#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/32/2013250.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013250_Fobs loop_ _publ_author_name 'Fronczek, Frank R.' 'Girald\'es, Jos\'e' 'McLaughlin, Mark L.' _publ_section_title ; Disordered syn--anti hydrogen-bonded chains in 3-(ferrocenylcarbonyl)propionic acid ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m159 _journal_page_last m161 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.433 _cell_angle_gamma 90.000 _cell_length_a 5.6733 _cell_length_b 26.8920 _cell_length_c 7.7637 _exptl_crystal_F_000 592.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file de1207Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Giraldes11' _shelx_refln_list_code 4 _shelx_f_calc_maximum 189.98 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4049.24 3886.24 108.33 o 4 0 0 734.27 726.53 21.03 o 6 0 0 416.90 390.28 36.04 o 1 1 0 7299.37 6860.07 165.68 o 2 1 0 674.89 687.75 18.03 o 3 1 0 813.22 786.99 18.03 o 4 1 0 1042.49 968.22 22.91 o 5 1 0 67.87 67.94 7.32 o 6 1 0 1046.86 1135.14 45.44 o 7 1 0 29.12 27.78 31.53 o 1 2 0 117.48 125.97 4.13 o 2 2 0 608.83 625.31 15.40 o 3 2 0 114.40 81.28 5.26 o 4 2 0 499.33 539.03 14.83 o 5 2 0 2443.37 2468.87 54.50 o 6 2 0 311.34 259.80 26.09 o 7 2 0 507.63 528.45 52.19 o 1 3 0 36092.68 35137.00 578.16 o 2 3 0 269.17 282.75 8.64 o 3 3 0 2384.95 2295.45 43.82 o 4 3 0 460.75 464.67 11.83 o 5 3 0 1002.11 987.41 25.92 o 6 3 0 3.55 14.26 12.95 o 7 3 0 19.21 9.76 48.42 o 0 4 0 6816.10 6354.65 321.15 o 1 4 0 4133.65 4210.44 71.94 o 2 4 0 31.57 27.78 3.00 o 3 4 0 409.94 376.07 9.58 o 4 4 0 10.56 15.95 5.26 o 5 4 0 1146.21 1163.46 28.17 o 6 4 0 0.07 19.33 18.02 o 7 4 0 218.93 169.12 38.67 o 1 5 0 99.79 93.86 4.13 o 2 5 0 1077.86 1069.89 18.04 o 3 5 0 1163.01 1169.53 21.98 o 4 5 0 805.02 813.68 17.84 o 5 5 0 146.15 143.03 9.76 o 6 5 0 305.22 345.95 37.17 o 7 5 0 5.78 -39.41 52.74 o 0 6 0 26226.19 24818.14 996.14 o 1 6 0 14.25 21.77 2.63 o 2 6 0 2900.44 2756.82 43.50 o 3 6 0 62.03 79.02 6.76 o 4 6 0 1861.28 1814.18 31.95 o 5 6 0 216.26 172.50 11.45 o 6 6 0 88.03 69.26 18.77 o 7 6 0 26.78 -49.55 49.55 o 1 7 0 281.37 297.05 7.14 o 2 7 0 444.43 406.54 10.70 o 3 7 0 466.59 419.45 11.83 o 4 7 0 618.55 622.99 15.21 o 5 7 0 53.98 38.85 8.82 o 6 7 0 631.36 602.65 43.74 o 7 7 0 374.61 335.45 62.88 o 0 8 0 1022.98 988.13 46.25 o 1 8 0 631.23 678.90 11.83 o 2 8 0 1250.09 1199.21 20.86 o 3 8 0 1512.61 1477.39 28.00 o 4 8 0 464.33 490.01 14.64 o 5 8 0 1349.61 1407.36 43.39 o 6 8 0 205.57 204.41 39.61 o 7 8 0 71.51 88.03 51.61 o 1 9 0 13823.82 13723.67 211.27 o 2 9 0 1169.44 1168.21 21.99 o 3 9 0 3053.97 3076.99 69.61 o 4 9 0 161.77 142.66 9.20 o 5 9 0 1211.29 1112.57 31.18 o 6 9 0 21.29 41.29 24.02 o 7 9 0 37.46 80.33 63.63 o 0 10 0 805.21 774.46 23.67 o 1 10 0 6916.32 6917.70 102.00 o 2 10 0 335.92 319.73 9.20 o 3 10 0 1036.94 979.18 21.98 o 4 10 0 136.30 147.16 9.76 o 5 10 0 67.63 80.52 10.51 o 6 10 0 10.60 -11.64 34.91 o 1 11 0 992.25 959.18 18.98 o 2 11 0 589.72 583.45 15.40 o 3 11 0 389.58 438.18 13.33 o 4 11 0 3213.42 3262.23 65.44 o 5 11 0 6.55 16.14 15.77 o 6 11 0 554.22 614.26 92.36 o 0 12 0 7703.78 7451.78 235.65 o 1 12 0 485.20 485.97 14.46 o 2 12 0 12166.63 12549.88 199.72 o 3 12 0 127.78 132.89 8.07 o 4 12 0 4140.42 4229.54 97.65 o 5 12 0 10.94 -15.58 15.58 o 6 12 0 0.96 -7.51 33.60 o 1 13 0 1189.66 1236.75 24.80 o 2 13 0 2696.09 2796.74 54.93 o 3 13 0 624.91 643.48 17.84 o 4 13 0 102.34 110.37 9.76 o 5 13 0 205.13 179.45 17.08 o 6 13 0 493.07 507.43 58.57 o 0 14 0 98.70 94.60 10.70 o 1 14 0 1286.87 1324.53 30.06 o 2 14 0 754.84 719.64 19.53 o 3 14 0 1630.25 1681.63 33.82 o 4 14 0 9.54 -7.70 8.45 o 5 14 0 760.02 844.34 47.13 o 6 14 0 26.10 56.68 33.41 o 1 15 0 10310.36 10364.68 165.28 o 2 15 0 190.33 177.01 10.70 o 3 15 0 2976.00 2992.26 55.29 o 4 15 0 18.38 25.53 12.95 o 5 15 0 139.49 130.07 21.40 o 6 15 0 0.06 -34.16 34.16 o 0 16 0 2759.21 3058.44 104.22 o 1 16 0 1723.70 1838.85 43.79 o 2 16 0 204.55 188.65 10.51 o 3 16 0 269.04 270.12 14.08 o 4 16 0 47.93 48.05 10.89 o 5 16 0 315.08 333.94 26.09 o 6 16 0 15.75 22.15 33.22 o 1 17 0 244.94 245.54 11.08 o 2 17 0 8.41 11.45 7.32 o 3 17 0 88.28 87.47 9.76 o 4 17 0 1035.95 978.95 34.55 o 5 17 0 6.50 9.76 24.40 o 6 17 0 395.31 360.23 59.32 o 0 18 0 3722.97 3815.18 105.59 o 1 18 0 423.44 398.58 12.77 o 2 18 0 3750.94 3863.37 82.41 o 3 18 0 143.90 136.83 13.89 o 4 18 0 1007.97 973.10 40.94 o 5 18 0 179.78 150.35 29.47 o 6 18 0 57.79 67.94 51.80 o 1 19 0 962.68 977.74 24.98 o 2 19 0 762.12 801.43 24.04 o 3 19 0 224.37 192.21 16.71 o 4 19 0 282.81 261.67 23.46 o 5 19 0 27.84 15.95 26.46 o 6 19 0 236.64 233.32 52.74 o 0 20 0 1255.48 1220.24 40.76 o 1 20 0 250.46 248.72 12.58 o 2 20 0 17.42 18.58 12.76 o 3 20 0 251.97 233.51 19.15 o 4 20 0 162.21 154.10 20.46 o 5 20 0 597.41 646.56 39.61 o 1 21 0 2101.10 2153.36 55.06 o 2 21 0 31.73 17.08 15.77 o 3 21 0 3574.85 3680.54 145.18 o 4 21 0 13.00 0.00 18.77 o 5 21 0 7.19 20.65 60.25 o 0 22 0 457.82 435.93 29.10 o 1 22 0 5.09 -12.01 12.01 o 2 22 0 204.54 192.77 15.39 o 3 22 0 2.22 -17.64 17.64 o 4 22 0 2.52 -7.13 19.33 o 5 22 0 1157.37 1199.92 69.29 o 1 23 0 385.53 378.08 18.40 o 2 23 0 79.27 61.00 12.95 o 3 23 0 8.75 33.03 20.27 o 4 23 0 938.91 1006.25 54.83 o 5 23 0 0.06 -24.40 47.11 o 0 24 0 3532.02 3608.81 164.18 o 1 24 0 13.81 15.77 12.57 o 2 24 0 2744.88 2732.98 76.12 o 3 24 0 207.26 194.65 23.84 o 4 24 0 526.14 460.32 41.68 o 5 24 0 5.47 -29.09 30.78 o 1 25 0 967.84 1031.12 37.37 o 2 25 0 1.88 -16.33 16.33 o 3 25 0 146.32 118.06 22.52 o 4 25 0 267.06 350.64 36.04 o 5 25 0 15.27 -30.22 30.22 o 0 26 0 1559.59 1684.94 78.89 o 1 26 0 14.16 26.84 17.45 o 2 26 0 90.92 90.84 20.46 o 3 26 0 396.27 407.92 33.23 o 4 26 0 1.47 -25.53 25.53 o 1 27 0 2011.14 2252.66 93.38 o 2 27 0 0.16 -14.64 20.46 o 3 27 0 1883.47 1731.23 173.20 o 4 27 0 100.11 43.17 26.84 o 0 28 0 369.45 377.88 44.68 o 1 28 0 1.34 -12.39 23.84 o 2 28 0 492.98 477.21 31.73 o 3 28 0 73.47 -21.40 21.40 o 4 28 0 0.87 8.45 29.47 o 1 29 0 516.89 531.28 40.93 o 2 29 0 453.08 422.00 39.61 o 3 29 0 61.98 85.21 31.72 o 4 29 0 137.36 134.20 34.72 o 0 30 0 1679.33 1848.48 135.62 o 1 30 0 131.04 95.16 34.54 o 2 30 0 1373.68 1440.45 63.67 o 3 30 0 25.53 -17.08 41.29 o 1 31 0 117.63 117.68 42.98 o 2 31 0 9.46 -31.16 31.16 o 3 31 0 34.45 45.04 38.66 o 0 32 0 452.20 465.74 68.71 o 1 32 0 19.71 76.76 29.65 o 2 32 0 35.65 37.91 30.03 o 1 33 0 1042.61 1059.21 64.78 o 2 33 0 71.13 58.56 47.67 o 0 34 0 374.64 350.28 60.07 o 1 34 0 16.17 -39.23 39.23 o -7 0 1 1247.02 1497.42 181.03 o -5 0 1 53.42 58.18 7.32 o -3 0 1 11869.19 12252.46 385.79 o -1 0 1 20499.58 20760.63 396.34 o 1 0 1 3952.13 3545.82 98.38 o 3 0 1 132.18 186.20 15.39 o 5 0 1 453.92 443.42 58.38 o 7 0 1 274.29 250.03 82.22 o -7 1 1 165.36 219.98 35.85 o -6 1 1 63.35 48.61 50.68 o -5 1 1 623.42 562.88 14.83 o -4 1 1 1339.62 1389.44 25.55 o -3 1 1 480.99 511.11 12.96 o -2 1 1 19.36 26.09 2.82 o -1 1 1 7561.32 7733.45 97.81 o 1 1 1 10071.93 10124.98 211.37 o 2 1 1 54.27 55.18 5.44 o 3 1 1 543.52 436.38 11.64 o 4 1 1 1045.09 1054.97 31.74 o 5 1 1 1655.64 1665.54 38.70 o 6 1 1 46.33 53.30 16.89 o 7 1 1 33.42 -29.28 39.98 o -7 2 1 231.52 299.20 42.05 o -6 2 1 891.07 856.22 36.05 o -5 2 1 1362.19 1408.94 26.30 o -4 2 1 160.12 154.11 6.76 o -3 2 1 111.37 105.30 3.00 o -2 2 1 1443.52 1359.59 30.46 o -1 2 1 667.37 691.35 11.28 o 1 2 1 1162.82 1112.10 19.38 o 2 2 1 1777.40 1627.32 26.90 o 3 2 1 1611.53 1633.61 30.82 o 4 2 1 2130.12 2115.03 43.04 o 5 2 1 1537.56 1632.75 38.32 o 6 2 1 0.31 -25.34 25.34 o 7 2 1 66.61 54.24 37.73 o -7 3 1 0.21 -8.63 33.41 o -6 3 1 518.40 603.37 45.43 o -5 3 1 19.43 13.33 9.20 o -4 3 1 3417.93 3424.67 59.08 o -3 3 1 1473.16 1556.32 40.97 o -2 3 1 5125.82 4994.50 101.84 o -1 3 1 406.40 437.87 8.27 o 0 3 1 1680.87 1591.61 29.98 o 1 3 1 846.01 846.47 14.47 o 2 3 1 4.14 14.45 3.19 o 3 3 1 550.11 577.96 13.90 o 4 3 1 560.12 556.69 18.02 o 5 3 1 11.89 15.95 12.95 o 6 3 1 1026.00 1132.48 49.39 o 7 3 1 70.30 52.55 31.34 o -7 4 1 155.58 159.35 40.17 o -6 4 1 88.45 99.48 21.02 o -5 4 1 44.99 60.06 13.70 o -4 4 1 44.24 51.80 4.50 o -3 4 1 600.95 624.77 13.52 o -2 4 1 4211.41 4137.88 73.96 o -1 4 1 312.45 306.49 7.51 o 0 4 1 17450.33 17853.32 314.54 o 1 4 1 30.89 46.92 3.75 o 2 4 1 1317.56 1171.23 24.06 o 3 4 1 733.70 730.35 17.28 o 4 4 1 1798.39 1810.12 36.45 o 5 4 1 32.46 47.11 10.14 o 6 4 1 108.86 104.73 22.34 o 7 4 1 145.61 134.02 32.47 o -7 5 1 112.41 89.72 36.41 o -6 5 1 297.29 261.30 34.35 o -5 5 1 1.95 -27.40 27.40 o -4 5 1 1509.82 1443.30 40.77 o -3 5 1 544.55 507.74 12.58 o -2 5 1 348.25 371.77 9.58 o -1 5 1 4969.91 5022.75 90.13 o 0 5 1 4671.31 4624.98 66.92 o 1 5 1 7604.92 7375.89 113.80 o 2 5 1 3008.63 3214.11 57.25 o 3 5 1 481.33 410.44 12.39 o 4 5 1 1287.07 1347.58 27.99 o 5 5 1 543.72 524.92 18.59 o 6 5 1 355.96 330.57 28.53 o 7 5 1 42.88 37.35 24.59 o -7 6 1 774.42 768.45 55.39 o -6 6 1 5.52 -20.27 28.34 o -5 6 1 1116.53 1109.35 38.88 o -4 6 1 29.79 40.92 6.94 o -3 6 1 5312.80 5242.00 95.03 o -2 6 1 385.05 378.35 12.96 o -1 6 1 1382.13 1362.09 24.64 o 0 6 1 540.61 533.38 12.02 o 1 6 1 565.71 548.88 10.71 o 2 6 1 187.80 217.19 6.76 o 3 6 1 496.53 458.13 14.27 o 4 6 1 28.10 24.40 9.20 o 5 6 1 917.42 981.89 26.66 o 6 6 1 0.00 -20.65 26.84 o -7 7 1 28.41 -22.33 40.35 o -6 7 1 344.69 349.53 35.48 o -5 7 1 8.61 15.58 9.01 o -4 7 1 1147.27 1148.77 22.54 o -3 7 1 1203.77 1245.05 27.05 o -2 7 1 184.22 187.35 8.07 o -1 7 1 684.19 644.04 14.09 o 0 7 1 1187.02 1250.22 22.76 o 1 7 1 2977.74 2938.46 53.90 o 2 7 1 88.49 87.84 6.57 o 3 7 1 1898.92 1789.26 35.90 o 4 7 1 1832.09 1858.94 43.59 o 5 7 1 491.54 505.01 19.15 o 6 7 1 297.60 291.33 29.66 o -7 8 1 5.55 -38.10 38.10 o -6 8 1 88.61 111.68 22.90 o -5 8 1 1476.45 1422.50 48.65 o -4 8 1 1399.97 1335.30 30.25 o -3 8 1 102.46 131.58 10.70 o -2 8 1 793.19 730.14 15.59 o -1 8 1 133.73 130.46 6.01 o 0 8 1 70.19 65.88 4.50 o 1 8 1 460.85 466.11 12.58 o 2 8 1 8929.36 9159.55 144.27 o 3 8 1 549.86 579.82 19.90 o 4 8 1 1096.81 1148.48 24.98 o 5 8 1 387.87 410.55 18.96 o 6 8 1 1.33 3.75 18.96 o -7 9 1 6.74 -12.76 35.47 o -6 9 1 830.42 751.79 57.64 o -5 9 1 397.07 404.17 14.83 o -4 9 1 2873.96 2781.23 63.74 o -3 9 1 263.31 295.85 12.39 o -2 9 1 6211.80 6209.32 97.07 o -1 9 1 2388.38 2509.93 47.63 o 0 9 1 1.50 2.82 3.38 o 1 9 1 10.88 27.59 4.50 o 2 9 1 428.84 432.41 11.27 o 3 9 1 12.57 12.95 6.38 o 4 9 1 94.30 94.41 8.82 o 5 9 1 637.11 610.74 29.48 o 6 9 1 609.37 678.11 49.56 o -7 10 1 63.01 54.43 58.00 o -6 10 1 8.23 63.63 31.72 o -5 10 1 532.73 534.87 15.96 o -4 10 1 554.45 548.98 20.84 o -3 10 1 2898.78 2941.60 56.24 o -2 10 1 544.77 483.73 11.45 o -1 10 1 121.13 116.38 7.13 o 0 10 1 8386.55 8255.94 120.23 o 1 10 1 75.68 90.10 6.76 o 2 10 1 1510.63 1469.52 34.39 o 3 10 1 1154.05 1169.33 23.10 o 4 10 1 49.99 40.92 10.89 o 5 10 1 451.51 426.14 23.65 o 6 10 1 93.36 90.47 35.29 o -6 11 1 330.09 287.01 52.94 o -5 11 1 21.72 9.38 13.14 o -4 11 1 183.90 180.01 13.70 o -3 11 1 659.36 636.00 15.40 o -2 11 1 71.08 100.61 6.76 o -1 11 1 17.05 10.32 3.94 o 0 11 1 6.04 4.50 4.32 o 1 11 1 6329.80 6308.26 91.25 o 2 11 1 444.16 449.87 11.64 o 3 11 1 3932.77 4009.65 68.70 o 4 11 1 65.36 50.49 9.38 o 5 11 1 30.56 -27.40 27.40 o 6 11 1 298.75 320.98 49.37 o -6 12 1 16.52 27.97 33.41 o -5 12 1 3688.44 3783.93 103.62 o -4 12 1 0.33 -8.07 8.07 o -3 12 1 1922.02 1922.88 40.41 o -2 12 1 10.02 17.27 8.07 o -1 12 1 259.57 248.75 8.82 o 0 12 1 553.45 559.25 12.77 o 1 12 1 1949.61 2185.24 48.70 o 2 12 1 283.57 295.11 10.51 o 3 12 1 7.08 11.26 8.07 o 4 12 1 471.34 458.26 21.59 o 5 12 1 506.06 552.69 37.73 o 6 12 1 2.19 -28.34 33.22 o -6 13 1 233.10 344.25 44.49 o -5 13 1 146.53 156.73 13.51 o -4 13 1 803.62 792.22 22.91 o -3 13 1 2.30 -3.00 9.57 o -2 13 1 573.07 550.55 16.52 o -1 13 1 4599.41 4461.84 65.60 o 0 13 1 35.23 39.04 5.26 o 1 13 1 5390.13 5477.18 95.82 o 2 13 1 1.53 4.13 6.57 o 3 13 1 1298.03 1391.58 29.49 o 4 13 1 255.40 253.79 15.20 o 5 13 1 105.18 124.82 26.65 o 6 13 1 452.38 451.85 39.61 o -6 14 1 312.62 200.66 45.43 o -5 14 1 563.18 567.35 27.03 o -4 14 1 109.97 118.44 13.33 o -3 14 1 475.08 460.16 17.84 o -2 14 1 360.96 310.71 13.52 o -1 14 1 64.40 65.32 8.63 o 0 14 1 5408.18 5301.62 76.02 o 1 14 1 476.15 490.06 14.27 o 2 14 1 4170.16 4253.82 77.95 o 3 14 1 354.66 354.06 15.58 o 4 14 1 99.40 104.55 12.20 o 5 14 1 1.01 -15.95 16.52 o 6 14 1 7.91 50.30 36.97 o -6 15 1 826.73 940.65 75.29 o -5 15 1 77.61 65.50 16.89 o -4 15 1 2705.31 2837.30 122.94 o -3 15 1 149.27 145.66 11.45 o -2 15 1 2142.98 2162.06 45.31 o -1 15 1 666.68 651.44 15.59 o 0 15 1 724.02 706.14 15.40 o 1 15 1 134.01 136.84 9.39 o 2 15 1 484.38 461.87 14.46 o 3 15 1 113.62 109.62 11.07 o 4 15 1 4.40 9.38 11.07 o 5 15 1 9.25 9.95 26.46 o 6 15 1 669.67 776.12 89.36 o -6 16 1 6.60 26.09 41.10 o -5 16 1 316.90 364.17 32.10 o -4 16 1 2.64 15.20 13.51 o -3 16 1 312.72 313.31 15.77 o -2 16 1 1345.17 1317.70 26.68 o -1 16 1 7.13 4.88 6.38 o 0 16 1 5173.36 5246.53 82.18 o 1 16 1 192.96 221.50 10.89 o 2 16 1 3270.97 3352.78 62.08 o 3 16 1 8.42 18.77 13.14 o 4 16 1 638.93 619.57 29.66 o 5 16 1 540.56 525.28 43.74 o 6 16 1 70.50 61.00 29.28 o -6 17 1 169.50 219.42 50.30 o -5 17 1 175.23 169.87 27.03 o -4 17 1 509.24 511.96 22.15 o -3 17 1 1465.32 1410.98 37.57 o -2 17 1 379.43 388.98 16.33 o -1 17 1 599.57 587.72 17.09 o 0 17 1 46.82 64.75 9.20 o 1 17 1 3983.73 4087.06 62.68 o 2 17 1 607.82 586.19 20.65 o 3 17 1 1943.33 1992.34 43.59 o 4 17 1 39.98 46.73 12.01 o 5 17 1 22.97 -23.27 23.27 o 6 17 1 434.98 416.55 45.24 o -6 18 1 141.47 180.38 44.67 o -5 18 1 2148.97 2313.90 89.43 o -4 18 1 207.36 165.56 15.77 o -3 18 1 704.02 723.83 27.23 o -2 18 1 169.60 158.24 10.32 o -1 18 1 1030.72 1064.59 24.98 o 0 18 1 1549.46 1600.71 34.01 o 1 18 1 47.29 47.49 9.01 o 2 18 1 359.54 368.89 17.27 o 3 18 1 367.34 371.69 21.40 o 4 18 1 6.00 27.59 18.77 o 5 18 1 608.40 652.20 39.61 o 6 18 1 4.52 14.45 28.72 o -6 19 1 74.60 95.91 41.48 o -5 19 1 40.28 36.22 18.77 o -4 19 1 70.02 75.26 15.58 o -3 19 1 367.59 333.21 20.84 o -2 19 1 580.08 569.83 16.71 o -1 19 1 1210.94 1163.49 29.87 o 0 19 1 141.04 153.35 10.89 o 1 19 1 2266.39 2297.59 46.81 o 2 19 1 752.16 783.76 28.54 o 3 19 1 301.37 306.17 19.15 o 4 19 1 3.04 14.08 15.58 o 5 19 1 261.71 279.50 31.53 o -6 20 1 73.78 89.34 46.73 o -5 20 1 42.59 -26.28 26.28 o -4 20 1 6.78 1.88 12.76 o -3 20 1 226.26 193.34 17.46 o -2 20 1 947.48 1021.60 28.36 o -1 20 1 745.34 761.81 26.10 o 0 20 1 2101.34 2086.99 40.60 o 1 20 1 285.76 280.45 15.96 o 2 20 1 1030.62 1096.39 43.95 o 3 20 1 175.90 151.29 17.27 o 4 20 1 160.02 137.96 20.27 o 5 20 1 27.52 27.97 25.15 o -5 21 1 0.26 37.54 35.28 o -4 21 1 1578.71 1635.65 58.79 o -3 21 1 2.81 -5.44 19.89 o -2 21 1 3.71 3.19 9.76 o -1 21 1 1012.88 1021.47 27.42 o 0 21 1 2360.97 2445.48 59.77 o 1 21 1 57.46 65.69 9.95 o 2 21 1 182.01 165.37 15.58 o 3 21 1 70.91 66.82 15.20 o 4 21 1 746.59 688.30 42.62 o 5 21 1 2.01 36.04 27.97 o -5 22 1 202.61 212.48 33.41 o -4 22 1 412.31 339.97 30.79 o -3 22 1 159.06 170.62 18.77 o -2 22 1 290.61 258.48 17.65 o -1 22 1 229.42 212.11 14.45 o 0 22 1 88.11 104.92 12.58 o 1 22 1 65.75 85.21 12.95 o 2 22 1 428.22 433.66 26.66 o 3 22 1 95.19 114.12 19.52 o 4 22 1 557.13 567.15 34.17 o 5 22 1 451.64 485.26 49.37 o -5 23 1 78.74 67.76 33.60 o -4 23 1 144.91 146.22 23.46 o -3 23 1 439.52 385.22 22.90 o -2 23 1 10.31 18.02 14.64 o -1 23 1 255.44 241.21 17.08 o 0 23 1 79.35 77.14 14.83 o 1 23 1 659.95 677.05 23.09 o 2 23 1 311.17 302.41 19.90 o 3 23 1 575.52 600.02 32.10 o 4 23 1 25.33 22.71 32.28 o 5 23 1 130.59 87.09 37.35 o -5 24 1 827.15 873.80 66.84 o -4 24 1 28.43 28.15 25.53 o -3 24 1 488.26 498.43 34.35 o -2 24 1 42.00 36.22 13.14 o -1 24 1 1445.86 1453.11 53.53 o 0 24 1 18.60 40.92 15.77 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