#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013196.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013196_Fobs loop_ _publ_author_name 'Bowes, Katharine F.' 'Glidewell, Christopher' 'Low, John N.' 'Melguizo, Manuel' 'Quesada, Antonio' _publ_section_title ; Two polymorphs, with Z' = 1 and 2, of 2-amino-4-chloro-6-morpholinopyrimidine in P2~1~/c, and 2-amino-4-chloro-6-piperidinopyrimidine, which is isomorphous and almost isostructural with the Z' = 2 polymorph ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o4 _journal_page_last o8 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 121.613 _cell_angle_gamma 90.000 _cell_length_a 13.9215 _cell_length_b 8.1803 _cell_length_c 19.6390 _exptl_crystal_F_000 896.00 _reflns_d_resolution_high 0.7709 _[local]_cod_data_source_file sk1595Ibsup3.hkl _[local]_cod_data_source_block Ib #BEGIN Tags that were not found in dictionaries: _shelx_title ' 312 - SHELXL' _shelx_refln_list_code 4 _shelx_f_calc_maximum 222.55 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1371.78 1293.40 214.53 o 3 0 0 12266.82 11598.29 283.54 o 4 0 0 2845.33 2705.02 64.01 o 5 0 0 30778.42 32998.69 714.01 o 6 0 0 457.99 460.95 13.81 o 7 0 0 6146.99 6745.31 208.66 o 8 0 0 1678.86 1730.71 57.80 o 9 0 0 287.14 255.10 15.47 o 10 0 0 188.55 202.07 18.56 o 11 0 0 911.78 924.08 56.88 o 12 0 0 2096.09 2147.17 153.47 o 13 0 0 1414.96 1504.70 116.94 o 14 0 0 31.87 73.06 14.63 o 15 0 0 432.79 387.21 43.88 o 1 1 0 852.57 770.49 35.97 o 2 1 0 10786.75 10031.60 202.31 o 3 1 0 22.32 21.84 7.28 o 4 1 0 2234.33 2178.42 49.25 o 5 1 0 510.36 552.88 11.39 o 6 1 0 145.43 165.42 3.43 o 7 1 0 133.34 142.15 8.83 o 8 1 0 913.67 875.01 19.20 o 9 1 0 615.46 649.62 17.25 o 10 1 0 12.66 5.82 3.26 o 11 1 0 1136.89 1227.70 39.87 o 12 1 0 1400.63 1372.85 62.03 o 13 1 0 1584.13 1627.38 80.01 o 14 1 0 488.77 482.80 34.13 o 15 1 0 263.53 241.26 25.83 o 0 2 0 3296.90 3278.83 127.63 o 1 2 0 6755.35 6243.92 196.40 o 2 2 0 1291.25 1198.81 25.91 o 3 2 0 1040.82 964.95 20.11 o 4 2 0 120.39 177.30 4.39 o 5 2 0 639.47 543.24 9.78 o 6 2 0 2.33 1.82 3.64 o 7 2 0 95.88 99.07 3.53 o 8 2 0 2.88 0.00 2.97 o 9 2 0 88.96 54.93 3.90 o 10 2 0 1352.54 1397.68 37.99 o 11 2 0 3.14 10.42 8.40 o 12 2 0 230.58 178.16 10.92 o 13 2 0 135.30 121.91 12.63 o 14 2 0 9.11 7.31 12.15 o 15 2 0 165.92 111.52 22.85 o 1 3 0 236.18 233.29 6.44 o 2 3 0 31.26 18.05 5.12 o 3 3 0 131.95 163.88 4.63 o 4 3 0 37.26 48.19 3.86 o 5 3 0 263.56 275.54 10.39 o 6 3 0 121.44 130.52 4.96 o 7 3 0 0.05 1.44 3.26 o 8 3 0 23.62 32.70 3.77 o 9 3 0 270.24 244.77 10.52 o 10 3 0 0.14 -3.25 3.25 o 11 3 0 47.63 43.40 7.46 o 12 3 0 55.94 42.25 9.18 o 13 3 0 114.75 119.70 12.61 o 14 3 0 86.75 82.50 17.54 o 0 4 0 1045.76 902.14 39.33 o 1 4 0 624.84 568.66 15.35 o 2 4 0 0.76 -1.80 3.61 o 3 4 0 276.89 251.24 5.94 o 4 4 0 1596.17 1523.65 29.68 o 5 4 0 620.09 622.18 16.26 o 6 4 0 31.18 35.63 5.01 o 7 4 0 157.77 163.82 10.16 o 8 4 0 13.91 13.11 3.26 o 9 4 0 403.40 386.91 14.27 o 10 4 0 86.25 72.93 5.48 o 11 4 0 68.71 59.89 5.12 o 12 4 0 451.31 465.09 24.39 o 13 4 0 69.94 109.76 15.44 o 14 4 0 74.64 80.96 33.38 o 1 5 0 1258.60 1203.16 34.27 o 2 5 0 1980.85 2124.23 60.69 o 3 5 0 705.22 712.94 24.63 o 4 5 0 1711.63 1661.50 43.11 o 5 5 0 550.78 528.95 14.42 o 6 5 0 274.05 256.92 6.90 o 7 5 0 1458.69 1586.62 39.66 o 8 5 0 3840.54 4241.35 104.53 o 9 5 0 154.74 169.15 7.96 o 10 5 0 504.23 477.02 16.78 o 11 5 0 7.55 3.62 5.91 o 12 5 0 396.79 342.58 35.12 o 13 5 0 1772.03 1874.15 188.21 o 0 6 0 3257.12 3289.28 133.97 o 1 6 0 2.49 3.62 3.62 o 2 6 0 71.42 78.81 3.25 o 3 6 0 18.76 25.50 3.26 o 4 6 0 312.36 327.11 12.98 o 5 6 0 1441.74 1445.72 37.86 o 6 6 0 12.04 10.22 3.26 o 7 6 0 1303.51 1390.90 40.70 o 8 6 0 47.15 50.09 3.88 o 9 6 0 481.31 488.40 16.24 o 10 6 0 130.12 152.69 15.73 o 11 6 0 155.16 133.81 12.40 o 12 6 0 755.84 707.35 55.51 o 1 7 0 9.31 9.68 2.96 o 2 7 0 0.04 0.00 3.25 o 3 7 0 230.08 235.41 7.99 o 4 7 0 36.05 41.45 3.95 o 5 7 0 203.50 206.74 13.83 o 6 7 0 227.83 225.11 9.57 o 7 7 0 111.15 93.20 7.18 o 8 7 0 190.95 156.97 9.49 o 9 7 0 65.70 79.95 10.42 o 10 7 0 91.53 90.88 13.88 o 11 7 0 0.78 0.00 12.07 o 0 8 0 186.08 174.75 15.31 o 1 8 0 762.43 790.63 21.45 o 2 8 0 306.99 304.89 9.24 o 3 8 0 56.86 61.33 3.91 o 4 8 0 742.97 764.44 24.13 o 5 8 0 47.67 49.92 7.29 o 6 8 0 210.76 196.11 12.63 o 7 8 0 5.06 3.64 5.94 o 8 8 0 19.69 15.89 15.71 o 9 8 0 233.63 209.07 36.76 o 10 8 0 304.22 267.61 33.28 o 1 9 0 106.04 121.62 8.40 o 2 9 0 228.38 210.35 10.89 o 3 9 0 14.51 7.27 4.02 o 4 9 0 106.85 108.84 10.27 o 5 9 0 129.44 120.98 12.08 o 6 9 0 83.09 71.12 7.35 o 7 9 0 78.32 73.71 12.01 o 8 9 0 768.36 811.59 53.46 o 0 10 0 57.63 43.62 14.56 o 1 10 0 0.29 7.28 7.28 o 2 10 0 0.02 0.00 5.12 o 3 10 0 24.88 39.83 10.25 o 4 10 0 569.82 599.17 40.04 o 5 10 0 192.43 194.68 21.65 o -15 1 1 385.33 460.19 33.30 o -14 1 1 232.71 239.64 40.79 o -13 1 1 13.99 18.27 11.02 o -12 1 1 761.61 748.79 38.51 o -11 1 1 280.26 255.38 12.38 o -10 1 1 1876.39 1906.26 56.91 o -9 1 1 13.06 11.62 3.26 o -8 1 1 119.58 99.98 4.14 o -7 1 1 27.00 55.43 2.96 o -6 1 1 1591.45 1711.34 32.40 o -5 1 1 912.08 993.18 19.28 o -4 1 1 335.32 350.00 7.86 o -3 1 1 1147.23 1181.17 26.25 o -2 1 1 1361.02 1305.79 68.92 o 1 1 1 753.13 771.43 21.18 o 2 1 1 3702.92 3610.72 68.96 o 3 1 1 5725.33 5452.40 110.23 o 4 1 1 216.06 266.31 6.51 o 5 1 1 2703.27 2801.68 72.84 o 6 1 1 18.33 10.14 3.24 o 7 1 1 1074.48 1069.13 22.48 o 8 1 1 28.41 33.68 3.38 o 9 1 1 119.01 101.93 5.78 o 10 1 1 71.49 52.71 4.39 o 11 1 1 384.94 367.34 27.69 o 12 1 1 516.17 460.52 25.83 o 13 1 1 460.92 387.58 25.83 o 14 1 1 950.56 975.32 62.03 o -15 2 1 1731.07 2076.77 113.72 o -14 2 1 746.92 766.57 86.38 o -13 2 1 11.04 3.66 10.99 o -12 2 1 218.57 188.31 9.34 o -11 2 1 1973.72 2098.62 58.91 o -10 2 1 3885.65 4193.29 112.05 o -9 2 1 38.96 39.25 4.80 o -8 2 1 1374.81 1414.60 30.56 o -7 2 1 182.11 152.15 5.98 o -6 2 1 5309.31 5501.07 136.20 o -5 2 1 2105.52 2135.33 49.44 o -4 2 1 2518.92 2545.97 49.95 o -3 2 1 8139.75 7305.02 201.13 o -2 2 1 40.42 35.94 5.08 o -1 2 1 21.85 45.72 4.14 o 0 2 1 2118.11 2066.97 48.64 o 2 2 1 1058.24 985.34 18.67 o 3 2 1 38.02 38.59 4.83 o 4 2 1 1436.11 1621.05 34.43 o 5 2 1 697.81 687.86 14.09 o 6 2 1 3790.52 3700.67 81.56 o 7 2 1 13.13 11.64 3.26 o 8 2 1 22.02 28.07 3.63 o 9 2 1 1.60 6.63 3.18 o 10 2 1 390.27 358.08 12.44 o 11 2 1 134.71 144.46 9.53 o 12 2 1 147.46 127.65 9.56 o 13 2 1 607.34 551.98 44.13 o 14 2 1 6.14 20.48 12.18 o -15 3 1 191.40 172.14 20.64 o -14 3 1 457.78 472.67 54.28 o -13 3 1 91.65 92.68 10.62 o -12 3 1 1981.61 2107.09 76.81 o -11 3 1 561.13 550.87 14.82 o -10 3 1 522.86 525.10 13.74 o -9 3 1 24.33 38.20 3.95 o -8 3 1 898.30 926.60 28.24 o -7 3 1 2069.69 2079.98 50.54 o -6 3 1 73.04 78.18 4.20 o -5 3 1 119.29 130.27 3.54 o -4 3 1 459.89 450.46 10.30 o -3 3 1 7063.26 6877.36 121.52 o -2 3 1 425.21 370.14 7.92 o 0 3 1 1809.32 1824.56 45.31 o 1 3 1 2678.99 2969.11 57.28 o 2 3 1 4964.90 4641.32 136.18 o 3 3 1 355.46 409.09 8.11 o 4 3 1 1.95 3.64 3.64 o 5 3 1 3029.71 3021.30 84.60 o 6 3 1 821.51 807.81 19.13 o 7 3 1 383.81 349.14 8.75 o 8 3 1 1639.19 1693.03 36.83 o 9 3 1 2004.97 2017.36 50.16 o 10 3 1 1912.82 1958.97 51.68 o 11 3 1 200.85 190.36 11.57 o 12 3 1 4.69 3.64 7.38 o 13 3 1 19.81 18.22 10.32 o 14 3 1 774.48 718.73 52.69 o -14 4 1 142.79 151.62 19.44 o -13 4 1 8.78 0.00 10.29 o -12 4 1 22.83 24.35 4.24 o -11 4 1 3.66 -2.51 3.70 o -10 4 1 494.55 532.47 16.52 o -9 4 1 136.56 132.95 6.51 o -8 4 1 2487.52 2702.05 61.38 o -7 4 1 678.15 710.25 14.73 o -6 4 1 1456.25 1474.32 31.41 o -5 4 1 334.53 314.96 6.90 o -4 4 1 21.78 36.88 2.97 o -3 4 1 2514.06 2575.62 50.58 o -2 4 1 550.14 513.35 13.35 o -1 4 1 401.40 419.72 11.58 o 0 4 1 429.29 473.80 12.13 o 1 4 1 2033.56 1957.85 51.76 o 2 4 1 667.13 792.82 15.13 o 3 4 1 114.32 144.06 3.17 o 4 4 1 638.02 701.22 14.45 o 5 4 1 10.49 13.08 3.25 o 6 4 1 853.26 877.65 20.08 o 7 4 1 1.93 -1.44 3.50 o 8 4 1 385.38 384.27 12.11 o 9 4 1 31.58 23.78 3.82 o 10 4 1 3.46 1.61 5.41 o 11 4 1 256.68 260.15 14.55 o 12 4 1 43.01 75.06 12.07 o 13 4 1 275.39 291.40 22.83 o -13 5 1 262.01 229.94 22.73 o -12 5 1 46.23 51.45 8.37 o -11 5 1 126.02 129.78 12.76 o -10 5 1 71.12 76.33 6.51 o -9 5 1 33.56 30.89 4.14 o -8 5 1 138.73 142.59 6.51 o -7 5 1 1951.71 1935.82 44.24 o -6 5 1 1790.26 1819.86 45.78 o -5 5 1 299.80 301.98 8.77 o -4 5 1 14.85 17.52 3.26 o -3 5 1 128.99 127.48 5.62 o -2 5 1 713.62 787.86 24.92 o -1 5 1 145.32 128.65 4.50 o 0 5 1 0.03 7.22 7.22 o 1 5 1 74.09 71.28 3.23 o 2 5 1 139.07 184.58 6.50 o 3 5 1 119.91 118.18 3.90 o 4 5 1 3.34 2.42 2.98 o 5 5 1 30.80 35.36 3.52 o 6 5 1 433.35 422.44 10.76 o 7 5 1 62.57 57.08 3.52 o 8 5 1 677.62 714.40 20.66 o 9 5 1 0.01 3.64 6.16 o 10 5 1 147.23 145.21 13.97 o 11 5 1 77.15 65.14 8.97 o 12 5 1 176.48 187.71 17.51 o 13 5 1 384.43 475.47 33.22 o -13 6 1 99.43 93.54 28.80 o -12 6 1 86.15 94.49 17.43 o -11 6 1 378.65 378.10 22.73 o -10 6 1 94.22 74.20 9.52 o -9 6 1 516.14 457.96 17.34 o -8 6 1 69.70 64.73 4.18 o -7 6 1 167.61 175.57 9.57 o -6 6 1 137.69 128.63 4.39 o -5 6 1 130.97 127.74 5.28 o -4 6 1 18.95 19.40 4.19 o -3 6 1 174.09 162.58 5.16 o -2 6 1 1671.62 1726.08 46.41 o -1 6 1 922.99 1042.45 34.41 o 0 6 1 235.56 259.09 7.45 o 1 6 1 115.49 106.24 3.95 o 2 6 1 24.53 19.55 3.26 o 3 6 1 97.97 83.57 3.85 o 4 6 1 35.84 37.78 3.55 o 5 6 1 1336.54 1432.52 41.96 o 6 6 1 203.43 172.01 7.41 o 7 6 1 991.12 987.00 26.74 o 8 6 1 137.69 126.39 7.39 o 9 6 1 6.23 3.63 4.60 o 10 6 1 453.53 436.15 25.71 o 11 6 1 196.53 194.76 17.50 o 12 6 1 372.37 410.95 29.64 o -11 7 1 108.45 124.91 25.97 o -10 7 1 312.93 333.72 24.20 o -9 7 1 9.97 2.42 7.33 o -8 7 1 73.56 60.37 5.22 o -7 7 1 2199.81 2259.60 76.37 o -6 7 1 1499.09 1568.11 49.49 o -5 7 1 810.90 803.77 22.68 o -4 7 1 19.10 21.96 4.06 o -3 7 1 487.14 500.68 15.46 o -2 7 1 1651.25 1625.18 43.98 o -1 7 1 1576.47 1631.48 45.78 o 0 7 1 856.85 881.11 25.92 o 1 7 1 936.82 914.71 22.37 o 2 7 1 1185.01 1142.62 35.30 o 3 7 1 581.74 572.50 16.73 o 4 7 1 2.21 3.25 3.54 o 5 7 1 123.09 113.99 5.18 o 6 7 1 72.11 72.88 5.15 o 7 7 1 1273.01 1370.73 44.45 o 8 7 1 280.16 256.44 16.82 o 9 7 1 1152.82 1188.46 151.60 o 10 7 1 403.03 429.56 50.21 o 11 7 1 247.72 203.22 17.42 o -10 8 1 5.77 20.26 12.04 o -9 8 1 345.47 324.77 22.64 o -8 8 1 1.16 -2.42 7.25 o -7 8 1 363.10 359.24 21.02 o -6 8 1 1460.46 1476.88 65.26 o -5 8 1 39.50 43.73 5.03 o -4 8 1 974.74 1009.66 32.29 o -3 8 1 285.08 311.29 10.24 o -2 8 1 849.12 866.42 23.67 o -1 8 1 106.96 97.24 4.18 o 0 8 1 2.18 -1.21 2.95 o 1 8 1 1122.98 1156.71 30.96 o 2 8 1 2.49 7.29 3.26 o 3 8 1 682.56 749.73 24.10 o 4 8 1 13.83 13.35 5.24 o 5 8 1 1335.03 1316.96 49.09 o 6 8 1 1395.93 1440.70 67.08 o 7 8 1 7.19 5.45 10.70 o 8 8 1 105.72 102.00 12.08 o 9 8 1 2.14 2.42 7.25 o -8 9 1 33.27 30.26 6.85 o -7 9 1 110.14 128.55 12.91 o -6 9 1 2.23 7.24 10.86 o -5 9 1 202.52 211.17 22.30 o -4 9 1 38.82 48.31 7.44 o -3 9 1 47.99 43.35 9.40 o -2 9 1 4.47 3.63 4.60 o -1 9 1 168.49 205.00 10.81 o 0 9 1 519.14 536.54 20.69 o 1 9 1 35.43 36.34 3.62 o 2 9 1 0.59 1.82 7.26 o 3 9 1 92.40 107.98 13.65 o 4 9 1 128.16 119.65 13.75 o 5 9 1 29.07 16.34 6.90 o 6 9 1 61.68 73.15 10.25 o 7 9 1 147.17 149.97 17.35 o -5 10 1 9.05 4.81 7.22 o -4 10 1 633.05 656.99 48.35 o -3 10 1 111.76 101.76 10.23 o -2 10 1 12.83 7.25 7.22 o -1 10 1 34.36 31.03 6.51 o 0 10 1 10.78 18.14 5.15 o 1 10 1 146.91 174.75 15.42 o 2 10 1 35.21 36.32 10.27 o 3 10 1 3.21 0.00 5.12 o 4 10 1 4.37 -7.28 14.50 o -16 0 2 0.15 7.28 14.63 o -15 0 2 146.62 109.59 21.91 o -14 0 2 1490.92 1731.36 117.00 o -13 0 2 2674.34 2842.29 190.19 o -12 0 2 156.54 143.63 25.81 o -11 0 2 401.85 408.86 18.81 o -10 0 2 4684.90 5099.80 207.12 o -9 0 2 5144.45 5359.74 200.07 o -8 0 2 7.06 3.64 5.15 o -7 0 2 4888.13 5295.53 176.86 o -6 0 2 1919.52 2097.11 56.04 o -5 0 2 529.35 507.60 14.26 o -4 0 2 1151.12 1059.69 29.47 o -3 0 2 1207.57 1181.65 32.03 o 1 0 2 221.46 207.48 5.15 o 2 0 2 4713.43 4676.64 149.08 o 3 0 2 2319.62 2313.03 64.11 o 4 0 2 13286.11 13810.52 325.63 o 5 0 2 1489.37 1845.00 48.27 o 6 0 2 3143.31 3300.90 87.50 o 7 0 2 2074.35 2099.83 60.34 o 8 0 2 343.51 291.22 15.42 o 9 0 2 947.75 1001.19 41.23 o 10 0 2 1.62 0.00 7.28 o 11 0 2 922.15 1058.47 65.78 o 12 0 2 139.79 146.06 21.91 o 13 0 2 5.34 7.28 14.63 o 14 0 2 12.26 29.25 14.63 o -16 1 2 1.30 4.38 14.63 o -15 1 2 28.09 36.45 32.99 o -14 1 2 192.00 225.49 40.76 o -13 1 2 646.58 664.81 31.02 o -12 1 2 3.98 1.83 5.95 o -11 1 2 990.82 995.00 31.53 o -10 1 2 1142.62 1167.78 32.81 o -9 1 2 1150.46 1100.44 24.70 o -8 1 2 1121.75 1231.02 26.32 o -7 1 2 623.99 721.54 13.93 o -6 1 2 783.45 768.77 13.68 o -5 1 2 870.03 974.79 19.21 o -4 1 2 4295.93 4087.91 94.64 o -3 1 2 39.58 39.69 4.23 o -2 1 2 514.11 513.14 21.98 o -1 1 2 439.80 382.86 12.52 o 0 1 2 2540.67 2286.17 47.00 o 1 1 2 9964.38 9234.16 161.57 o 2 1 2 326.69 288.97 5.96 o 3 1 2 1536.56 1374.49 25.08 o 4 1 2 1281.37 1266.12 37.45 o 5 1 2 2855.13 3138.40 65.43 o 6 1 2 1996.94 2150.54 46.30 o 7 1 2 228.13 181.76 10.20 o 8 1 2 109.46 106.98 4.55 o 9 1 2 172.75 175.61 6.51 o 10 1 2 51.03 31.04 4.39 o 11 1 2 726.78 806.25 33.30 o 12 1 2 1445.90 1618.70 123.92 o 13 1 2 259.16 284.18 22.85 o 14 1 2 0.69 21.91 20.68 o -15 2 2 29.47 36.50 15.47 o -14 2 2 385.34 399.16 45.63 o -13 2 2 13.59 10.97 10.34 o -12 2 2 8.85 4.84 14.71 o -11 2 2 58.71 45.70 3.91 o -10 2 2 946.62 940.15 24.01 o -9 2 2 902.42 919.80 20.63 o -8 2 2 563.98 598.43 13.64 o -7 2 2 371.17 337.23 8.75 o -6 2 2 2182.92 2420.97 55.19 o -5 2 2 34.77 43.51 4.20 o -2 2 2 3291.50 2876.84 77.18 o -1 2 2 2199.40 2105.96 75.52 o 0 2 2 3400.56 3178.70 64.74 o 2 2 2 419.50 414.92 8.91 o 3 2 2 176.97 154.16 9.35 o 4 2 2 62.57 73.70 3.26 o 5 2 2 31.97 27.87 4.72 o 6 2 2 592.45 613.04 12.47 o 7 2 2 67.38 60.12 3.26 o 8 2 2 438.31 439.64 13.01 o 9 2 2 1143.62 1196.38 27.73 o 10 2 2 973.36 959.42 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