#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/32/2013209.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013209_Fobs loop_ _publ_author_name 'Glidewell, Christopher' 'Low, John N.' 'Skakle, Janet M. S.' 'Wardell, James L.' _publ_section_title ; A chain of edge-fused rings generated by the combination of an N---H···O hydrogen bond and an iodo--nitro interaction in 2-iodobenzaldehyde 4-nitrophenylhydrazone versus disordered and effectively isolated molecules in 2-iodobenzaldehyde 2,4-dinitrophenylhydrazone ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o98 _journal_page_last o101 _journal_volume 59 _journal_year 2003 _space_group_IT_number 29 _symmetry_space_group_name_Hall 'P 2c -2ac' _symmetry_space_group_name_H-M 'P c a 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 24.0858 _cell_length_b 5.0699 _cell_length_c 10.5080 _exptl_crystal_F_000 712.00 _reflns_d_resolution_high 0.7717 _[local]_cod_data_source_file sk1609IIsup2.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' 459 eadp' _shelx_refln_list_code 4 _shelx_f_calc_maximum 194.97 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y, z' '-x+1/2, y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 -13 1050.58 959.69 161.02 o 4 1 -13 83.05 113.62 120.51 o 5 1 -13 831.98 938.63 160.82 o 6 1 -13 367.89 369.57 160.82 o 0 0 -12 7637.33 7044.58 797.43 o 2 0 -12 295.34 312.88 120.71 o 4 0 -12 4907.52 4776.16 342.06 o 6 0 -12 108.85 -28.43 80.81 o 8 0 -12 3374.59 3229.84 347.73 o 10 0 -12 25.89 0.00 170.72 o 12 0 -12 2771.75 1887.03 286.43 o 14 0 -12 126.36 0.00 171.86 o 0 1 -12 307.21 284.14 170.14 o 1 1 -12 1145.36 1203.34 160.61 o 2 1 -12 24.54 -28.50 120.51 o 3 1 -12 1564.69 1736.83 160.82 o 4 1 -12 560.88 654.59 120.71 o 5 1 -12 1836.33 1550.98 177.82 o 6 1 -12 74.98 57.04 136.57 o 7 1 -12 1467.26 1511.26 161.01 o 8 1 -12 294.68 572.30 171.86 o 9 1 -12 1704.37 1442.87 264.95 o 10 1 -12 53.55 57.29 171.86 o 11 1 -12 910.81 849.51 178.36 o 12 1 -12 165.24 172.43 172.43 o 13 1 -12 745.70 627.52 136.85 o 0 2 -12 1633.95 1872.71 284.14 o 1 2 -12 538.03 736.71 226.86 o 2 2 -12 35.85 32.33 170.14 o 3 2 -12 601.39 340.57 160.61 o 4 2 -12 1960.04 1958.35 237.45 o 5 2 -12 585.11 369.52 160.60 o 6 2 -12 18.80 0.00 225.71 o 7 2 -12 399.47 281.85 225.14 o 8 2 -12 1753.86 1350.83 225.14 o 9 2 -12 194.26 393.56 225.14 o 10 2 -12 65.48 168.42 281.28 o 11 2 -12 529.89 281.28 281.28 o 0 3 -12 2249.11 2112.17 342.58 o 1 3 -12 520.04 520.19 200.79 o 2 3 -12 38.95 0.00 227.43 o 3 3 -12 188.60 0.00 226.86 o 2 0 -11 800.88 778.50 94.71 o 4 0 -11 459.59 406.26 140.07 o 6 0 -11 4535.54 4707.27 625.00 o 8 0 -11 144.79 57.28 114.86 o 10 0 -11 4148.98 3818.18 513.86 o 12 0 -11 135.20 288.73 173.58 o 14 0 -11 2381.45 2371.11 232.01 o 16 0 -11 4.56 -173.58 173.58 o 18 0 -11 1247.29 1267.76 346.01 o 1 1 -11 1279.89 1228.57 128.96 o 2 1 -11 633.49 648.00 79.66 o 3 1 -11 2982.74 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3 -11 246.93 398.14 227.43 o 4 3 -11 10.96 -226.86 226.86 o 5 3 -11 232.69 0.00 226.28 o 6 3 -11 2013.24 1751.84 339.14 o 7 3 -11 459.54 56.14 225.71 o 8 3 -11 47.40 225.14 225.14 o 9 3 -11 339.63 195.21 149.47 o 10 3 -11 1489.96 1347.96 224.56 o 11 3 -11 180.08 262.22 133.48 o 0 0 -10 8869.50 7575.87 2448.44 o 2 0 -10 1122.33 958.92 224.58 o 4 0 -10 7113.13 7362.52 907.43 o 6 0 -10 168.32 171.42 80.81 o 8 0 -10 5671.38 5612.45 384.02 o 10 0 -10 110.43 227.43 114.00 o 12 0 -10 5103.92 5759.09 358.26 o 14 0 -10 17.71 -116.29 116.29 o 16 0 -10 2022.19 2104.15 234.30 o 18 0 -10 22.62 86.78 123.13 o 20 0 -10 3334.69 3419.46 237.82 o 0 1 -10 295.21 337.12 73.10 o 1 1 -10 4494.76 4117.85 286.60 o 2 1 -10 174.03 171.98 54.37 o 3 1 -10 2271.18 2250.18 133.05 o 4 1 -10 1352.31 1275.78 81.10 o 5 1 -10 3285.30 3176.22 189.33 o 6 1 -10 103.07 14.40 35.59 o 7 1 -10 3181.70 3123.34 266.40 o 8 1 -10 323.41 326.20 72.85 o 9 1 -10 2245.81 2069.24 121.50 o 10 1 -10 16.21 -66.45 66.45 o 11 1 -10 2132.74 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o 22 0 -9 1859.10 1715.74 229.15 o 1 1 -9 2436.27 2305.39 154.89 o 2 1 -9 1401.79 1286.35 70.60 o 3 1 -9 622.48 581.97 51.33 o 4 1 -9 446.34 482.71 40.62 o 5 1 -9 3613.53 3476.26 243.76 o 6 1 -9 908.32 884.14 65.38 o 7 1 -9 2556.19 2448.12 91.48 o 8 1 -9 14.64 9.73 41.13 o 9 1 -9 2234.27 2279.37 163.89 o 10 1 -9 941.07 926.39 86.28 o 11 1 -9 1839.43 1583.07 216.64 o 12 1 -9 83.30 28.85 47.33 o 13 1 -9 2048.06 1960.63 110.88 o 14 1 -9 170.55 200.68 73.09 o 15 1 -9 1275.75 1415.33 98.88 o 16 1 -9 165.80 81.26 68.20 o 17 1 -9 1343.74 1599.04 137.92 o 18 1 -9 213.24 164.82 62.95 o 19 1 -9 1229.87 1565.79 182.68 o 20 1 -9 8.86 60.15 127.40 o 21 1 -9 1090.42 1095.83 138.58 o 22 1 -9 203.15 136.88 135.40 o 1 2 -9 1282.52 1161.08 68.90 o 2 2 -9 3522.87 3519.67 208.07 o 3 2 -9 679.77 710.01 68.79 o 4 2 -9 166.89 159.78 58.12 o 5 2 -9 1152.66 1071.58 92.81 o 6 2 -9 3403.54 3187.43 184.40 o 7 2 -9 1056.26 1531.28 177.02 o 8 2 -9 153.93 201.11 149.52 o 9 2 -9 1722.21 2005.04 222.85 o 10 2 -9 2466.91 2750.40 203.29 o 11 2 -9 960.56 1165.22 166.71 o 12 2 -9 63.36 55.57 166.13 o 13 2 -9 1147.13 1057.41 110.85 o 14 2 -9 2679.93 2655.82 277.27 o 15 2 -9 572.85 807.23 122.22 o 16 2 -9 134.74 74.65 139.81 o 17 2 -9 250.87 353.44 110.78 o 18 2 -9 1094.83 1239.26 155.82 o 19 2 -9 322.75 398.16 109.10 o 20 2 -9 40.86 196.97 128.19 o 21 2 -9 563.48 504.22 117.97 o 1 3 -9 270.69 315.41 121.73 o 2 3 -9 3395.28 3702.65 261.56 o 3 3 -9 545.99 524.20 109.13 o 4 3 -9 46.66 172.31 121.90 o 5 3 -9 887.57 954.86 121.88 o 6 3 -9 2218.65 2426.10 282.42 o 7 3 -9 672.99 619.27 225.14 o 8 3 -9 156.84 143.15 54.77 o 9 3 -9 447.80 417.22 96.85 o 10 3 -9 2612.76 3074.59 335.70 o 11 3 -9 444.42 557.97 167.28 o 12 3 -9 224.20 174.64 105.08 o 13 3 -9 281.75 176.35 106.19 o 14 3 -9 2157.14 2306.17 224.49 o 15 3 -9 125.68 181.03 120.88 o 16 3 -9 14.56 71.94 113.64 o 17 3 -9 420.54 405.72 128.08 o 18 3 -9 1413.24 1697.43 188.14 o 1 4 -9 1028.80 1146.88 162.03 o 2 4 -9 258.56 105.98 258.36 o 3 4 -9 864.40 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34.44 114.00 o 5 4 -8 2015.95 2175.10 201.94 o 6 4 -8 147.19 57.39 94.80 o 7 4 -8 2753.34 2711.60 235.98 o 8 4 -8 53.30 10.46 51.95 o 9 4 -8 829.57 890.09 103.32 o 10 4 -8 55.46 23.07 85.07 o 11 4 -8 1668.13 1663.68 145.00 o 12 4 -8 185.14 230.04 103.27 o 13 4 -8 1707.30 1516.31 149.04 o 14 4 -8 36.08 -116.87 116.87 o 15 4 -8 2273.53 2385.76 201.90 o 16 4 -8 249.07 234.88 117.44 o 0 5 -8 1393.15 1475.71 340.86 o 1 5 -8 82.99 -105.50 136.24 o 2 5 -8 21.49 56.71 226.28 o 3 5 -8 23.61 228.57 228.57 o 5 5 -8 2.15 451.99 282.42 o 6 5 -8 20.55 451.42 282.42 o 7 5 -8 104.31 0.00 225.71 o 8 5 -8 1893.87 -112.86 338.57 o 2 0 -7 11825.80 12182.38 368.75 o 4 0 -7 142.76 147.88 46.06 o 6 0 -7 9698.50 9601.62 354.56 o 8 0 -7 820.69 837.29 110.11 o 10 0 -7 8037.02 8272.34 291.83 o 12 0 -7 360.70 377.43 74.16 o 14 0 -7 7252.23 6306.27 449.13 o 18 0 -7 4036.58 4003.49 246.88 o 20 0 -7 231.33 245.28 97.89 o 22 0 -7 2221.83 2405.49 195.70 o 24 0 -7 48.71 0.00 119.73 o 26 0 -7 1675.19 1553.62 239.46 o 1 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5 5 52.50 -57.29 114.57 o 8 5 5 21.58 57.29 114.57 o 9 5 5 37.66 0.00 114.00 o 10 5 5 1925.20 2277.73 284.72 o 13 5 5 172.20 283.57 170.14 o 14 5 5 1227.88 1362.28 226.86 o 15 5 5 7.06 -170.14 170.14 o 16 5 5 130.08 113.43 170.14 o 1 6 5 633.28 571.89 127.40 o 2 6 5 296.94 299.89 85.06 o 3 6 5 517.78 655.36 178.74 o 5 6 5 415.50 474.34 177.59 o 0 0 6 23161.15 24806.51 1412.70 o 2 0 6 0.72 19.86 34.39 o 4 0 6 10798.76 11036.14 456.21 o 6 0 6 822.21 832.22 45.47 o 8 0 6 23996.04 25155.08 1059.87 o 10 0 6 143.06 116.41 41.22 o 12 0 6 11851.71 13124.44 726.40 o 14 0 6 141.01 117.96 53.22 o 16 0 6 7378.11 8436.08 430.23 o 18 0 6 30.44 -61.30 122.59 o 20 0 6 4341.61 4221.48 306.49 o 22 0 6 411.92 244.62 122.02 o 24 0 6 3272.61 3664.07 367.21 o 26 0 6 49.05 182.75 182.75 o 28 0 6 3453.43 3716.20 366.06 o 0 1 6 4775.98 5073.76 158.59 o 1 1 6 4334.55 4612.76 130.97 o 2 1 6 418.92 447.00 24.24 o 3 1 6 10466.76 11238.14 253.44 o 4 1 6 3850.82 4161.05 110.88 o 5 1 6 7160.52 6962.10 181.29 o 6 1 6 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18 3 6 170.21 232.01 115.72 o 19 3 6 537.38 579.74 115.72 o 21 3 6 402.00 406.16 174.15 o 22 3 6 22.49 0.00 116.29 o 23 3 6 178.76 232.01 232.01 o 0 4 6 1254.82 1091.89 172.43 o 1 4 6 2657.44 2705.94 162.84 o 2 4 6 13.56 76.76 51.59 o 3 4 6 1473.17 1439.66 122.30 o 4 4 6 272.92 288.36 81.59 o 5 4 6 1631.13 1513.78 146.94 o 6 4 6 69.18 43.74 47.84 o 7 4 6 1524.20 1561.82 97.81 o 8 4 6 150.46 138.01 38.20 o 9 4 6 2101.07 1980.98 226.28 o 10 4 6 16.31 0.00 113.43 o 15 4 6 1291.21 1251.72 227.43 o 16 4 6 20.95 56.71 170.72 o 17 4 6 1246.64 1310.73 228.00 o 18 4 6 62.26 0.00 171.29 o 19 4 6 787.04 742.44 171.29 o 20 4 6 207.09 171.29 171.29 o 0 5 6 1898.78 1580.55 234.30 o 1 5 6 47.47 87.79 87.36 o 2 5 6 35.14 58.43 116.58 o 3 5 6 32.85 -29.28 82.82 o 4 5 6 3689.71 3598.67 248.60 o 5 5 6 1.73 -58.41 82.78 o 6 5 6 51.26 29.35 145.51 o 7 5 6 89.07 114.00 114.00 o 8 5 6 2199.69 1989.58 284.72 o 11 5 6 10.25 169.57 169.57 o 12 5 6 2764.46 2603.12 283.00 o 13 5 6 42.57 226.28 169.57 o 14 5 6 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128.61 o 26 1 7 108.32 8.70 145.32 o 1 2 7 2457.36 2615.35 97.31 o 2 2 7 5213.32 5525.96 124.41 o 3 2 7 2330.38 2156.09 70.73 o 4 2 7 486.04 490.57 36.99 o 5 2 7 1170.81 1127.57 70.53 o 6 2 7 3755.89 3973.45 137.79 o 7 2 7 1955.76 2012.59 103.41 o 8 2 7 227.00 251.09 32.75 o 9 2 7 1208.99 1229.28 88.14 o 10 2 7 3861.61 3754.74 179.93 o 11 2 7 459.38 403.48 80.77 o 12 2 7 130.25 129.63 39.38 o 13 2 7 1224.69 1125.12 96.24 o 14 2 7 2681.56 2881.98 142.87 o 15 2 7 900.42 918.88 172.43 o 16 2 7 285.41 302.48 120.88 o 17 2 7 1737.30 1621.75 196.78 o 18 2 7 2576.39 2608.27 243.47 o 19 2 7 412.77 445.29 124.31 o 20 2 7 153.32 -59.58 119.16 o 21 2 7 789.15 727.54 182.17 o 22 2 7 1207.32 1543.88 297.32 o 23 2 7 320.80 0.00 181.60 o 24 2 7 61.32 356.32 237.74 o 1 3 7 1156.52 1031.81 83.37 o 2 3 7 4386.53 4148.46 181.95 o 3 3 7 878.11 734.38 90.59 o 4 3 7 47.30 58.05 33.51 o 5 3 7 805.80 692.52 37.06 o 6 3 7 4328.35 4439.98 190.12 o 7 3 7 256.41 296.41 44.48 o 8 3 7 46.43 41.97 32.53 o 9 3 7 130.40 147.57 37.42 o 10 3 7 4643.91 4515.70 204.99 o 11 3 7 279.87 385.48 57.29 o 12 3 7 578.70 535.19 84.15 o 14 3 7 2351.05 2039.42 233.16 o 15 3 7 489.34 407.88 116.29 o 16 3 7 27.60 58.43 116.29 o 17 3 7 580.57 582.04 116.29 o 18 3 7 1920.20 1978.12 291.02 o 19 3 7 126.39 174.15 174.73 o 20 3 7 46.05 -174.15 174.15 o 21 3 7 546.28 465.17 174.15 o 22 3 7 1284.84 1452.80 290.44 o 1 4 7 1559.33 1693.62 121.52 o 2 4 7 45.67 114.71 81.21 o 3 4 7 2321.13 2298.11 162.61 o 4 4 7 27.78 0.00 81.39 o 5 4 7 1929.65 2104.77 139.14 o 6 4 7 282.21 115.38 113.14 o 7 4 7 1973.11 1996.84 163.72 o 8 4 7 56.46 57.64 51.16 o 9 4 7 1495.09 1359.99 170.14 o 13 4 7 1408.88 1421.86 227.43 o 14 4 7 617.16 682.86 170.72 o 15 4 7 428.77 569.43 170.72 o 16 4 7 132.90 57.29 114.00 o 17 4 7 1366.13 1197.87 228.00 o 18 4 7 13.81 114.00 171.29 o 1 5 7 34.19 58.14 123.34 o 2 5 7 2089.01 2246.31 205.55 o 3 5 7 152.52 59.01 176.44 o 4 5 7 9.80 -57.96 96.28 o 5 5 7 133.98 59.58 178.16 o 6 5 7 1859.18 2203.39 297.61 o 7 5 7 41.83 -56.71 170.14 o 9 5 7 33.78 169.57 169.57 o 0 0 8 11524.68 13396.83 960.42 o 2 0 8 516.08 522.79 39.93 o 4 0 8 10588.05 11549.88 420.95 o 6 0 8 399.63 318.80 39.59 o 8 0 8 8930.50 9783.46 286.07 o 10 0 8 31.44 19.60 118.87 o 12 0 8 7256.17 8056.84 482.93 o 16 0 8 6115.90 6553.05 426.79 o 18 0 8 384.74 243.47 121.45 o 20 0 8 4012.34 4145.28 366.64 o 24 0 8 1947.57 1828.03 304.77 o 0 1 8 1570.52 1670.63 108.66 o 1 1 8 5886.97 6438.82 185.01 o 2 1 8 355.54 389.42 30.79 o 3 1 8 5456.30 5745.23 131.48 o 4 1 8 382.94 340.31 35.93 o 5 1 8 3152.55 3128.79 86.91 o 6 1 8 110.27 141.08 26.02 o 7 1 8 3886.65 3981.70 102.24 o 8 1 8 1044.96 972.25 63.39 o 9 1 8 3268.55 3525.43 157.83 o 10 1 8 142.93 118.41 48.20 o 11 1 8 5135.37 5325.74 200.84 o 12 1 8 837.54 708.94 83.01 o 13 1 8 3492.68 3523.72 289.30 o 14 1 8 72.29 179.31 119.73 o 15 1 8 2292.78 2101.86 181.03 o 16 1 8 723.19 757.33 85.47 o 17 1 8 2537.55 2643.19 171.75 o 18 1 8 281.50 242.32 121.73 o 19 1 8 2127.84 2242.21 242.90 o 20 1 8 467.31 667.39 182.17 o 21 1 8 550.97 528.94 101.05 o 22 1 8 14.28 109.30 101.05 o 23 1 8 1128.82 828.48 145.61 o 24 1 8 188.20 60.72 242.32 o 0 2 8 6294.86 6408.09 270.11 o 1 2 8 1841.54 1880.59 93.27 o 2 2 8 85.20 133.76 29.64 o 3 2 8 2513.69 2702.27 85.69 o 4 2 8 5561.39 5533.15 170.57 o 5 2 8 1828.61 1884.67 89.07 o 6 2 8 238.66 73.65 47.94 o 7 2 8 2925.44 2756.96 108.67 o 8 2 8 3895.83 4214.67 139.25 o 9 2 8 1543.31 1528.61 78.08 o 10 2 8 55.57 19.80 59.86 o 11 2 8 2032.16 2064.76 240.89 o 12 2 8 2604.34 2383.73 137.21 o 13 2 8 778.01 654.18 136.34 o 14 2 8 127.44 0.00 115.72 o 15 2 8 1326.69 1325.62 181.03 o 16 2 8 2234.33 2174.04 242.32 o 17 2 8 568.74 482.34 100.23 o 18 2 8 43.21 -29.93 90.23 o 19 2 8 1087.41 1075.28 179.31 o 20 2 8 1627.88 1547.71 170.32 o 21 2 8 193.40 -59.58 178.74 o 22 2 8 21.42 59.58 119.16 o 23 2 8 467.97 714.94 238.31 o 0 3 8 4542.44 4610.50 270.70 o 1 3 8 932.50 800.49 74.88 o 2 3 8 26.50 -11.66 38.91 o 3 3 8 935.12 837.59 86.94 o 4 3 8 3490.81 3666.01 181.93 o 5 3 8 444.90 433.36 47.94 o 6 3 8 259.56 150.96 32.52 o 7 3 8 1089.81 968.28 86.12 o 8 3 8 3125.59 2995.95 208.25 o 9 3 8 648.35 430.70 68.45 o 10 3 8 67.87 88.50 83.43 o 11 3 8 1230.72 993.36 175.30 o 16 3 8 1497.40 1520.40 233.73 o 18 3 8 7.24 350.60 175.30 o 19 3 8 338.56 525.32 233.16 o 0 4 8 10.99 57.29 114.57 o 1 4 8 1687.82 1601.15 161.83 o 2 4 8 20.38 143.36 144.08 o 3 4 8 2010.56 2034.54 162.22 o 4 4 8 213.48 85.99 81.20 o 5 4 8 2025.55 1811.21 162.79 o 6 4 8 146.61 86.27 145.51 o 7 4 8 2731.95 2588.80 235.45 o 8 4 8 56.06 28.92 81.78 o 9 4 8 806.33 919.52 126.03 o 10 4 8 55.78 56.71 113.43 o 14 4 8 36.73 57.29 114.00 o 16 4 8 243.69 228.57 171.29 o 0 5 8 1428.27 1617.21 288.73 o 1 5 8 70.22 104.01 96.41 o 2 5 8 20.92 -57.29 171.86 o 3 5 8 16.64 -96.54 96.54 o 4 5 8 1787.57 1853.77 180.14 o 5 5 8 3.64 118.01 177.02 o 6 5 8 23.05 86.89 122.86 o 7 5 8 106.88 80.36 176.73 o 8 5 8 1970.87 2370.53 282.42 o 2 0 9 10607.43 11421.53 462.14 o 4 0 9 94.89 119.79 34.51 o 6 0 9 7321.67 8223.36 276.56 o 8 0 9 83.48 95.50 39.84 o 10 0 9 4049.91 4410.52 358.62 o 18 0 9 3903.85 3335.82 364.35 o 20 0 9 543.72 425.64 182.17 o 22 0 9 2129.05 1887.03 244.04 o 1 1 9 2409.73 2308.34 80.70 o 2 1 9 1537.95 1496.03 54.45 o 3 1 9 704.11 766.55 49.03 o 4 1 9 444.75 511.19 42.28 o 5 1 9 3491.52 3497.81 111.35 o 6 1 9 918.91 881.35 53.44 o 7 1 9 2544.71 2593.36 88.38 o 8 1 9 14.00 -29.64 29.78 o 9 1 9 2320.71 2528.21 122.37 o 10 1 9 908.46 808.25 79.95 o 11 1 9 1784.75 1642.13 113.08 o 12 1 9 80.87 99.66 53.48 o 13 1 9 2120.35 2318.98 238.31 o 15 1 9 1231.84 1273.49 182.17 o 16 1 9 171.01 181.02 119.44 o 17 1 9 1287.14 1289.64 144.85 o 18 1 9 218.20 145.14 180.74 o 19 1 9 1267.43 1032.88 242.90 o 20 1 9 6.78 182.17 121.45 o 21 1 9 1115.61 1069.78 183.89 o 1 2 9 1194.54 1009.39 64.15 o 2 2 9 3587.18 3693.42 133.37 o 3 2 9 712.86 676.01 59.58 o 4 2 9 163.81 136.84 37.34 o 5 2 9 1223.95 1239.36 64.35 o 6 2 9 3458.35 3418.56 139.51 o 7 2 9 1055.61 969.34 64.01 o 8 2 9 156.18 118.09 44.40 o 9 2 9 1608.08 1593.29 94.35 o 10 2 9 2461.49 2691.85 192.41 o 11 2 9 988.38 899.98 180.45 o 12 2 9 58.94 -60.15 120.30 o 13 2 9 1086.34 1047.55 120.02 o 14 2 9 2693.31 2359.11 188.16 o 15 2 9 606.82 542.51 120.88 o 16 2 9 137.97 -60.15 120.88 o 17 2 9 229.83 300.18 120.30 o 18 2 9 1126.73 1199.59 179.88 o 19 2 9 301.44 479.49 179.88 o 20 2 9 32.54 -179.88 179.88 o 21 2 9 529.94 418.77 179.31 o 1 3 9 280.14 260.73 87.36 o 2 3 9 3505.48 3895.56 223.37 o 3 3 9 545.40 523.47 96.71 o 4 3 9 48.42 145.72 146.08 o 5 3 9 870.88 970.00 123.95 o 6 3 9 2290.09 2203.45 165.47 o 7 3 9 731.09 765.93 177.02 o 8 3 9 147.39 0.00 118.01 o 9 3 9 460.31 533.34 177.59 o 10 3 9 2625.83 3030.48 297.32 o 11 3 9 464.73 352.31 117.44 o 16 3 9 20.59 -58.43 175.87 o 17 3 9 378.79 410.75 234.88 o 18 3 9 1449.87 1758.71 293.31 o 1 4 9 1017.70 1014.95 226.28 o 2 4 9 260.39 251.71 173.01 o 3 4 9 900.24 865.61 173.01 o 4 4 9 7.42 -11.57 95.79 o 5 4 9 1195.15 1685.95 232.59 o 6 4 9 128.50 58.43 175.30 o 7 4 9 451.62 586.05 175.87 o 8 4 9 109.07 -176.44 176.44 o 9 4 9 1247.80 1415.56 236.02 o 11 4 9 1056.52 913.15 171.29 o 12 4 9 68.11 57.29 171.29 o 13 4 9 571.43 514.44 228.57 o 0 0 10 8530.61 8990.04 544.80 o 2 0 10 1112.41 1058.76 77.20 o 4 0 10 6969.74 7176.29 253.37 o 6 0 10 175.04 179.58 69.12 o 8 0 10 5467.81 6025.73 297.68 o 10 0 10 120.28 59.58 118.58 o 16 0 10 2056.13 2105.30 241.18 o 18 0 10 14.07 -120.88 120.88 o 20 0 10 3163.52 3152.50 364.35 o 0 1 10 237.70 270.82 91.37 o 1 1 10 4355.65 4380.89 191.83 o 2 1 10 175.18 210.67 42.53 o 3 1 10 2385.65 2356.02 89.09 o 4 1 10 1337.75 1337.41 86.25 o 5 1 10 3286.64 3328.58 129.25 o 6 1 10 105.61 79.96 42.38 o 7 1 10 3354.61 3215.88 133.10 o 8 1 10 313.48 331.13 59.57 o 9 1 10 2367.46 1972.89 162.99 o 10 1 10 15.77 -68.67 68.67 o 13 1 10 1512.17 1246.56 178.16 o 14 1 10 26.60 -60.01 84.86 o 15 1 10 1683.64 1624.81 170.12 o 16 1 10 455.26 381.63 152.67 o 17 1 10 669.60 561.55 100.05 o 18 1 10 77.32 182.17 182.17 o 19 1 10 1354.88 1148.88 171.14 o 20 1 10 231.80 30.18 171.14 o 0 2 10 2924.82 2741.84 197.64 o 1 2 10 1220.68 1131.78 103.28 o 2 2 10 2.71 47.80 45.25 o 3 2 10 728.26 646.27 86.24 o 4 2 10 2497.03 2691.38 119.80 o 5 2 10 711.52 570.06 77.09 o 6 2 10 96.03 59.79 84.98 o 7 2 10 649.89 636.66 88.80 o 8 2 10 2867.19 2696.06 147.94 o 9 2 10 615.07 572.91 92.50 o 10 2 10 21.66 0.10 84.95 o 11 2 10 437.81 180.45 120.30 o 15 2 10 1236.47 1083.87 240.61 o 17 2 10 472.69 602.09 240.61 o 18 2 10 4.10 -240.61 240.61 o 0 3 10 2549.42 2914.19 291.59 o 1 3 10 319.56 326.33 116.58 o 2 3 10 129.61 175.30 175.30 o 3 3 10 344.80 438.15 123.75 o 4 3 10 3227.28 2929.65 293.31 o 5 3 10 572.43 352.31 176.44 o 6 3 10 8.71 58.66 146.65 o 7 3 10 376.11 341.06 97.86 o 8 3 10 2312.77 2424.38 295.60 o 9 3 10 126.63 59.01 177.59 o 10 3 10 8.91 236.01 149.23 o 0 4 10 142.52 229.15 171.86 o 1 4 10 1061.85 1205.89 287.01 o 2 4 10 3.71 115.15 115.15 o 3 4 10 1821.44 1782.19 392.70 o 4 4 10 56.62 11.64 201.36 o 5 4 10 1533.82 1089.46 239.17 o 6 4 10 3.16 0.00 81.41 o 7 4 10 742.05 759.63 233.73 o 8 4 10 297.22 586.05 234.30 o 9 4 10 1190.96 1170.88 188.76 o 2 0 11 843.35 863.37 104.29 o 4 0 11 461.32 361.15 85.25 o 6 0 11 4817.70 5531.64 314.79 o 8 0 11 132.86 304.77 122.02 o 14 0 11 2439.70 2324.13 298.47 o 16 0 11 5.91 119.73 179.88 o 18 0 11 1234.32 1204.17 241.18 o 1 1 11 1250.96 1235.40 90.58 o 2 1 11 635.33 468.35 81.77 o 3 1 11 3031.19 2964.40 133.19 o 4 1 11 67.80 -0.22 60.22 o 5 1 11 2222.09 1944.88 110.14 o 6 1 11 203.39 375.36 64.71 o 7 1 11 1242.54 1047.34 104.50 o 8 1 11 77.18 30.14 149.81 o 9 1 11 2129.85 2491.98 243.47 o 10 1 11 663.36 603.21 128.00 o 11 1 11 617.59 779.68 179.88 o 13 1 11 2319.96 2237.93 229.83 o 14 1 11 543.43 512.92 242.61 o 15 1 11 786.17 659.70 169.52 o 16 1 11 23.21 -90.03 127.59 o 17 1 11 1464.26 1159.90 188.41 o 1 2 11 794.19 838.84 126.38 o 2 2 11 1764.47 1769.84 143.11 o 3 2 11 868.86 638.88 99.47 o 4 2 11 40.73 47.80 99.24 o 5 2 11 965.13 782.35 126.99 o 6 2 11 1603.01 1535.75 242.90 o 7 2 11 526.29 700.15 99.77 o 8 2 11 36.20 0.00 180.45 o 9 2 11 635.28 843.26 180.45 o 10 2 11 1879.35 1707.44 187.75 o 14 2 11 574.69 481.78 241.18 o 15 2 11 462.55 181.03 241.18 o 1 3 11 486.93 469.18 175.87 o 2 3 11 1280.81 1174.38 234.88 o 3 3 11 242.23 234.88 176.44 o 4 3 11 11.75 59.01 118.01 o 5 3 11 240.97 177.02 177.02 o 6 3 11 2031.07 1948.90 295.60 o 7 3 11 472.60 295.60 236.60 o 8 3 11 46.48 11.89 98.29 o 9 3 11 338.22 653.07 237.74 o 10 3 11 1504.89 1486.60 237.74 o 0 0 12 8065.77 7969.19 665.67 o 2 0 12 298.54 331.77 128.00 o 4 0 12 4680.82 4730.36 334.47 o 6 0 12 117.06 108.66 100.57 o 8 0 12 3460.89 3670.38 367.78 o 12 0 12 2791.97 2720.56 355.18 o 14 0 12 128.41 -59.58 237.74 o 0 1 12 294.79 217.09 100.29 o 1 1 12 1180.88 1298.38 102.56 o 2 1 12 24.42 60.32 71.16 o 3 1 12 1487.42 1572.85 200.59 o 4 1 12 598.51 637.66 105.17 o 5 1 12 1825.88 1692.95 139.67 o 6 1 12 72.66 174.27 70.58 o 7 1 12 1364.01 1254.25 139.66 o 8 1 12 314.72 183.32 183.32 o 9 1 12 1575.63 1465.40 244.04 o 10 1 12 51.95 120.18 127.55 o 11 1 12 833.82 770.51 237.17 o 12 1 12 138.07 119.73 179.31 o 13 1 12 764.61 779.68 240.03 o 1 2 12 542.69 548.53 149.23 o 2 2 12 36.89 -71.88 99.67 o 3 2 12 616.99 636.42 143.99 o 4 2 12 1978.98 1894.24 245.76 o 5 2 12 645.51 377.19 301.33 o 6 2 12 20.16 11.91 99.86 o 8 2 12 1790.66 2235.34 302.48 o 9 2 12 194.14 103.14 144.31 o 10 2 12 66.28 -60.72 181.60 o 1 3 12 560.29 708.07 177.02 o 3 3 12 172.67 591.20 236.60 o 2 0 13 2977.41 2725.35 232.29 o 4 0 13 30.77 0.00 122.02 o 6 0 13 2723.79 2819.09 367.78 o 8 0 13 24.10 183.89 183.89 o 1 1 13 1115.09 784.83 241.18 o 2 1 13 289.31 242.32 120.88 o 3 1 13 442.48 537.92 179.31 o 4 1 13 84.19 -182.75 182.75 o 7 1 13 595.61 244.62 183.32 o