#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013128.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013128_Fobs loop_ _publ_author_name 'Z\'u\~niga, F. J.' 'Darriet, J.' _publ_section_title ; NaCa~4~Nb~5~O~17~: a layered perovskite A~n~B~n~O~3n~+2 compound ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first i18 _journal_page_last i20 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2bc' _symmetry_space_group_name_H-M 'P 1 1 21/b' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 96.820 _cell_length_a 7.7098 _cell_length_b 32.3497 _cell_length_c 5.4838 _exptl_crystal_F_000 1728.00 _reflns_d_resolution_high 0.5534 _[local]_cod_data_source_file fa1002Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' NaCa4Nb5O17' _shelx_refln_list_code 4 _shelx_f_calc_maximum 984.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y+1/2, z+1/2' '-x, -y, -z' 'x, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 9 -28 0 360.09 433.59 117.98 o 11 -28 0 6.71 -21.24 106.78 o 7 -26 0 326.24 357.41 33.08 o 9 -26 0 2452.58 2677.65 163.61 o 11 -26 0 285.98 326.03 107.80 o 13 -26 0 336.94 326.71 150.01 o 5 -24 0 3121.79 3172.03 54.72 o 7 -24 0 2028.70 1974.68 53.56 o 9 -24 0 398.66 504.34 40.75 o 11 -24 0 59.06 52.75 85.70 o 13 -24 0 225.44 146.81 104.09 o 3 -22 0 7006.40 6522.51 318.58 o 5 -22 0 538.98 552.31 29.79 o 7 -22 0 641.25 612.50 36.85 o 9 -22 0 337.13 428.13 41.33 o 11 -22 0 280.74 337.31 89.53 o 13 -22 0 638.98 685.81 100.95 o 1 -20 0 232.14 -135.53 135.53 o 3 -20 0 2748.49 2714.88 92.70 o 5 -20 0 201.64 142.15 68.90 o 7 -20 0 611.69 593.15 35.24 o 9 -20 0 681.55 706.64 44.64 o 11 -20 0 1236.03 1195.62 62.79 o 13 -20 0 2.61 -92.60 104.87 o -1 -18 0 3801.76 3627.53 63.22 o 1 -18 0 144.40 -52.68 52.68 o 3 -18 0 1087.07 1165.93 63.35 o 5 -18 0 452.92 481.11 43.74 o 7 -18 0 1326.07 1388.13 44.77 o 9 -18 0 17.41 60.54 65.41 o 11 -18 0 1538.68 1498.73 71.85 o 13 -18 0 261.55 421.78 90.07 o -3 -16 0 215.02 -149.51 264.18 o -1 -16 0 1353.98 1421.75 28.61 o 1 -16 0 103.02 2.39 49.07 o 3 -16 0 1171.73 1172.91 41.22 o 5 -16 0 342.97 314.34 27.13 o 7 -16 0 4460.83 4201.08 67.10 o 9 -16 0 98.50 189.46 64.12 o 11 -16 0 6.78 94.88 300.50 o 13 -16 0 130.60 -47.26 145.42 o -5 -14 0 477.97 539.83 30.20 o -3 -14 0 8.64 -40.75 40.75 o -1 -14 0 742.63 796.72 43.50 o 1 -14 0 61.63 -33.87 45.76 o 3 -14 0 7830.90 7664.24 105.42 o 5 -14 0 6.41 -48.00 48.00 o 7 -14 0 188.93 86.38 62.49 o 9 -14 0 108.54 165.30 93.81 o 11 -14 0 92.03 257.06 78.15 o 13 -14 0 195.59 309.93 117.71 o -7 -12 0 98.29 98.59 58.55 o -5 -12 0 5.67 46.96 43.03 o -3 -12 0 672.41 646.52 25.17 o -1 -12 0 192.53 55.63 63.82 o 1 -12 0 1660.53 1323.65 130.15 o 3 -12 0 1242.07 1268.05 27.17 o 5 -12 0 5.06 -45.81 45.81 o 7 -12 0 10.83 -2.99 65.85 o 9 -12 0 161.66 183.30 63.25 o 11 -12 0 195.57 349.22 88.15 o -9 -10 0 289.90 32.34 148.74 o -7 -10 0 173.48 125.35 59.37 o -5 -10 0 755.65 831.73 31.82 o -3 -10 0 10271.32 10079.11 130.69 o -1 -10 0 1036.13 831.32 24.66 o 1 -10 0 123.69 70.30 43.99 o 3 -10 0 579.91 561.89 22.12 o 5 -10 0 5.52 29.58 41.90 o 7 -10 0 534.39 529.63 32.54 o 9 -10 0 0.49 -38.76 78.56 o -11 -8 0 1.10 -82.38 93.81 o -9 -8 0 180.30 209.45 64.47 o -7 -8 0 5342.63 5071.09 177.13 o -5 -8 0 246.20 209.53 51.58 o -3 -8 0 982.87 1008.23 25.70 o -1 -8 0 10.25 103.56 44.24 o 1 -8 0 207.45 236.30 19.06 o 3 -8 0 1025.87 1037.26 25.37 o 5 -8 0 198.62 239.91 57.72 o 7 -8 0 1207.90 1186.75 49.86 o -13 -6 0 8.03 -21.23 153.05 o -11 -6 0 1717.45 1676.05 74.37 o -9 -6 0 134.52 178.19 63.20 o -7 -6 0 350.89 369.74 70.69 o -5 -6 0 88.83 95.98 45.30 o -3 -6 0 401.27 427.05 21.21 o -1 -6 0 0.97 111.58 36.85 o 1 -6 0 546.72 519.47 19.61 o 3 -6 0 1020.79 961.54 25.01 o 5 -6 0 577.22 586.97 26.75 o -13 -4 0 142.62 193.07 119.41 o -11 -4 0 109.36 86.38 83.65 o -9 -4 0 0.58 47.78 67.88 o -7 -4 0 457.07 478.57 31.43 o -5 -4 0 455.33 453.55 38.40 o -3 -4 0 15.44 39.75 38.45 o -1 -4 0 133.14 124.14 36.50 o 1 -4 0 329.30 310.73 17.45 o 3 -4 0 143.42 90.06 40.80 o -13 -2 0 15.81 78.37 304.82 o -11 -2 0 437.29 426.58 60.43 o -9 -2 0 424.14 366.66 38.59 o -7 -2 0 44.42 58.47 116.18 o -5 -2 0 173.86 177.38 28.69 o -3 -2 0 136.26 116.82 40.23 o -1 -2 0 690.48 783.49 113.10 o 1 -2 0 305.32 460.11 15.29 o -13 0 0 331.88 304.11 101.96 o -11 0 0 104.20 164.31 120.76 o -9 0 0 555.69 494.17 49.84 o -7 0 0 119.50 114.98 51.91 o -5 0 0 144.42 195.72 45.12 o -3 0 0 53.74 -6.28 38.64 o -1 0 0 29.21 179.20 81.11 o 1 0 0 23.34 43.48 32.72 o 2 0 0 143886.06 131952.77 682.71 o 3 0 0 42.94 43.63 39.73 o 4 0 0 4506.03 4397.01 162.80 o 5 0 0 115.41 129.58 45.84 o 6 0 0 7096.55 6970.72 99.44 o 7 0 0 95.49 93.35 56.44 o 8 0 0 1268.43 1198.00 114.21 o 9 0 0 444.05 347.64 45.59 o 10 0 0 268.08 311.10 71.95 o 11 0 0 83.27 -47.95 79.76 o 12 0 0 797.05 830.90 73.75 o 13 0 0 265.24 194.84 103.93 o -13 2 0 543.86 283.26 108.96 o -13 2 0 434.61 353.97 103.70 o -12 2 0 1057.41 971.99 67.98 o -11 2 0 34.11 -73.82 82.32 o -11 2 0 27.26 -103.13 112.62 o -10 2 0 2218.26 2066.92 68.36 o -9 2 0 24.13 -54.19 59.79 o -9 2 0 30.20 63.02 64.28 o -8 2 0 2008.46 1927.57 53.36 o -7 2 0 358.35 309.56 30.01 o -7 2 0 448.47 522.82 30.87 o -6 2 0 28557.05 28234.75 550.73 o -5 2 0 6.41 38.98 128.64 o -5 2 0 5.12 -1.61 44.38 o -4 2 0 969567.25 798230.44 24148.58 o -3 2 0 18.73 14.54 49.32 o -3 2 0 14.97 48.58 39.36 o -2 2 0 143248.28 134745.55 2121.81 o -1 2 0 243.93 345.39 110.67 o 1 2 0 551.76 491.97 17.46 o 2 2 0 28432.49 28546.12 347.13 o 3 2 0 108.89 40.53 39.89 o 4 2 0 1628.93 1671.13 30.59 o 5 2 0 138.94 142.94 43.71 o 6 2 0 602.32 524.39 30.55 o 7 2 0 35.50 70.01 52.48 o 8 2 0 1294.41 1332.87 52.91 o 9 2 0 338.95 293.96 44.44 o 10 2 0 1427.70 1294.37 154.14 o 11 2 0 349.48 342.45 87.04 o 12 2 0 1848.94 1829.14 76.26 o 13 2 0 12.63 -20.14 145.16 o -13 4 0 65.32 5.33 96.09 o -13 4 0 81.75 64.68 98.48 o -12 4 0 1405.52 1489.44 74.98 o -11 4 0 740.70 665.09 55.37 o -11 4 0 591.85 514.76 68.15 o -10 4 0 8300.85 7778.79 114.68 o -9 4 0 23.15 -7.22 135.76 o -9 4 0 28.97 -24.45 66.69 o -8 4 0 243860.00 226752.27 5732.95 o -7 4 0 0.25 -52.86 127.37 o -7 4 0 0.31 6.54 51.28 o -6 4 0 28248.63 28022.90 427.44 o -5 4 0 0.09 38.39 40.63 o -5 4 0 0.12 91.62 43.98 o -4 4 0 3859.80 3772.66 52.99 o -3 4 0 114.59 129.12 38.64 o -2 4 0 28590.49 29195.61 153.60 o -1 4 0 263.08 236.08 17.27 o 0 4 0 2318.12 2176.20 29.40 o 1 4 0 106.39 56.17 37.40 o 2 4 0 2147.06 2189.74 47.17 o 3 4 0 12.34 -8.16 38.26 o 4 4 0 1981.49 2020.82 54.74 o 5 4 0 363.93 369.01 25.35 o 6 4 0 1832.07 1781.49 86.02 o 7 4 0 365.30 267.83 39.43 o 8 4 0 5168.94 4966.51 113.89 o 9 4 0 0.46 73.28 75.25 o 10 4 0 1613.32 1486.53 61.51 o 11 4 0 87.40 30.37 98.13 o 12 4 0 37798.65 35175.61 568.17 o 13 4 0 114.00 -65.55 115.61 o -13 6 0 51.00 -19.58 203.13 o -13 6 0 40.75 -105.47 105.47 o -12 6 0 87311.73 80702.70 772.10 o -11 6 0 5.78 16.60 85.42 o -11 6 0 7.24 0.50 72.05 o -10 6 0 8214.47 7661.06 114.85 o -9 6 0 268.48 79.83 71.29 o -9 6 0 336.04 390.84 67.13 o -8 6 0 1615.54 1511.21 49.98 o -7 6 0 463.01 435.32 31.46 o -7 6 0 579.54 557.33 32.55 o -6 6 0 7289.25 7194.43 114.36 o -5 6 0 461.12 453.12 46.79 o -4 6 0 1308.60 1274.70 61.33 o -3 6 0 815.45 780.53 47.84 o -2 6 0 2298.14 2473.21 35.13 o -1 6 0 436.76 431.82 18.89 o 0 6 0 2743.73 2455.54 34.01 o 1 6 0 0.78 -40.98 40.98 o 2 6 0 3218.90 2916.66 47.99 o 3 6 0 320.70 324.33 20.09 o 4 6 0 12167.23 11713.66 148.57 o 5 6 0 71.03 63.88 89.49 o 6 6 0 2638.46 2703.63 48.57 o 7 6 0 280.43 253.59 57.64 o 8 6 0 93190.52 88475.48 1590.95 o 9 6 0 107.50 162.45 75.76 o 10 6 0 57097.68 52236.84 967.32 o 11 6 0 1372.63 1321.60 81.39 o 12 6 0 56322.70 51163.20 2358.76 o 13 6 0 6.42 -117.35 117.35 o -13 8 0 345.11 256.83 74.84 o -13 8 0 431.94 312.49 113.81 o -12 8 0 1124.23 1031.63 72.11 o -11 8 0 748.19 674.18 100.19 o -11 8 0 936.46 879.72 57.22 o -10 8 0 2366.76 2137.56 70.27 o -9 8 0 240.50 239.96 64.15 o -9 8 0 301.02 336.42 51.11 o -8 8 0 1015.19 868.59 44.06 o -7 8 0 964.95 851.45 36.04 o -6 8 0 741.17 795.70 56.97 o -5 8 0 158.65 137.74 47.81 o -4 8 0 1636.66 1566.17 29.85 o -3 8 0 819.39 804.21 23.57 o -2 8 0 2978.57 2570.12 35.87 o -1 8 0 165.72 162.04 38.63 o 0 8 0 19371.72 17573.63 118.43 o 1 8 0 8.19 -18.69 39.36 o 2 8 0 3924.18 3727.57 196.87 o 3 8 0 785.68 753.81 23.20 o 4 8 0 206851.53 200304.67 2567.69 o 5 8 0 196.71 156.69 50.68 o 6 8 0 89996.91 86999.43 500.97 o 7 8 0 4270.84 3854.52 63.71 o 8 8 0 110081.75 102599.38 652.02 o 9 8 0 144.14 134.52 187.12 o 10 8 0 855.68 844.26 51.77 o 11 8 0 0.88 28.82 74.26 o 12 8 0 82.30 -72.81 167.29 o 13 8 0 394.97 235.18 110.86 o -13 10 0 177.44 176.51 139.07 o -13 10 0 141.76 196.38 86.24 o -12 10 0 844.79 623.23 127.91 o -11 10 0 965.00 717.85 97.66 o -11 10 0 770.94 690.63 52.11 o -10 10 0 302.38 331.33 139.59 o -9 10 0 0.39 -18.09 82.88 o -8 10 0 1046.08 897.94 43.97 o -7 10 0 426.88 402.31 30.51 o -6 10 0 1552.28 1456.48 38.84 o -5 10 0 4.41 36.76 79.07 o -4 10 0 11682.23 10946.95 141.08 o -3 10 0 463.09 433.84 21.58 o -2 10 0 3725.95 3207.67 62.29 o -1 10 0 98.81 -22.74 42.58 o 0 10 0 325584.06 264012.31 3572.84 o 1 10 0 827.97 426.41 41.48 o 2 10 0 75807.06 63804.38 294.20 o 3 10 0 8211.03 7129.44 181.45 o 4 10 0 165778.70 156899.88 691.42 o 5 10 0 604.35 561.55 56.46 o 6 10 0 806.14 804.97 34.12 o 7 10 0 138.66 199.15 55.54 o 8 10 0 211.60 203.05 69.57 o 9 10 0 231.72 290.90 46.71 o 10 10 0 6191.63 5964.94 105.21 o 11 10 0 149.11 176.01 82.96 o 12 10 0 846.25 801.15 92.31 o 13 10 0 8.77 -58.76 92.94 o -13 12 0 18.21 202.26 88.03 o -13 12 0 14.55 58.41 89.22 o -12 12 0 642.59 676.73 139.60 o -11 12 0 156.23 280.60 78.84 o -10 12 0 1191.01 1110.16 113.43 o -9 12 0 129.14 107.70 66.08 o -8 12 0 4919.29 4745.69 76.56 o -7 12 0 8.65 -53.51 53.51 o -6 12 0 2423.97 4137.65 287.91 o -5 12 0 4.04 44.09 44.94 o -4 12 0 208776.06 197551.42 614.49 o -3 12 0 991.93 921.10 25.71 o -2 12 0 76093.56 64432.99 294.85 o -1 12 0 1326.69 1002.84 98.28 o 0 12 0 178363.33 148047.64 432.99 o 1 12 0 153.82 -158.40 159.93 o 2 12 0 14773.52 16132.38 154.63 o 3 12 0 537.58 516.22 71.21 o 4 12 0 26.63 122.38 50.08 o 5 12 0 4.54 76.01 42.42 o 6 12 0 12559.45 12417.54 195.69 o 7 12 0 78.58 29.90 53.39 o 8 12 0 2735.22 2580.39 227.02 o 9 12 0 60.65 41.58 73.02 o 10 12 0 6122.15 5931.74 105.86 o 11 12 0 37.34 131.30 70.17 o 12 12 0 1145.58 1040.72 78.08 o 13 12 0 620.91 604.29 132.73 o -13 14 0 156.23 130.43 103.35 o -12 14 0 1754.88 1649.38 74.78 o -11 14 0 73.51 138.47 78.98 o -10 14 0 1492.09 1397.97 123.88 o -9 14 0 86.72 109.05 97.12 o -8 14 0 95098.39 94235.77 2904.64 o -7 14 0 150.86 125.61 52.33 o -6 14 0 91354.67 87747.51 1227.61 o -5 14 0 5.14 27.09 52.88 o -4 14 0 162817.25 155340.34 574.92 o -3 14 0 6253.40 5589.12 266.46 o -2 14 0 15268.14 17109.91 160.16 o -1 14 0 49.22 -41.88 41.88 o 0 14 0 252.63 278.40 48.32 o 1 14 0 593.52 586.49 22.10 o 2 14 0 16754.16 15070.46 168.76 o 3 14 0 6.91 -72.96 72.96 o 4 14 0 7564.03 7652.13 103.84 o 5 14 0 382.09 321.52 56.70 o 6 14 0 12926.95 12757.41 215.64 o 7 14 0 8.97 0.69 54.91 o 8 14 0 3742.41 3540.56 72.05 o 9 14 0 961.11 862.13 50.17 o 10 14 0 3129.94 2914.37 80.79 o 11 14 0 27.61 56.33 70.76 o 12 14 0 10.38 -40.94 103.39 o 13 14 0 767.03 829.20 276.92 o -13 16 0 104.34 90.91 96.02 o -12 16 0 39037.13 36445.44 1218.90 o -11 16 0 5.41 69.38 75.98 o -10 16 0 58772.44 55646.27 556.05 o -9 16 0 78.71 77.54 92.29 o -8 16 0 107531.84 102530.05 633.67 o -7 16 0 3562.51 3227.44 304.30 o -6 16 0 1007.57 1101.04 48.84 o -5 16 0 273.81 266.86 62.04 o -4 16 0 21.52 85.69 69.91 o -3 16 0 935.70 913.37 34.34 o -2 16 0 16123.04 15104.02 158.42 o -1 16 0 82.30 -45.65 45.65 o 0 16 0 12954.09 12840.12 141.42 o 1 16 0 1082.08 1007.96 26.26 o 2 16 0 21836.73 20352.10 194.68 o 3 16 0 171.92 -134.50 134.50 o 4 16 0 8579.88 8380.01 119.94 o 5 16 0 1594.81 1525.72 39.94 o 6 16 0 5578.75 5559.77 190.65 o 7 16 0 70.57 20.25 74.24 o 8 16 0 140.83 146.19 65.60 o 9 16 0 1293.93 1301.01 56.78 o 10 16 0 11950.63 11730.75 164.96 o 11 16 0 37.09 0.45 86.31 o 12 16 0 42443.73 42314.50 575.01 o -13 18 0 208.92 271.51 87.31 o -12 18 0 54764.90 50486.02 615.43 o -11 18 0 1229.06 1228.39 66.18 o -10 18 0 725.06 706.30 51.58 o -9 18 0 13.91 -47.21 61.62 o -8 18 0 220.11 388.93 91.78 o -7 18 0 1058.97 1041.92 54.94 o -6 18 0 11550.79 11563.35 233.69 o -5 18 0 361.74 319.36 97.39 o -4 18 0 7625.47 7398.49 189.26 o -3 18 0 868.08 834.75 47.31 o -2 18 0 21470.69 20299.39 208.38 o -1 18 0 115.36 -54.47 54.47 o 0 18 0 12793.33 11984.04 144.84 o 1 18 0 3038.29 2644.57 38.73 o 2 18 0 10433.64 10298.61 199.44 o 3 18 0 34.35 -312.96 312.96 o 4 18 0 590.85 525.79 29.99 o 5 18 0 2149.54 2038.00 89.58 o 6 18 0 21331.41 21132.00 1073.55 o 7 18 0 262.02 219.93 39.79 o 8 18 0 89241.30 86732.67 647.61 o 9 18 0 849.78 854.48 50.51 o 10 18 0 15899.37 15523.76 225.91 o 11 18 0 8.60 -96.84 96.84 o 12 18 0 9313.21 9657.55 158.76 o 9 -48 0 573.67 592.91 101.20 o 7 -46 0 0.06 -125.01 201.60 o 9 -46 0 262.66 352.54 94.88 o 5 -44 0 252.80 119.22 107.29 o 7 -44 0 116.09 129.91 75.21 o 9 -44 0 3.35 -6.73 77.96 o 3 -42 0 13.92 -67.51 67.51 o 5 -42 0 11.41 -78.29 78.29 o 7 -42 0 66.07 -48.52 147.96 o 9 -42 0 184.96 200.52 92.07 o 1 -40 0 25.76 -68.64 68.64 o 3 -40 0 17.80 -163.47 163.47 o 5 -40 0 434.44 183.95 92.73 o 7 -40 0 75.86 -229.51 231.35 o 9 -40 0 100.41 121.83 77.65 o 11 -40 0 1392.86 1505.43 76.33 o -3 -38 0 62.75 47.60 77.03 o -1 -38 0 25.01 -68.03 68.03 o 1 -38 0 586.68 503.79 42.07 o 3 -38 0 2.15 -142.18 142.18 o 5 -38 0 18.28 -280.67 280.67 o 7 -38 0 5179.20 5715.92 102.92 o 9 -38 0 297.11 421.68 61.89 o 11 -38 0 198.20 215.33 302.04 o -5 -36 0 147.76 -4.68 75.58 o -3 -36 0 717.34 707.68 50.10 o -1 -36 0 682.26 492.19 46.71 o 1 -36 0 1105.69 591.41 72.20 o 3 -36 0 7377.58 6459.83 478.87 o 5 -36 0 381.39 122.66 159.68 o 7 -36 0 325.04 324.70 42.24 o 9 -36 0 139.49 207.01 83.63 o 11 -36 0 1716.65 1866.47 108.10 o -7 -34 0 967.03 1043.82 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101.09 151.33 78.13 o 0 8 9 718.85 742.61 53.04 o 1 8 9 89.90 119.60 93.05 o 2 8 9 1781.27 1755.45 74.28 o 3 8 9 475.02 506.49 148.24 o 4 8 9 3281.83 3389.34 132.33 o 5 8 9 295.69 109.81 92.91 o -5 9 9 35.22 57.09 81.25 o -4 9 9 4056.27 4137.89 104.03 o -3 9 9 69.40 30.77 73.70 o -2 9 9 1018.74 978.69 72.22 o -1 9 9 93.45 -79.19 98.64 o 0 9 9 1152.09 1077.15 61.32 o 1 9 9 480.72 438.14 90.52 o 2 9 9 286.33 341.30 86.07 o 3 9 9 147.00 191.30 105.51 o 4 9 9 44.22 109.32 81.92 o 5 9 9 634.54 539.85 113.41 o -5 10 9 152.94 196.48 76.26 o -4 10 9 472.11 474.35 54.29 o -3 10 9 173.75 147.37 55.60 o -2 10 9 1818.90 1712.96 124.90 o -1 10 9 384.62 140.09 91.66 o 0 10 9 3777.72 3708.10 93.77 o 1 10 9 188.32 189.34 51.16 o 2 10 9 1165.48 1219.81 62.72 o 3 10 9 211.33 162.50 118.22 o 4 10 9 348.48 386.38 95.21 o 5 10 9 912.25 724.24 90.02 o -5 11 9 43.35 145.95 84.15 o -4 11 9 799.19 760.85 59.50 o -3 11 9 592.39 676.00 194.52 o -2 11 9 298.73 212.10 107.55 o -1 11 9 180.63 110.60 81.75 o 0 11 9 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1024.89 172.42 o 3 18 9 54.64 -37.02 85.45 o -4 19 9 13110.87 13264.06 184.98 o -3 19 9 61.93 26.25 80.48 o -2 19 9 15961.88 16074.10 228.15 o -1 19 9 281.72 297.29 89.86 o 0 19 9 74.49 88.15 88.85 o 1 19 9 57.59 121.85 93.81 o 2 19 9 12.43 69.45 81.78 o 3 19 9 538.93 657.59 56.59 o -3 20 9 246.37 250.38 92.14 o -2 20 9 952.65 921.13 64.52 o -1 20 9 70.92 -51.23 84.67 o 0 20 9 785.02 784.69 139.10 o 1 20 9 529.58 531.20 52.32 o 2 20 9 2540.84 2525.20 86.47 o -3 21 9 49.88 -51.93 147.96 o -2 21 9 10.75 231.22 81.22 o -1 21 9 578.68 582.43 53.85 o 0 21 9 202.56 194.60 89.98 o 1 21 9 20.40 -43.31 101.69 o 2 21 9 961.12 854.19 62.56 o -3 22 9 527.47 429.81 72.15 o -2 22 9 2577.53 2461.37 90.07 o -1 22 9 17.62 19.23 68.60 o 0 22 9 1443.13 1348.01 73.76 o 1 22 9 738.68 759.37 180.80 o -2 23 9 941.33 822.80 64.02 o -1 23 9 790.61 755.18 59.51 o 0 23 9 16.46 25.34 141.10 o 1 23 9 93.58 102.86 78.36 o -1 24 9 80.71 18.03 89.58 o 0 24 9 9443.65 9390.09 150.14 o