#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/32/2013212.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013212_Fobs loop_ _publ_author_name 'Quesada, Antonio' 'Marchal, Antonio' 'Low, John N.' 'Glidewell, Christopher' _publ_section_title ; 2-Amino-5-nitro-4,6-dipiperidinopyrimidinium hydrogensulfate monohydrate: hydrogen-bonded sheets containing highly distorted cations ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o102 _journal_page_last o104 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.485 _cell_angle_gamma 90.000 _cell_length_a 14.0307 _cell_length_b 6.1277 _cell_length_c 21.5135 _exptl_crystal_F_000 896.00 _reflns_d_resolution_high 0.7707 _[local]_cod_data_source_file sk1612Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 02SRC326 in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 177.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 0 0 622.38 786.78 21.56 o 4 0 0 28348.73 28165.98 733.60 o 5 0 0 668.28 766.99 30.18 o 6 0 0 1799.97 1802.20 51.03 o 7 0 0 721.58 754.42 25.47 o 8 0 0 115.35 89.57 6.46 o 9 0 0 4140.49 4336.45 122.75 o 10 0 0 2301.00 2372.16 65.96 o 11 0 0 7.04 18.63 5.01 o 12 0 0 262.56 285.18 22.40 o 13 0 0 0.57 16.80 11.20 o 14 0 0 91.73 78.41 11.20 o 15 0 0 11.01 5.60 11.20 o 16 0 0 1572.00 1525.22 101.10 o 1 1 0 834.40 745.16 17.09 o 2 1 0 22987.48 20320.36 555.42 o 3 1 0 3525.71 3631.37 56.40 o 4 1 0 4558.55 4514.83 78.69 o 5 1 0 1405.55 1465.26 27.51 o 6 1 0 576.37 547.61 10.42 o 7 1 0 1558.49 1620.46 29.22 o 8 1 0 2424.54 2585.36 46.31 o 9 1 0 157.88 145.18 5.01 o 10 1 0 105.98 86.45 5.01 o 11 1 0 25.10 43.09 6.46 o 12 1 0 577.96 651.14 33.31 o 13 1 0 1280.46 1362.36 52.67 o 14 1 0 1396.25 1499.95 62.13 o 15 1 0 90.94 87.07 11.90 o 16 1 0 309.89 309.58 28.17 o 17 1 0 429.05 420.62 44.92 o 18 1 0 694.12 713.00 78.64 o 0 2 0 6254.77 5068.39 227.79 o 1 2 0 327.41 280.42 4.93 o 2 2 0 1070.00 1022.99 16.24 o 3 2 0 1328.87 1341.12 20.50 o 4 2 0 1260.74 1219.48 23.21 o 5 2 0 5321.72 5513.63 111.55 o 6 2 0 223.87 181.97 5.08 o 7 2 0 1201.16 1416.98 28.78 o 8 2 0 9.13 18.40 2.72 o 9 2 0 127.56 105.23 5.02 o 10 2 0 859.56 929.38 24.98 o 11 2 0 1415.70 1463.28 41.87 o 12 2 0 195.83 200.33 9.37 o 13 2 0 21.37 50.75 11.26 o 14 2 0 4.35 11.26 7.96 o 15 2 0 48.58 45.66 11.96 o 16 2 0 122.31 101.73 16.97 o 17 2 0 102.37 102.57 19.52 o 1 3 0 241.11 262.70 5.96 o 2 3 0 1004.36 1058.09 18.80 o 3 3 0 26.47 25.59 2.37 o 4 3 0 6.75 10.38 2.58 o 5 3 0 6.99 8.20 2.17 o 6 3 0 2063.56 2276.28 45.41 o 7 3 0 3.67 11.08 2.86 o 8 3 0 830.87 824.90 15.89 o 9 3 0 1165.21 1146.55 48.19 o 10 3 0 18.76 17.27 3.83 o 11 3 0 1.36 1.12 3.74 o 12 3 0 30.69 9.40 5.02 o 13 3 0 67.95 70.51 11.46 o 14 3 0 40.75 22.52 11.26 o 15 3 0 35.65 40.36 8.00 o 16 3 0 11.18 0.00 17.03 o 0 4 0 679.44 725.98 17.39 o 1 4 0 528.52 593.50 14.39 o 2 4 0 19.32 21.94 1.94 o 3 4 0 7.44 8.27 2.19 o 4 4 0 13.29 13.67 2.19 o 5 4 0 381.09 420.15 9.45 o 6 4 0 88.69 81.86 4.13 o 7 4 0 142.95 137.51 5.72 o 8 4 0 259.94 201.57 17.32 o 9 4 0 828.67 803.61 34.13 o 10 4 0 1682.69 1788.64 227.03 o 11 4 0 844.06 688.80 188.08 o 12 4 0 1.31 1.89 11.32 o 14 4 0 3.80 0.00 11.32 o 15 4 0 94.07 73.72 22.69 o 1 5 0 39.21 47.20 2.41 o 2 5 0 4.91 1.67 2.21 o 3 5 0 642.70 614.12 13.55 o 4 5 0 959.12 989.27 30.95 o 5 5 0 689.65 744.58 22.81 o 6 5 0 39.70 36.96 5.86 o 7 5 0 147.90 146.54 6.77 o 8 5 0 1272.07 1376.21 70.78 o 9 5 0 118.29 113.39 15.14 o 10 5 0 29.70 35.66 5.14 o 11 5 0 17.10 28.49 8.04 o 12 5 0 7.62 2.84 8.04 o 13 5 0 1.24 -0.01 8.06 o 14 5 0 22.64 45.72 11.43 o 0 6 0 40.59 41.21 5.89 o 1 6 0 430.08 452.14 15.18 o 2 6 0 13.54 9.10 2.84 o 3 6 0 17.71 15.71 2.74 o 4 6 0 817.99 857.17 28.68 o 5 6 0 280.94 280.31 17.45 o 6 6 0 29.93 28.25 6.57 o 7 6 0 8.96 12.44 3.63 o 9 6 0 161.62 167.96 17.43 o 10 6 0 30.30 23.20 5.83 o 11 6 0 57.22 75.55 11.66 o 1 7 0 1.33 6.81 3.69 o 2 7 0 45.25 54.58 6.85 o 3 7 0 163.81 189.70 10.18 o 4 7 0 164.30 181.92 10.87 o 5 7 0 211.23 230.74 18.69 o 6 7 0 537.24 535.41 50.63 o 7 7 0 144.10 133.07 12.26 o 8 7 0 11.24 12.98 8.63 o -17 1 1 178.52 151.33 22.46 o -16 1 1 7.33 0.00 11.26 o -15 1 1 6.90 16.86 7.94 o -14 1 1 283.98 265.37 17.69 o -13 1 1 1018.51 1029.73 45.35 o -12 1 1 48.11 40.02 7.92 o -11 1 1 970.55 1045.43 30.12 o -10 1 1 323.47 329.33 12.25 o -9 1 1 1073.64 1139.28 23.99 o -8 1 1 101.18 115.37 5.00 o -7 1 1 258.94 223.42 5.32 o -6 1 1 376.71 433.34 10.26 o -5 1 1 197.22 238.86 5.34 o -4 1 1 978.32 925.26 15.99 o -3 1 1 239.51 232.50 5.04 o -2 1 1 480.01 439.71 14.91 o -1 1 1 2852.37 2799.85 42.78 o 0 1 1 81.04 76.25 2.66 o 2 1 1 355.47 300.27 4.49 o 3 1 1 2052.52 2077.91 33.82 o 4 1 1 11752.16 11653.43 187.02 o 5 1 1 16.31 24.56 2.29 o 6 1 1 67.55 66.17 3.42 o 7 1 1 6386.90 7055.31 119.41 o 8 1 1 417.90 455.64 9.63 o 9 1 1 686.89 705.19 19.90 o 10 1 1 1.62 1.88 2.29 o 11 1 1 0.42 1.88 6.47 o 12 1 1 2100.46 2127.65 60.28 o 13 1 1 0.92 2.80 7.92 o 14 1 1 1072.93 1096.33 43.70 o 15 1 1 1142.29 1248.04 60.75 o 16 1 1 54.40 33.78 16.86 o 17 1 1 62.76 67.55 16.92 o 18 1 1 76.76 67.44 22.46 o -17 2 1 158.79 150.00 15.96 o -16 2 1 67.74 79.21 16.97 o -15 2 1 0.28 0.00 7.96 o -14 2 1 8.84 14.04 8.49 o -13 2 1 1565.88 1626.24 63.81 o -12 2 1 53.77 64.78 7.96 o -11 2 1 1890.87 1942.74 55.84 o -10 2 1 258.60 270.04 12.72 o -9 2 1 2499.46 2466.96 49.08 o -8 2 1 1028.98 1112.93 23.75 o -7 2 1 1573.09 1798.61 35.68 o -6 2 1 268.75 305.79 6.92 o -5 2 1 0.27 7.57 2.31 o -4 2 1 816.12 837.72 14.29 o -3 2 1 2685.20 2596.46 54.59 o -2 2 1 226.78 258.63 6.28 o -1 2 1 3168.43 2759.36 121.18 o 0 2 1 459.75 374.27 7.93 o 1 2 1 27564.11 22717.31 690.81 o 2 2 1 368.01 318.55 6.16 o 3 2 1 675.24 726.48 13.34 o 4 2 1 2394.14 2512.33 40.24 o 5 2 1 654.62 532.27 8.62 o 6 2 1 335.04 401.44 6.91 o 7 2 1 2877.33 3089.62 49.86 o 8 2 1 337.85 316.59 8.26 o 9 2 1 362.03 395.40 11.72 o 10 2 1 424.57 488.25 14.39 o 11 2 1 1337.04 1404.32 41.54 o 12 2 1 13.58 14.96 5.01 o 13 2 1 196.94 169.11 16.92 o 14 2 1 290.43 248.09 15.94 o 15 2 1 4.07 11.32 11.32 o 16 2 1 30.81 27.05 9.38 o 17 2 1 480.36 373.19 39.60 o -16 3 1 236.24 274.61 20.02 o -15 3 1 126.64 122.13 13.56 o -14 3 1 24.49 22.60 9.38 o -13 3 1 57.70 57.52 9.38 o -12 3 1 109.91 124.32 11.98 o -11 3 1 744.42 689.53 22.96 o -10 3 1 991.03 1019.16 62.26 o -9 3 1 602.69 606.49 28.88 o -8 3 1 71.88 81.45 4.67 o -7 3 1 2193.31 2188.94 39.80 o -6 3 1 595.13 590.72 11.20 o -5 3 1 872.38 826.03 19.38 o -4 3 1 210.98 244.39 4.36 o -3 3 1 8667.82 8788.97 195.90 o -2 3 1 3391.61 3235.77 47.93 o -1 3 1 1825.41 1491.38 24.53 o 0 3 1 214.57 165.24 4.43 o 1 3 1 4.94 7.36 2.95 o 2 3 1 10.25 11.68 2.38 o 3 3 1 478.68 410.33 13.92 o 4 3 1 779.29 689.89 11.39 o 5 3 1 1233.78 1257.31 21.93 o 6 3 1 1.92 7.50 2.29 o 7 3 1 1028.99 1038.48 22.04 o 8 3 1 142.73 120.35 6.18 o 9 3 1 1704.06 1796.54 54.61 o 10 3 1 580.09 595.16 25.62 o 11 3 1 631.93 591.19 67.88 o 12 3 1 444.92 398.46 20.86 o 13 3 1 414.45 429.35 23.96 o 14 3 1 519.01 484.86 39.55 o 15 3 1 194.98 175.56 34.00 o 16 3 1 6.02 17.03 17.03 o -15 4 1 115.48 92.70 13.62 o -14 4 1 66.89 73.69 9.45 o -13 4 1 275.69 254.49 22.63 o -12 4 1 296.70 226.03 22.63 o -11 4 1 89.80 75.25 22.46 o -10 4 1 562.25 488.38 24.32 o -9 4 1 4309.65 4300.24 158.38 o -8 4 1 1854.81 2047.16 111.93 o -7 4 1 300.51 293.39 19.99 o -6 4 1 42.67 59.35 3.84 o -5 4 1 259.62 245.42 7.35 o -4 4 1 2742.75 2720.09 83.32 o -3 4 1 3423.15 3553.84 60.93 o -2 4 1 565.07 586.26 12.79 o -1 4 1 1.79 2.94 4.16 o 0 4 1 1814.45 1754.59 46.43 o 1 4 1 466.78 451.94 14.03 o 2 4 1 416.23 392.55 12.82 o 3 4 1 666.33 607.07 16.66 o 4 4 1 13.45 13.05 2.36 o 5 4 1 18.17 21.84 2.58 o 6 4 1 2120.86 2214.81 54.57 o 7 4 1 1706.12 1708.62 52.99 o 8 4 1 13.17 19.66 3.42 o 9 4 1 102.83 88.40 19.55 o 10 4 1 305.48 268.04 16.12 o 11 4 1 838.74 895.20 56.75 o 12 4 1 749.48 794.86 37.95 o 13 4 1 3.30 11.32 5.66 o 14 4 1 15.10 0.00 17.03 o 15 4 1 4.87 11.37 17.03 o -14 5 1 62.70 68.58 11.43 o -13 5 1 403.70 424.84 25.95 o -12 5 1 35.38 34.15 9.48 o -11 5 1 106.62 118.76 16.97 o -10 5 1 318.44 316.50 22.63 o -9 5 1 13.25 5.77 5.77 o -8 5 1 13.81 28.29 5.66 o -7 5 1 300.25 318.51 27.72 o -6 5 1 840.19 893.13 42.38 o -5 5 1 633.12 635.07 32.88 o -4 5 1 8.74 7.91 2.03 o -3 5 1 1.00 0.96 2.35 o -2 5 1 1469.03 1540.65 31.07 o -1 5 1 25.41 26.01 2.89 o 0 5 1 31.78 22.60 2.18 o 1 5 1 768.29 801.14 15.85 o 2 5 1 1709.73 1710.89 29.29 o 3 5 1 1028.56 968.47 23.42 o 4 5 1 160.31 161.33 6.50 o 5 5 1 261.06 277.34 12.16 o 6 5 1 47.73 50.92 4.72 o 7 5 1 14.33 11.51 3.27 o 8 5 1 128.60 125.21 10.16 o 9 5 1 6.85 9.58 5.15 o 10 5 1 500.51 594.32 26.18 o 11 5 1 128.51 129.09 12.12 o 12 5 1 159.47 188.48 16.14 o 13 5 1 175.73 171.34 16.14 o 14 5 1 310.88 343.41 34.40 o -11 6 1 80.83 75.32 11.60 o -10 6 1 108.61 133.16 17.37 o -9 6 1 4.72 0.00 5.77 o -8 6 1 21.88 23.09 5.77 o -7 6 1 183.99 207.51 17.32 o -6 6 1 14.37 7.39 3.18 o -5 6 1 550.35 588.85 29.70 o -4 6 1 662.99 683.88 36.39 o -3 6 1 5.07 11.56 2.90 o -2 6 1 5.64 11.00 2.82 o -1 6 1 864.67 861.55 23.44 o 0 6 1 182.81 178.67 12.49 o 1 6 1 254.61 228.71 7.20 o 2 6 1 445.06 421.36 11.49 o 3 6 1 602.59 610.31 14.15 o 4 6 1 459.28 418.25 22.63 o 5 6 1 210.51 215.96 8.41 o 6 6 1 11.62 10.49 3.74 o 7 6 1 27.38 22.16 5.86 o 8 6 1 353.49 300.95 40.52 o 9 6 1 92.98 104.36 11.60 o 10 6 1 85.70 87.27 11.66 o 11 6 1 10.06 29.15 11.66 o -8 7 1 42.11 36.32 9.63 o -7 7 1 3.26 11.56 8.60 o -6 7 1 146.88 117.12 13.85 o -5 7 1 8.61 -5.75 8.77 o -4 7 1 21.02 28.77 6.76 o -3 7 1 172.62 169.41 8.30 o -2 7 1 24.70 29.49 3.78 o -1 7 1 131.38 139.68 8.22 o 0 7 1 61.12 59.21 4.81 o 1 7 1 80.10 80.25 6.87 o 2 7 1 199.75 196.42 20.07 o 3 7 1 2.83 7.56 10.10 o 4 7 1 325.75 346.28 16.91 o 5 7 1 40.39 40.61 9.64 o 6 7 1 279.96 330.76 30.12 o 7 7 1 34.17 33.80 7.67 o 8 7 1 63.83 38.42 11.32 o -18 0 2 303.76 235.97 33.72 o -16 0 2 999.59 847.25 61.78 o -15 0 2 0.34 5.60 11.20 o -14 0 2 470.98 459.49 33.66 o -13 0 2 30.95 22.40 11.20 o -12 0 2 21779.68 22617.53 987.89 o -11 0 2 139.04 123.31 25.15 o -10 0 2 219.52 218.06 9.32 o -9 0 2 752.37 805.95 44.78 o -8 0 2 2244.88 2111.62 59.49 o -7 0 2 716.26 642.19 22.46 o -6 0 2 1214.10 1284.39 61.66 o -5 0 2 298.08 265.52 7.96 o -4 0 2 947.11 982.45 27.90 o -3 0 2 23304.96 21589.80 794.10 o -2 0 2 6622.71 6203.94 182.84 o 3 0 2 17246.37 16241.33 299.64 o 4 0 2 5768.89 5801.55 124.28 o 5 0 2 1615.10 1854.87 41.33 o 6 0 2 2613.49 2435.85 53.92 o 7 0 2 320.75 235.70 7.15 o 8 0 2 4979.40 5092.44 110.32 o 9 0 2 1998.61 1993.45 50.20 o 10 0 2 54.12 54.12 4.57 o 11 0 2 1334.15 1323.34 47.08 o 12 0 2 110.01 106.18 11.20 o 13 0 2 1482.50 1538.13 72.92 o 14 0 2 37.62 16.80 11.20 o 15 0 2 1233.24 1053.27 61.78 o 16 0 2 1155.24 1457.72 112.30 o 17 0 2 110.00 140.25 16.86 o 18 0 2 480.24 488.52 44.98 o -18 1 2 9.08 16.92 16.92 o -17 1 2 134.97 128.93 16.80 o -16 1 2 442.26 417.19 33.89 o -15 1 2 9.47 5.61 7.94 o -14 1 2 1146.06 1340.57 67.78 o -13 1 2 1034.13 968.33 33.63 o -12 1 2 514.39 480.78 26.92 o -11 1 2 379.16 369.93 12.96 o -10 1 2 2931.22 2997.35 80.51 o -9 1 2 9.62 7.83 2.50 o -8 1 2 899.18 908.65 17.99 o -7 1 2 1104.10 1306.91 23.87 o -6 1 2 560.66 546.04 16.23 o -5 1 2 15.57 14.60 3.22 o -4 1 2 138.36 156.66 9.09 o -3 1 2 95.44 98.33 4.71 o -2 1 2 9611.74 8868.35 160.48 o -1 1 2 451.71 442.66 7.41 o 0 1 2 914.45 698.76 25.32 o 2 1 2 10570.56 9210.91 127.80 o 3 1 2 430.03 532.11 8.02 o 4 1 2 5946.20 5874.35 85.29 o 5 1 2 3495.46 3799.88 59.85 o 6 1 2 4041.79 4249.08 68.78 o 7 1 2 1083.76 1261.64 22.74 o 8 1 2 2650.14 3010.41 53.46 o 9 1 2 1750.44 1966.46 37.30 o 10 1 2 1153.23 1194.07 25.74 o 11 1 2 1947.34 2053.58 55.52 o 12 1 2 20.22 26.85 6.48 o 14 1 2 939.04 876.76 37.61 o 15 1 2 394.15 370.12 30.52 o 16 1 2 8.31 3.36 11.23 o 17 1 2 240.07 213.80 28.12 o -17 2 2 33.42 31.05 11.96 o -16 2 2 6.43 0.00 11.32 o -15 2 2 32.19 16.92 7.96 o -14 2 2 44.11 54.61 9.35 o -13 2 2 90.20 90.44 7.96 o -12 2 2 860.25 785.47 45.32 o -11 2 2 13.73 30.13 3.75 o -10 2 2 440.70 446.42 13.87 o -9 2 2 1360.34 1349.64 28.60 o -8 2 2 2459.77 2561.74 50.97 o -7 2 2 6193.78 6858.05 117.91 o -6 2 2 799.75 935.73 17.65 o -5 2 2 5160.33 5832.97 169.42 o -4 2 2 494.63 473.40 7.27 o -3 2 2 146.61 118.91 3.12 o -2 2 2 1328.45 1186.64 20.66 o -1 2 2 1945.34 1690.73 33.73 o 0 2 2 1256.15 1248.06 24.00 o 1 2 2 4393.32 3928.40 94.44 o 2 2 2 1601.46 1774.44 69.62 o 3 2 2 33.35 54.09 2.75 o 4 2 2 385.96 428.55 10.75 o 5 2 2 527.48 619.99 10.35 o 6 2 2 2503.18 3092.29 45.67 o 7 2 2 336.25 278.82 5.93 o 8 2 2 348.05 373.73 10.12 o 9 2 2 403.78 388.62 10.57 o 10 2 2 143.79 159.64 7.18 o 11 2 2 585.63 662.74 18.29 o 12 2 2 81.40 73.32 6.51 o 14 2 2 163.24 160.50 11.94 o 15 2 2 235.85 197.51 22.57 o 16 2 2 69.80 91.31 28.29 o -16 3 2 48.87 51.25 12.02 o -15 3 2 59.61 73.67 16.97 o -14 3 2 24.68 34.00 11.32 o -13 3 2 1.18 0.00 5.06 o -12 3 2 76.15 57.03 7.98 o -11 3 2 53.24 54.96 8.40 o -10 3 2 6.97 7.91 3.75 o -9 3 2 14.87 14.15 4.64 o -8 3 2 10.67 12.07 3.01 o -7 3 2 2163.31 2339.30 40.87 o -6 3 2 31.98 26.62 2.78 o -5 3 2 14.50 29.67 3.33 o -4 3 2 1514.15 1618.01 31.23 o -3 3 2 101.36 128.57 2.58 o -2 3 2 218.01 221.67 7.00 o -1 3 2 8.72 9.00 4.24 o 0 3 2 1532.76 1550.41 33.89 o 1 3 2 1127.40 1151.67 20.96 o 2 3 2 706.71 692.23 16.97 o 3 3 2 110.40 118.78 3.46 o 4 3 2 234.79 245.70 5.00 o 5 3 2 244.37 239.38 4.96 o 6 3 2 1938.12 2028.54 38.84 o 7 3 2 203.15 191.14 7.50 o 8 3 2 978.02 1011.41 34.04 o 9 3 2 1607.00 1642.31 41.98 o 10 3 2 583.83 574.09 26.22 o 11 3 2 83.94 64.92 7.96 o 12 3 2 548.73 558.38 20.00 o 13 3 2 0.06 5.64 7.98 o 14 3 2 4.40 11.26 11.26 o 15 3 2 29.97 22.69 22.69 o 16 3 2 60.09 51.03 17.03 o -15 4 2 12.69 -11.32 16.97 o -14 4 2 18.86 22.63 11.32 o -13 4 2 13.81 5.66 8.00 o -12 4 2 101.67 84.75 16.97 o -11 4 2 427.00 344.82 42.41 o -10 4 2 506.29 448.19 18.38 o -9 4 2 77.72 62.89 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104.14 3.04 o 1 5 2 332.04 359.90 7.07 o 2 5 2 0.01 0.84 2.21 o 3 5 2 927.33 977.73 24.29 o 4 5 2 0.02 -0.83 2.28 o 5 5 2 1752.52 1921.85 65.38 o 6 5 2 111.45 116.41 6.70 o 7 5 2 108.66 113.06 6.24 o 8 5 2 391.40 390.48 22.23 o 9 5 2 119.40 129.99 7.34 o 10 5 2 573.96 623.61 49.35 o 11 5 2 563.65 573.81 44.72 o 12 5 2 156.15 168.55 16.72 o 13 5 2 8.93 0.00 9.53 o 14 5 2 391.78 414.96 30.17 o -11 6 2 50.38 40.40 11.54 o -10 6 2 73.81 63.55 11.54 o -9 6 2 196.33 156.02 11.60 o -8 6 2 1254.50 1363.20 81.38 o -7 6 2 230.56 248.20 17.37 o -6 6 2 68.30 54.47 11.52 o -5 6 2 7.42 16.13 4.36 o -4 6 2 802.93 828.31 28.18 o -3 6 2 410.23 477.78 22.05 o -2 6 2 101.87 99.39 5.42 o -1 6 2 12.01 10.87 3.24 o 0 6 2 410.48 410.57 12.67 o 1 6 2 465.33 457.72 17.29 o 2 6 2 2.66 2.02 2.81 o 3 6 2 0.97 4.68 2.76 o 4 6 2 636.89 655.30 19.55 o 5 6 2 97.59 93.80 6.27 o 6 6 2 157.25 147.47 14.66 o 7 6 2 0.74 0.82 4.52 o 8 6 2 345.05 353.15 16.00 o 9 6 2 135.16 146.62 17.17 o 10 6 2 31.12 29.15 11.66 o 11 6 2 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9.27 o -7 2 25 0.99 -6.65 10.73 o -6 2 25 24.32 9.15 8.51 o -5 2 25 203.33 198.92 15.58 o -4 2 25 114.84 116.19 12.92 o -3 2 25 13.95 13.64 7.21 o -2 2 25 123.98 136.53 16.82 o -1 2 25 885.77 1044.10 47.90 o 0 2 25 4.50 14.36 5.03 o 1 2 25 115.08 80.77 8.47 o 2 2 25 0.74 -3.86 6.69 o 3 2 25 114.68 136.55 16.19 o 4 2 25 41.28 47.57 8.35 o 5 2 25 68.35 76.74 9.31 o 6 2 25 122.88 114.14 13.06 o -4 3 25 70.54 66.67 20.49 o -3 3 25 64.77 94.17 13.95 o -2 3 25 24.99 35.59 20.37 o -1 3 25 2.64 5.83 12.37 o 0 3 25 180.88 197.29 18.25 o 1 3 25 33.95 35.03 13.99 o 2 3 25 384.72 389.16 35.03 o 3 3 25 59.96 77.92 13.99 o -7 0 26 235.94 168.36 29.03 o -6 0 26 0.73 0.00 17.37 o -5 0 26 43.41 57.78 17.32 o -4 0 26 9.52 0.00 11.54 o -3 0 26 150.92 190.54 23.15 o -2 0 26 134.12 115.56 17.37 o -1 0 26 6.03 -11.54 11.54 o 0 0 26 44.61 52.01 11.54 o 1 0 26 426.51 548.18 52.01 o 2 0 26 468.89 460.57 51.89 o 3 0 26 201.25 252.60 34.46 o 5 0 26 220.34 325.30 40.00 o 6 0 26 599.70 723.06 74.12 o -6 1 26 116.47 104.95 11.94 o -5 1 26 785.49 763.81 51.26 o -4 1 26 0.05 -2.31 9.61 o -3 1 26 1.22 -6.24 8.92 o -2 1 26 340.99 387.40 25.53 o -1 1 26 406.30 437.06 24.45 o 0 1 26 188.66 195.06 14.28 o 1 1 26 171.54 187.67 13.36 o 2 1 26 177.09 174.15 14.22 o 3 1 26 33.13 40.27 9.96 o 4 1 26 719.76 693.41 44.58 o 5 1 26 28.63 30.67 15.34 o -5 2 26 107.38 122.07 12.09 o -4 2 26 23.89 40.94 10.14 o -3 2 26 215.16 228.14 15.60 o -2 2 26 133.34 172.55 13.52 o -1 2 26 35.45 35.25 8.59 o 0 2 26 14.03 5.80 17.40 o 1 2 26 1.60 11.63 8.46 o 2 2 26 84.79 83.40 9.76 o 3 2 26 83.29 82.57 11.86 o 4 2 26 15.68 4.93 8.36 o -4 1 27 121.43 135.76 16.33 o -3 1 27 4.27 8.66 14.43 o -2 1 27 98.93 107.37 11.97 o -1 1 27 4.94 7.27 7.43 o 0 1 27 1511.60 1755.42 164.31 o 1 1 27 136.88 147.14 13.35 o 2 1 27 103.31 101.98 11.90 o 3 1 27 63.47 57.99 11.34 o -1 2 27 0.33 -5.01 8.56 o 0 2 27 38.62 33.27 10.53 o