#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/31/2013146.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013146_Fobs loop_ _publ_author_name 'Bajue, Stanley A.' 'Gumbs, Shellie' 'Jones, Lauren' 'Bramwell, Fitzgerald B.' 'Patrick, Brian O.' 'Selegue, John P.' 'Brock, Carolyn Pratt' _publ_section_title ; Dichloro[1,1'-(5,9-dithia-2,12-diazoniatrideca-1,12-diene-1,13-diyl)dinaphthalen-2-olato-\k^2^O,O']dimethyltin(IV) acetonitrile solvate ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m10 _journal_page_last m12 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 84.320 _cell_angle_beta 66.410 _cell_angle_gamma 71.100 _cell_length_a 12.3340 _cell_length_b 12.7650 _cell_length_c 12.8320 _exptl_crystal_F_000 780.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file fr1402Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SB-III/38B' _shelx_refln_list_code 4 _shelx_f_calc_maximum 116.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ 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0 35.57 22.71 4.69 o -10 2 0 253.25 258.95 17.96 o -9 2 0 9.52 7.86 5.01 o -8 2 0 1.52 15.89 12.48 o -7 2 0 2085.14 2050.55 89.85 o -6 2 0 46.26 40.82 4.65 o -5 2 0 6875.52 6790.95 299.95 o -4 2 0 1190.39 1177.33 57.93 o -3 2 0 11610.68 11227.43 574.66 o -2 2 0 7339.33 7265.08 427.02 o -1 2 0 6109.43 6078.44 523.00 o 0 2 0 5506.31 4962.27 382.48 o 1 2 0 182.24 180.84 10.82 o 2 2 0 2076.75 2051.35 135.83 o 3 2 0 140.41 186.54 9.36 o 4 2 0 4047.89 3691.77 279.08 o 5 2 0 8197.02 7493.78 556.11 o 6 2 0 691.74 755.81 37.23 o 7 2 0 3396.07 3505.86 165.84 o 8 2 0 21.23 35.75 19.20 o 9 2 0 290.65 298.86 14.57 o 10 2 0 89.69 83.97 5.46 o 11 2 0 7.26 24.12 15.61 o 12 2 0 379.30 425.11 20.86 o 13 2 0 10.23 27.25 10.12 o -11 3 0 39.88 41.69 14.22 o -10 3 0 94.55 113.31 10.96 o -9 3 0 535.49 537.84 26.41 o -8 3 0 69.38 73.37 6.65 o -7 3 0 14.13 18.93 16.44 o -6 3 0 3811.30 3875.98 173.87 o -5 3 0 43.35 51.29 4.25 o -4 3 0 11438.35 11160.10 817.04 o -3 3 0 1369.15 1346.70 90.94 o -2 3 0 8138.63 7840.46 336.19 o 2 3 0 2069.66 2051.35 191.59 o 3 3 0 294.41 251.12 14.21 o 4 3 0 3059.04 2859.35 154.41 o 5 3 0 1953.15 1773.06 99.85 o 6 3 0 171.74 171.21 9.82 o 7 3 0 24.47 16.51 2.51 o 8 3 0 520.60 527.92 24.38 o 9 3 0 461.79 471.92 21.14 o 10 3 0 60.01 65.18 5.97 o 11 3 0 490.11 515.67 26.83 o 12 3 0 2.98 9.53 6.91 o 13 3 0 430.38 432.53 22.94 o -11 4 0 23.52 36.86 9.01 o -10 4 0 59.55 84.64 17.29 o -9 4 0 0.44 18.38 23.18 o -8 4 0 281.26 275.99 13.06 o -7 4 0 34.55 35.75 3.96 o -6 4 0 300.19 319.35 15.79 o -5 4 0 6724.51 6946.45 277.55 o -4 4 0 28.77 28.52 5.30 o -2 4 0 8.46 21.08 11.46 o -1 4 0 1348.99 1338.61 54.36 o 1 4 0 177.48 209.49 12.11 o 3 4 0 284.17 240.11 14.61 o 4 4 0 1323.37 1384.41 77.09 o 5 4 0 2173.88 2154.96 114.11 o 6 4 0 636.52 597.74 36.68 o 7 4 0 43.77 31.96 5.42 o 8 4 0 327.57 311.01 14.51 o 9 4 0 33.48 35.86 6.94 o 10 4 0 502.55 482.14 18.76 o 11 4 0 151.25 154.95 8.81 o 12 4 0 404.65 372.23 19.22 o 13 4 0 6.01 20.56 14.23 o -10 5 0 0.16 5.22 4.53 o -9 5 0 77.67 66.07 8.98 o -8 5 0 485.86 500.12 26.18 o -7 5 0 631.91 624.41 23.62 o -6 5 0 621.55 613.61 26.40 o -5 5 0 886.05 953.40 138.41 o -4 5 0 3097.50 3160.56 119.53 o -3 5 0 132.75 129.39 7.29 o -2 5 0 8348.83 8516.59 415.45 o -1 5 0 4498.52 4489.05 202.45 o 0 5 0 1928.17 1932.68 82.32 o 2 5 0 139.07 167.32 7.36 o 3 5 0 4008.69 3626.73 190.60 o 4 5 0 2.29 1.29 1.67 o 5 5 0 24.93 26.31 2.84 o 6 5 0 1938.67 1872.34 109.49 o 7 5 0 15.55 14.07 5.21 o 8 5 0 718.32 695.68 35.95 o 9 5 0 133.76 136.45 13.75 o 10 5 0 220.66 220.49 12.48 o 11 5 0 512.64 501.34 22.60 o 12 5 0 14.52 36.36 13.83 o 13 5 0 118.02 106.06 10.50 o -10 6 0 253.57 257.28 15.90 o -9 6 0 14.75 26.38 10.80 o -8 6 0 340.48 329.59 14.42 o -7 6 0 628.55 674.52 31.56 o -6 6 0 576.94 581.28 21.47 o -5 6 0 1189.20 1163.47 43.20 o -4 6 0 15.91 25.20 7.11 o -3 6 0 2190.16 2337.55 103.61 o -2 6 0 3332.80 3376.68 150.97 o -1 6 0 9680.65 9891.12 662.44 o 0 6 0 4821.49 5122.72 211.83 o 1 6 0 1353.37 1419.67 58.83 o 2 6 0 3603.71 3669.84 159.34 o 3 6 0 59.25 82.37 4.08 o 4 6 0 788.75 736.94 50.07 o 5 6 0 124.23 122.12 7.10 o 6 6 0 863.24 788.54 45.97 o 7 6 0 1620.59 1563.88 75.55 o 8 6 0 14.91 12.22 8.64 o 9 6 0 1772.51 1938.55 84.55 o 10 6 0 18.92 19.65 6.96 o 11 6 0 344.92 337.53 16.79 o 12 6 0 279.57 273.65 12.60 o 13 6 0 0.01 3.37 4.02 o -9 7 0 337.23 311.02 25.13 o -8 7 0 32.36 41.09 23.37 o -7 7 0 495.76 507.27 24.75 o -6 7 0 547.06 528.05 23.42 o -5 7 0 194.21 195.65 10.45 o -4 7 0 3355.08 3469.23 137.54 o -3 7 0 2.98 2.31 4.26 o -2 7 0 3322.02 3311.55 137.92 o -1 7 0 4253.05 4442.91 173.70 o 0 7 0 5327.93 5574.56 219.08 o 1 7 0 2549.20 2722.27 113.07 o 2 7 0 809.99 831.61 29.68 o 3 7 0 4.64 3.02 2.82 o 4 7 0 1849.68 1778.29 88.70 o 5 7 0 354.73 321.59 16.30 o 6 7 0 757.01 718.95 40.73 o 7 7 0 6.19 7.53 6.17 o 8 7 0 506.46 523.73 24.82 o 9 7 0 58.93 59.58 7.42 o 10 7 0 232.80 228.00 12.79 o 11 7 0 48.26 68.62 13.48 o 12 7 0 98.73 70.80 7.46 o 13 7 0 428.40 406.39 28.02 o -8 8 0 561.26 509.57 22.91 o -7 8 0 0.50 6.01 9.10 o -6 8 0 579.82 570.32 103.73 o -5 8 0 773.86 749.78 29.76 o -4 8 0 39.31 35.63 5.90 o -3 8 0 4196.30 4334.30 170.04 o -2 8 0 129.58 138.65 11.86 o -1 8 0 2769.70 2848.65 106.97 o 0 8 0 1092.86 1163.64 44.59 o 1 8 0 4.10 7.11 8.97 o 2 8 0 3706.17 3775.73 129.55 o 3 8 0 280.39 291.07 11.26 o 4 8 0 1520.17 1543.25 77.26 o 5 8 0 856.71 895.80 45.95 o 6 8 0 830.84 786.59 41.12 o 7 8 0 181.23 164.51 9.79 o 8 8 0 3.60 9.76 3.89 o 9 8 0 82.10 72.02 5.56 o 10 8 0 219.37 233.40 220.99 o 11 8 0 292.26 309.98 19.16 o 12 8 0 161.21 146.49 24.53 o 13 8 0 4.14 34.19 9.98 o -7 9 0 654.11 587.00 28.01 o -6 9 0 366.15 386.98 18.47 o -5 9 0 1645.46 1611.88 59.81 o -4 9 0 1163.82 1213.70 48.85 o -3 9 0 105.70 108.04 137.57 o -2 9 0 1487.07 1519.90 61.76 o -1 9 0 39.98 41.80 11.50 o 0 9 0 57.97 60.67 3.95 o 1 9 0 1146.03 1147.01 38.19 o 2 9 0 77.92 96.46 4.63 o 3 9 0 4149.34 4199.60 174.59 o 4 9 0 44.76 47.77 4.76 o 5 9 0 1053.33 1042.43 50.74 o 6 9 0 440.36 469.09 25.58 o 7 9 0 99.70 99.46 36.76 o 8 9 0 182.11 193.62 24.76 o 9 9 0 1.22 24.44 12.04 o 10 9 0 218.41 230.56 13.23 o 11 9 0 261.86 250.15 13.05 o 12 9 0 117.40 146.06 16.84 o -6 10 0 261.03 264.96 13.94 o -5 10 0 1143.29 1104.02 46.71 o -4 10 0 355.98 360.52 15.79 o -3 10 0 1450.71 1468.95 58.97 o -2 10 0 23.27 65.40 10.19 o 0 10 0 427.63 460.26 18.30 o 1 10 0 27.92 27.13 10.87 o 2 10 0 396.09 384.61 20.12 o 3 10 0 30.65 26.40 4.86 o 4 10 0 1672.23 1754.32 67.90 o 5 10 0 255.44 245.67 10.25 o 6 10 0 138.93 149.50 16.53 o 7 10 0 386.52 371.91 19.15 o 8 10 0 3.26 27.20 15.08 o 9 10 0 816.62 801.26 41.34 o 10 10 0 0.75 7.16 3.44 o 11 10 0 295.87 301.06 31.76 o 12 10 0 51.55 62.13 12.68 o -5 11 0 182.42 173.96 12.30 o -4 11 0 257.45 304.30 17.51 o -3 11 0 174.84 171.93 11.77 o -2 11 0 722.40 738.90 28.97 o -1 11 0 931.86 954.64 35.51 o 0 11 0 864.71 834.70 34.86 o 1 11 0 2599.06 2655.78 129.33 o 2 11 0 1183.76 1295.65 73.29 o 3 11 0 763.87 783.15 44.17 o 5 11 0 132.90 118.81 5.78 o 6 11 0 405.74 366.68 21.12 o 7 11 0 30.60 26.61 3.53 o 8 11 0 504.97 458.59 21.79 o 9 11 0 251.57 254.85 38.72 o 10 11 0 649.91 527.63 191.06 o 11 11 0 16.49 12.25 28.57 o -4 12 0 72.98 77.90 7.70 o -3 12 0 444.06 437.60 23.29 o -2 12 0 38.59 31.00 9.36 o -1 12 0 748.69 772.02 30.43 o 0 12 0 77.67 83.41 4.75 o 1 12 0 318.00 308.06 18.01 o 2 12 0 494.04 508.74 37.38 o 3 12 0 11.37 -0.56 8.57 o 4 12 0 488.18 496.00 45.70 o 5 12 0 792.78 831.58 62.81 o 6 12 0 165.73 148.54 12.10 o 7 12 0 152.93 152.66 8.67 o 8 12 0 329.85 307.60 95.08 o 9 12 0 15.83 24.19 9.64 o 10 12 0 64.84 70.39 7.44 o 11 12 0 137.15 134.50 13.41 o -2 13 0 809.68 780.07 31.30 o -1 13 0 15.74 30.62 12.59 o 0 13 0 410.32 392.12 15.35 o 1 13 0 30.31 31.22 7.50 o 2 13 0 1.21 50.67 24.72 o 3 13 0 273.71 301.72 26.05 o 4 13 0 5.71 28.13 14.82 o 5 13 0 396.09 407.54 23.58 o 6 13 0 196.31 217.33 19.31 o 7 13 0 266.79 224.28 10.88 o 8 13 0 345.01 318.58 14.92 o 9 13 0 27.76 45.21 16.67 o 10 13 0 28.70 38.82 17.79 o 0 14 0 101.69 115.53 11.88 o 1 14 0 158.63 160.24 16.98 o 2 14 0 29.70 27.71 9.31 o 3 14 0 4.65 38.87 47.14 o 4 14 0 203.84 209.72 15.55 o 5 14 0 16.59 8.99 8.43 o 6 14 0 277.05 256.66 28.07 o 7 14 0 0.35 0.48 7.29 o 8 14 0 28.64 32.20 5.27 o 3 15 0 176.66 172.87 15.77 o 4 15 0 6.18 -2.30 12.75 o 5 15 0 184.34 171.42 19.84 o -8 -14 1 82.15 85.23 6.43 o -7 -14 1 129.33 130.91 17.71 o -6 -14 1 59.28 81.65 14.12 o -5 -14 1 4.60 46.06 29.46 o -4 -14 1 31.57 49.33 20.40 o -3 -14 1 86.67 119.99 22.65 o -2 -14 1 472.61 471.70 39.77 o -1 -14 1 36.02 26.07 6.20 o 0 -14 1 334.06 304.43 18.28 o -9 -13 1 134.50 125.43 13.17 o -8 -13 1 54.05 56.39 4.91 o -7 -13 1 1.12 11.77 13.11 o -6 -13 1 292.51 270.15 17.22 o -5 -13 1 6.82 13.59 5.37 o -4 -13 1 410.34 434.74 25.34 o -3 -13 1 304.41 319.81 23.14 o -2 -13 1 43.78 56.33 11.61 o -1 -13 1 348.76 337.82 28.47 o 0 -13 1 105.83 135.68 10.99 o 1 -13 1 178.51 163.25 12.89 o 2 -13 1 374.38 353.68 19.99 o 3 -13 1 78.45 76.63 27.96 o -10 -12 1 242.42 203.61 10.78 o -9 -12 1 39.02 35.07 5.69 o 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o -7 -10 1 750.87 717.12 36.80 o -6 -10 1 1179.44 1186.08 55.15 o -5 -10 1 1070.37 1058.79 56.17 o -4 -10 1 99.14 108.54 6.85 o -3 -10 1 114.01 112.45 11.68 o -2 -10 1 218.03 228.17 10.69 o -1 -10 1 40.89 42.45 4.84 o 0 -10 1 2790.92 2906.19 116.49 o 1 -10 1 516.47 590.45 31.83 o 3 -10 1 1334.69 1345.87 55.85 o 4 -10 1 1211.77 1231.06 43.28 o 5 -10 1 18.74 20.33 6.31 o 6 -10 1 1.64 33.98 10.60 o 7 -10 1 47.29 46.52 9.24 o -12 -9 1 45.90 48.93 13.24 o -11 -9 1 124.94 119.52 26.33 o -10 -9 1 0.91 3.01 4.79 o -9 -9 1 293.76 302.27 15.79 o -8 -9 1 85.17 86.13 7.47 o -7 -9 1 142.20 141.76 8.71 o -6 -9 1 1062.92 1039.69 53.04 o -5 -9 1 100.75 99.74 9.31 o -4 -9 1 1773.01 1794.01 91.45 o -3 -9 1 161.85 169.13 8.12 o -2 -9 1 780.65 779.46 31.35 o -1 -9 1 4685.55 4858.28 180.09 o 0 -9 1 155.76 179.99 10.36 o 1 -9 1 582.35 602.36 24.91 o 2 -9 1 450.81 444.13 20.21 o 3 -9 1 843.02 871.44 31.54 o 4 -9 1 1942.51 2005.24 77.38 o 5 -9 1 14.49 32.37 6.90 o 6 -9 1 693.08 684.54 27.43 o 7 -9 1 7.95 23.75 7.49 o 8 -9 1 465.21 383.74 20.78 o -12 -8 1 23.26 14.23 3.59 o -11 -8 1 92.27 88.26 8.86 o -10 -8 1 429.88 427.03 22.59 o -9 -8 1 44.15 39.87 4.64 o -8 -8 1 780.68 793.76 41.77 o -7 -8 1 8.96 25.97 19.50 o -6 -8 1 203.64 184.04 9.15 o -5 -8 1 1235.90 1227.45 59.81 o -4 -8 1 227.59 233.17 11.85 o -3 -8 1 3734.47 3707.59 139.83 o -2 -8 1 2802.17 2907.22 103.77 o -1 -8 1 903.53 900.13 31.35 o 1 -8 1 470.79 497.21 20.00 o 2 -8 1 2578.08 2695.76 103.81 o 3 -8 1 16.54 36.96 8.77 o 4 -8 1 3.51 -0.73 3.14 o 5 -8 1 109.64 117.58 8.89 o 6 -8 1 203.12 195.73 47.07 o 7 -8 1 421.77 363.19 16.11 o 8 -8 1 231.81 195.04 30.84 o -12 -7 1 67.03 75.23 15.02 o -11 -7 1 98.39 111.79 7.15 o -10 -7 1 203.96 202.82 11.38 o -9 -7 1 49.83 64.98 7.67 o -8 -7 1 9.01 16.81 4.09 o -7 -7 1 369.84 367.82 18.95 o -6 -7 1 863.58 878.18 45.15 o -5 -7 1 185.69 173.12 9.28 o -4 -7 1 5677.77 5629.27 292.51 o -3 -7 1 1133.14 1115.73 50.78 o -1 -7 1 1262.23 1342.43 45.83 o 0 -7 1 1173.00 1227.28 45.17 o 1 -7 1 6593.78 6838.93 301.68 o 2 -7 1 308.66 305.86 14.43 o 3 -7 1 2259.87 2396.81 102.02 o 4 -7 1 275.37 292.24 14.74 o 5 -7 1 19.07 35.96 6.93 o 6 -7 1 852.36 868.61 34.95 o 7 -7 1 120.45 123.14 7.72 o 8 -7 1 105.72 99.90 24.42 o 9 -7 1 7.74 28.54 20.43 o -12 -6 1 162.08 148.60 35.31 o -11 -6 1 167.67 169.07 23.31 o -10 -6 1 956.64 969.50 42.89 o -9 -6 1 19.74 25.77 4.80 o -8 -6 1 4.98 6.99 6.28 o -7 -6 1 2.77 4.87 2.76 o -6 -6 1 465.66 524.45 27.00 o -5 -6 1 4514.37 4371.40 219.36 o -4 -6 1 252.04 243.12 13.43 o -3 -6 1 6224.52 5653.00 411.79 o -2 -6 1 1276.04 1285.69 56.93 o -1 -6 1 9542.64 9666.37 617.63 o 0 -6 1 3590.60 3845.35 171.93 o 1 -6 1 883.80 902.04 38.35 o 2 -6 1 2187.67 2310.19 104.99 o 3 -6 1 1574.35 1646.71 76.14 o 4 -6 1 2402.52 2477.69 94.99 o 5 -6 1 483.86 486.65 22.21 o 6 -6 1 134.69 136.70 11.85 o 7 -6 1 629.48 608.06 27.92 o 8 -6 1 0.12 24.89 13.51 o 9 -6 1 219.11 227.01 15.12 o 10 -6 1 7.67 16.66 5.07 o -13 -5 1 2.66 21.83 12.61 o -12 -5 1 231.98 201.12 20.12 o -11 -5 1 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6.63 o 4 0 13 107.61 109.84 8.27 o 5 0 13 136.92 122.77 9.09 o 6 0 13 173.96 169.56 10.89 o 7 0 13 109.78 109.51 11.89 o 8 0 13 143.73 126.30 14.37 o 9 0 13 105.38 112.00 20.72 o 10 0 13 396.75 427.21 23.49 o 11 0 13 0.71 6.02 4.47 o -1 1 13 511.23 530.30 28.44 o 0 1 13 47.68 46.13 5.67 o 1 1 13 548.87 570.68 34.69 o 2 1 13 1.37 16.46 7.49 o 3 1 13 277.33 295.18 20.34 o 4 1 13 11.22 8.43 12.65 o 5 1 13 70.84 57.76 11.04 o 6 1 13 503.24 472.72 31.23 o 7 1 13 11.60 16.78 11.70 o 8 1 13 405.05 422.33 26.60 o 9 1 13 258.93 248.63 16.42 o 10 1 13 22.23 31.13 7.31 o 11 1 13 530.75 488.87 22.28 o -1 2 13 184.05 202.30 13.42 o 0 2 13 269.19 249.24 24.64 o 1 2 13 3.46 22.27 11.55 o 2 2 13 334.56 328.62 19.74 o 3 2 13 151.84 145.99 29.18 o 4 2 13 118.31 143.52 36.87 o 5 2 13 1.89 13.18 10.89 o 6 2 13 13.18 15.08 11.89 o 7 2 13 603.96 632.21 62.31 o 8 2 13 232.43 235.13 18.16 o 9 2 13 140.15 156.62 15.96 o 10 2 13 506.81 460.15 27.45 o 11 2 13 37.25 29.17 10.15 o -1 3 13 319.21 289.73 18.90 o 0 3 13 162.64 167.50 13.24 o 1 3 13 72.32 113.85 25.60 o 2 3 13 0.66 6.86 10.42 o 3 3 13 72.70 68.67 8.63 o 4 3 13 615.37 619.96 42.05 o 5 3 13 170.30 181.48 17.22 o 6 3 13 146.83 157.66 18.04 o 7 3 13 9.09 19.20 7.63 o 8 3 13 398.70 385.21 18.30 o 9 3 13 173.64 183.86 9.91 o 10 3 13 136.30 139.54 24.73 o 11 3 13 611.69 572.71 24.92 o 12 3 13 160.61 141.46 11.06 o 0 4 13 109.97 93.33 7.95 o 1 4 13 0.04 10.54 14.44 o 2 4 13 421.31 402.45 20.61 o 3 4 13 1.84 5.97 10.35 o 4 4 13 196.52 187.71 10.16 o 5 4 13 204.02 191.28 8.87 o 6 4 13 213.13 215.66 11.69 o 7 4 13 215.21 202.35 12.83 o 8 4 13 233.16 204.99 13.07 o 9 4 13 37.60 32.44 7.10 o 10 4 13 561.62 539.60 41.08 o 11 4 13 105.00 100.26 23.09 o 12 4 13 696.05 661.63 29.86 o 1 5 13 375.53 348.43 21.63 o 2 5 13 19.42 40.24 8.71 o 3 5 13 649.94 622.19 27.42 o 4 5 13 117.35 132.37 18.66 o 5 5 13 121.39 125.85 12.54 o 6 5 13 134.64 139.15 14.58 o 7 5 13 6.70 27.69 14.26 o 8 5 13 665.71 694.55 38.21 o 9 5 13 461.06 413.59 20.62 o 10 5 13 55.51 62.07 7.78 o 11 5 13 737.17 701.59 61.76 o 1 6 13 2.41 12.86 8.80 o 2 6 13 128.85 115.65 8.82 o 3 6 13 0.13 8.14 17.48 o 4 6 13 284.84 288.41 16.91 o 5 6 13 2.93 38.70 158.17 o 6 6 13 1.21 25.05 13.32 o 7 6 13 410.32 363.39 20.42 o 8 6 13 132.18 154.86 13.52 o 9 6 13 1108.32 1146.90 60.72 o 10 6 13 467.65 488.17 25.54 o 11 6 13 111.35 115.31 8.78 o 2 7 13 84.85 98.41 15.66 o 3 7 13 0.66 15.59 12.66 o 4 7 13 7.16 18.70 8.72 o 5 7 13 44.47 38.44 7.76 o 6 7 13 203.04 194.00 18.02 o 7 7 13 14.80 36.14 8.39 o 8 7 13 649.80 616.49 28.53 o 9 7 13 192.84 181.88 20.17 o 10 7 13 678.63 664.11 32.36 o 11 7 13 340.29 323.69 20.38 o 4 8 13 52.44 30.34 15.48 o 5 8 13 334.47 257.96 22.14 o 6 8 13 45.45 34.37 19.51 o 7 8 13 507.63 487.88 28.17 o 8 8 13 6.46 19.94 6.42 o 9 8 13 397.88 365.92 18.97 o 10 8 13 263.85 66.08 29.90 o 6 9 13 204.20 147.32 21.84 o 7 9 13 11.05 17.36 15.92 o 8 9 13 542.58 539.44 37.39 o 2 -4 14 302.64 317.27 26.15 o 3 -4 14 40.01 31.04 19.44 o 4 -4 14 117.07 134.04 27.04 o 5 -4 14 67.55 78.41 19.84 o 6 -4 14 30.89 47.47 12.94 o 1 -3 14 83.18 129.68 115.58 o 2 -3 14 145.29 184.47 34.52 o 3 -3 14 515.15 586.63 45.11 o 4 -3 14 101.54 142.01 54.36 o 5 -3 14 21.97 51.23 25.08 o 6 -3 14 16.34 39.96 18.26 o 7 -3 14 9.46 43.01 26.71 o 1 -2 14 317.98 323.20 28.66 o 2 -2 14 2.42 19.05 15.22 o 3 -2 14 65.26 60.68 7.99 o 4 -2 14 232.14 228.40 15.27 o 5 -2 14 25.23 14.53 6.02 o 6 -2 14 72.12 84.39 8.12 o 8 -2 14 32.43 44.47 14.52 o 1 -1 14 52.69 55.97 8.15 o 2 -1 14 193.08 188.13 16.02 o 3 -1 14 28.52 28.80 9.91 o 4 -1 14 18.97 36.64 11.47 o 5 -1 14 255.35 268.43 19.13 o 6 -1 14 194.46 214.08 19.17 o 8 -1 14 425.21 414.58 25.71 o 9 -1 14 92.29 90.14 16.18 o 1 0 14 0.83 40.86 26.54 o 2 0 14 140.33 128.08 13.75 o 3 0 14 6.44 24.88 10.31 o 4 0 14 318.63 351.31 29.88 o 5 0 14 19.88 43.32 15.48 o 6 0 14 393.32 406.58 31.83 o 7 0 14 400.12 410.09 28.13 o 8 0 14 240.11 244.42 15.79 o 9 0 14 490.42 513.37 45.06 o 1 1 14 9.89 11.46 10.15 o 2 1 14 16.00 26.88 22.83 o 3 1 14 415.65 459.10 39.57 o 4 1 14 1.78 22.05 30.39 o 5 1 14 788.72 785.80 58.40 o 6 1 14 21.46 32.20 30.27 o 7 1 14 142.86 165.88 31.71 o 8 1 14 709.73 705.66 47.38 o 9 1 14 46.95 104.29 24.34 o 10 1 14 669.54 625.48 39.47 o 1 2 14 273.52 268.16 22.75 o 2 2 14 42.01 54.45 29.24 o 3 2 14 51.98 63.03 8.64 o 4 2 14 194.14 256.66 27.56 o 5 2 14 0.38 140.88 146.88 o 6 2 14 301.88 488.99 156.72 o 7 2 14 249.28 232.48 27.92 o 8 2 14 2.55 16.59 8.74 o 9 2 14 1586.72 1470.13 105.41 o 10 2 14 25.41 37.58 17.23 o 1 3 14 143.54 163.45 25.83 o 2 3 14 431.32 417.47 30.31 o 3 3 14 61.77 66.85 10.45 o 4 3 14 127.23 130.23 17.29 o 5 3 14 181.28 166.70 16.31 o 6 3 14 342.89 318.39 20.00 o 7 3 14 264.14 269.05 15.50 o 8 3 14 508.98 512.75 23.71 o 9 3 14 47.81 53.28 13.57 o 10 3 14 1225.14 1142.64 136.47 o 2 4 14 20.31 32.68 10.51 o 3 4 14 135.11 111.75 10.86 o 4 4 14 243.32 271.38 23.46 o 5 4 14 0.05 24.50 8.30 o 6 4 14 308.62 301.46 15.11 o 7 4 14 815.30 747.73 37.50 o 8 4 14 443.53 443.43 22.83 o 9 4 14 925.09 884.67 55.10 o 10 4 14 12.57 22.73 8.41 o 3 5 14 60.00 55.74 13.79 o 4 5 14 6.12 18.19 38.67 o 5 5 14 878.31 827.49 35.54 o 6 5 14 0.59 25.53 13.78 o 7 5 14 604.07 566.90 25.83 o 8 5 14 586.46 547.20 23.08 o 9 5 14 163.84 176.03 9.03 o 10 5 14 731.33 702.63 62.71 o 4 6 14 414.71 374.46 29.63 o 5 6 14 12.00 37.21 13.28 o 6 6 14 1237.93 1190.72 52.40 o 7 6 14 6.99 14.05 13.09 o 8 6 14 417.11 427.60 23.05 o 9 6 14 377.37 331.25 23.71 o 6 7 14 1.06 17.23 10.03 o 7 7 14 903.60 850.34 53.85 o 8 7 14 153.99 160.64 15.60 o 5 -1 15 86.50 99.35 11.64 o 6 -1 15 78.18 98.72 11.14 o 4 0 15 127.88 139.76 14.37 o 5 0 15 205.35 216.17 16.71 o 6 0 15 360.37 347.77 21.49 o 7 0 15 3.09 9.04 8.31 o 4 1 15 136.21 127.01 10.14 o 5 1 15 393.69 364.45 26.51 o 6 1 15 91.10 97.01 12.75 o 7 1 15 760.77 706.92 46.16 o 4 2 15 74.73 80.66 18.71 o 5 2 15 203.26 248.63 21.66 o 6 2 15 694.67 735.74 47.52 o 7 2 15 110.60 133.31 16.77 o 8 2 15 1015.18 1027.15 66.77 o 5 3 15 237.01 240.00 29.83 o 6 3 15 418.33 426.55 27.39 o 7 3 15 421.71 425.25 30.92 o 8 3 15 6.62 46.86 16.97 o 6 4 15 241.26 274.14 24.30 o 7 4 15 192.34 228.88 20.78 o