90 o 5 18 2 1748.29 1833.81 47.02 o 6 18 2 31.73 -29.66 40.89 o 7 18 2 2060.34 2004.98 65.85 o 8 18 2 22.88 49.30 49.59 o 1 19 2 2444.42 2930.93 49.43 o 2 19 2 507.27 542.88 48.48 o 3 19 2 3489.63 3971.00 52.19 o 4 19 2 0.81 11.09 41.08 o 5 19 2 1032.39 1090.90 40.08 o 6 19 2 1.42 62.37 51.43 o 7 19 2 122.38 113.46 45.63 o 8 19 2 78.48 121.24 53.83 o 0 20 2 2505.29 2319.91 66.90 o 1 20 2 1152.83 1123.55 45.50 o 2 20 2 69.99 71.22 43.14 o 3 20 2 49.00 108.82 37.61 o 4 20 2 331.86 329.22 42.11 o 5 20 2 940.83 850.84 42.97 o 6 20 2 148.64 189.97 48.13 o 7 20 2 373.04 406.30 48.63 o 8 20 2 130.83 206.45 53.46 o 1 21 2 73.89 24.08 40.24 o 2 21 2 35.76 -8.55 41.28 o 3 21 2 1.14 40.94 42.06 o 4 21 2 108.90 119.76 39.96 o 5 21 2 68.58 76.13 49.95 o 6 21 2 206.74 219.03 43.88 o 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26.79 41.15 o 2 15 25 9.03 42.78 40.99 o 3 15 25 1277.50 1182.79 50.98 o 4 15 25 72.71 78.86 72.47 o 5 15 25 558.54 543.67 65.15 o 6 15 25 13.48 -53.23 53.23 o 0 16 25 903.58 1046.00 52.16 o 1 16 25 12.37 18.88 35.06 o 2 16 25 12.34 50.69 39.59 o 3 16 25 2.08 26.94 45.54 o 4 16 25 187.63 236.85 59.03 o 5 16 25 75.63 142.67 51.00 o 6 16 25 62.69 107.55 61.83 o 1 17 25 0.03 27.87 37.28 o 2 17 25 171.85 246.53 45.70 o 3 17 25 12.03 -5.94 40.15 o 4 17 25 12.41 30.24 49.33 o 5 17 25 12.62 28.20 54.19 o 6 17 25 43.53 10.31 87.66 o 0 18 25 1546.94 1659.48 96.63 o 1 18 25 126.88 125.43 64.36 o 2 18 25 322.30 336.39 47.69 o 3 18 25 30.27 47.88 47.13 o 4 18 25 680.75 530.34 46.18 o 5 18 25 468.64 322.29 71.99 o 1 19 25 578.23 642.72 42.16 o 2 19 25 101.82 115.34 44.76 o 3 19 25 381.99 367.20 42.14 o 4 19 25 9.57 9.01 39.45 o 5 19 25 200.42 217.06 49.28 o 0 20 25 3406.75 3372.68 174.97 o 1 20 25 9.80 36.29 41.80 o 2 20 25 126.84 133.52 39.05 o 3 20 25 526.56 503.26 48.14 o 4 20 25 48.35 44.75 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164.82 63.31 o 1 11 26 2391.07 2488.02 124.93 o 2 11 26 0.27 -8.06 58.19 o 3 11 26 1133.53 1146.21 53.44 o 4 11 26 17.46 31.18 52.56 o 5 11 26 406.59 448.69 69.54 o 6 11 26 23.96 -3.84 64.91 o 7 11 26 122.80 45.29 71.50 o 0 12 26 372.48 371.34 77.31 o 1 12 26 1277.50 1331.65 67.11 o 2 12 26 402.23 395.06 52.71 o 3 12 26 6.72 -32.58 54.87 o 4 12 26 289.97 228.46 52.21 o 5 12 26 253.62 243.45 60.66 o 6 12 26 33.17 -25.47 67.21 o 7 12 26 1.27 -28.03 72.70 o 1 13 26 1.45 52.78 56.70 o 2 13 26 5.92 -8.63 61.98 o 3 13 26 0.09 5.17 52.74 o 4 13 26 269.36 347.13 71.25 o 5 13 26 9.08 55.56 65.40 o 6 13 26 2.76 27.72 55.06 o 7 13 26 17.94 0.93 71.14 o 0 14 26 865.51 1031.89 91.11 o 1 14 26 31.16 35.29 55.36 o 2 14 26 281.22 379.59 49.78 o 3 14 26 1184.94 1085.79 49.78 o 4 14 26 104.63 109.06 103.53 o 5 14 26 148.89 179.54 64.66 o 6 14 26 20.58 9.66 59.77 o 1 15 26 5755.05 6572.99 123.93 o 2 15 26 498.77 555.31 45.69 o 3 15 26 428.98 460.74 63.84 o 4 15 26 1.69 9.32 66.38 o 5 15 26 18.98 -50.74 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51.56 o 7 4 27 3.28 3.70 47.03 o 8 4 27 456.78 288.61 53.68 o 1 5 27 73.69 130.34 88.00 o 2 5 27 251.71 225.11 66.00 o 3 5 27 1.45 2.78 69.30 o 4 5 27 1110.36 1272.86 67.60 o 5 5 27 85.73 60.61 54.19 o 6 5 27 1042.83 1068.49 85.89 o 7 5 27 1.95 -1.94 45.28 o 8 5 27 1464.56 1421.99 91.75 o 0 6 27 2292.43 2742.95 111.13 o 1 6 27 349.71 380.72 80.07 o 2 6 27 3213.57 3553.38 78.34 o 3 6 27 93.38 88.04 68.32 o 4 6 27 867.26 1050.22 66.37 o 5 6 27 231.42 197.31 60.03 o 6 6 27 382.90 456.90 56.55 o 7 6 27 12.51 22.97 46.35 o 8 6 27 53.27 -70.40 113.89 o 1 7 27 414.20 504.61 73.21 o 2 7 27 98.07 98.72 62.85 o 3 7 27 1284.16 1519.17 69.55 o 4 7 27 394.78 426.29 100.77 o 5 7 27 61.23 76.88 58.80 o 6 7 27 446.25 461.61 61.02 o 7 7 27 24.71 0.99 56.08 o 0 8 27 1154.56 1372.86 103.53 o 1 8 27 293.68 303.76 58.32 o 2 8 27 179.63 116.65 56.13 o 3 8 27 205.25 252.93 73.16 o 4 8 27 1697.48 1797.03 58.76 o 5 8 27 253.54 222.18 72.48 o 6 8 27 220.91 202.49 66.12 o 7 8 27 1.42 -38.04 55.38 o 1 9 27 4.73 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36.27 o 4 19 27 281.41 212.59 57.35 o 0 20 27 904.99 799.82 54.83 o 1 20 27 25.03 54.16 40.41 o 2 20 27 789.00 685.45 64.86 o 3 20 27 1.60 27.13 44.01 o 4 20 27 12.43 115.75 107.65 o 1 21 27 186.93 147.73 37.32 o 2 21 27 424.80 400.42 44.37 o 3 21 27 3.05 -4.33 43.98 o 0 22 27 1311.02 1142.53 74.60 o 1 22 27 13.03 42.34 42.71 o 2 22 27 451.77 420.76 42.61 o 0 0 28 1879.85 2674.62 94.56 o 1 0 28 1116.99 1040.49 63.94 o 2 0 28 442.77 524.97 66.96 o 3 0 28 332.99 424.82 57.83 o 4 0 28 2666.63 3115.39 64.80 o 5 0 28 1082.22 958.08 64.42 o 6 0 28 504.72 564.57 71.00 o 7 0 28 54.43 85.88 64.67 o 8 0 28 6.62 57.63 79.03 o 1 1 28 3332.36 3760.06 84.18 o 2 1 28 160.39 125.21 49.22 o 3 1 28 41.23 25.26 44.20 o 4 1 28 641.09 508.49 42.38 o 5 1 28 92.05 61.44 43.65 o 6 1 28 352.06 329.80 49.95 o 7 1 28 33.03 56.23 50.48 o 8 1 28 1518.41 1167.91 59.32 o 0 2 28 1200.97 1555.08 110.44 o 1 2 28 8.15 -8.35 89.04 o 2 2 28 375.11 284.74 73.69 o 3 2 28 458.68 450.74 49.76 o 4 2 28 32.49 47.71 41.80 o 5 2 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2144.09 2087.31 80.76 o 2 7 28 10.13 27.81 76.96 o 3 7 28 679.63 731.26 66.13 o 4 7 28 1272.61 1229.56 57.20 o 5 7 28 679.63 614.45 71.96 o 6 7 28 1403.07 1239.87 68.32 o 7 7 28 34.49 30.67 53.36 o 0 8 28 1012.97 946.30 82.14 o 1 8 28 164.07 187.05 68.82 o 2 8 28 2552.35 2707.72 70.52 o 3 8 28 144.55 2.46 57.05 o 4 8 28 907.32 732.55 61.24 o 5 8 28 30.35 15.53 62.02 o 6 8 28 176.97 127.19 64.89 o 7 8 28 770.78 754.46 63.54 o 1 9 28 785.60 793.14 105.26 o 2 9 28 35.66 57.52 88.69 o 3 9 28 514.09 517.13 56.05 o 4 9 28 277.07 283.61 68.33 o 5 9 28 2.97 0.69 67.84 o 6 9 28 70.94 18.95 63.44 o 7 9 28 24.95 42.87 70.04 o 0 10 28 2174.49 2242.54 81.45 o 1 10 28 647.37 668.85 145.29 o 2 10 28 851.53 960.29 57.83 o 3 10 28 2.56 25.08 60.76 o 4 10 28 1819.00 1883.88 74.67 o 5 10 28 116.84 174.52 60.17 o 6 10 28 310.24 172.24 63.68 o 7 10 28 453.91 276.99 69.79 o 1 11 28 728.87 830.13 53.20 o 2 11 28 108.60 75.14 75.23 o 3 11 28 256.68 223.12 48.56 o 4 11 28 158.44 152.26 102.50 o 5 11 28 49.22 39.93 65.88 o 6 11 28 262.38 163.86 122.17 o 7 11 28 34.58 -32.44 95.25 o 0 12 28 15.25 -40.03 88.35 o 1 12 28 44.64 76.11 55.04 o 2 12 28 242.63 231.96 55.91 o 3 12 28 237.13 261.27 52.04 o 4 12 28 111.71 179.87 61.51 o 5 12 28 49.68 83.11 89.04 o 6 12 28 51.56 47.85 54.05 o 1 13 28 0.98 -0.69 53.56 o 2 13 28 17.58 56.68 52.07 o 3 13 28 19.91 69.02 64.88 o 4 13 28 23.57 -59.55 60.02 o 5 13 28 4.01 25.16 69.02 o 6 13 28 6.93 38.48 71.50 o 0 14 28 2686.82 2682.90 75.23 o 1 14 28 741.27 731.80 53.38 o 2 14 28 847.46 978.60 72.96 o 3 14 28 6.79 -6.41 69.02 o 4 14 28 60.63 70.25 53.44 o 5 14 28 68.42 -4.68 71.78 o 6 14 28 81.59 98.03 68.81 o 1 15 28 314.83 268.35 64.34 o 2 15 28 9.61 -108.02 125.28 o 3 15 28 1112.60 981.59 68.08 o 4 15 28 623.72 568.38 53.19 o 5 15 28 206.11 83.54 59.70 o 6 15 28 511.54 245.72 97.32 o 0 16 28 3219.86 3186.08 87.66 o 1 16 28 30.37 50.18 90.42 o 2 16 28 411.36 508.37 60.17 o 3 16 28 393.52 361.20 58.54 o 4 16 28 491.90 445.48 122.86 o 5 16 28 58.54 101.43 63.31 o 1 17 28 816.87 849.23 49.55 o 2 17 28 70.44 91.49 57.69 o 3 17 28 1171.28 1117.48 65.64 o 4 17 28 363.31 308.60 60.39 o 5 17 28 321.46 301.22 69.06 o 0 18 28 418.61 486.30 61.32 o 1 18 28 85.70 58.08 44.96 o 2 18 28 82.37 38.75 49.04 o 3 18 28 2.20 -12.52 50.26 o 4 18 28 549.30 574.43 158.75 o 1 19 28 213.67 211.46 39.01 o 2 19 28 134.41 102.29 38.28 o 3 19 28 12.02 -48.03 52.89 o 4 19 28 181.84 158.09 68.56 o 0 20 28 699.59 710.89 65.26 o 1 20 28 8.34 28.11 42.54 o 2 20 28 662.12 597.63 42.67 o 3 20 28 1.15 5.34 46.84 o 1 21 28 0.67 6.66 67.75 o 2 21 28 167.99 152.54 47.46 o 0 22 28 91.26 54.08 62.68 o 1 22 28 41.92 -1.52 46.27 o 1 1 29 594.54 845.43 45.10 o 2 1 29 129.28 116.88 41.15 o 3 1 29 503.80 676.92 46.00 o 4 1 29 142.56 119.06 42.77 o 5 1 29 433.51 579.99 50.02 o 6 1 29 43.93 45.47 48.39 o 7 1 29 74.91 79.64 46.03 o 0 2 29 411.65 365.13 85.59 o 1 2 29 45.55 -1.00 65.47 o 2 2 29 951.62 976.71 71.09 o 3 2 29 615.52 664.39 51.70 o 4 2 29 843.31 895.30 46.24 o 5 2 29 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7 29 376.38 443.45 87.31 o 4 7 29 243.02 215.56 53.70 o 5 7 29 86.33 99.95 70.40 o 6 7 29 109.17 103.70 46.33 o 7 7 29 56.30 13.13 50.79 o 0 8 29 366.88 216.04 78.00 o 1 8 29 7.98 -66.38 66.38 o 2 8 29 1418.24 1218.77 60.35 o 3 8 29 267.04 297.68 55.71 o 4 8 29 113.32 62.91 50.71 o 5 8 29 475.03 489.74 68.32 o 6 8 29 29.93 -25.94 63.44 o 7 8 29 57.78 115.07 59.72 o 1 9 29 59.71 -26.11 58.36 o 2 9 29 6.24 -20.98 60.39 o 3 9 29 17.00 13.59 55.56 o 4 9 29 38.80 66.45 71.49 o 5 9 29 53.83 81.45 66.38 o 6 9 29 46.08 37.17 62.47 o 7 9 29 30.14 37.98 56.14 o 0 10 29 51.94 149.78 90.42 o 1 10 29 30.26 29.25 54.53 o 2 10 29 218.92 258.14 75.58 o 3 10 29 64.07 44.05 48.07 o 4 10 29 234.09 181.68 62.85 o 5 10 29 1050.37 886.42 60.80 o 6 10 29 5.93 7.33 61.24 o 1 11 29 186.83 262.85 61.74 o 2 11 29 271.56 268.97 54.22 o 3 11 29 1547.96 1637.48 61.86 o 4 11 29 0.04 40.61 55.39 o 5 11 29 494.07 339.87 65.63 o 6 11 29 34.72 -24.60 58.43 o 0 12 29 156.94 119.41 86.28 o 1 12 29 82.65 162.64 60.74 o 2 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