#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:41:46 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180800 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/31/2013182.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013182_Fobs loop_ _publ_author_name 'Glidewell, Christopher' 'Low, John N.' 'Melguizo, Manuel' 'Quesada, Antonio' _publ_section_title ; Hydrogen bonding in 2-amino-4-methoxy-6-methylpyrimidine, 2-benzylamino-4-benzyloxy-6-methylpyrimidine and 4-benzylamino-2,6-bis(benzyloxy)pyrimidine: \p-stacked chains of fused R~2~^2^(8) rings, and centrosymmetric R~2~^2^(8) dimers ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o9 _journal_page_last o13 _journal_volume 59 _journal_year 2003 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2ac 2n' _symmetry_space_group_name_H-M 'P n m a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.1442 _cell_length_b 6.5456 _cell_length_c 12.2850 _exptl_crystal_F_000 296.00 _reflns_d_resolution_high 0.7714 _cod_data_source_file na1584Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 257 - SHELXL' _shelx_refln_list_code 4 _shelx_f_calc_maximum 87.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z-1/2' 'x, -y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 265.23 234.35 7.18 o 4 0 0 46.04 43.96 2.38 o 6 0 0 1862.81 1880.12 74.32 o 8 0 0 227.12 226.24 14.77 o 10 0 0 16.78 3.04 10.96 o 2 1 0 26.00 25.90 0.77 o 4 1 0 138.71 129.49 2.87 o 6 1 0 519.02 529.89 18.27 o 8 1 0 12.54 14.73 3.43 o 10 1 0 23.50 28.58 5.75 o 2 2 0 54.87 59.14 1.37 o 4 2 0 20.85 19.03 1.26 o 6 2 0 1469.24 1592.29 47.54 o 8 2 0 183.55 171.55 9.38 o 10 2 0 13.07 1.00 8.19 o 2 3 0 56.84 56.80 1.60 o 4 3 0 93.25 95.72 4.29 o 6 3 0 303.08 320.64 8.97 o 8 3 0 6.30 6.74 4.30 o 0 4 0 7657.16 9166.61 323.34 o 2 4 0 4.36 2.98 2.91 o 4 4 0 3.11 1.82 2.19 o 6 4 0 791.29 909.97 41.87 o 8 4 0 113.74 109.49 11.85 o 2 5 0 12.60 11.24 2.35 o 4 5 0 26.89 38.07 4.32 o 6 5 0 125.46 144.50 8.12 o 8 5 0 1.33 1.46 7.19 o 0 6 0 1947.31 2382.37 139.31 o 2 6 0 1.90 3.37 2.91 o 4 6 0 0.18 7.57 4.78 o 6 6 0 336.48 361.06 17.07 o 2 7 0 1.68 2.16 5.73 o 4 7 0 6.12 7.98 9.39 o 0 8 0 543.96 553.00 26.85 o 2 8 0 0.13 -0.17 6.76 o 1 0 1 2792.30 2094.97 147.43 o 2 0 1 27.41 23.55 0.78 o 3 0 1 17.66 17.58 0.78 o 4 0 1 6.54 3.12 0.99 o 5 0 1 227.49 219.35 6.71 o 6 0 1 12.24 13.61 2.85 o 7 0 1 1430.05 1482.72 41.05 o 8 0 1 49.63 46.44 4.61 o 9 0 1 18.16 18.28 4.81 o 10 0 1 18.69 30.99 5.56 o 0 1 1 1128.96 1083.42 24.29 o 1 1 1 180.44 162.30 2.27 o 2 1 1 2077.81 1764.63 24.67 o 3 1 1 225.91 211.36 3.20 o 4 1 1 45.20 41.07 1.08 o 5 1 1 89.42 91.08 3.84 o 6 1 1 329.68 338.37 6.88 o 7 1 1 207.28 203.87 4.90 o 8 1 1 183.07 170.14 5.55 o 9 1 1 0.11 -0.09 3.01 o 10 1 1 6.26 9.84 4.25 o 1 2 1 1592.56 1498.17 39.51 o 2 2 1 31.19 27.80 0.75 o 3 2 1 0.36 0.06 0.70 o 4 2 1 10.94 13.59 1.01 o 5 2 1 163.12 161.34 4.45 o 6 2 1 10.94 14.85 1.70 o 7 2 1 1167.09 1289.83 28.90 o 8 2 1 41.00 40.86 2.91 o 9 2 1 14.48 13.02 3.32 o 10 2 1 16.05 16.20 4.72 o 0 3 1 654.70 731.91 16.07 o 1 3 1 101.27 94.90 2.05 o 2 3 1 474.35 473.92 6.71 o 3 3 1 52.70 47.78 1.95 o 4 3 1 9.25 8.28 1.00 o 5 3 1 27.77 26.71 1.57 o 6 3 1 180.31 198.01 4.58 o 7 3 1 134.57 126.71 5.44 o 8 3 1 126.62 123.06 6.39 o 9 3 1 0.06 3.50 4.55 o 1 4 1 491.91 553.34 8.75 o 2 4 1 11.37 12.46 1.14 o 3 4 1 2.06 1.76 1.20 o 4 4 1 7.18 8.34 1.26 o 5 4 1 62.14 69.73 2.56 o 6 4 1 5.84 4.23 2.30 o 7 4 1 652.08 741.12 23.26 o 8 4 1 22.78 21.78 4.17 o 9 4 1 7.06 1.04 4.77 o 0 5 1 149.83 160.81 5.20 o 1 5 1 20.20 17.94 1.47 o 2 5 1 114.83 115.32 4.11 o 3 5 1 11.66 13.19 2.11 o 4 5 1 2.92 3.32 2.79 o 5 5 1 9.90 9.83 3.37 o 6 5 1 78.52 88.26 4.60 o 7 5 1 68.90 73.83 4.87 o 8 5 1 60.05 69.64 5.75 o 1 6 1 160.37 161.34 4.55 o 2 6 1 1.61 2.82 2.30 o 3 6 1 2.01 0.96 2.88 o 4 6 1 1.71 8.36 3.29 o 5 6 1 14.68 16.86 4.00 o 6 6 1 1.59 1.68 4.59 o 7 6 1 281.01 274.64 14.50 o 0 7 1 33.96 33.78 3.81 o 1 7 1 2.41 3.82 3.04 o 2 7 1 33.35 33.46 3.75 o 3 7 1 2.48 5.73 3.39 o 4 7 1 1.23 3.55 4.25 o 5 7 1 3.04 9.68 4.96 o 1 8 1 59.56 37.53 5.35 o 2 8 1 0.26 0.89 4.39 o 3 8 1 2.10 0.57 4.33 o 0 0 2 3568.41 3380.64 70.82 o 1 0 2 549.77 467.18 8.92 o 2 0 2 2154.25 1836.16 34.97 o 3 0 2 424.35 382.30 8.50 o 4 0 2 666.29 695.31 14.13 o 5 0 2 53.10 55.78 2.33 o 6 0 2 54.45 47.16 2.74 o 7 0 2 0.09 3.73 2.58 o 8 0 2 8.24 10.45 3.43 o 9 0 2 11.84 12.88 5.13 o 10 0 2 40.66 48.48 9.44 o 1 1 2 1212.92 1157.19 14.09 o 2 1 2 83.08 65.27 1.09 o 3 1 2 3205.08 3267.45 41.98 o 4 1 2 16.17 18.64 0.92 o 5 1 2 189.75 181.07 3.42 o 6 1 2 71.04 69.21 2.40 o 7 1 2 13.70 12.23 2.14 o 8 1 2 5.10 5.80 2.45 o 9 1 2 1.01 -2.38 3.38 o 10 1 2 2.17 11.43 4.42 o 0 2 2 1850.52 2025.80 44.29 o 1 2 2 261.41 253.02 3.39 o 2 2 2 1368.33 1334.18 20.67 o 3 2 2 192.20 186.32 2.60 o 4 2 2 351.17 364.78 5.57 o 5 2 2 20.75 22.85 1.63 o 6 2 2 37.94 35.46 2.17 o 7 2 2 0.57 1.13 2.36 o 8 2 2 5.13 6.54 3.15 o 9 2 2 10.03 10.41 3.68 o 10 2 2 35.54 38.92 4.90 o 1 3 2 377.46 402.92 7.06 o 2 3 2 7.66 6.13 0.68 o 3 3 2 1201.37 1272.75 21.73 o 4 3 2 5.65 4.94 1.07 o 5 3 2 104.77 102.77 3.40 o 6 3 2 31.73 31.99 2.58 o 7 3 2 9.81 12.03 2.48 o 8 3 2 1.76 5.95 3.42 o 9 3 2 0.52 7.20 3.90 o 0 4 2 528.16 641.26 17.60 o 1 4 2 60.71 58.50 1.64 o 2 4 2 403.75 435.76 8.96 o 3 4 2 52.40 49.35 1.57 o 4 4 2 128.64 120.83 6.34 o 5 4 2 5.32 7.22 2.04 o 6 4 2 25.12 29.52 2.89 o 7 4 2 0.86 3.46 3.48 o 8 4 2 1.28 5.28 4.17 o 9 4 2 5.99 14.61 5.14 o 1 5 2 109.36 113.83 2.93 o 2 5 2 1.64 2.00 1.56 o 3 5 2 334.97 332.33 18.34 o 4 5 2 0.72 3.36 2.39 o 5 5 2 39.27 47.86 3.22 o 6 5 2 12.30 13.13 3.61 o 7 5 2 8.71 6.57 4.34 o 8 5 2 0.32 4.02 4.86 o 0 6 2 162.84 185.80 6.00 o 1 6 2 14.86 13.62 2.31 o 2 6 2 84.68 83.07 3.50 o 3 6 2 18.18 16.42 3.07 o 4 6 2 60.29 60.19 4.38 o 5 6 2 2.57 7.03 4.11 o 6 6 2 16.83 9.70 4.81 o 7 6 2 0.41 3.90 5.35 o 1 7 2 36.03 30.10 2.99 o 2 7 2 0.61 2.47 3.00 o 3 7 2 89.44 90.51 5.00 o 4 7 2 0.14 1.46 4.28 o 5 7 2 12.51 8.95 4.39 o 0 8 2 55.21 40.91 8.27 o 1 8 2 3.15 6.02 4.25 o 2 8 2 18.41 5.45 4.26 o 3 8 2 4.69 2.20 5.26 o 1 0 3 29.70 26.61 0.64 o 2 0 3 0.62 0.66 0.69 o 3 0 3 9.04 13.02 1.15 o 4 0 3 20.61 24.02 1.27 o 5 0 3 76.67 74.79 2.67 o 6 0 3 28.35 29.48 2.40 o 7 0 3 15.05 18.15 2.94 o 8 0 3 23.98 28.06 4.00 o 9 0 3 0.74 2.61 4.88 o 10 0 3 91.64 107.78 7.40 o 0 1 3 1066.54 959.44 30.92 o 1 1 3 157.03 143.77 2.19 o 2 1 3 216.37 231.98 3.41 o 3 1 3 0.03 1.47 0.57 o 4 1 3 1736.34 1797.93 23.59 o 5 1 3 9.42 8.32 1.27 o 6 1 3 14.64 14.78 1.70 o 7 1 3 36.57 32.16 2.53 o 8 1 3 1.48 2.31 2.56 o 9 1 3 10.89 14.00 3.46 o 10 1 3 203.20 221.85 15.99 o 1 2 3 21.85 20.27 0.62 o 2 2 3 3.03 2.95 0.50 o 3 2 3 1.27 1.83 0.68 o 4 2 3 9.84 9.61 1.04 o 5 2 3 54.28 54.64 2.06 o 6 2 3 17.56 17.48 1.96 o 7 2 3 11.45 10.38 2.24 o 8 2 3 17.15 16.69 2.76 o 9 2 3 0.64 -0.06 4.43 o 10 2 3 76.50 93.90 6.68 o 0 3 3 261.33 253.12 5.65 o 1 3 3 4.18 3.08 0.57 o 2 3 3 76.04 72.94 1.45 o 3 3 3 1.41 -0.08 0.89 o 4 3 3 917.40 1000.74 18.04 o 5 3 3 9.40 8.87 1.67 o 6 3 3 4.90 5.39 2.08 o 7 3 3 32.31 37.01 3.07 o 8 3 3 1.02 -0.89 3.11 o 9 3 3 8.73 2.77 4.01 o 1 4 3 6.59 7.09 1.17 o 2 4 3 2.77 4.00 1.15 o 3 4 3 0.68 0.93 1.28 o 4 4 3 4.11 2.37 1.75 o 5 4 3 25.66 27.20 3.16 o 6 4 3 6.86 7.70 2.59 o 7 4 3 6.02 5.30 3.28 o 8 4 3 8.17 4.89 4.39 o 9 4 3 0.23 1.02 4.76 o 0 5 3 48.44 49.01 3.01 o 1 5 3 2.93 2.08 1.52 o 2 5 3 24.20 23.02 2.14 o 3 5 3 0.18 -1.05 1.97 o 4 5 3 304.72 341.95 8.72 o 5 5 3 3.58 6.78 3.14 o 6 5 3 1.80 0.32 3.61 o 7 5 3 17.58 12.09 4.33 o 8 5 3 0.58 -4.45 4.45 o 1 6 3 1.33 0.43 2.06 o 2 6 3 0.20 1.96 2.65 o 3 6 3 3.15 2.28 3.13 o 4 6 3 2.62 3.93 3.09 o 5 6 3 10.63 1.31 3.77 o 6 6 3 2.23 3.54 4.28 o 7 6 3 2.74 -5.19 5.19 o 0 7 3 7.78 5.17 4.60 o 1 7 3 3.15 3.70 3.03 o 2 7 3 8.72 7.15 3.26 o 3 7 3 0.80 4.30 3.75 o 4 7 3 90.90 96.35 5.84 o 5 7 3 0.93 0.06 4.96 o 1 8 3 0.33 -2.37 4.70 o 2 8 3 0.03 -3.52 4.56 o 0 0 4 78.39 73.31 2.02 o 1 0 4 170.67 175.61 3.29 o 2 0 4 66.95 74.47 1.61 o 3 0 4 42.66 40.84 1.39 o 4 0 4 89.97 80.43 2.49 o 5 0 4 11.02 9.96 1.72 o 6 0 4 0.52 0.65 2.56 o 7 0 4 42.32 32.63 3.69 o 8 0 4 6.51 7.06 3.74 o 9 0 4 0.23 0.83 5.46 o 10 0 4 8.86 2.23 6.34 o 1 1 4 8.21 6.77 0.46 o 2 1 4 19.12 19.44 0.50 o 3 1 4 1171.15 1192.11 16.01 o 4 1 4 0.99 0.98 0.80 o 5 1 4 1.41 0.78 1.16 o 6 1 4 1.64 0.47 1.46 o 7 1 4 22.28 17.75 2.40 o 8 1 4 0.22 0.00 2.79 o 9 1 4 22.07 29.37 4.10 o 10 1 4 1.86 -4.20 4.74 o 0 2 4 44.66 44.39 1.12 o 1 2 4 15.43 17.67 0.57 o 2 2 4 27.71 27.72 0.79 o 3 2 4 47.94 47.26 1.34 o 4 2 4 62.16 61.49 1.44 o 5 2 4 8.92 8.20 1.28 o 6 2 4 0.72 -0.49 1.74 o 7 2 4 38.11 39.97 2.95 o 8 2 4 4.97 1.89 2.90 o 9 2 4 0.11 2.76 3.99 o 1 3 4 0.06 0.80 0.65 o 2 3 4 5.15 6.49 0.81 o 3 3 4 489.04 540.01 8.20 o 4 3 4 2.12 2.70 1.34 o 5 3 4 0.24 -0.07 1.42 o 6 3 4 0.31 0.97 1.86 o 7 3 4 15.42 12.43 2.81 o 8 3 4 0.06 -2.82 3.25 o 9 3 4 19.34 28.19 4.45 o 0 4 4 14.77 14.56 1.44 o 1 4 4 0.10 -0.67 1.20 o 2 4 4 3.57 3.82 1.23 o 3 4 4 21.69 22.69 1.63 o 4 4 4 17.31 17.02 1.77 o 5 4 4 3.80 1.74 2.06 o 6 4 4 0.87 -0.03 2.84 o 7 4 4 23.28 25.52 3.83 o 8 4 4 2.42 0.18 4.23 o 1 5 4 1.55 -1.12 1.52 o 2 5 4 1.37 0.75 1.78 o 3 5 4 196.17 200.29 5.41 o 4 5 4 1.51 1.52 2.69 o 5 5 4 2.40 5.57 2.94 o 6 5 4 0.02 0.31 3.78 o 7 5 4 7.89 9.58 4.11 o 8 5 4 0.00 -0.42 3.88 o 0 6 4 5.19 2.05 3.22 o 1 6 4 2.47 4.81 2.48 o 2 6 4 0.28 0.63 2.65 o 3 6 4 3.72 7.20 3.01 o 4 6 4 1.37 0.56 3.32 o 5 6 4 0.60 3.58 3.79 o 6 6 4 0.46 -0.49 4.87 o 1 7 4 2.51 3.99 2.93 o 2 7 4 0.37 3.47 3.64 o 3 7 4 75.85 69.85 5.12 o 4 7 4 0.36 -2.28 4.64 o 5 7 4 2.92 1.31 4.38 o 0 8 4 1.77 1.91 6.59 o 1 8 4 1.21 2.73 4.10 o 2 8 4 0.00 3.96 4.75 o 1 0 5 281.59 299.24 9.91 o 2 0 5 33.72 35.10 1.13 o 3 0 5 6.87 7.58 0.87 o 4 0 5 30.01 26.86 1.79 o 5 0 5 39.29 31.10 2.00 o 6 0 5 9.06 8.50 2.45 o 7 0 5 0.05 3.02 3.21 o 8 0 5 0.21 -1.28 4.29 o 9 0 5 2.33 -4.52 5.02 o 10 0 5 38.33 42.05 15.67 o 0 1 5 1410.22 1661.61 34.20 o 1 1 5 97.73 97.84 2.46 o 2 1 5 29.37 33.44 0.72 o 3 1 5 34.17 33.12 0.91 o 4 1 5 14.02 18.29 1.06 o 5 1 5 9.44 8.89 1.27 o 6 1 5 107.09 80.13 2.88 o 7 1 5 1.65 -0.23 2.77 o 8 1 5 1.78 5.57 3.02 o 9 1 5 0.23 1.30 4.07 o 1 2 5 163.06 164.22 2.30 o 2 2 5 11.90 15.23 0.73 o 3 2 5 9.11 8.63 0.74 o 4 2 5 23.47 24.97 1.24 o 5 2 5 35.97 31.69 1.69 o 6 2 5 4.53 2.22 2.42 o 7 2 5 0.35 -2.55 2.58 o 8 2 5 0.01 4.70 3.17 o 9 2 5 1.76 5.63 4.01 o 0 3 5 637.93 746.07 19.77 o 1 3 5 10.36 8.88 0.88 o 2 3 5 12.48 13.01 1.02 o 3 3 5 3.61 2.76 1.21 o 4 3 5 22.36 26.33 1.57 o 5 3 5 3.11 2.16 1.64 o 6 3 5 71.56 65.72 3.84 o 7 3 5 1.33 -0.60 2.89 o 8 3 5 2.29 2.34 3.61 o 9 3 5 0.23 2.98 4.31 o 1 4 5 32.05 30.29 1.32 o 2 4 5 4.22 3.89 1.30 o 3 4 5 4.00 0.97 1.58 o 4 4 5 16.85 16.23 2.18 o 5 4 5 19.97 19.03 2.29 o 6 4 5 1.33 1.50 2.80 o 7 4 5 1.14 3.35 3.64 o 8 4 5 0.09 -4.43 4.43 o 0 5 5 223.22 219.35 19.86 o 1 5 5 2.36 2.80 1.68 o 2 5 5 0.03 1.46 2.03 o 3 5 5 0.68 2.24 2.28 o 4 5 5 13.61 16.24 2.53 o 5 5 5 1.37 3.38 2.92 o 6 5 5 43.84 39.29 3.89 o 7 5 5 1.30 2.06 6.62 o 1 6 5 1.89 7.18 2.84 o 2 6 5 2.48 2.79 2.43 o 3 6 5 0.36 0.13 2.65 o 4 6 5 9.59 8.65 3.38 o 5 6 5 5.98 6.63 3.61 o 6 6 5 0.59 -2.69 3.88 o 0 7 5 72.10 67.51 6.16 o 1 7 5 0.71 5.83 3.65 o 2 7 5 2.10 6.59 3.78 o 3 7 5 0.35 -0.06 4.62 o 4 7 5 7.09 15.83 4.79 o 1 8 5 0.01 -3.93 4.39 o 0 0 6 528.90 687.88 14.69 o 1 0 6 33.15 37.01 3.07 o 2 0 6 114.42 113.54 2.31 o 3 0 6 64.04 69.67 1.70 o 4 0 6 17.50 18.86 1.72 o 5 0 6 36.93 36.01 2.22 o 6 0 6 0.26 0.21 2.69 o 7 0 6 86.99 78.80 4.84 o 8 0 6 2.10 1.89 4.01 o 9 0 6 0.08 -3.39 4.70 o 1 1 6 611.29 727.55 8.84 o 2 1 6 47.06 52.65 1.13 o 3 1 6 173.38 179.29 2.88 o 4 1 6 96.72 98.65 2.11 o 5 1 6 1.15 0.30 1.33 o 6 1 6 48.05 51.81 2.55 o 7 1 6 392.47 352.50 9.08 o 8 1 6 2.85 2.69 3.08 o 9 1 6 2.33 -1.02 3.87 o 0 2 6 303.68 326.19 20.29 o 1 2 6 13.61 13.41 0.93 o 2 2 6 57.63 59.16 1.19 o 3 2 6 28.30 30.81 1.07 o 4 2 6 20.11 20.89 1.31 o 5 2 6 19.40 19.62 1.58 o 6 2 6 2.09 0.72 2.20 o 7 2 6 68.84 70.83 3.38 o 8 2 6 2.04 3.19 3.32 o 9 2 6 0.08 -1.80 3.85 o 1 3 6 290.91 326.73 6.89 o 2 3 6 21.92 22.37 1.32 o 3 3 6 90.00 94.38 2.53 o 4 3 6 54.03 50.40 1.78 o 5 3 6 0.73 2.56 1.96 o 6 3 6 34.07 32.80 2.72 o 7 3 6 264.92 267.00 10.41 o 8 3 6 2.08 4.36 3.94 o 9 3 6 1.63 -2.87 6.23 o 0 4 6 113.79 128.01 4.79 o 1 4 6 0.88 0.96 1.10 o 2 4 6 16.86 20.40 1.59 o 3 4 6 6.60 7.10 1.86 o 4 4 6 10.65 10.27 2.23 o 5 4 6 6.33 9.63 2.64 o 6 4 6 4.95 4.76 3.01 o 7 4 6 38.67 37.79 4.17 o 8 4 6 2.18 -1.61 4.67 o 1 5 6 93.80 111.12 3.34 o 2 5 6 9.13 6.84 2.04 o 3 5 6 36.99 36.38 2.90 o 4 5 6 22.85 26.03 2.81 o 5 5 6 0.02 -4.07 4.07 o 6 5 6 15.46 7.21 4.02 o 7 5 6 122.76 116.05 5.80 o 0 6 6 54.42 51.40 4.21 o 1 6 6 0.00 -3.13 3.13 o 2 6 6 5.32 2.59 2.79 o 3 6 6 2.15 -4.54 4.54 o 4 6 6 2.93 5.13 3.84 o 5 6 6 2.12 9.11 4.35 o 6 6 6 4.36 8.71 6.26 o 1 7 6 29.26 27.97 4.36 o 2 7 6 2.88 1.59 4.19 o 3 7 6 11.17 5.54 5.18 o 4 7 6 7.93 1.24 5.67 o 1 0 7 650.16 596.19 45.21 o 2 0 7 5.57 6.32 0.74 o 3 0 7 121.50 108.59 3.29 o 4 0 7 27.05 30.01 1.65 o 5 0 7 8.60 12.03 2.14 o 6 0 7 97.35 92.26 3.91 o 7 0 7 265.41 238.93 8.13 o 8 0 7 41.07 44.04 5.33 o 9 0 7 1.64 2.51 6.01 o 0 1 7 2138.68 2667.33 53.80 o 1 1 7 24.87 22.31 0.85 o 2 1 7 435.04 398.22 17.30 o 3 1 7 0.08 0.20 0.99 o 4 1 7 2.69 4.61 1.05 o 5 1 7 0.06 -1.31 1.31 o 6 1 7 79.59 76.37 2.79 o 7 1 7 0.24 1.90 2.61 o 8 1 7 1.42 4.97 3.49 o 9 1 7 1.45 2.10 4.55 o 1 2 7 437.73 475.17 13.84 o 2 2 7 4.94 4.74 0.74 o 3 2 7 92.66 93.50 2.58 o 4 2 7 20.47 19.77 1.31 o 5 2 7 5.81 2.62 1.72 o 6 2 7 75.78 72.48 3.69 o 7 2 7 216.02 200.32 9.19 o 8 2 7 33.39 35.90 4.42 o 9 2 7 1.47 5.67 4.41 o 0 3 7 921.23 995.28 41.34 o 1 3 7 14.89 14.86 0.92 o 2 3 7 188.15 201.35 5.93 o 3 3 7 0.17 2.76 1.48 o 4 3 7 0.08 -1.37 1.37 o 5 3 7 0.14 -1.51 2.24 o 6 3 7 54.84 58.72 3.19 o 7 3 7 0.45 2.37 3.35 o 8 3 7 1.53 2.21 4.37 o 1 4 7 185.40 199.07 5.82 o 2 4 7 1.03 3.73 1.90 o 3 4 7 59.64 64.40 3.96 o 4 4 7 7.19 2.15 2.55 o 5 4 7 1.71 1.54 2.84 o 6 4 7 37.66 44.60 3.79 o 7 4 7 129.02 124.86 6.69 o 8 4 7 18.09 22.41 5.70 o 0 5 7 309.29 305.93 23.40 o 1 5 7 7.44 7.01 2.23 o 2 5 7 70.41 77.46 3.09 o 3 5 7 0.00 -1.97 2.64 o 4 5 7 0.09 3.63 3.56 o 5 5 7 0.10 -0.41 3.66 o 6 5 7 24.12 19.88 4.94 o 7 5 7 0.49 2.89 5.25 o 1 6 7 67.40 72.66 4.21 o 2 6 7 0.00 -0.82 3.62 o 3 6 7 34.41 26.59 3.99 o 4 6 7 1.32 0.24 3.84 o 5 6 7 0.24 -2.89 3.81 o 0 7 7 87.83 72.97 7.51 o 1 7 7 2.13 2.84 4.40 o 2 7 7 23.04 20.10 4.72 o 3 7 7 0.04 4.55 4.96 o 0 0 8 125.17 145.98 9.88 o 1 0 8 248.43 256.14 6.49 o 2 0 8 18.88 15.41 1.02 o 3 0 8 100.33 97.46 3.37 o 4 0 8 717.49 705.66 24.99 o 5 0 8 26.92 30.39 2.71 o 6 0 8 63.88 53.69 3.65 o 7 0 8 1.94 -1.85 3.66 o 8 0 8 31.22 41.95 6.56 o 9 0 8 2.21 -7.48 8.68 o 1 1 8 243.78 257.26 5.25 o 2 1 8 0.50 1.22 0.81 o 3 1 8 1.85 0.71 0.97 o 4 1 8 42.68 40.04 1.52 o 5 1 8 458.96 451.36 11.70 o 6 1 8 1.15 2.25 2.07 o 7 1 8 19.58 16.89 2.70 o 8 1 8 14.06 12.63 3.74 o 9 1 8 69.42 70.33 5.97 o 0 2 8 128.14 140.88 4.69 o 1 2 8 169.41 161.91 5.76 o 2 2 8 28.12 28.43 1.92 o 3 2 8 70.04 65.57 2.43 o 4 2 8 564.35 539.29 14.79 o 5 2 8 19.67 19.60 1.94 o 6 2 8 49.05 44.28 3.14 o 7 2 8 1.54 0.78 3.33 o 8 2 8 27.40 24.97 4.33 o 1 3 8 130.46 122.16 7.24 o 2 3 8 0.43 0.61 1.24 o 3 3 8 1.36 0.67 1.53 o 4 3 8 25.97 27.00 2.20 o 5 3 8 288.17 290.32 10.81 o 6 3 8 0.92 1.93 3.26 o 7 3 8 12.05 11.71 3.60 o 8 3 8 9.24 4.34 4.81 o 0 4 8 70.30 62.73 7.07 o 1 4 8 65.95 59.81 3.72 o 2 4 8 25.21 33.51 2.44 o 3 4 8 29.36 30.08 2.84 o 4 4 8 318.71 335.10 13.20 o 5 4 8 8.99 9.15 3.57 o 6 4 8 25.65 22.89 3.61 o 7 4 8 0.84 -1.44 4.48 o 1 5 8 50.31 64.21 3.62 o 2 5 8 0.01 1.76 4.18 o 3 5 8 0.66 4.63 3.45 o 4 5 8 14.96 13.32 4.06 o 5 5 8 125.37 118.83 8.78 o 6 5 8 0.58 -4.33 4.33 o 0 6 8 25.88 26.91 6.01 o 1 6 8 20.01 16.43 3.71 o 2 6 8 13.54 14.03 3.75 o 3 6 8 9.33 8.45 4.65 o 4 6 8 152.90 138.30 6.92 o 5 6 8 2.90 -3.88 6.42 o 1 7 8 16.15 6.97 4.33 o 2 7 8 0.03 -1.79 4.68 o 1 0 9 1.41 1.48 1.02 o 2 0 9 2.19 2.20 1.29 o 3 0 9 2606.92 2695.60 107.11 o 4 0 9 9.23 8.54 2.10 o 5 0 9 36.32 32.33 3.05 o 6 0 9 31.48 30.42 4.00 o 7 0 9 14.35 13.99 5.30 o 8 0 9 37.03 33.45 11.63 o 0 1 9 24.28 30.71 1.83 o 1 1 9 53.31 62.72 1.62 o 2 1 9 62.41 62.85 2.19 o 3 1 9 134.13 119.31 4.81 o 4 1 9 73.15 69.06 2.22 o 5 1 9 9.24 8.31 1.95 o 6 1 9 12.73 13.54 2.77 o 7 1 9 0.83 1.86 3.33 o 8 1 9 25.21 19.87 4.28 o 1 2 9 0.91 0.92 1.39 o 2 2 9 1.10 0.60 1.22 o 3 2 9 2044.50 2252.84 42.82 o 4 2 9 5.71 4.27 1.82 o 5 2 9 30.83 29.30 2.80 o 6 2 9 24.13 23.41 3.16 o 7 2 9 11.51 6.84 3.77 o 8 2 9 30.21 21.56 4.97 o 0 3 9 15.99 14.71 2.40 o 1 3 9 22.70 17.63 1.35 o 2 3 9 42.05 45.24 2.26 o 3 3 9 75.96 71.62 3.76 o 4 3 9 53.26 54.92 2.95 o 5 3 9 3.69 5.02 2.96 o 6 3 9 10.12 12.81 3.42 o 7 3 9 0.31 0.83 4.44 o 1 4 9 0.67 0.34 2.23 o 2 4 9 0.29 0.19 2.20 o 3 4 9 1113.51 1269.07 56.61 o 4 4 9 1.81 8.06 3.65 o 5 4 9 21.39 23.47 3.72 o 6 4 9 11.96 14.20 4.25 o 7 4 9 4.72 4.96 5.76 o 0 5 9 2.74 0.52 4.34 o 1 5 9 6.08 9.49 3.00 o 2 5 9 13.98 16.73 3.16 o 3 5 9 34.84 28.32 3.75 o 4 5 9 25.64 24.82 3.99 o 5 5 9 1.33 -1.88 4.84 o 6 5 9 5.47 4.66 5.36 o 1 6 9 0.40 3.22 3.90 o 2 6 9 0.06 -0.96 4.56 o 3 6 9 478.83 452.28 19.45 o 4 6 9 0.35 0.81 5.63 o 0 7 9 0.04 0.48 6.80 o 1 0 10 3.93 3.56 6.69 o 2 0 10 0.57 -0.29 0.89 o 3 0 10 10.26 8.00 1.97 o 4 0 10 644.90 633.12 36.26 o 5 0 10 1.29 2.02 2.93 o 6 0 10 0.68 -2.20 4.04 o 7 0 10 3.09 4.76 5.67 o 8 0 10 26.28 18.22 8.27 o 1 1 10 0.07 1.08 1.53 o 2 1 10 21.22 24.13 1.72 o 3 1 10 620.58 610.31 19.34 o 4 1 10 0.17 2.79 1.86 o 5 1 10 39.35 41.72 2.89 o 6 1 10 19.48 18.22 3.20 o 7 1 10 1.65 3.84 3.94 o 8 1 10 27.42 27.69 5.37 o 0 2 10 51.33 39.58 6.22 o 1 2 10 4.56 2.51 1.81 o 2 2 10 0.25 0.00 1.88 o 3 2 10 10.45 11.33 1.67 o 4 2 10 544.55 547.11 17.35 o 5 2 10 0.62 3.67 3.14 o 6 2 10 0.31 3.86 3.23 o 7 2 10 2.46 3.67 4.17 o 1 3 10 0.00 -2.67 2.67 o 2 3 10 12.59 5.34 3.67 o 3 3 10 398.03 377.20 21.75 o 4 3 10 0.00 0.62 2.59 o 5 3 10 29.07 29.91 3.94 o 6 3 10 11.31 13.72 4.43 o 7 3 10 2.21 6.18 4.46 o 0 4 10 25.19 20.85 4.65 o 1 4 10 3.02 5.68 2.75 o 2 4 10 0.17 0.17 2.82 o 3 4 10 6.05 3.18 3.85 o 4 4 10 323.99 292.52 24.87 o 5 4 10 0.32 -4.22 4.22 o 6 4 10 0.07 -1.68 4.84 o 1 5 10 0.06 2.36 3.56 o 2 5 10 4.49 11.60 4.46 o 3 5 10 186.52 162.78 18.39 o 4 5 10 0.17 3.44 5.08 o 5 5 10 15.03 6.70 6.26 o 0 6 10 6.66 4.48 9.85 o 1 6 10 0.91 7.30 7.80 o 2 6 10 1.52 -5.41 6.48 o 3 6 10 1.87 -10.69 10.69 o 1 0 11 111.89 111.54 15.32 o 2 0 11 0.54 2.04 5.24 o 3 0 11 120.34 116.66 5.82 o 4 0 11 12.45 13.99 4.24 o 5 0 11 94.49 102.72 9.31 o 6 0 11 12.44 17.27 4.99 o 7 0 11 2.95 8.93 9.62 o 0 1 11 311.49 323.84 18.25 o 1 1 11 3.03 3.78 2.64 o 2 1 11 61.32 56.62 4.53 o 3 1 11 33.42 35.37 3.76 o 4 1 11 132.40 131.14 6.57 o 5 1 11 17.12 15.78 2.93 o 6 1 11 46.11 63.90 6.86 o 7 1 11 2.25 5.24 3.91 o 1 2 11 88.36 90.99 5.32 o 2 2 11 0.66 1.91 3.15 o 3 2 11 98.56 106.41 5.24 o 4 2 11 10.53 12.64 3.32 o 5 2 11 71.53 74.88 5.55 o 6 2 11 10.03 13.58 3.41 o 7 2 11 2.84 1.99 4.28 o 0 3 11 207.11 227.96 14.86 o 1 3 11 2.86 0.82 3.63 o 2 3 11 45.69 45.02 7.29 o 3 3 11 24.83 27.89 5.93 o 4 3 11 91.92 91.47 6.94 o 5 3 11 11.80 18.20 4.46 o 6 3 11 32.64 30.42 6.96 o 1 4 11 48.73 56.33 5.78 o 2 4 11 0.39 -1.11 4.92 o 3 4 11 61.26 63.87 6.08 o 4 4 11 6.23 2.26 5.65 o 5 4 11 33.69 34.60 7.18 o 0 5 11 103.99 122.23 18.82 o 1 5 11 0.63 2.35 5.87 o 2 5 11 25.54 23.30 5.89 o 3 5 11 11.15 2.34 8.15 o 4 5 11 52.08 47.21 6.99 o 1 6 11 20.54 13.64 7.17 o 1 0 12 0.06 -9.05 9.05 o 2 0 12 29.56 17.87 8.85 o 3 0 12 0.12 -1.10 5.62 o 4 0 12 2.28 9.30 5.19 o 5 0 12 0.25 3.22 8.86 o 6 0 12 6.36 5.40 6.11 o 1 1 12 168.64 170.45 18.14 o 2 1 12 0.08 0.44 3.33 o 3 1 12 1.28 4.10 2.46 o 4 1 12 2.91 8.50 4.17 o 5 1 12 4.71 7.92 3.57 o 6 1 12 0.00 -4.00 4.24 o 0 2 12 44.96 47.47 5.64 o 1 2 12 0.39 2.33 3.69 o 2 2 12 23.46 23.39 3.80 o 3 2 12 0.20 0.32 3.49 o 4 2 12 1.82 -2.11 4.51 o 5 2 12 0.17 1.33 4.49 o 6 2 12 4.68 3.20 5.48 o 1 3 12 116.87 108.30 14.27 o 2 3 12 0.10 0.45 4.54 o 3 3 12 0.21 2.58 4.71 o 4 3 12 2.22 -0.97 4.80 o 5 3 12 3.12 -1.09 4.99 o 0 4 12 18.12 17.62 9.04 o 1 4 12 0.36 -1.19 6.64 o 2 4 12 12.38 12.15 5.74 o 3 4 12 0.15 -1.96 5.62 o 4 4 12 0.84 -5.05 6.17 o 1 5 12 57.89 55.69 6.47 o 2 5 12 0.10 -1.94 8.21 o 3 5 12 0.01 1.07 9.12 o 2 0 13 3.59 10.00 7.03 o 3 0 13 12.76 7.16 6.93 o 4 0 13 8.90 4.81 7.24 o 5 0 13 0.77 -4.43 13.31 o 1 1 13 0.86 -7.07 7.07 o 2 1 13 7.77 2.28 11.35 o 3 1 13 1.42 -1.59 4.63 o 4 1 13 1.53 -3.88 8.60 o 5 1 13 3.86 4.33 9.79 o 1 2 13 11.59 5.95 4.95 o 2 2 13 2.55 1.76 5.09 o 3 2 13 10.18 5.76 5.08 o 4 2 13 7.31 3.64 5.28 o 5 2 13 0.61 4.31 7.18 o 0 3 13 94.75 83.99 13.87 o 1 3 13 1.19 -0.42 4.32 o 2 3 13 6.25 2.14 6.04 o 3 3 13 0.71 -2.17 4.79 o 4 3 13 1.68 -0.96 6.06 o 1 4 13 5.19 4.74 5.30 o 2 4 13 1.27 -1.32 5.88 o 3 4 13 5.01 -4.47 6.24 o 2 0 14 22.92 20.12 7.08 o 3 0 14 0.49 8.97 10.02 o 4 0 14 0.98 -9.03 9.03 o 2 1 14 0.03 10.05 13.41 o 3 1 14 32.45 40.43 8.32 o 4 1 14 0.08 -4.50 7.02 o 1 2 14 11.92 2.26 13.52 o 2 2 14 16.74 7.82 9.47 o 3 2 14 0.50 4.02 7.44 o 4 2 14 0.76 0.80 6.35 o 1 3 14 4.94 5.06 8.56 o 2 3 14 0.07 4.05 11.06 o 3 3 14 24.43 26.58 16.82 o 0 4 14 11.79 8.36 8.36 o 3 0 15 37.82 59.43 11.46 o 2 1 15 22.01 45.01 17.79 o 3 1 15 15.25 16.40 8.67 o 1 2 15 14.19 11.33 13.59 o 2 2 15 1.10 0.45 7.52 o