#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:41:46 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180800 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/31/2013129.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013129_Fobs loop_ _publ_author_name '\'Slepokura, Katarzyna' 'Lis, Tadeusz' _publ_section_title ; Polymeric bis(phosphonomethylcarboxylato)calcium(II) at 85K ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m76 _journal_page_last m78 _journal_volume 59 _journal_year 2003 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yc' _symmetry_space_group_name_H-M 'P 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 106.500 _cell_angle_gamma 90.000 _cell_length_a 13.0210 _cell_length_b 5.5160 _cell_length_c 7.3580 _exptl_crystal_F_000 324.00 _reflns_d_resolution_high 0.6196 _cod_data_source_file fa1003Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' caap1 in P2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 109.58 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 1327.29 1260.09 13.43 o 4 0 0 3969.07 3977.93 95.89 o 5 0 0 2802.91 2654.67 38.33 o 6 0 0 1634.59 1488.59 8.30 o 7 0 0 6656.67 6553.17 82.40 o 8 0 0 176.15 172.23 3.92 o 9 0 0 1802.09 1780.37 10.68 o 10 0 0 196.20 195.31 3.11 o 11 0 0 222.90 206.03 3.42 o 12 0 0 918.24 927.73 10.68 o 13 0 0 2495.63 2505.06 46.32 o 14 0 0 1178.68 1211.78 38.41 o 15 0 0 38.26 36.29 2.92 o 16 0 0 0.07 2.23 1.82 o 17 0 0 1.11 3.41 2.60 o 18 0 0 659.51 697.16 10.24 o 19 0 0 236.99 236.93 6.73 o 0 1 0 1158.92 1177.83 6.75 o 1 1 0 1080.59 1122.59 10.66 o 2 1 0 1291.16 1329.32 4.18 o 3 1 0 1509.86 1571.00 4.12 o 4 1 0 5503.22 5554.71 11.32 o 5 1 0 0.73 3.11 0.68 o 6 1 0 5.74 5.05 0.75 o 7 1 0 53.39 57.71 1.45 o 8 1 0 310.27 321.44 3.17 o 9 1 0 1064.35 1054.30 4.51 o 10 1 0 300.43 304.72 2.44 o 11 1 0 680.14 687.89 3.57 o 12 1 0 229.16 227.88 2.85 o 13 1 0 30.58 32.96 1.78 o 14 1 0 89.65 87.85 4.44 o 15 1 0 41.40 39.17 1.93 o 16 1 0 288.29 306.43 4.93 o 17 1 0 335.51 349.08 10.93 o 18 1 0 48.72 55.34 4.56 o 19 1 0 20.20 20.23 3.20 o 20 1 0 0.14 2.52 3.22 o 0 2 0 6706.76 6691.14 54.32 o 1 2 0 348.90 391.59 3.15 o 2 2 0 113.04 124.39 1.89 o 3 2 0 1124.51 1080.11 10.58 o 4 2 0 5.01 3.40 0.70 o 5 2 0 2.02 4.07 0.74 o 6 2 0 216.79 202.68 2.66 o 7 2 0 545.69 528.52 3.06 o 8 2 0 806.98 821.11 8.28 o 9 2 0 607.65 572.15 3.15 o 10 2 0 517.89 508.81 4.96 o 11 2 0 229.32 220.06 2.58 o 12 2 0 263.28 263.98 2.81 o 13 2 0 138.58 137.39 2.29 o 14 2 0 234.30 236.34 3.81 o 15 2 0 214.06 211.17 4.62 o 16 2 0 71.98 70.51 4.83 o 17 2 0 2.63 7.78 2.98 o 18 2 0 164.11 160.00 6.35 o 19 2 0 71.70 69.02 5.25 o 0 3 0 115.82 116.47 3.27 o 1 3 0 161.33 187.42 2.58 o 2 3 0 1973.45 2136.74 13.76 o 3 3 0 1224.09 1206.48 5.73 o 4 3 0 1586.33 1562.92 6.57 o 5 3 0 100.88 104.16 1.62 o 6 3 0 484.32 498.77 3.40 o 7 3 0 81.33 76.45 1.62 o 8 3 0 250.90 236.96 2.34 o 9 3 0 990.12 997.78 4.92 o 10 3 0 726.95 728.09 4.48 o 11 3 0 332.99 340.50 3.79 o 12 3 0 94.75 86.50 2.99 o 13 3 0 106.69 106.55 2.52 o 14 3 0 49.64 50.18 2.57 o 15 3 0 365.02 369.23 12.51 o 16 3 0 747.71 772.34 11.12 o 17 3 0 517.70 521.12 9.75 o 18 3 0 26.20 22.58 4.26 o 0 4 0 1190.22 1092.83 9.48 o 1 4 0 696.46 710.63 11.57 o 2 4 0 526.66 545.90 5.41 o 3 4 0 201.51 234.85 3.86 o 4 4 0 86.54 76.37 1.42 o 5 4 0 683.85 695.22 5.64 o 6 4 0 567.47 566.79 4.96 o 7 4 0 190.09 183.71 1.95 o 8 4 0 1115.02 1092.69 11.48 o 9 4 0 56.79 56.19 1.73 o 10 4 0 65.11 63.31 1.87 o 11 4 0 10.05 11.47 1.51 o 12 4 0 119.72 117.04 2.66 o 13 4 0 793.18 811.61 9.97 o 14 4 0 112.81 107.22 3.26 o 15 4 0 219.58 221.14 4.92 o 16 4 0 196.57 199.35 4.77 o 17 4 0 0.98 4.15 2.43 o 18 4 0 25.43 27.04 4.23 o 0 5 0 152.20 112.28 4.43 o 1 5 0 377.91 385.50 3.67 o 2 5 0 21.13 24.49 1.48 o 3 5 0 21.03 22.30 1.85 o 4 5 0 407.41 396.70 3.50 o 5 5 0 12.23 14.55 1.24 o 6 5 0 961.09 977.75 7.85 o 7 5 0 268.38 264.55 3.02 o 8 5 0 195.08 187.11 2.45 o 9 5 0 30.38 29.76 1.60 o 10 5 0 1.86 2.83 1.12 o 11 5 0 74.13 67.91 2.28 o 12 5 0 232.19 243.06 4.00 o 13 5 0 151.43 150.32 3.15 o 14 5 0 59.00 55.12 2.37 o 15 5 0 9.35 9.76 2.00 o 16 5 0 153.37 143.72 3.22 o 0 6 0 199.11 186.77 6.06 o 1 6 0 360.92 354.43 6.12 o 2 6 0 0.76 2.61 0.91 o 3 6 0 321.60 311.99 3.94 o 4 6 0 80.18 83.82 2.01 o 5 6 0 25.62 24.14 1.59 o 6 6 0 327.14 329.58 5.70 o 7 6 0 0.61 2.67 1.23 o 8 6 0 103.44 101.38 3.03 o 9 6 0 113.88 113.29 3.89 o 10 6 0 396.91 402.79 8.13 o 11 6 0 17.37 13.57 2.63 o 12 6 0 389.28 385.70 6.58 o 13 6 0 343.56 341.49 6.39 o 14 6 0 35.96 36.99 2.47 o 0 7 0 6.31 8.42 3.11 o 1 7 0 129.72 121.99 4.26 o 2 7 0 80.66 74.54 2.58 o 3 7 0 183.85 177.02 3.79 o 4 7 0 108.67 109.55 3.41 o 5 7 0 15.70 14.42 2.09 o 6 7 0 32.10 28.70 2.33 o 7 7 0 104.94 106.82 3.32 o 8 7 0 277.35 279.05 5.27 o 9 7 0 101.24 94.04 4.17 o 10 7 0 211.60 213.39 4.66 o 11 7 0 1.19 2.91 1.91 o 12 7 0 22.82 20.72 3.31 o 2 8 0 85.74 85.03 5.08 o 3 8 0 960.45 968.43 12.12 o 4 8 0 575.60 561.26 14.83 o 5 8 0 23.35 23.58 2.80 o 6 8 0 2.29 3.11 1.59 o 7 8 0 2.63 3.88 2.00 o 8 8 0 414.66 411.99 11.45 o -19 1 1 129.07 131.84 5.23 o -18 1 1 297.32 301.94 7.16 o -17 1 1 222.43 231.97 6.06 o -16 1 1 318.44 312.73 6.31 o -15 1 1 3.35 3.21 1.43 o -14 1 1 43.84 39.69 2.26 o -13 1 1 103.25 97.35 1.83 o -12 1 1 16.45 15.26 1.05 o -11 1 1 2195.62 2171.71 22.80 o -10 1 1 2298.77 2232.27 19.63 o -9 1 1 1098.82 1142.07 13.27 o -8 1 1 49.10 49.78 1.86 o -7 1 1 148.89 133.83 2.67 o -6 1 1 18.24 14.30 1.05 o -5 1 1 434.17 568.52 6.29 o -4 1 1 2926.03 2842.60 12.19 o -3 1 1 1176.30 1130.35 25.63 o -2 1 1 144.94 133.75 1.47 o -1 1 1 3783.91 3501.10 33.17 o 0 1 1 1.83 2.43 0.74 o 1 1 1 3830.25 3694.00 55.20 o 2 1 1 1682.90 1690.81 20.97 o 3 1 1 8510.59 8130.43 80.13 o 4 1 1 1095.87 1181.74 10.81 o 5 1 1 18.42 22.18 0.94 o 6 1 1 387.00 374.70 2.89 o 7 1 1 1091.24 1065.98 5.78 o 8 1 1 2253.18 2190.37 18.09 o 9 1 1 781.77 785.41 3.56 o 10 1 1 0.19 1.96 0.64 o 11 1 1 394.40 384.23 3.50 o 12 1 1 222.54 227.41 3.21 o 13 1 1 99.58 99.86 2.39 o 14 1 1 1397.67 1421.76 11.53 o 15 1 1 1016.36 1010.06 13.23 o 16 1 1 162.05 169.81 7.19 o 17 1 1 0.05 1.40 1.73 o 18 1 1 87.31 88.59 4.90 o 19 1 1 113.20 108.05 3.94 o -20 2 1 737.27 767.72 11.69 o -19 2 1 157.94 160.92 6.28 o -18 2 1 42.33 42.17 4.03 o -17 2 1 26.33 23.90 3.21 o -16 2 1 32.89 30.06 3.05 o -15 2 1 385.44 385.47 4.33 o -14 2 1 1262.26 1291.56 7.89 o -13 2 1 757.32 769.57 5.31 o -12 2 1 394.18 376.21 4.53 o -11 2 1 19.16 21.72 1.16 o -10 2 1 9.13 8.99 0.95 o -9 2 1 1239.15 1209.89 14.92 o -8 2 1 936.10 937.93 11.54 o -7 2 1 1709.37 1769.68 5.50 o -6 2 1 420.85 449.44 5.31 o -5 2 1 47.56 40.71 1.72 o -4 2 1 259.83 283.75 2.83 o -3 2 1 0.27 4.84 0.68 o -2 2 1 1870.28 1845.97 13.62 o -1 2 1 276.47 198.43 1.85 o 0 2 1 413.34 373.84 2.76 o 1 2 1 434.10 454.50 3.10 o 2 2 1 529.29 626.82 6.76 o 3 2 1 3944.00 4206.29 53.61 o 4 2 1 1635.08 1641.70 20.08 o 5 2 1 3708.41 3779.82 26.35 o 6 2 1 305.73 298.96 2.29 o 7 2 1 44.81 52.52 1.17 o 8 2 1 30.24 29.01 1.17 o 9 2 1 10.68 14.71 1.08 o 10 2 1 869.41 858.12 4.73 o 11 2 1 383.39 383.31 3.04 o 12 2 1 454.04 468.13 4.09 o 13 2 1 120.21 116.58 2.46 o 14 2 1 74.89 74.70 2.80 o 15 2 1 14.97 14.07 2.53 o 16 2 1 124.53 127.35 3.71 o 17 2 1 455.17 478.89 6.53 o 18 2 1 985.29 1003.27 13.12 o 19 2 1 198.90 205.19 7.68 o -19 3 1 111.61 107.11 5.96 o -18 3 1 62.51 59.78 5.29 o -17 3 1 5.08 6.25 2.19 o -16 3 1 360.30 371.61 5.75 o -15 3 1 156.71 148.10 3.27 o -14 3 1 29.61 26.21 1.69 o -13 3 1 39.22 43.36 1.81 o -12 3 1 33.68 35.32 1.88 o -11 3 1 10.03 14.35 1.33 o -10 3 1 6.10 9.06 1.25 o -9 3 1 112.14 104.84 1.81 o -8 3 1 1130.08 1107.75 9.24 o -7 3 1 141.65 141.44 1.56 o -6 3 1 243.37 240.79 2.89 o -5 3 1 293.25 306.94 1.93 o -4 3 1 166.13 186.98 2.61 o -3 3 1 315.48 319.91 3.42 o -2 3 1 226.53 228.50 2.45 o -1 3 1 4589.98 4884.88 21.67 o 0 3 1 785.37 804.26 4.41 o 1 3 1 1.00 5.17 1.80 o 2 3 1 64.14 63.50 2.05 o 3 3 1 981.59 1054.77 5.72 o 4 3 1 236.73 244.16 3.26 o 5 3 1 274.54 278.75 2.39 o 6 3 1 2026.50 2079.77 10.68 o 7 3 1 372.64 380.00 2.41 o 8 3 1 80.19 75.64 2.14 o 9 3 1 101.10 99.76 1.81 o 10 3 1 3.42 5.50 1.05 o 11 3 1 181.70 176.97 2.81 o 12 3 1 438.23 432.31 3.33 o 13 3 1 351.16 354.38 3.78 o 14 3 1 124.21 125.36 2.88 o 15 3 1 10.53 9.74 2.20 o 16 3 1 28.56 25.17 3.75 o 17 3 1 96.52 97.40 5.78 o 18 3 1 0.16 4.96 3.36 o -18 4 1 212.55 212.60 4.45 o -17 4 1 576.36 598.64 7.45 o -16 4 1 0.01 3.18 1.71 o -15 4 1 156.99 155.62 2.95 o -14 4 1 462.36 456.28 4.69 o -13 4 1 240.22 253.17 4.28 o -12 4 1 392.68 386.70 4.36 o -11 4 1 69.19 69.34 1.95 o -10 4 1 251.16 245.83 2.73 o -9 4 1 845.55 814.72 9.81 o -8 4 1 1676.18 1658.53 12.42 o -7 4 1 92.94 95.88 1.52 o -6 4 1 2.51 2.90 0.66 o -5 4 1 3091.00 3046.89 27.90 o -4 4 1 793.19 793.09 12.47 o -3 4 1 95.01 109.40 1.65 o -2 4 1 443.18 429.87 5.08 o -1 4 1 1223.05 1283.91 17.63 o 0 4 1 2.81 5.11 1.31 o 1 4 1 321.60 363.13 3.40 o 2 4 1 305.50 292.58 2.48 o 3 4 1 13.82 15.18 1.16 o 4 4 1 473.01 479.16 6.13 o 5 4 1 1597.18 1629.02 12.90 o 6 4 1 266.93 258.60 2.82 o 7 4 1 54.56 55.51 1.79 o 8 4 1 664.26 662.10 6.62 o 9 4 1 344.64 340.43 4.21 o 10 4 1 21.36 19.84 1.66 o 11 4 1 9.40 9.14 1.51 o 12 4 1 326.15 328.30 3.41 o 13 4 1 9.37 10.91 1.76 o 14 4 1 11.86 9.54 1.70 o 15 4 1 106.86 100.01 3.86 o 16 4 1 33.79 31.15 7.02 o 17 4 1 111.23 109.90 6.25 o -17 5 1 99.30 93.20 4.45 o -16 5 1 94.22 90.76 2.88 o -15 5 1 40.72 37.41 2.23 o -14 5 1 101.07 98.26 3.13 o -13 5 1 10.30 9.61 1.60 o -12 5 1 613.66 621.92 5.00 o -11 5 1 462.73 466.29 4.82 o -10 5 1 622.13 620.29 4.59 o -9 5 1 47.23 49.50 1.82 o -8 5 1 0.04 2.22 0.97 o -7 5 1 0.08 2.82 0.87 o -6 5 1 1.04 2.57 0.80 o -5 5 1 1420.45 1429.02 12.49 o -4 5 1 532.61 506.13 6.16 o -3 5 1 0.30 2.61 0.87 o -2 5 1 16.56 18.81 1.28 o -1 5 1 139.89 114.64 2.32 o 0 5 1 29.96 35.08 1.34 o 1 5 1 525.58 539.09 5.08 o 2 5 1 1061.50 1062.26 9.14 o 3 5 1 1320.50 1281.00 7.40 o 4 5 1 0.12 2.47 0.83 o 5 5 1 2.36 3.13 1.04 o 6 5 1 141.41 150.62 3.77 o 7 5 1 9.12 11.64 1.43 o 8 5 1 554.48 543.31 5.95 o 9 5 1 526.47 514.18 7.80 o 10 5 1 48.41 47.19 1.85 o 11 5 1 6.94 7.13 1.69 o 12 5 1 87.17 80.17 2.50 o 13 5 1 84.61 80.68 2.53 o 14 5 1 171.95 170.26 3.39 o 15 5 1 143.01 140.90 3.33 o 16 5 1 338.71 343.32 5.28 o -15 6 1 0.23 3.43 1.75 o -14 6 1 42.02 40.56 2.37 o -13 6 1 5.78 5.99 1.73 o -12 6 1 430.39 435.19 5.09 o -11 6 1 292.88 291.87 3.86 o -10 6 1 174.73 171.27 3.10 o -9 6 1 2.79 4.36 1.33 o -8 6 1 2.55 3.18 1.10 o -7 6 1 64.40 65.95 2.32 o -6 6 1 547.78 537.71 6.87 o -5 6 1 914.35 937.21 9.97 o -4 6 1 392.90 405.15 4.37 o -3 6 1 497.50 484.04 6.30 o -2 6 1 17.93 16.91 1.81 o -1 6 1 211.08 180.21 4.77 o 0 6 1 229.29 226.35 5.90 o 1 6 1 332.09 351.61 4.08 o 2 6 1 699.73 710.69 6.89 o 3 6 1 1.09 4.20 1.28 o 4 6 1 195.13 188.89 3.06 o 5 6 1 0.22 2.78 1.24 o 6 6 1 58.09 56.50 2.57 o 7 6 1 272.18 251.43 4.01 o 8 6 1 201.80 208.05 3.43 o 9 6 1 299.54 295.41 5.92 o 10 6 1 199.03 199.67 4.57 o 11 6 1 197.62 197.35 4.91 o 12 6 1 89.09 87.50 3.38 o 13 6 1 159.86 168.47 5.07 o 14 6 1 48.58 41.15 2.84 o -12 7 1 68.11 62.84 3.90 o -11 7 1 204.76 204.45 7.72 o -10 7 1 18.38 20.74 2.41 o -9 7 1 24.37 25.31 3.60 o -8 7 1 480.40 491.34 6.74 o -7 7 1 728.87 716.79 14.82 o -6 7 1 144.67 146.31 3.47 o -5 7 1 86.88 87.56 2.82 o -4 7 1 156.39 145.41 3.70 o -3 7 1 200.62 194.59 5.35 o -2 7 1 639.37 625.59 10.81 o -1 7 1 1183.48 1226.62 12.05 o 0 7 1 576.20 549.82 8.40 o 1 7 1 8.93 10.82 3.33 o 2 7 1 547.51 526.93 19.02 o 3 7 1 378.93 385.21 4.15 o 4 7 1 186.82 187.71 5.96 o 5 7 1 485.41 481.32 6.18 o 6 7 1 462.30 465.40 9.39 o 7 7 1 98.29 102.98 4.65 o 8 7 1 45.21 50.61 2.71 o 9 7 1 99.54 91.41 4.22 o 10 7 1 5.73 5.92 2.48 o 11 7 1 709.58 699.05 15.06 o -9 8 1 29.60 30.31 2.65 o -8 8 1 146.26 149.64 5.04 o -7 8 1 58.82 49.06 4.14 o -6 8 1 16.74 18.21 3.00 o -5 8 1 122.68 122.28 4.55 o -4 8 1 241.84 242.36 6.98 o -3 8 1 4.15 6.86 2.83 o 3 8 1 323.45 321.87 8.20 o 4 8 1 101.28 104.73 6.35 o 5 8 1 143.31 142.92 8.51 o 6 8 1 177.53 168.70 4.05 o 7 8 1 62.57 63.61 3.70 o 8 8 1 132.52 128.61 3.76 o -16 0 2 224.25 205.64 6.88 o -15 0 2 688.40 667.34 21.60 o -14 0 2 5.01 7.49 2.79 o -13 0 2 93.27 85.96 4.34 o -12 0 2 20.71 22.42 1.28 o -11 0 2 35.79 29.51 1.65 o -10 0 2 2762.68 2578.51 77.61 o -9 0 2 3889.02 3665.89 173.57 o -8 0 2 1104.42 1096.61 43.62 o -7 0 2 1323.78 1302.96 51.15 o -6 0 2 720.74 847.10 45.06 o -5 0 2 289.76 339.31 44.65 o -4 0 2 2618.96 2619.93 105.17 o -3 0 2 2148.10 2101.22 66.76 o -2 0 2 7741.32 7343.92 13.67 o -1 0 2 2298.45 2152.82 7.41 o 0 0 2 4693.91 4655.13 76.59 o 1 0 2 1242.22 1185.98 8.75 o 2 0 2 7987.96 8080.81 96.51 o 3 0 2 542.29 502.42 8.56 o 4 0 2 7593.11 7499.25 20.20 o 5 0 2 3301.09 3400.92 64.97 o 6 0 2 4113.31 4319.78 45.78 o 7 0 2 303.07 296.51 3.48 o 8 0 2 73.10 62.76 3.31 o 9 0 2 190.08 173.30 4.33 o 10 0 2 665.37 687.62 5.87 o 11 0 2 3029.21 3113.70 15.26 o 12 0 2 786.00 792.02 6.99 o 13 0 2 78.85 76.16 2.87 o 14 0 2 223.07 219.32 4.61 o 15 0 2 7.17 6.04 2.33 o 16 0 2 129.38 133.09 5.76 o 17 0 2 534.43 564.03 10.25 o 18 0 2 272.32 267.59 7.96 o -17 1 2 5.31 6.61 4.60 o -16 1 2 0.31 4.44 1.39 o -15 1 2 13.64 15.34 1.80 o -14 1 2 3.42 3.50 1.08 o -13 1 2 832.90 844.16 12.06 o -12 1 2 255.28 248.36 4.63 o -11 1 2 460.65 453.11 6.56 o -10 1 2 3.30 5.00 0.80 o -9 1 2 430.09 427.03 9.00 o -8 1 2 709.58 692.90 18.08 o -7 1 2 233.24 235.70 4.82 o -6 1 2 5108.98 5180.44 89.21 o -5 1 2 3498.09 3743.91 19.18 o -4 1 2 69.28 73.19 1.63 o -3 1 2 132.38 121.73 1.47 o -2 1 2 2136.88 2285.45 12.36 o -1 1 2 85.21 82.01 1.58 o 0 1 2 2942.49 2949.01 6.68 o 1 1 2 916.80 909.60 3.64 o 2 1 2 2613.90 2665.32 17.40 o 3 1 2 45.22 52.03 1.30 o 4 1 2 301.69 318.13 4.18 o 5 1 2 206.94 201.11 2.24 o 6 1 2 77.68 76.51 1.93 o 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148.43 143.79 4.21 o -4 4 9 378.71 371.39 8.44 o -3 4 9 32.83 29.01 3.93 o -2 4 9 46.06 41.11 2.80 o -1 4 9 748.95 755.35 20.99 o 0 4 9 258.89 267.81 5.69 o 1 4 9 1.20 3.73 2.06 o 2 4 9 279.42 272.44 11.92 o 3 4 9 504.07 520.10 7.36 o 4 4 9 2.92 3.40 2.39 o 5 4 9 50.74 47.06 3.61 o -11 5 9 26.62 22.55 3.07 o -10 5 9 25.84 26.10 3.31 o -9 5 9 171.08 174.22 6.66 o -8 5 9 495.34 501.70 11.05 o -7 5 9 281.78 281.36 5.79 o -6 5 9 124.92 119.30 4.16 o -5 5 9 5.85 8.62 3.59 o -4 5 9 0.28 3.82 2.10 o -3 5 9 1.14 0.49 2.13 o -2 5 9 30.63 27.09 3.33 o -1 5 9 564.35 563.46 14.90 o 0 5 9 108.33 115.62 4.75 o 1 5 9 1.65 2.80 2.45 o 2 5 9 6.73 5.23 2.86 o -15 0 10 321.47 318.60 8.32 o -14 0 10 91.39 94.92 5.58 o -13 0 10 737.20 740.24 11.16 o -12 0 10 664.85 683.37 10.91 o -11 0 10 711.52 716.03 10.99 o -10 0 10 1.55 2.78 2.16 o -9 0 10 237.45 241.37 7.28 o -8 0 10 2.92 2.86 2.16 o -7 0 10 24.44 28.83 4.09 o -6 0 10 2622.31 2699.52 18.95 o -5 0 10 1898.87 1949.86 16.29 o -4 0 10 120.31 122.57 5.43 o 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157.04 5.24 o -6 1 11 75.60 72.37 3.68 o -5 1 11 226.70 218.80 5.14 o -4 1 11 393.46 394.28 6.37 o -3 1 11 595.68 611.40 10.51 o -2 1 11 290.27 302.63 8.03 o -11 2 11 0.63 5.16 2.75 o -10 2 11 2.11 4.52 2.76 o -9 2 11 45.25 41.74 3.43 o -8 2 11 151.13 149.77 10.00 o -7 2 11 268.30 275.77 8.17 o -6 2 11 148.72 147.78 6.23 o -5 2 11 13.93 18.27 3.70 o -4 2 11 18.96 18.22 3.69 o -3 2 11 102.15 94.26 5.75 o 0 2 11 316.98 325.39 8.50 o -8 3 11 16.11 12.36 3.27 o -7 3 11 299.24 294.41 5.81 o -6 3 11 293.84 300.62 11.38 o -5 3 11 57.06 58.97 3.49 o -4 3 11 24.60 16.16 3.64 o -3 3 11 2.66 1.92 2.99 o