#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/32/2013249.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013249_Fobs loop_ _publ_author_name 'Dielemann, Cedric' 'Matt, Dominique' 'Jones, Peter G.' 'Th\"onnessen, Holger' _publ_section_title ; The host--guest complex between cone-25,26:27,28-bis(methylenedioxy)calix[4]arene and dichloromethane ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o247 _journal_page_last o249 _journal_volume 59 _journal_year 2003 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.490 _cell_angle_gamma 90.000 _cell_length_a 16.0419 _cell_length_b 9.4781 _cell_length_c 17.5992 _exptl_crystal_F_000 1112.00 _reflns_d_resolution_high 0.8410 _[local]_cod_data_source_file bm1530Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 292.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5743.40 5095.69 80.65 o 6 0 0 103.62 113.54 8.36 o 8 0 0 2699.34 2914.77 17.82 o 10 0 0 356.18 273.56 8.25 o 12 0 0 7991.56 8052.89 37.81 o 14 0 0 590.03 502.58 13.09 o 16 0 0 810.81 665.50 15.95 o 3 1 0 705.81 763.40 7.26 o 5 1 0 3089.92 3064.88 10.11 o 7 1 0 779.85 728.37 6.68 o 9 1 0 789.73 723.43 10.41 o 11 1 0 355.18 384.34 9.71 o 13 1 0 137.66 133.09 8.77 o 15 1 0 12.73 28.34 8.54 o 17 1 0 0.23 9.12 8.77 o 0 2 0 1278.90 1399.64 7.72 o 2 2 0 26804.99 24208.66 542.41 o 4 2 0 5011.43 4753.75 56.19 o 6 2 0 1599.02 1623.59 24.59 o 8 2 0 1164.72 1405.96 13.58 o 10 2 0 746.07 787.66 12.06 o 12 2 0 1410.81 1365.64 17.20 o 14 2 0 279.69 309.93 11.20 o 16 2 0 121.19 130.39 10.00 o 1 3 0 4384.09 4390.47 18.77 o 3 3 0 781.92 758.48 11.49 o 5 3 0 398.80 470.29 5.54 o 7 3 0 1272.87 1290.58 9.02 o 9 3 0 3796.87 3868.16 23.65 o 11 3 0 67.40 70.34 7.47 o 13 3 0 0.89 0.88 7.43 o 15 3 0 368.97 385.62 12.88 o 17 3 0 0.36 -0.89 9.55 o 0 4 0 526.64 431.22 7.06 o 2 4 0 1791.84 1769.58 9.09 o 4 4 0 459.67 588.57 6.25 o 6 4 0 987.26 1093.11 8.66 o 8 4 0 552.39 593.97 10.68 o 10 4 0 917.13 955.66 14.47 o 12 4 0 522.32 530.79 12.84 o 14 4 0 1269.21 1303.64 20.33 o 16 4 0 540.74 498.48 15.35 o 1 5 0 3708.13 3984.95 14.65 o 3 5 0 314.81 381.30 5.74 o 5 5 0 11.16 16.81 3.80 o 7 5 0 368.82 359.61 20.98 o 9 5 0 91.80 109.22 7.99 o 11 5 0 320.99 342.59 11.30 o 13 5 0 671.35 585.53 14.76 o 15 5 0 0.83 -4.44 8.87 o 0 6 0 1.02 0.43 4.86 o 2 6 0 330.68 412.83 6.42 o 4 6 0 2927.63 3042.88 30.72 o 6 6 0 18.71 15.16 4.66 o 8 6 0 0.29 -5.99 7.29 o 10 6 0 175.24 171.33 10.02 o 12 6 0 943.78 951.25 17.66 o 14 6 0 19.08 22.91 9.40 o 1 7 0 1019.79 1117.29 14.89 o 3 7 0 634.17 687.61 12.42 o 5 7 0 521.61 499.14 8.42 o 7 7 0 11.06 1.38 5.23 o 9 7 0 85.33 62.97 8.87 o 11 7 0 367.10 354.07 12.62 o 13 7 0 3.37 3.83 9.08 o 0 8 0 303.02 299.50 10.43 o 2 8 0 1237.09 1288.56 12.20 o 4 8 0 2331.76 2267.61 21.55 o 6 8 0 627.70 670.88 19.82 o 8 8 0 2469.67 2430.54 25.70 o 10 8 0 238.69 238.23 12.25 o 12 8 0 94.35 110.04 11.15 o 1 9 0 8.16 9.95 5.54 o 3 9 0 28.71 44.49 6.00 o 5 9 0 114.80 89.02 6.84 o 7 9 0 215.67 211.26 8.27 o 9 9 0 1200.01 1218.05 21.61 o 0 10 0 41.93 23.26 9.16 o 2 10 0 43.58 30.59 6.51 o 4 10 0 2.92 -1.98 6.13 o 6 10 0 25.40 26.11 6.73 o 8 10 0 303.93 313.65 13.73 o 1 11 0 220.02 213.17 13.71 o 3 11 0 0.48 -0.28 6.75 o -17 1 1 69.90 59.95 9.41 o -15 1 1 2.80 0.58 7.78 o -13 1 1 868.35 860.91 14.82 o -11 1 1 13.28 8.29 6.40 o -9 1 1 2630.60 2634.11 18.11 o -7 1 1 3715.88 4175.17 18.70 o -5 1 1 335.25 313.61 3.73 o -3 1 1 24803.42 21625.38 243.53 o 1 1 1 6340.97 6010.84 124.35 o 3 1 1 22255.44 20603.51 357.02 o 5 1 1 10847.16 11606.41 109.99 o 7 1 1 809.18 769.36 7.08 o 9 1 1 47.99 49.88 5.58 o 11 1 1 13.46 14.53 6.61 o 13 1 1 2079.65 1824.36 20.68 o 15 1 1 22.40 22.53 8.44 o 17 1 1 36.47 32.68 9.92 o -16 2 1 81.77 44.68 8.77 o -14 2 1 1904.70 1842.60 21.46 o -12 2 1 946.12 858.38 14.14 o -10 2 1 2720.51 2657.18 19.86 o -8 2 1 6067.43 6249.33 26.36 o -6 2 1 1825.26 1844.59 17.29 o -4 2 1 214.45 199.66 3.22 o -2 2 1 2007.70 2062.77 31.33 o 0 2 1 28990.90 26198.53 1445.55 o 2 2 1 7418.72 7862.54 228.04 o 4 2 1 65.74 73.15 3.22 o 6 2 1 3689.24 3835.33 38.46 o 8 2 1 162.01 171.59 6.75 o 10 2 1 13.62 15.44 6.11 o 12 2 1 998.24 1045.71 15.85 o 14 2 1 1.34 3.42 8.19 o 16 2 1 225.92 221.13 11.98 o -17 3 1 671.54 726.34 17.76 o -15 3 1 1003.80 976.73 17.95 o -13 3 1 269.81 216.60 10.31 o -11 3 1 279.17 255.04 9.10 o -9 3 1 143.84 100.90 6.77 o -7 3 1 679.89 676.03 6.86 o -5 3 1 0.02 5.04 3.56 o -3 3 1 2368.48 2439.61 17.16 o -1 3 1 2309.77 2103.95 42.98 o 1 3 1 13114.02 13276.87 142.69 o 3 3 1 62.50 53.48 2.93 o 5 3 1 80.74 75.06 3.84 o 7 3 1 29.05 40.26 3.82 o 9 3 1 641.42 677.38 11.30 o 11 3 1 207.39 190.55 9.30 o 13 3 1 900.34 919.58 16.26 o 15 3 1 26.69 37.17 9.05 o -16 4 1 696.62 723.43 17.25 o -14 4 1 3.35 8.46 8.27 o -12 4 1 3021.06 3046.01 25.95 o -10 4 1 1387.07 1426.54 16.73 o -8 4 1 484.59 483.56 9.61 o -6 4 1 4716.73 4849.29 16.71 o -4 4 1 1065.63 1168.42 8.13 o -2 4 1 430.33 487.86 5.42 o 0 4 1 668.61 502.42 9.64 o 2 4 1 13387.23 13618.05 132.57 o 4 4 1 2893.14 2892.57 25.46 o 6 4 1 194.86 166.04 11.05 o 8 4 1 97.34 140.17 7.37 o 10 4 1 1067.04 1077.59 15.44 o 12 4 1 449.83 456.60 12.47 o 14 4 1 1434.31 1457.86 21.51 o 16 4 1 122.87 101.44 10.83 o -15 5 1 63.17 72.03 9.96 o -13 5 1 6.44 3.33 8.23 o -11 5 1 718.32 752.74 14.43 o -9 5 1 482.37 470.35 11.28 o -7 5 1 37.94 20.11 4.37 o -5 5 1 20.41 31.21 3.88 o -3 5 1 360.86 451.43 6.02 o -1 5 1 4083.74 4217.21 15.05 o 1 5 1 974.13 879.84 7.61 o 3 5 1 289.62 297.92 5.48 o 5 5 1 0.47 8.77 3.72 o 7 5 1 141.74 130.59 5.31 o 9 5 1 3152.28 3172.55 24.67 o 11 5 1 42.35 45.81 8.25 o 13 5 1 6.68 -0.47 8.34 o 15 5 1 968.53 1019.70 19.61 o -14 6 1 403.84 443.59 14.26 o -12 6 1 346.27 384.22 12.59 o -10 6 1 3393.87 3442.23 27.95 o -8 6 1 1976.25 2011.86 20.15 o -6 6 1 1136.22 1181.35 33.65 o -4 6 1 367.83 397.09 12.78 o -2 6 1 2697.14 2785.89 13.90 o 0 6 1 322.86 334.05 6.79 o 2 6 1 473.22 531.40 7.03 o 4 6 1 636.87 676.85 8.05 o 6 6 1 571.39 586.78 8.21 o 8 6 1 100.56 139.90 8.99 o 10 6 1 17.01 8.64 7.94 o 12 6 1 727.68 772.48 16.51 o 14 6 1 455.56 495.13 15.60 o -13 7 1 53.77 50.60 9.49 o -11 7 1 318.64 348.35 12.37 o -9 7 1 266.05 253.58 10.83 o -7 7 1 25.14 25.23 5.34 o -5 7 1 233.76 215.12 6.63 o -3 7 1 454.16 432.01 7.41 o -1 7 1 73.53 44.39 6.39 o 1 7 1 68.80 48.72 4.82 o 3 7 1 356.78 342.88 6.88 o 5 7 1 298.77 286.89 12.39 o 7 7 1 829.57 871.43 10.76 o 9 7 1 1.81 4.92 8.33 o 11 7 1 1017.21 1078.97 19.30 o 13 7 1 211.10 234.57 12.76 o -12 8 1 5.78 1.07 9.32 o -10 8 1 35.74 25.62 8.95 o -8 8 1 3.39 0.45 8.42 o -6 8 1 75.28 70.39 6.10 o -4 8 1 2181.34 2246.69 43.54 o -2 8 1 459.25 521.28 8.68 o 0 8 1 29.09 29.68 5.45 o 2 8 1 125.68 98.29 6.06 o 4 8 1 1432.34 1342.84 12.90 o 6 8 1 0.07 -0.19 5.59 o 8 8 1 583.86 651.28 15.72 o 10 8 1 510.57 526.30 14.94 o 12 8 1 847.91 806.64 19.12 o -9 9 1 1340.13 1411.12 22.35 o -7 9 1 80.78 76.63 6.95 o -5 9 1 2393.22 2213.82 36.29 o -3 9 1 1.44 3.80 5.67 o -1 9 1 2.02 0.26 5.67 o 1 9 1 74.39 63.88 6.36 o 3 9 1 566.10 462.27 9.41 o 5 9 1 1.36 2.22 5.93 o 7 9 1 47.33 57.47 6.74 o 9 9 1 42.89 39.90 10.08 o -8 10 1 92.94 106.68 11.03 o -6 10 1 606.59 658.34 11.66 o -4 10 1 132.25 122.12 7.28 o -2 10 1 155.02 156.86 7.56 o 0 10 1 90.97 104.66 7.21 o 2 10 1 1267.38 1223.07 24.11 o 4 10 1 0.03 -4.36 6.33 o 6 10 1 307.67 309.49 13.93 o -3 11 1 7.67 10.80 6.56 o -1 11 1 138.17 129.12 12.12 o 1 11 1 14.88 20.67 6.84 o 3 11 1 1.04 0.74 6.66 o -18 0 2 180.97 232.45 12.47 o -16 0 2 81.23 131.73 9.78 o -14 0 2 1425.43 1296.08 17.84 o -12 0 2 1248.73 1165.22 15.31 o -10 0 2 1952.25 2353.03 17.97 o -8 0 2 5628.71 5412.21 23.15 o -6 0 2 5900.29 5546.30 43.16 o -4 0 2 728.61 717.59 19.16 o 2 0 2 1143.41 1243.10 9.54 o 4 0 2 85762.79 66868.53 470.32 o 6 0 2 23137.02 23383.24 277.42 o 8 0 2 1256.41 1145.59 12.43 o 10 0 2 2299.43 2368.59 19.71 o 12 0 2 300.99 353.83 10.76 o 14 0 2 33.71 7.43 7.96 o 16 0 2 1698.01 1771.80 24.32 o -17 1 2 155.74 200.32 11.38 o -15 1 2 741.64 767.41 15.25 o -13 1 2 39.11 22.33 7.35 o -11 1 2 3458.26 3446.94 23.01 o -9 1 2 4574.62 4414.68 22.72 o -7 1 2 135.00 70.98 5.10 o -5 1 2 1043.36 904.07 24.90 o -3 1 2 849.01 841.28 7.22 o -1 1 2 397.30 374.91 2.72 o 1 1 2 2255.82 2088.47 23.40 o 3 1 2 45590.24 37939.38 526.99 o 5 1 2 1007.87 1308.29 7.94 o 7 1 2 116.92 104.48 4.11 o 9 1 2 339.36 387.74 8.95 o 11 1 2 153.66 168.12 8.73 o 13 1 2 176.24 160.62 9.69 o 15 1 2 581.41 613.50 15.19 o -18 2 2 66.46 90.24 10.82 o -16 2 2 0.35 -1.42 8.11 o -14 2 2 47.00 48.49 8.03 o -12 2 2 125.44 120.21 8.09 o -10 2 2 240.45 302.07 8.31 o -8 2 2 3848.20 3696.04 20.33 o -6 2 2 1225.16 1187.66 11.46 o -4 2 2 728.83 698.21 5.43 o -2 2 2 45499.85 38209.44 1591.52 o 0 2 2 31847.96 28468.43 1604.36 o 2 2 2 11391.83 11164.41 396.08 o 4 2 2 1618.96 1595.53 17.17 o 6 2 2 19.76 11.16 10.40 o 8 2 2 575.28 598.58 9.94 o 10 2 2 498.77 507.31 11.01 o 12 2 2 1462.64 1421.93 18.36 o 14 2 2 1300.13 1189.71 18.93 o 16 2 2 5.94 15.11 9.24 o -17 3 2 461.18 455.82 15.09 o -15 3 2 35.39 30.93 8.40 o -13 3 2 15.97 24.94 7.59 o -11 3 2 361.49 370.78 9.88 o -9 3 2 1280.55 1248.17 13.77 o -7 3 2 115.34 134.04 6.09 o -5 3 2 1041.36 978.26 32.91 o -3 3 2 17184.51 16594.54 139.68 o -1 3 2 230.08 245.71 4.52 o 1 3 2 4279.65 4177.20 73.07 o 3 3 2 239.81 187.11 7.51 o 5 3 2 6869.76 7187.81 147.74 o 7 3 2 0.35 15.20 10.50 o 9 3 2 458.18 464.73 10.35 o 11 3 2 570.61 544.54 12.39 o 13 3 2 201.65 143.73 9.98 o 15 3 2 4.45 15.04 8.46 o -16 4 2 1.67 2.06 8.70 o -14 4 2 37.75 36.53 8.46 o -12 4 2 2732.79 2550.06 23.85 o -10 4 2 465.45 516.98 11.28 o -8 4 2 11.07 5.15 5.66 o -6 4 2 230.96 283.34 5.34 o -4 4 2 3406.77 3578.08 13.30 o -2 4 2 137.78 155.81 8.40 o 0 4 2 1965.19 2091.42 39.35 o 2 4 2 719.98 839.09 10.62 o 4 4 2 1878.33 2132.86 16.53 o 6 4 2 3081.99 3278.73 14.65 o 8 4 2 5.22 3.85 6.13 o 10 4 2 406.19 364.30 11.15 o 12 4 2 1156.07 1124.22 17.35 o 14 4 2 353.26 359.16 13.15 o -15 5 2 541.80 528.16 14.80 o -13 5 2 7.28 -0.41 8.11 o -11 5 2 3569.33 3609.87 27.93 o -9 5 2 187.46 180.83 8.70 o -7 5 2 62.22 68.23 14.43 o -5 5 2 987.35 1209.37 28.76 o -3 5 2 324.48 337.00 7.09 o -1 5 2 1181.67 1315.08 14.02 o 1 5 2 5458.82 5805.45 72.26 o 3 5 2 2312.40 2391.45 44.73 o 5 5 2 501.64 538.14 7.00 o 7 5 2 37.45 39.12 4.70 o 9 5 2 242.94 288.05 10.10 o 11 5 2 74.51 89.07 8.79 o 13 5 2 52.91 33.63 8.87 o 15 5 2 23.51 18.03 9.63 o -14 6 2 39.43 34.84 9.34 o -12 6 2 335.53 311.51 11.65 o -10 6 2 5620.52 5644.89 34.82 o -8 6 2 455.80 443.41 11.34 o -6 6 2 56.60 61.53 4.95 o -4 6 2 751.56 810.15 8.51 o -2 6 2 16.68 28.64 4.12 o 0 6 2 318.71 309.45 11.58 o 2 6 2 3594.14 3951.13 16.72 o 4 6 2 3697.75 3823.41 18.29 o 6 6 2 96.89 96.87 9.08 o 8 6 2 16.81 13.17 7.16 o 10 6 2 476.44 456.33 12.96 o 12 6 2 685.15 697.92 16.15 o 14 6 2 55.55 48.03 10.12 o -13 7 2 180.59 204.42 11.55 o -11 7 2 10.91 8.64 8.44 o -9 7 2 243.69 222.73 10.74 o -7 7 2 3.10 0.65 5.21 o -5 7 2 72.68 70.78 6.00 o -3 7 2 477.19 457.52 7.66 o -1 7 2 98.77 108.26 5.39 o 1 7 2 509.75 545.60 8.00 o 3 7 2 38.13 50.31 5.14 o 5 7 2 0.14 -3.07 5.04 o 7 7 2 485.61 448.45 8.74 o 9 7 2 1814.63 1766.04 22.08 o 11 7 2 839.44 862.96 18.29 o 13 7 2 395.44 375.83 14.53 o -12 8 2 86.75 74.87 10.48 o -10 8 2 598.00 611.87 15.29 o -8 8 2 678.49 654.97 15.17 o -6 8 2 945.28 904.14 11.31 o -4 8 2 937.75 1021.39 14.01 o -2 8 2 199.71 186.56 6.72 o 0 8 2 119.27 119.74 6.16 o 2 8 2 1911.87 1832.52 14.42 o 4 8 2 90.45 90.14 6.32 o 6 8 2 25.05 35.95 6.09 o 8 8 2 2144.87 2136.58 24.94 o 10 8 2 134.31 138.38 11.40 o -11 9 2 94.98 95.08 10.85 o -9 9 2 126.21 138.71 11.50 o -7 9 2 742.34 758.59 11.70 o -5 9 2 7.22 0.79 5.98 o -3 9 2 1.71 2.92 5.83 o -1 9 2 1495.69 1425.87 22.01 o 1 9 2 135.25 138.16 6.82 o 3 9 2 0.04 -3.18 5.73 o 5 9 2 175.07 143.87 7.41 o 7 9 2 1.05 9.07 6.27 o 9 9 2 644.74 643.40 16.94 o -8 10 2 101.91 101.60 10.93 o -6 10 2 27.75 29.83 6.88 o -4 10 2 26.92 23.45 6.37 o -2 10 2 45.11 29.72 6.42 o 0 10 2 255.67 233.11 8.33 o 2 10 2 521.72 489.16 10.44 o 4 10 2 186.99 184.82 8.20 o 6 10 2 28.21 18.43 6.64 o -3 11 2 1.87 8.96 6.71 o -1 11 2 16.34 8.84 6.59 o 1 11 2 14.52 29.80 7.81 o -17 1 3 15.40 0.76 8.52 o -15 1 3 26.33 39.51 8.11 o -13 1 3 169.92 144.10 8.46 o -11 1 3 2832.99 2820.56 20.79 o -9 1 3 36.87 40.44 5.33 o -7 1 3 55.44 51.10 4.77 o -5 1 3 275.13 307.98 15.26 o -3 1 3 1273.61 1171.29 5.38 o -1 1 3 17764.25 16785.44 180.23 o 1 1 3 18783.97 17880.40 107.73 o 3 1 3 11120.49 11121.44 101.03 o 5 1 3 92.37 128.44 11.04 o 7 1 3 69.19 133.61 4.48 o 9 1 3 4.04 -2.35 5.62 o 11 1 3 55.12 40.32 7.37 o 13 1 3 253.86 230.00 10.52 o 15 1 3 32.04 37.78 9.10 o -18 2 3 27.38 15.00 9.40 o -16 2 3 0.21 3.64 8.01 o -14 2 3 498.25 487.84 12.45 o -12 2 3 659.09 627.47 11.98 o -10 2 3 5.49 2.98 5.25 o -8 2 3 3737.29 3698.49 20.07 o -6 2 3 7954.00 7473.75 125.92 o -4 2 3 7053.51 6653.16 86.29 o -2 2 3 26113.43 24006.62 455.91 o 0 2 3 10245.75 10539.91 226.29 o 2 2 3 64.39 74.74 3.64 o 4 2 3 25479.98 25345.81 174.38 o 6 2 3 13130.59 13661.08 146.37 o 8 2 3 53.48 72.46 6.15 o 10 2 3 403.35 427.89 10.76 o 12 2 3 66.21 76.23 8.66 o 14 2 3 106.44 74.89 9.08 o 16 2 3 1461.12 1446.48 23.26 o -17 3 3 39.20 58.38 9.82 o -15 3 3 181.11 230.41 10.89 o -13 3 3 2360.87 2481.37 23.40 o -11 3 3 416.45 430.13 10.37 o -9 3 3 1670.96 1519.82 14.84 o -7 3 3 143.21 172.89 6.22 o -5 3 3 2167.18 2212.20 15.27 o -3 3 3 842.19 893.73 26.77 o -1 3 3 5054.33 4961.22 49.88 o 1 3 3 72.54 114.50 3.22 o 3 3 3 1855.08 1968.60 20.26 o 5 3 3 786.79 763.43 12.76 o 7 3 3 15.53 13.77 3.82 o 9 3 3 33.25 53.51 6.83 o 11 3 3 62.12 67.11 8.34 o 13 3 3 307.90 328.88 11.69 o 15 3 3 11.84 18.21 9.34 o -16 4 3 293.84 285.99 12.39 o -14 4 3 274.41 287.83 11.44 o -12 4 3 6317.91 6014.84 35.07 o -10 4 3 5349.21 5349.38 29.84 o -8 4 3 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