#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/32/2013221.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013221_Fobs loop_ _publ_author_name 'Clarke, Rachael' 'Latham, Kay' 'Rix, Colin' 'White, Jonathan' _publ_section_title ; Two polymorphs of bis(1,10-phenanthroline-\k^2^N,N')copper(I) iodide ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m7 _journal_page_last m9 _journal_volume 59 _journal_year 2003 _space_group_IT_number 50 _symmetry_space_group_name_Hall '-P 2ab 2b' _symmetry_space_group_name_H-M 'P b a n :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.2150 _cell_length_b 7.4582 _cell_length_c 9.4927 _exptl_crystal_F_000 540.00 _reflns_d_resolution_high 0.7685 _[local]_cod_data_source_file ta1392Iasup2.hkl _[local]_cod_data_source_block Ia #BEGIN Tags that were not found in dictionaries: _shelx_title ' cuip1a in Pban' _shelx_refln_list_code 4 _shelx_f_calc_maximum 206.59 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' 'x, -y+1/2, -z' '-x+1/2, y, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z' '-x, y-1/2, z' 'x-1/2, -y, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 628.24 654.03 11.98 o 4 0 0 8299.06 7676.85 58.47 o 6 0 0 8482.77 7945.75 71.75 o 8 0 0 9114.46 9503.62 91.21 o 10 0 0 7432.95 8084.49 95.31 o 12 0 0 1580.24 1769.65 50.33 o 14 0 0 834.70 951.42 41.04 o 16 0 0 509.55 647.85 37.56 o 18 0 0 250.21 333.76 30.30 o 1 1 0 3.41 16.90 2.12 o 3 1 0 2848.77 3044.03 212.92 o 5 1 0 3263.65 3265.51 119.17 o 7 1 0 1064.58 972.93 37.60 o 9 1 0 479.44 443.36 12.15 o 11 1 0 253.53 225.50 10.37 o 13 1 0 1208.69 1258.54 31.84 o 15 1 0 107.81 183.35 25.89 o 17 1 0 22.20 15.35 12.81 o 0 2 0 42679.20 42707.40 1049.52 o 2 2 0 8862.17 8681.01 308.52 o 4 2 0 7432.80 7437.91 596.05 o 6 2 0 7380.63 7018.45 517.07 o 8 2 0 6352.06 5669.98 445.32 o 10 2 0 3338.72 2741.89 288.23 o 12 2 0 1264.81 1076.79 82.88 o 14 2 0 919.65 806.27 75.97 o 16 2 0 371.64 391.07 31.87 o 18 2 0 132.84 93.47 16.62 o 1 3 0 2848.88 2713.14 55.12 o 3 3 0 85.93 88.90 7.73 o 5 3 0 38.27 40.14 5.61 o 7 3 0 1064.63 1136.15 126.75 o 9 3 0 244.70 210.88 21.60 o 11 3 0 84.40 77.13 10.24 o 13 3 0 107.63 99.56 12.29 o 15 3 0 57.67 49.47 19.07 o 17 3 0 16.72 10.49 10.64 o 0 4 0 1899.13 1810.63 33.15 o 2 4 0 5018.67 4772.51 103.83 o 4 4 0 3024.80 3023.07 204.18 o 6 4 0 4698.30 4536.39 521.85 o 8 4 0 1181.74 1126.63 139.23 o 10 4 0 731.29 700.06 92.26 o 12 4 0 528.82 474.79 50.49 o 14 4 0 439.59 455.68 21.93 o 16 4 0 191.12 69.52 27.50 o 1 5 0 442.24 403.24 12.19 o 3 5 0 272.40 240.93 18.79 o 5 5 0 81.61 104.51 11.19 o 7 5 0 471.25 448.20 62.73 o 9 5 0 100.85 127.27 27.43 o 11 5 0 71.17 64.85 12.88 o 13 5 0 15.63 15.41 10.47 o 15 5 0 13.50 14.43 12.44 o 0 6 0 690.32 651.86 22.56 o 2 6 0 612.28 607.60 15.54 o 4 6 0 517.10 494.50 19.25 o 6 6 0 862.10 877.91 92.28 o 8 6 0 160.27 200.20 32.51 o 10 6 0 150.48 198.26 29.14 o 12 6 0 118.06 120.92 16.46 o 14 6 0 62.66 64.97 16.46 o 1 7 0 42.82 51.16 7.81 o 3 7 0 39.83 56.30 9.71 o 5 7 0 4.56 14.23 7.02 o 7 7 0 38.98 59.14 13.79 o 9 7 0 14.25 10.26 9.63 o 11 7 0 14.88 23.25 11.88 o 0 8 0 20.56 26.25 9.95 o 2 8 0 96.32 95.60 12.09 o 4 8 0 55.40 80.57 12.17 o 6 8 0 38.71 69.05 16.94 o 8 8 0 40.02 42.62 13.29 o 10 8 0 8.85 15.90 12.50 o 1 9 0 8.51 12.25 9.28 o 3 9 0 0.02 6.04 7.63 o 5 9 0 6.90 10.15 9.77 o 0 0 1 4599.69 4935.41 52.14 o 2 0 1 4589.72 5548.16 775.25 o 4 0 1 5201.34 5687.66 315.42 o 6 0 1 1303.09 1307.84 20.59 o 8 0 1 137.76 143.08 6.32 o 10 0 1 138.01 136.63 7.22 o 12 0 1 517.13 551.06 24.96 o 14 0 1 83.41 121.14 16.68 o 16 0 1 67.14 99.36 14.89 o 18 0 1 42.68 101.48 24.18 o 1 1 1 21512.04 23448.47 794.81 o 2 1 1 2560.02 2836.40 89.44 o 3 1 1 18809.21 20058.01 699.34 o 4 1 1 120.76 136.02 5.37 o 5 1 1 11747.91 11814.41 592.59 o 6 1 1 305.25 339.92 17.28 o 7 1 1 6180.10 5953.84 359.20 o 8 1 1 0.71 1.89 2.48 o 9 1 1 5366.24 5386.71 160.13 o 10 1 1 60.08 77.46 6.49 o 11 1 1 4899.85 5051.70 121.15 o 12 1 1 219.42 215.69 9.47 o 13 1 1 693.15 695.00 23.59 o 14 1 1 20.48 16.88 5.79 o 15 1 1 613.00 688.35 33.96 o 16 1 1 1.01 1.15 4.95 o 17 1 1 384.52 473.71 26.14 o 18 1 1 0.69 4.22 8.48 o 0 2 1 3883.79 4094.93 151.07 o 1 2 1 13605.68 14221.04 327.11 o 2 2 1 4765.39 5091.04 132.58 o 3 2 1 0.67 3.23 1.17 o 4 2 1 2438.07 2460.56 128.88 o 5 2 1 54.28 66.50 6.05 o 6 2 1 253.19 227.20 12.52 o 7 2 1 443.46 490.60 20.71 o 8 2 1 476.41 444.40 21.24 o 9 2 1 33.25 27.68 3.10 o 10 2 1 131.19 111.53 9.69 o 11 2 1 96.41 86.63 9.59 o 12 2 1 297.64 263.94 11.89 o 13 2 1 11.41 10.59 4.47 o 14 2 1 82.86 96.41 16.49 o 15 2 1 3.33 -0.78 4.11 o 16 2 1 33.62 30.83 7.04 o 17 2 1 8.21 13.26 6.34 o 18 2 1 42.53 39.22 8.44 o 1 3 1 8851.67 8704.57 153.92 o 2 3 1 314.16 339.13 5.50 o 3 3 1 6141.34 6121.91 187.75 o 4 3 1 376.32 424.39 15.33 o 5 3 1 8281.42 8272.76 365.88 o 6 3 1 446.54 510.34 27.50 o 7 3 1 2531.62 2407.04 135.94 o 8 3 1 0.85 8.56 2.74 o 9 3 1 2087.82 1881.53 140.16 o 10 3 1 49.24 57.38 9.31 o 11 3 1 2375.60 2220.21 183.92 o 12 3 1 194.16 162.97 17.68 o 13 3 1 405.00 380.48 22.62 o 14 3 1 13.73 15.75 5.67 o 15 3 1 356.08 329.20 35.57 o 16 3 1 1.05 5.46 6.31 o 17 3 1 191.27 168.53 38.53 o 0 4 1 0.69 7.17 2.79 o 1 4 1 169.53 167.67 4.54 o 2 4 1 954.45 934.44 17.40 o 3 4 1 3.10 3.22 2.22 o 4 4 1 424.76 414.65 16.45 o 5 4 1 7.93 11.63 3.23 o 6 4 1 49.01 59.42 4.99 o 7 4 1 100.63 120.58 6.69 o 8 4 1 286.33 273.36 23.30 o 9 4 1 1.29 4.56 3.86 o 10 4 1 147.05 145.06 15.23 o 11 4 1 4.75 8.89 4.45 o 12 4 1 78.82 81.75 14.65 o 13 4 1 0.12 1.49 4.98 o 14 4 1 30.81 31.53 7.17 o 15 4 1 1.05 3.47 6.95 o 16 4 1 9.36 10.25 7.68 o 1 5 1 1375.93 1288.57 12.45 o 2 5 1 31.24 52.92 4.09 o 3 5 1 1839.52 1746.76 37.47 o 4 5 1 0.16 27.65 4.46 o 5 5 1 1980.15 1913.91 81.54 o 6 5 1 4.32 22.25 4.45 o 7 5 1 610.57 612.15 45.77 o 8 5 1 1.20 15.00 4.79 o 9 5 1 541.92 555.24 56.57 o 10 5 1 1.79 19.31 5.99 o 11 5 1 388.62 361.07 39.21 o 12 5 1 2.61 7.33 5.44 o 13 5 1 196.92 186.16 33.57 o 14 5 1 0.24 2.94 5.82 o 15 5 1 102.16 120.18 33.32 o 0 6 1 302.83 250.47 9.40 o 1 6 1 0.09 -0.74 3.22 o 2 6 1 47.79 52.85 5.09 o 3 6 1 0.24 -2.07 3.28 o 4 6 1 73.51 91.28 6.67 o 5 6 1 11.38 15.98 5.07 o 6 6 1 14.67 22.86 5.48 o 7 6 1 20.70 20.38 5.49 o 8 6 1 59.68 70.65 8.28 o 9 6 1 1.25 4.74 5.77 o 10 6 1 63.38 64.00 8.73 o 11 6 1 0.03 -5.45 5.61 o 12 6 1 14.45 11.50 6.57 o 13 6 1 1.05 -2.52 5.75 o 14 6 1 4.13 3.06 8.51 o 1 7 1 152.78 166.83 8.44 o 2 7 1 1.03 8.56 3.99 o 3 7 1 235.76 256.79 17.85 o 4 7 1 20.16 43.63 6.70 o 5 7 1 268.37 275.16 18.54 o 6 7 1 23.29 30.23 6.78 o 7 7 1 79.53 103.24 9.84 o 8 7 1 1.01 7.31 5.57 o 9 7 1 87.58 104.97 9.93 o 10 7 1 1.33 12.16 6.27 o 11 7 1 24.27 42.76 8.26 o 12 7 1 1.73 1.80 8.12 o 0 8 1 70.49 66.38 10.61 o 1 8 1 12.04 11.64 4.98 o 2 8 1 0.95 9.92 5.28 o 3 8 1 0.46 3.54 5.38 o 4 8 1 11.79 16.42 6.04 o 5 8 1 2.76 6.95 5.15 o 6 8 1 1.96 14.44 5.84 o 7 8 1 3.80 7.85 5.93 o 8 8 1 8.33 17.51 6.42 o 9 8 1 0.75 3.62 7.25 o 10 8 1 9.29 5.13 8.25 o 1 9 1 12.79 26.62 7.59 o 2 9 1 0.10 8.57 6.93 o 3 9 1 17.56 23.83 6.85 o 4 9 1 0.75 5.81 5.94 o 5 9 1 12.14 28.60 7.26 o 6 9 1 1.22 7.78 6.98 o 0 0 2 8038.26 8977.27 58.16 o 2 0 2 23917.29 24736.37 2020.92 o 4 0 2 10540.38 10633.01 1306.19 o 6 0 2 18207.63 21146.46 2815.33 o 8 0 2 4962.11 5080.39 283.19 o 10 0 2 2982.82 3026.34 41.31 o 12 0 2 1791.48 1959.97 108.36 o 14 0 2 1300.74 1507.02 53.65 o 16 0 2 602.18 615.39 200.01 o 18 0 2 108.08 201.87 32.17 o 1 1 2 3907.24 3984.33 229.32 o 2 1 2 43.20 48.37 2.40 o 3 1 2 1018.99 1045.62 66.33 o 4 1 2 519.72 575.64 34.24 o 5 1 2 84.84 117.91 7.61 o 6 1 2 305.62 335.65 16.15 o 7 1 2 1976.16 2134.31 97.54 o 8 1 2 16.38 17.80 2.37 o 9 1 2 375.48 366.55 18.78 o 10 1 2 4.35 5.65 2.74 o 11 1 2 215.79 183.63 12.37 o 12 1 2 13.41 16.16 4.55 o 13 1 2 121.56 138.86 14.02 o 14 1 2 0.16 -1.47 3.28 o 15 1 2 99.90 116.59 16.28 o 16 1 2 1.57 6.66 5.72 o 17 1 2 18.99 32.43 7.62 o 18 1 2 0.13 -3.31 14.27 o 0 2 2 24736.24 25452.25 1818.04 o 1 2 2 433.82 448.93 19.52 o 2 2 2 8979.72 8668.16 389.33 o 3 2 2 325.02 327.18 15.97 o 4 2 2 7125.35 7541.78 277.64 o 5 2 2 0.48 11.91 2.23 o 6 2 2 8854.17 9314.49 468.62 o 7 2 2 413.37 470.58 23.46 o 8 2 2 3951.55 3628.07 173.15 o 9 2 2 0.08 5.32 2.09 o 10 2 2 2831.78 2615.23 115.83 o 11 2 2 63.28 60.86 6.33 o 12 2 2 1144.40 1037.81 80.36 o 13 2 2 3.07 0.36 3.78 o 14 2 2 752.69 703.63 56.25 o 15 2 2 1.25 5.97 6.00 o 16 2 2 415.99 491.64 34.35 o 17 2 2 5.53 2.14 7.24 o 1 3 2 171.46 167.82 5.42 o 2 3 2 243.89 238.71 7.04 o 3 3 2 846.10 813.67 30.63 o 4 3 2 70.30 79.14 3.80 o 5 3 2 488.87 416.84 24.73 o 6 3 2 115.94 118.85 7.54 o 7 3 2 552.73 523.38 35.26 o 8 3 2 18.40 19.73 2.78 o 9 3 2 232.68 205.52 13.34 o 10 3 2 24.55 26.04 4.13 o 11 3 2 1.57 3.14 3.45 o 12 3 2 164.04 133.12 11.90 o 13 3 2 274.44 209.46 27.30 o 14 3 2 11.96 13.79 5.42 o 15 3 2 44.90 46.26 9.62 o 16 3 2 3.69 4.72 5.61 o 17 3 2 15.54 17.53 8.71 o 0 4 2 10385.13 9922.98 326.60 o 1 4 2 2113.15 2055.28 36.89 o 2 4 2 1960.69 1943.15 36.47 o 3 4 2 0.13 11.82 2.35 o 4 4 2 2650.64 2602.51 69.92 o 5 4 2 15.40 35.93 4.11 o 6 4 2 1849.57 1827.20 93.52 o 7 4 2 11.84 39.92 5.22 o 8 4 2 1731.23 1671.86 101.13 o 9 4 2 27.22 51.70 5.94 o 10 4 2 1122.02 957.65 102.64 o 11 4 2 40.42 37.38 6.39 o 12 4 2 434.53 381.36 32.17 o 13 4 2 0.23 6.87 4.36 o 14 4 2 240.38 188.62 29.78 o 15 4 2 0.78 1.56 4.92 o 16 4 2 131.23 96.69 21.37 o 1 5 2 177.62 172.16 5.63 o 2 5 2 77.35 76.36 4.58 o 3 5 2 115.58 123.99 5.32 o 4 5 2 3.81 2.03 3.31 o 5 5 2 214.06 201.68 10.82 o 6 5 2 0.44 -1.13 3.49 o 7 5 2 102.58 108.20 12.48 o 8 5 2 1.57 1.01 4.07 o 9 5 2 96.33 97.33 10.73 o 10 5 2 51.94 51.34 7.43 o 11 5 2 5.88 13.62 6.04 o 12 5 2 109.18 93.05 13.91 o 13 5 2 53.93 49.24 12.63 o 14 5 2 11.88 17.37 7.88 o 15 5 2 13.77 6.22 8.57 o 0 6 2 496.72 476.47 13.79 o 1 6 2 241.53 227.32 7.10 o 2 6 2 596.63 584.57 10.88 o 3 6 2 8.75 26.32 4.41 o 4 6 2 551.73 507.91 14.73 o 5 6 2 1.97 21.01 4.97 o 6 6 2 402.11 387.76 23.31 o 7 6 2 0.03 15.91 5.07 o 8 6 2 276.04 277.32 12.39 o 9 6 2 1.43 7.66 5.86 o 10 6 2 134.30 159.46 17.17 o 11 6 2 1.44 9.45 6.70 o 12 6 2 104.82 120.51 19.67 o 13 6 2 0.00 -0.92 6.42 o 14 6 2 62.90 67.86 10.29 o 1 7 2 61.93 66.67 6.33 o 2 7 2 1.30 1.51 3.78 o 3 7 2 18.97 30.99 5.16 o 4 7 2 1.79 -0.15 4.17 o 5 7 2 4.43 13.78 5.01 o 6 7 2 10.01 3.90 4.84 o 7 7 2 28.38 38.19 7.47 o 8 7 2 0.90 6.27 5.64 o 9 7 2 15.11 19.42 7.01 o 10 7 2 5.81 8.32 6.37 o 11 7 2 15.63 15.86 7.48 o 12 7 2 7.09 12.60 8.06 o 0 8 2 18.83 37.64 11.54 o 1 8 2 2.13 10.61 5.54 o 2 8 2 78.27 85.84 8.92 o 3 8 2 0.84 10.27 5.42 o 4 8 2 48.61 59.44 9.13 o 5 8 2 2.70 8.76 5.98 o 6 8 2 52.82 72.66 9.14 o 7 8 2 6.04 22.25 6.46 o 8 8 2 21.73 35.71 7.89 o 9 8 2 0.25 1.78 6.51 o 10 8 2 12.39 10.22 19.20 o 1 9 2 2.79 5.08 6.37 o 2 9 2 0.32 17.99 8.25 o 3 9 2 2.95 -1.11 7.57 o 4 9 2 6.53 7.35 6.79 o 5 9 2 3.30 12.84 6.57 o 6 9 2 12.33 32.36 12.25 o 0 0 3 372.35 388.44 14.32 o 2 0 3 2782.83 3108.45 176.84 o 4 0 3 577.17 520.92 50.13 o 6 0 3 13.97 38.69 8.06 o 8 0 3 1343.42 1427.34 181.39 o 10 0 3 458.93 426.19 45.70 o 12 0 3 135.57 123.73 14.10 o 14 0 3 98.22 142.78 23.40 o 16 0 3 5.74 17.95 13.80 o 1 1 3 11905.01 12857.21 283.83 o 2 1 3 23.45 24.82 2.04 o 3 1 3 10639.50 10650.29 691.78 o 4 1 3 234.00 275.71 16.16 o 5 1 3 16814.76 18071.52 904.19 o 6 1 3 123.16 125.06 7.76 o 7 1 3 3943.38 3912.69 194.16 o 8 1 3 2.16 3.67 1.90 o 9 1 3 3244.49 3324.36 134.56 o 10 1 3 0.42 0.55 2.57 o 11 1 3 2075.62 2017.63 116.83 o 12 1 3 0.22 2.80 3.18 o 13 1 3 1269.84 1159.10 104.67 o 14 1 3 0.44 -0.80 3.90 o 15 1 3 557.73 574.21 69.37 o 16 1 3 0.92 10.28 8.57 o 17 1 3 256.21 308.58 21.22 o 0 2 3 2884.40 3051.89 198.44 o 1 2 3 6.82 8.45 1.31 o 2 2 3 310.84 279.30 10.96 o 3 2 3 21.05 28.51 6.04 o 4 2 3 776.23 768.69 38.21 o 5 2 3 216.17 214.09 8.23 o 6 2 3 136.75 117.04 8.64 o 7 2 3 91.53 95.88 5.16 o 8 2 3 362.93 363.48 18.41 o 9 2 3 7.15 11.25 3.25 o 10 2 3 348.38 329.86 17.73 o 11 2 3 1.00 3.61 3.89 o 12 2 3 154.13 159.94 16.10 o 13 2 3 1.24 5.50 5.30 o 14 2 3 41.40 52.07 8.60 o 15 2 3 0.22 4.20 5.29 o 16 2 3 18.75 32.25 7.80 o 17 2 3 1.24 7.94 13.70 o 1 3 3 4766.82 4581.43 175.73 o 2 3 3 28.13 46.35 3.39 o 3 3 3 6691.34 6581.90 249.62 o 4 3 3 28.34 42.35 2.86 o 5 3 3 4276.09 3915.52 257.83 o 6 3 3 28.14 33.46 3.45 o 7 3 3 2594.78 2214.30 199.90 o 8 3 3 28.74 36.06 5.60 o 9 3 3 2100.75 1928.95 186.98 o 10 3 3 4.76 10.18 3.36 o 11 3 3 852.63 775.20 65.28 o 12 3 3 45.05 36.50 8.61 o 13 3 3 710.66 580.37 50.55 o 14 3 3 3.52 3.36 4.95 o 15 3 3 242.01 203.71 20.00 o 16 3 3 3.54 6.44 5.38 o 17 3 3 142.30 190.20 32.06 o 0 4 3 463.17 485.49 19.61 o 1 4 3 936.14 929.66 20.84 o 2 4 3 133.49 128.86 5.95 o 3 4 3 19.63 13.48 2.61 o 4 4 3 430.91 409.09 13.63 o 5 4 3 24.73 26.88 3.79 o 6 4 3 185.46 165.06 7.98 o 7 4 3 15.63 21.05 4.61 o 8 4 3 102.86 105.87 8.51 o 9 4 3 10.57 12.38 3.82 o 10 4 3 63.93 61.74 8.34 o 11 4 3 42.31 36.83 5.25 o 12 4 3 101.39 91.94 16.96 o 13 4 3 1.04 5.25 4.75 o 14 4 3 20.26 30.57 6.47 o 15 4 3 0.62 -0.90 4.67 o 16 4 3 16.94 10.28 6.97 o 1 5 3 1672.29 1586.43 29.54 o 2 5 3 65.72 86.69 6.18 o 3 5 3 1033.06 1017.95 20.37 o 4 5 3 8.93 25.94 3.76 o 5 5 3 914.66 870.77 36.00 o 6 5 3 5.64 23.44 5.20 o 7 5 3 700.04 651.14 37.29 o 8 5 3 12.13 21.55 5.17 o 9 5 3 466.89 445.32 30.76 o 10 5 3 26.07 40.91 6.31 o 11 5 3 377.61 371.32 35.89 o 12 5 3 107.43 92.34 14.12 o 13 5 3 100.51 100.35 24.66 o 14 5 3 10.51 3.26 7.18 o 15 5 3 74.34 65.62 14.71 o 0 6 3 27.68 29.27 8.73 o 1 6 3 339.61 250.10 8.38 o 2 6 3 200.31 182.50 10.18 o 3 6 3 2.75 7.15 4.02 o 4 6 3 61.63 75.32 7.21 o 5 6 3 2.71 1.02 4.42 o 6 6 3 69.04 73.64 7.47 o 7 6 3 1.49 3.47 4.60 o 8 6 3 31.73 35.65 6.15 o 9 6 3 4.75 1.75 4.94 o 10 6 3 4.63 7.28 5.54 o 11 6 3 8.75 7.58 6.24 o 12 6 3 18.99 23.73 7.24 o 13 6 3 0.21 -6.35 6.35 o 1 7 3 246.13 245.50 16.17 o 2 7 3 0.05 13.99 4.81 o 3 7 3 129.39 154.31 10.50 o 4 7 3 5.89 12.19 5.03 o 5 7 3 63.20 74.95 7.77 o 6 7 3 14.81 12.40 5.40 o 7 7 3 136.56 155.79 10.48 o 8 7 3 0.76 5.38 5.13 o 9 7 3 48.44 78.52 9.95 o 10 7 3 13.15 26.29 7.72 o 11 7 3 82.88 106.76 11.41 o 12 7 3 14.18 22.98 20.86 o 0 8 3 0.76 12.19 8.91 o 1 8 3 8.80 7.12 6.07 o 2 8 3 23.52 33.84 9.42 o 3 8 3 3.89 8.50 5.91 o 4 8 3 2.97 12.19 6.10 o 5 8 3 4.88 15.17 6.06 o 6 8 3 28.91 38.90 6.89 o 7 8 3 15.40 18.23 5.73 o 8 8 3 0.09 3.18 6.64 o 9 8 3 1.38 -1.03 6.82 o 1 9 3 13.56 35.95 9.88 o 2 9 3 0.27 11.08 7.94 o 3 9 3 18.12 37.07 10.53 o 4 9 3 11.62 19.75 9.49 o 5 9 3 1.06 14.27 22.67 o 0 0 4 6186.88 6315.15 65.01 o 2 0 4 13233.89 13845.89 335.04 o 4 0 4 10327.10 10660.15 802.99 o 6 0 4 5728.17 5984.27 629.64 o 8 0 4 4643.24 4594.65 572.31 o 10 0 4 2030.21 1968.87 158.88 o 12 0 4 1291.41 1352.04 147.47 o 14 0 4 803.98 785.12 127.40 o 16 0 4 357.40 351.60 54.01 o 1 1 4 1260.19 1343.26 20.00 o 2 1 4 82.74 84.29 4.34 o 3 1 4 267.36 290.28 15.82 o 4 1 4 82.52 93.09 6.26 o 5 1 4 256.90 220.16 11.72 o 6 1 4 86.63 109.56 6.34 o 7 1 4 486.27 516.97 31.71 o 8 1 4 2.94 4.38 2.70 o 9 1 4 304.27 289.61 17.96 o 10 1 4 16.13 18.65 4.71 o 11 1 4 337.56 313.16 17.97 o 12 1 4 24.46 27.32 5.53 o 13 1 4 21.50 31.62 7.86 o 14 1 4 5.01 7.64 6.42 o 15 1 4 46.67 73.06 14.10 o 16 1 4 0.01 8.51 8.97 o 17 1 4 38.69 50.49 10.93 o 0 2 4 3351.11 3108.58 110.73 o 1 2 4 957.94 1080.97 25.18 o 2 2 4 8273.71 8254.89 429.33 o 3 2 4 36.59 55.64 4.17 o 4 2 4 6748.12 6376.18 473.83 o 5 2 4 21.49 33.77 4.52 o 6 2 4 5941.81 5838.15 451.21 o 7 2 4 41.01 54.41 5.30 o 8 2 4 2303.13 2239.64 130.39 o 9 2 4 11.57 17.74 3.81 o 10 2 4 1353.76 1337.57 80.98 o 11 2 4 1.45 2.45 3.85 o 12 2 4 1052.94 1020.80 55.36 o 13 2 4 0.43 3.88 6.06 o 14 2 4 538.95 522.06 20.25 o 15 2 4 3.62 8.84 6.63 o 16 2 4 297.79 322.11 17.44 o 17 2 4 3.71 -6.39 8.01 o 1 3 4 695.54 636.53 30.55 o 2 3 4 3.63 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9 0.00 -4.13 4.13 o 9 1 9 496.81 475.25 36.20 o 10 1 9 0.25 3.83 4.91 o 11 1 9 181.46 183.31 22.85 o 12 1 9 6.13 5.24 7.05 o 0 2 9 130.90 114.14 12.69 o 1 2 9 44.88 40.20 6.18 o 2 2 9 10.01 12.11 4.61 o 3 2 9 40.85 42.14 5.90 o 4 2 9 65.64 74.10 7.23 o 5 2 9 0.19 3.14 4.26 o 6 2 9 108.25 107.16 15.60 o 7 2 9 51.02 55.94 8.26 o 8 2 9 4.50 6.25 5.01 o 9 2 9 0.59 5.40 4.95 o 10 2 9 22.06 34.02 7.63 o 11 2 9 11.61 12.31 7.08 o 12 2 9 12.70 14.64 8.36 o 1 3 9 479.84 514.66 17.57 o 2 3 9 17.04 18.71 6.07 o 3 3 9 753.44 758.81 48.26 o 4 3 9 34.03 28.83 6.65 o 5 3 9 166.13 192.43 15.01 o 6 3 9 50.40 60.04 11.06 o 7 3 9 424.73 441.12 41.52 o 8 3 9 0.20 6.29 5.38 o 9 3 9 209.03 225.20 24.35 o 10 3 9 0.27 5.87 5.63 o 11 3 9 96.34 109.30 16.93 o 0 4 9 54.37 59.90 13.49 o 1 4 9 2.59 2.56 4.64 o 2 4 9 18.30 17.52 4.92 o 3 4 9 0.29 0.01 4.10 o 4 4 9 5.55 14.86 6.25 o 5 4 9 5.80 7.82 5.39 o 6 4 9 61.08 57.35 8.44 o 7 4 9 15.21 21.45 6.68 o 8 4 9 0.88 -0.90 4.39 o 9 4 9 0.18 1.94 4.11 o 10 4 9 24.87 21.00 7.37 o 1 5 9 126.04 170.92 25.72 o 2 5 9 4.41 12.27 7.22 o 3 5 9 147.91 172.86 24.91 o 4 5 9 6.10 7.34 4.77 o 5 5 9 106.29 112.60 12.43 o 6 5 9 1.88 3.41 4.58 o 7 5 9 97.14 97.07 12.53 o 8 5 9 0.05 0.29 5.30 o 0 6 9 11.01 13.35 11.42 o 1 6 9 6.27 6.18 7.54 o 2 6 9 11.46 12.23 8.17 o 3 6 9 0.03 -6.49 7.30 o 4 6 9 1.41 3.54 7.42 o 5 6 9 3.06 -0.03 5.85 o 0 0 10 230.43 260.45 23.55 o 2 0 10 770.64 751.89 27.75 o 4 0 10 700.60 744.77 70.09 o 6 0 10 437.86 439.87 41.53 o 8 0 10 297.45 279.64 28.28 o 10 0 10 113.56 121.20 24.07 o 1 1 10 79.10 81.66 8.20 o 2 1 10 11.02 10.48 4.61 o 3 1 10 14.25 12.32 5.01 o 4 1 10 2.10 3.70 4.41 o 5 1 10 13.52 13.56 5.23 o 6 1 10 0.03 0.76 4.24 o 7 1 10 26.03 24.97 7.19 o 8 1 10 2.31 3.45 5.18 o 9 1 10 11.30 12.17 6.58 o 10 1 10 0.60 8.38 7.83 o 0 2 10 384.77 385.15 20.37 o 1 2 10 3.67 -2.44 3.85 o 2 2 10 525.10 503.06 16.40 o 3 2 10 9.58 6.36 4.65 o 4 2 10 328.41 325.58 18.91 o 5 2 10 3.33 5.30 5.37 o 6 2 10 316.50 335.06 16.66 o 7 2 10 0.76 2.15 4.73 o 8 2 10 216.17 236.64 20.33 o 9 2 10 3.02 -1.47 5.11 o 10 2 10 128.26 150.29 16.51 o 1 3 10 6.47 11.89 5.81 o 2 3 10 2.77 2.57 4.56 o 3 3 10 33.29 36.71 7.70 o 4 3 10 14.85 16.08 6.25 o 5 3 10 50.46 55.60 8.33 o 6 3 10 18.15 19.68 6.57 o 7 3 10 3.62 3.94 5.47 o 8 3 10 1.79 1.39 5.75 o 9 3 10 9.01 8.42 6.61 o 0 4 10 249.48 241.93 26.72 o 1 4 10 1.10 2.56 7.89 o 2 4 10 168.65 191.03 21.96 o 3 4 10 12.04 6.36 5.59 o 4 4 10 102.32 120.76 11.21 o 5 4 10 2.27 4.41 5.62 o 6 4 10 105.30 136.82 20.84 o 7 4 10 29.79 21.41 7.82 o 1 5 10 7.21 9.15 8.87 o 2 5 10 0.16 -5.34 8.06 o 3 5 10 4.05 3.71 8.58 o 4 5 10 25.75 28.97 10.50 o 5 5 10 13.66 13.36 6.69 o 0 0 11 75.22 73.52 15.98 o 2 0 11 12.47 14.16 7.14 o 4 0 11 7.13 6.43 5.72 o 6 0 11 8.05 10.10 6.86 o 8 0 11 10.86 19.97 14.16 o 1 1 11 261.74 267.87 12.77 o 2 1 11 6.98 11.09 5.03 o 3 1 11 313.46 337.04 14.35 o 4 1 11 2.67 3.94 4.08 o 5 1 11 289.96 280.58 19.70 o 6 1 11 0.07 4.80 5.70 o 7 1 11 187.19 204.90 15.31 o 8 1 11 0.11 3.32 10.32 o 0 2 11 32.24 31.40 9.19 o 1 2 11 12.84 9.56 4.86 o 2 2 11 17.57 26.50 6.02 o 3 2 11 0.45 2.94 4.73 o 4 2 11 8.36 4.88 5.50 o 5 2 11 2.53 7.58 6.37 o 6 2 11 1.20 0.67 5.51 o 7 2 11 5.95 4.16 6.48 o 1 3 11 156.36 174.06 13.78 o 2 3 11 0.00 -1.11 4.83 o 3 3 11 123.21 130.60 12.95 o 4 3 11 4.87 0.59 5.66 o 5 3 11 191.85 193.72 15.63 o 6 3 11 5.50 10.53 7.43 o 0 4 11 14.90 11.62 14.32 o 1 4 11 0.42 3.00 8.48 o 2 4 11 4.47 3.39 9.30 o 3 4 11 8.36 2.25 7.29 o 0 0 12 215.71 246.28 26.56 o 2 0 12 125.14 146.53 24.20 o 4 0 12 153.07 181.07 25.47 o 1 1 12 11.76 8.56 5.10 o 2 1 12 0.06 1.48 4.80 o 3 1 12 18.09 19.14 6.32 o 0 2 12 73.65 90.78 18.44 o 1 2 12 0.01 3.72 5.41 o 2 2 12 117.96 100.13 20.49 o