#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013222.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013222_Fobs loop_ _publ_author_name 'Clarke, Rachael' 'Latham, Kay' 'Rix, Colin' 'White, Jonathan' _publ_section_title ; Two polymorphs of bis(1,10-phenanthroline-\k^2^N,N')copper(I) iodide ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m7 _journal_page_last m9 _journal_volume 59 _journal_year 2003 _space_group_IT_number 68 _symmetry_space_group_name_Hall '-C 2a 2ac' _symmetry_space_group_name_H-M 'C c c a :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.2547 _cell_length_b 29.4171 _cell_length_c 18.1262 _exptl_crystal_F_000 4320.00 _reflns_d_resolution_high 0.7379 _[local]_cod_data_source_file ta1392Ibsup3.hkl _[local]_cod_data_source_block Ib #BEGIN Tags that were not found in dictionaries: _shelx_title ' cuip1b in Ccca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 1109.05 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z' 'x+1/2, -y, -z+1/2' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1, -y+1/2, z' 'x+1, -y+1/2, -z+1/2' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z' '-x-1/2, y, z-1/2' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x, y+1/2, -z' '-x, y+1/2, z-1/2' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2869.00 2632.90 72.14 o 4 0 0 119843.67 130152.56 2137.95 o 6 0 0 25.97 -0.79 40.31 o 8 0 0 498766.91 491292.16 9203.94 o 10 0 0 326.70 331.73 82.94 o 12 0 0 20818.72 19444.62 507.53 o 14 0 0 368.01 232.43 96.02 o 16 0 0 32754.48 31344.35 786.93 o 18 0 0 140.71 198.16 110.33 o 20 0 0 877.54 1178.09 186.58 o 0 2 0 334.43 162.51 23.56 o 2 2 0 40370.77 49097.40 574.53 o 4 2 0 0.77 -7.30 24.37 o 6 2 0 306376.75 316805.25 3895.42 o 8 2 0 899.68 1025.43 52.39 o 10 2 0 215968.00 227167.25 3065.31 o 12 2 0 3.25 -63.47 63.47 o 14 2 0 30119.83 27974.26 490.84 o 16 2 0 11.89 -63.76 63.76 o 18 2 0 8335.40 8133.27 252.83 o 20 2 0 16.30 227.40 110.78 o 22 2 0 1223.38 1363.93 383.27 o 0 4 0 1001.74 1611.65 53.21 o 2 4 0 1281.90 1359.75 32.58 o 4 4 0 788656.63 776295.31 8869.40 o 6 4 0 5.68 6.04 17.55 o 8 4 0 4259.12 3623.58 95.15 o 10 4 0 2656.85 2472.46 90.69 o 12 4 0 112946.75 109352.66 1543.57 o 14 4 0 59.14 193.04 72.58 o 16 4 0 3049.88 3157.68 154.14 o 18 4 0 218.87 259.42 98.14 o 20 4 0 6704.45 6768.87 379.61 o 0 6 0 3019.20 2837.70 75.38 o 2 6 0 659596.31 696065.06 7963.17 o 4 6 0 783.10 858.49 34.70 o 6 6 0 215933.66 220047.72 2548.04 o 8 6 0 232.41 262.77 29.96 o 10 6 0 127171.70 126888.97 1621.25 o 12 6 0 1264.49 1281.74 96.36 o 14 6 0 35717.54 34460.21 578.90 o 16 6 0 326.06 444.21 117.32 o 18 6 0 6401.81 6168.07 248.38 o 20 6 0 36.55 131.55 113.71 o 0 8 0 944028.19 888500.38 15691.96 o 2 8 0 1758.75 1790.03 46.05 o 4 8 0 202518.39 211880.16 2617.75 o 6 8 0 695.30 629.86 37.56 o 8 8 0 415613.72 419497.28 5164.80 o 10 8 0 2117.00 2194.30 180.55 o 12 8 0 2619.82 2439.28 135.34 o 14 8 0 116.72 193.76 86.67 o 16 8 0 23532.33 22707.34 490.79 o 18 8 0 76.05 36.17 105.23 o 20 8 0 679.08 642.55 154.75 o 0 10 0 941.47 1010.80 54.04 o 2 10 0 368123.72 381177.06 4379.00 o 4 10 0 56.41 51.91 22.36 o 6 10 0 167153.81 173985.05 2170.02 o 8 10 0 912.86 910.59 52.44 o 10 10 0 115343.35 113761.80 1467.14 o 12 10 0 1258.91 1240.99 114.07 o 14 10 0 29726.59 28165.03 584.88 o 16 10 0 152.28 141.55 99.76 o 18 10 0 8605.98 8204.24 288.58 o 20 10 0 12.40 182.89 104.17 o 0 12 0 20644.71 19223.25 365.42 o 2 12 0 137.33 102.63 23.67 o 4 12 0 401753.03 400159.13 4915.09 o 6 12 0 1588.26 1647.86 86.01 o 8 12 0 30018.12 30182.47 408.19 o 10 12 0 7717.10 8121.99 202.71 o 12 12 0 49191.08 49518.36 847.47 o 14 12 0 35.19 85.18 78.83 o 16 12 0 4046.47 4547.37 213.44 o 18 12 0 218.09 175.29 98.78 o 20 12 0 2753.99 2262.27 305.66 o 0 14 0 73.39 107.83 48.37 o 2 14 0 76024.77 78627.02 1014.05 o 4 14 0 1567.06 1632.71 71.15 o 6 14 0 166927.48 168979.73 2292.26 o 8 14 0 410.03 413.83 60.84 o 10 14 0 4318.65 3730.99 141.34 o 12 14 0 204.42 113.91 94.84 o 14 14 0 18213.58 17318.32 399.06 o 16 14 0 19.09 -16.26 91.49 o 18 14 0 981.55 1185.46 141.50 o 20 14 0 10.09 113.56 301.65 o 0 16 0 274437.53 276633.50 4532.99 o 2 16 0 896.43 983.01 49.97 o 4 16 0 63596.85 66673.91 881.62 o 6 16 0 267.47 351.95 53.93 o 8 16 0 136007.00 139345.59 1931.83 o 10 16 0 1409.71 1372.36 101.72 o 12 16 0 22790.98 21504.08 450.31 o 14 16 0 441.65 494.34 102.16 o 16 16 0 11321.64 11281.31 328.89 o 18 16 0 47.40 -51.66 99.55 o 0 18 0 2152.45 2077.30 104.37 o 2 18 0 182649.63 193752.94 2269.89 o 4 18 0 88.51 58.00 46.44 o 6 18 0 34918.66 33584.00 579.66 o 8 18 0 1015.64 1096.39 89.08 o 10 18 0 26792.13 25784.69 502.55 o 12 18 0 2.72 -41.97 75.91 o 14 18 0 5517.09 5971.53 233.08 o 16 18 0 168.07 157.37 98.02 o 18 18 0 3106.86 3494.02 240.98 o 0 20 0 595.39 499.39 72.53 o 2 20 0 5.02 -30.16 43.58 o 4 20 0 86329.01 86117.73 1234.19 o 6 20 0 186.16 208.12 59.29 o 8 20 0 7208.79 6230.45 183.64 o 10 20 0 177.68 212.81 70.87 o 12 20 0 23296.20 22126.21 476.37 o 14 20 0 21.64 110.21 93.09 o 16 20 0 414.85 644.60 135.88 o 0 22 0 602.55 839.48 145.64 o 2 22 0 45718.99 45070.04 638.72 o 4 22 0 76.57 25.81 50.21 o 6 22 0 38109.87 38718.05 573.74 o 8 22 0 337.57 322.15 66.29 o 10 22 0 9737.55 9568.14 245.28 o 12 22 0 264.20 225.43 85.61 o 14 22 0 6931.36 6720.44 289.01 o 16 22 0 65.08 330.68 137.04 o 0 24 0 73191.05 73276.24 1895.85 o 2 24 0 13.02 -0.34 61.87 o 4 24 0 7691.75 7351.22 197.12 o 6 24 0 138.19 130.84 66.66 o 8 24 0 15408.69 15548.28 301.09 o 10 24 0 371.19 563.97 91.11 o 12 24 0 1760.15 1816.74 147.69 o 14 24 0 181.69 319.18 146.26 o 16 24 0 2225.28 2778.75 315.67 o 0 26 0 0.68 -87.28 87.28 o 2 26 0 16935.01 16598.71 404.36 o 4 26 0 237.40 104.30 69.53 o 6 26 0 11898.29 11142.02 302.69 o 8 26 0 234.19 265.28 98.43 o 10 26 0 8881.82 8754.13 346.40 o 12 26 0 63.29 78.11 102.47 o 14 26 0 515.17 857.51 174.37 o 0 28 0 5321.65 5385.66 286.84 o 2 28 0 0.40 36.46 71.08 o 4 28 0 13709.55 13638.71 339.68 o 6 28 0 25.44 66.47 78.34 o 8 28 0 2481.18 2231.71 177.22 o 10 28 0 119.08 103.95 119.46 o 12 28 0 5377.55 5336.11 266.75 o 14 28 0 30.33 202.28 261.43 o 0 30 0 155.62 131.59 125.30 o 2 30 0 5759.00 5755.51 255.34 o 4 30 0 5.11 68.01 76.15 o 6 30 0 5392.78 6213.76 348.87 o 8 30 0 152.75 52.69 115.00 o 10 30 0 1030.81 1269.97 157.28 o 12 30 0 83.99 33.30 115.24 o 14 30 0 326.24 338.32 270.89 o 0 32 0 6776.81 6431.24 835.16 o 2 32 0 38.85 -18.93 84.45 o 4 32 0 2802.79 2586.79 194.35 o 6 32 0 2.79 3.27 87.25 o 8 32 0 3153.63 2834.10 305.52 o 10 32 0 35.04 70.64 201.10 o 12 32 0 229.40 482.64 262.61 o 0 34 0 4.36 -102.60 237.18 o 2 34 0 1557.41 1498.06 162.93 o 4 34 0 14.23 -86.02 86.02 o 6 34 0 573.49 479.79 122.98 o 8 34 0 7.83 -135.77 135.77 o 10 34 0 1230.25 938.07 286.27 o 0 36 0 613.12 649.38 179.75 o 2 36 0 9.48 -89.96 89.96 o 4 36 0 1206.94 1248.67 165.19 o 6 36 0 15.25 223.31 158.31 o 0 38 0 33.18 -54.42 243.69 o 2 38 0 1446.82 1577.65 212.07 o 4 38 0 14.60 193.35 252.56 o 6 38 0 1024.99 844.62 277.99 o 1 1 1 221.38 875.43 20.12 o 3 1 1 25483.61 27086.71 240.40 o 5 1 1 3.98 88.97 22.80 o 7 1 1 248.27 327.17 22.63 o 9 1 1 2984.60 3314.13 100.83 o 11 1 1 584.16 636.11 54.10 o 13 1 1 628.08 477.13 55.05 o 15 1 1 199.44 197.75 53.96 o 17 1 1 88.70 107.10 53.59 o 19 1 1 251.47 350.39 65.73 o 21 1 1 105.58 177.58 92.79 o 2 2 1 15263.94 18010.38 156.05 o 4 2 1 393.29 619.26 25.58 o 6 2 1 37962.44 38795.15 350.79 o 8 2 1 4481.77 4290.10 87.53 o 10 2 1 13477.70 11123.25 152.38 o 12 2 1 726.01 648.95 58.54 o 14 2 1 6370.49 6256.98 135.91 o 16 2 1 316.48 302.75 56.44 o 18 2 1 1489.25 1421.90 91.72 o 20 2 1 89.57 84.34 72.66 o 1 3 1 1673.21 1682.35 25.79 o 3 3 1 709.78 827.87 20.28 o 5 3 1 76.86 98.31 15.46 o 7 3 1 4930.29 5310.62 85.28 o 9 3 1 7253.70 7537.28 107.24 o 11 3 1 19.26 25.77 37.24 o 13 3 1 700.21 678.06 57.83 o 15 3 1 98.11 34.20 46.09 o 17 3 1 478.13 440.90 65.85 o 19 3 1 138.55 117.05 69.49 o 21 3 1 67.06 -45.43 81.30 o 2 4 1 207.91 645.99 25.76 o 4 4 1 17673.77 17747.18 163.43 o 6 4 1 616.26 672.63 26.32 o 8 4 1 22792.53 25324.34 259.80 o 10 4 1 207.15 198.91 30.96 o 12 4 1 1939.11 1972.57 88.46 o 14 4 1 9.50 -25.02 43.48 o 16 4 1 257.34 221.69 56.23 o 18 4 1 17.60 12.83 64.83 o 20 4 1 261.82 349.85 81.51 o 1 5 1 33537.02 36247.86 315.92 o 3 5 1 79648.20 88867.01 734.57 o 5 5 1 935.74 1069.76 30.63 o 7 5 1 1728.15 1736.47 42.16 o 9 5 1 895.78 756.14 38.78 o 11 5 1 804.86 726.38 53.86 o 13 5 1 915.50 890.21 63.84 o 15 5 1 373.40 515.75 58.14 o 17 5 1 60.49 38.66 59.57 o 19 5 1 172.32 101.06 67.20 o 21 5 1 78.97 46.19 96.28 o 2 6 1 302710.69 329652.44 2852.61 o 4 6 1 806.58 804.37 24.27 o 6 6 1 48993.57 48147.28 417.60 o 8 6 1 1762.23 1682.37 44.85 o 10 6 1 41217.80 40502.00 402.85 o 12 6 1 1282.36 1239.17 65.99 o 14 6 1 3264.76 3261.55 108.11 o 16 6 1 294.30 391.55 65.29 o 18 6 1 1890.49 2009.88 122.45 o 20 6 1 262.00 242.90 75.79 o 1 7 1 105788.42 116697.80 988.69 o 3 7 1 1879.93 1698.31 37.33 o 5 7 1 794.12 820.93 28.75 o 7 7 1 309.14 328.20 23.36 o 9 7 1 43.27 76.04 25.57 o 11 7 1 2194.68 2224.57 76.66 o 13 7 1 254.87 223.44 49.90 o 15 7 1 115.08 133.74 53.32 o 17 7 1 543.87 550.78 77.47 o 19 7 1 125.63 74.96 79.86 o 21 7 1 98.58 63.41 170.06 o 2 8 1 201.24 247.69 19.53 o 4 8 1 646.25 563.58 23.51 o 6 8 1 96.12 74.31 17.48 o 8 8 1 3817.27 3524.57 65.52 o 10 8 1 70.15 55.70 30.60 o 12 8 1 15508.90 14960.28 214.35 o 14 8 1 109.81 68.19 50.98 o 16 8 1 1106.58 1075.10 88.53 o 18 8 1 140.26 66.86 61.67 o 20 8 1 21.56 91.89 75.69 o 1 9 1 596.91 572.66 21.41 o 3 9 1 118.28 142.88 18.48 o 5 9 1 1320.86 1340.11 34.41 o 7 9 1 728.41 803.88 32.16 o 9 9 1 1323.40 1294.97 45.54 o 11 9 1 246.69 279.27 42.85 o 13 9 1 1499.06 1356.09 84.82 o 15 9 1 373.09 345.38 73.23 o 17 9 1 9.82 61.75 59.77 o 19 9 1 72.41 73.72 66.35 o 21 9 1 54.94 424.68 261.43 o 2 10 1 16910.49 16138.93 162.05 o 4 10 1 548.74 578.08 27.63 o 6 10 1 36770.13 36563.74 330.48 o 8 10 1 1045.96 1087.21 38.70 o 10 10 1 71520.79 70360.30 665.63 o 12 10 1 615.39 788.48 71.17 o 14 10 1 742.15 874.15 77.15 o 16 10 1 329.44 524.30 81.66 o 18 10 1 819.38 746.47 97.52 o 20 10 1 33.65 -72.09 72.09 o 1 11 1 64.52 87.36 15.50 o 3 11 1 5014.71 4975.48 77.73 o 5 11 1 1497.28 1640.36 61.25 o 7 11 1 83.75 207.14 23.93 o 9 11 1 2707.23 2744.79 64.97 o 11 11 1 46.77 -2.49 43.48 o 13 11 1 1552.68 1521.44 88.37 o 15 11 1 324.34 219.39 70.97 o 17 11 1 388.85 276.99 71.66 o 19 11 1 8.48 107.87 79.64 o 2 12 1 680.23 670.29 28.66 o 4 12 1 6084.52 6375.09 88.32 o 6 12 1 424.69 463.53 27.07 o 8 12 1 1850.33 1932.39 59.52 o 10 12 1 2277.64 2274.62 78.75 o 12 12 1 903.23 878.49 74.83 o 14 12 1 67.64 -7.39 55.90 o 16 12 1 112.07 37.77 64.05 o 18 12 1 275.51 334.70 77.17 o 20 12 1 25.00 268.25 132.87 o 1 13 1 3104.18 3289.77 67.31 o 3 13 1 324.07 305.49 26.08 o 5 13 1 401.12 465.76 31.76 o 7 13 1 123.08 112.11 28.71 o 9 13 1 427.92 468.51 44.93 o 11 13 1 133.56 221.44 69.44 o 13 13 1 6.00 29.07 53.19 o 15 13 1 106.34 87.10 61.41 o 17 13 1 26.57 28.32 63.85 o 19 13 1 154.17 246.33 87.80 o 2 14 1 89932.17 92664.38 807.61 o 4 14 1 509.46 518.21 30.78 o 6 14 1 27689.73 27055.51 280.99 o 8 14 1 957.39 985.83 48.56 o 10 14 1 42835.88 42344.37 469.39 o 12 14 1 77.99 93.70 53.87 o 14 14 1 2560.86 2546.42 114.37 o 16 14 1 113.92 219.70 70.78 o 18 14 1 303.99 212.20 76.11 o 20 14 1 24.84 -267.23 267.35 o 1 15 1 1633.87 1578.35 41.09 o 3 15 1 4327.41 4484.54 78.11 o 5 15 1 22.38 26.38 25.10 o 7 15 1 312.20 327.30 37.37 o 9 15 1 46.38 21.30 40.05 o 11 15 1 734.20 849.61 63.52 o 13 15 1 257.62 310.42 64.73 o 15 15 1 13.02 67.64 63.17 o 17 15 1 114.02 152.23 72.15 o 19 15 1 13.35 36.01 83.26 o 2 16 1 1803.36 1666.87 48.79 o 4 16 1 389.62 614.92 53.50 o 6 16 1 1052.74 1031.04 49.60 o 8 16 1 1428.15 1575.36 62.03 o 10 16 1 735.43 721.45 60.01 o 12 16 1 1691.09 1843.01 95.43 o 14 16 1 149.03 107.38 61.54 o 16 16 1 301.69 367.52 79.10 o 18 16 1 67.38 18.09 71.74 o 1 17 1 1394.76 1548.56 44.48 o 3 17 1 77.21 9.82 27.62 o 5 17 1 199.83 142.85 35.19 o 7 17 1 276.69 244.41 38.64 o 9 17 1 2668.00 2566.90 87.04 o 11 17 1 8.57 -26.50 42.56 o 13 17 1 369.29 292.57 63.93 o 15 17 1 97.29 63.61 69.08 o 17 17 1 40.23 35.60 69.35 o 19 17 1 65.67 156.15 274.44 o 2 18 1 45816.32 46942.86 453.70 o 4 18 1 164.07 180.16 36.24 o 6 18 1 5341.41 5187.45 113.52 o 8 18 1 504.41 565.64 47.45 o 10 18 1 3289.95 3237.40 115.99 o 12 18 1 63.70 -28.12 51.96 o 14 18 1 1215.02 1131.18 91.01 o 16 18 1 273.92 319.20 74.22 o 18 18 1 306.00 301.68 92.89 o 1 19 1 2345.36 2231.64 60.90 o 3 19 1 676.50 809.04 48.21 o 5 19 1 1356.50 1312.06 57.16 o 7 19 1 1055.09 1130.04 62.93 o 9 19 1 375.03 426.90 55.32 o 11 19 1 429.70 432.77 64.65 o 13 19 1 161.85 215.79 63.96 o 15 19 1 10.64 -49.44 71.35 o 17 19 1 172.54 296.00 82.83 o 19 19 1 4.14 266.16 320.58 o 2 20 1 734.74 813.61 48.52 o 4 20 1 746.28 830.36 55.19 o 6 20 1 222.36 198.21 40.82 o 8 20 1 2050.99 2057.07 77.86 o 10 20 1 38.75 23.51 44.11 o 12 20 1 826.01 714.27 69.72 o 14 20 1 153.03 112.34 70.47 o 16 20 1 196.69 79.75 75.83 o 18 20 1 63.58 150.36 184.84 o 1 21 1 5.26 -3.78 35.32 o 3 21 1 145.17 62.95 36.30 o 5 21 1 1053.69 956.49 55.44 o 7 21 1 192.85 187.03 43.68 o 9 21 1 79.43 79.96 45.39 o 11 21 1 9.37 -48.00 48.00 o 13 21 1 148.75 197.30 76.01 o 15 21 1 11.10 -51.99 79.25 o 17 21 1 23.28 179.52 86.05 o 2 22 1 3834.11 4107.53 166.69 o 4 22 1 32.57 -14.50 34.32 o 6 22 1 1168.85 1198.78 71.52 o 8 22 1 53.61 52.13 39.51 o 10 22 1 2890.81 2671.31 99.71 o 12 22 1 221.32 308.68 61.06 o 14 22 1 535.80 561.48 90.55 o 16 22 1 53.10 30.96 83.61 o 1 23 1 268.09 305.92 46.32 o 3 23 1 1230.17 1303.07 61.30 o 5 23 1 6.23 -40.66 40.66 o 7 23 1 997.44 992.51 94.38 o 9 23 1 49.37 60.94 49.75 o 11 23 1 268.00 142.93 56.77 o 13 23 1 85.61 156.35 74.10 o 15 23 1 2.86 -17.05 69.22 o 17 23 1 29.90 149.05 267.35 o 2 24 1 254.82 145.32 44.77 o 4 24 1 49.41 61.51 41.27 o 6 24 1 20.64 17.39 40.77 o 8 24 1 1751.41 1602.07 77.29 o 10 24 1 150.29 167.73 54.39 o 12 24 1 91.98 65.00 62.61 o 14 24 1 134.57 333.59 96.59 o 16 24 1 19.53 113.89 144.94 o 1 25 1 1519.27 1461.47 80.94 o 3 25 1 367.42 320.68 51.88 o 5 25 1 439.59 411.72 50.50 o 7 25 1 21.46 65.29 45.21 o 9 25 1 313.38 470.23 63.03 o 11 25 1 0.91 -55.63 55.63 o 13 25 1 126.28 161.85 91.16 o 15 25 1 9.12 38.70 89.33 o 2 26 1 1952.98 2003.29 89.05 o 4 26 1 5.40 -43.39 43.39 o 6 26 1 2091.66 2068.14 87.23 o 8 26 1 82.83 171.71 59.14 o 10 26 1 1327.85 1277.94 87.44 o 12 26 1 122.68 197.05 68.73 o 14 26 1 155.16 349.14 101.41 o 16 26 1 0.73 -41.40 246.05 o 1 27 1 396.56 446.54 58.83 o 3 27 1 435.71 524.53 60.38 o 5 27 1 216.23 165.60 56.15 o 7 27 1 310.17 378.51 60.36 o 9 27 1 0.37 -26.47 61.44 o 11 27 1 322.83 191.16 74.84 o 13 27 1 2.51 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