#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:43:51 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180801 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/32/2013251.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013251_Fobs loop_ _publ_author_name 'Qi, Wen-Bin' 'Li, Yi-Zhi' 'Ni, Jun' 'Wang, Zhi-Lin' _publ_section_title ; 1,4,7-Tris(2-cyanoethyl)-4,7-triaza-1-azoniacyclononane perchlorate ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o343 _journal_page_last o345 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.544 _cell_angle_gamma 90.000 _cell_length_a 12.9727 _cell_length_b 9.7075 _cell_length_c 46.0432 _exptl_crystal_F_000 2472.00 _reflns_d_resolution_high 0.8409 _cod_data_source_file de1210Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sad in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 366.01 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 69100.58 72133.46 943.57 o 3 0 0 11169.50 11924.68 137.37 o 4 0 0 1.04 128.51 15.10 o 5 0 0 19967.83 19937.81 264.60 o 6 0 0 4482.33 3823.71 46.12 o 7 0 0 199.49 300.96 24.96 o 8 0 0 174.62 159.19 20.72 o 9 0 0 136.53 125.23 39.74 o 10 0 0 187.58 135.73 31.50 o 11 0 0 5.23 0.00 37.49 o 12 0 0 62.15 61.49 46.49 o 13 0 0 83.60 89.24 56.24 o 14 0 0 22.40 11.25 65.24 o 15 0 0 71.72 67.49 76.49 o 1 1 0 5603.58 5658.93 65.36 o 2 1 0 5459.61 5594.33 67.23 o 3 1 0 4591.69 4668.50 58.96 o 4 1 0 3515.79 3676.88 48.95 o 5 1 0 6655.20 7039.27 74.95 o 6 1 0 7319.50 7495.07 76.30 o 7 1 0 755.47 776.87 18.21 o 8 1 0 3.80 5.50 14.17 o 9 1 0 960.90 958.01 32.92 o 10 1 0 74.55 53.62 26.51 o 11 1 0 59.11 56.03 30.46 o 12 1 0 26.44 25.12 35.00 o 13 1 0 6.57 2.03 36.51 o 14 1 0 133.93 98.50 47.39 o 15 1 0 59.07 69.31 64.39 o 0 2 0 10968.58 10371.02 182.97 o 1 2 0 38412.82 39004.19 719.15 o 2 2 0 15189.76 15305.41 163.20 o 3 2 0 6986.48 6921.62 90.47 o 4 2 0 9620.65 9599.71 101.55 o 5 2 0 34.22 21.58 10.37 o 6 2 0 428.62 596.36 26.84 o 7 2 0 5.14 13.58 13.43 o 8 2 0 102.11 98.07 15.18 o 9 2 0 424.49 424.37 23.04 o 10 2 0 309.87 308.06 22.53 o 11 2 0 52.44 66.02 29.57 o 12 2 0 37.91 61.59 35.64 o 13 2 0 10.81 0.66 34.66 o 14 2 0 21.30 17.38 50.47 o 15 2 0 4.50 0.00 55.19 o 2 3 0 503.47 579.23 44.62 o 3 3 0 724.63 795.46 24.65 o 4 3 0 2014.21 2008.79 37.65 o 5 3 0 322.70 313.66 16.65 o 6 3 0 6079.50 5932.34 71.73 o 7 3 0 3248.00 3673.39 63.47 o 8 3 0 0.02 6.41 13.93 o 9 3 0 137.52 154.79 19.62 o 10 3 0 269.57 327.64 25.77 o 11 3 0 41.78 38.58 25.92 o 12 3 0 211.28 187.59 30.36 o 13 3 0 245.25 261.00 44.62 o 14 3 0 4.55 0.00 49.31 o 0 4 0 527.47 674.15 47.24 o 1 4 0 1043.12 1105.10 90.36 o 2 4 0 1119.55 1199.49 39.67 o 3 4 0 307.69 340.05 22.72 o 4 4 0 671.60 686.92 25.51 o 5 4 0 371.16 364.04 18.49 o 6 4 0 5558.27 5605.34 79.32 o 7 4 0 204.08 178.82 17.58 o 8 4 0 404.20 357.59 21.71 o 9 4 0 32.44 26.61 17.93 o 10 4 0 1.83 12.87 21.59 o 11 4 0 600.78 546.35 48.69 o 12 4 0 15.08 8.95 30.25 o 13 4 0 39.05 16.24 32.49 o 14 4 0 66.05 37.55 48.47 o 1 5 0 575.45 639.11 72.77 o 3 5 0 10.93 10.91 14.20 o 4 5 0 3401.62 3501.87 65.48 o 5 5 0 1246.03 1329.85 36.48 o 6 5 0 34.51 41.96 14.99 o 7 5 0 138.52 162.12 18.67 o 8 5 0 0.39 24.08 19.91 o 9 5 0 35.41 35.19 21.63 o 10 5 0 405.63 465.63 32.46 o 11 5 0 310.83 315.11 30.85 o 12 5 0 129.78 130.17 31.37 o 13 5 0 0.41 0.00 37.79 o 0 6 0 1437.36 1560.58 109.11 o 1 6 0 265.07 274.71 28.19 o 2 6 0 891.38 1103.09 69.74 o 3 6 0 726.73 701.00 36.09 o 4 6 0 0.58 12.97 17.25 o 5 6 0 1705.93 1521.44 36.14 o 6 6 0 184.81 187.99 21.15 o 7 6 0 1478.22 1433.09 40.18 o 8 6 0 7.72 10.40 23.26 o 9 6 0 0.68 0.00 23.85 o 10 6 0 176.63 185.93 28.62 o 11 6 0 16.39 37.92 29.02 o 12 6 0 4.92 9.64 37.82 o 13 6 0 13.39 0.00 53.29 o 1 7 0 6.38 20.07 26.24 o 2 7 0 26.38 43.37 26.05 o 3 7 0 43.70 64.32 26.98 o 4 7 0 390.36 441.19 28.04 o 5 7 0 8.33 0.00 19.33 o 6 7 0 6.52 14.13 22.13 o 7 7 0 247.71 245.65 27.74 o 8 7 0 4.05 0.00 25.74 o 9 7 0 338.24 365.71 34.57 o 10 7 0 3.45 16.11 31.71 o 11 7 0 46.37 54.49 57.00 o 12 7 0 2.11 0.00 56.18 o 0 8 0 89.42 85.76 44.61 o 1 8 0 1655.38 1591.89 66.78 o 2 8 0 1473.33 1546.27 54.76 o 3 8 0 65.77 48.88 23.98 o 4 8 0 95.66 102.44 25.08 o 5 8 0 31.78 59.43 25.44 o 6 8 0 23.37 47.45 32.19 o 7 8 0 6.23 18.13 33.53 o 8 8 0 16.00 0.00 38.85 o 9 8 0 64.49 62.60 54.79 o 10 8 0 1.42 25.86 50.94 o 11 8 0 13.49 12.66 65.29 o 1 9 0 35.24 60.35 41.60 o 2 9 0 96.03 126.15 35.76 o 3 9 0 69.19 59.78 33.30 o 4 9 0 44.77 27.79 33.11 o 5 9 0 42.29 59.58 37.05 o 6 9 0 148.50 156.18 39.95 o 7 9 0 10.65 40.91 50.39 o 8 9 0 32.41 29.38 57.15 o 9 9 0 104.49 141.24 64.10 o 0 10 0 18.64 50.99 80.99 o 1 10 0 6.57 4.39 46.87 o 2 10 0 42.62 54.37 52.66 o 3 10 0 62.63 64.52 55.40 o 4 10 0 42.91 32.30 55.56 o 5 10 0 65.56 49.49 90.74 o 6 10 0 10.45 0.00 107.98 o 7 10 0 30.13 48.74 116.23 o 1 11 0 89.36 122.27 62.70 o 2 11 0 52.33 0.00 104.99 o 3 11 0 208.23 230.97 110.98 o 4 11 0 78.26 84.74 110.23 o -15 1 1 4.40 0.00 53.55 o -14 1 1 8.72 0.00 42.13 o -13 1 1 1.37 0.65 33.82 o -12 1 1 130.24 113.17 34.87 o -11 1 1 504.17 503.35 38.95 o -10 1 1 1031.32 1042.61 49.84 o -9 1 1 922.05 868.02 31.20 o -8 1 1 20.15 13.29 13.66 o -7 1 1 3699.79 3387.23 35.03 o -6 1 1 531.95 536.68 17.90 o -5 1 1 541.65 486.31 11.08 o -4 1 1 40.88 38.14 8.66 o -3 1 1 49529.36 52494.29 577.11 o -2 1 1 26813.14 29304.32 334.23 o -1 1 1 5636.34 6029.16 92.26 o 0 1 1 4446.96 3660.98 53.99 o 1 1 1 2130.14 2148.66 24.96 o 2 1 1 835.66 981.48 19.17 o 3 1 1 39925.91 40611.54 420.95 o 4 1 1 2709.84 2970.31 36.97 o 5 1 1 16112.00 15843.68 131.27 o 6 1 1 1229.86 1586.74 31.76 o 7 1 1 362.09 525.38 19.91 o 8 1 1 5793.03 5746.38 73.50 o 9 1 1 253.01 321.32 25.48 o 10 1 1 82.69 88.77 25.30 o 11 1 1 60.44 93.71 35.24 o 12 1 1 83.68 90.20 33.51 o 13 1 1 116.93 108.78 38.65 o 14 1 1 70.80 80.26 45.81 o 15 1 1 5.42 0.00 57.73 o -15 2 1 7.70 11.24 57.21 o -14 2 1 117.21 124.50 50.30 o -13 2 1 4.27 10.12 36.06 o -12 2 1 2.69 0.00 32.86 o -11 2 1 305.51 317.51 31.71 o -10 2 1 122.76 135.45 19.32 o -9 2 1 1030.77 1033.52 32.03 o -8 2 1 123.62 103.32 14.15 o -7 2 1 1960.21 1835.46 33.54 o -6 2 1 53.01 55.24 11.72 o -5 2 1 14.69 7.76 11.08 o -4 2 1 816.27 800.13 22.73 o -3 2 1 12990.60 13611.03 166.52 o -2 2 1 84.36 119.01 10.86 o 0 2 1 15204.70 16646.88 347.95 o 1 2 1 8858.51 9652.66 151.61 o 2 2 1 3731.52 4072.09 60.81 o 3 2 1 24853.33 24985.79 232.51 o 4 2 1 29.46 28.54 9.79 o 5 2 1 9433.60 9684.79 95.48 o 6 2 1 1210.78 1100.31 17.97 o 7 2 1 634.21 603.82 16.15 o 8 2 1 110.65 103.67 15.26 o 9 2 1 763.08 783.72 28.43 o 10 2 1 497.46 496.64 26.10 o 11 2 1 2620.77 2600.51 78.99 o 12 2 1 492.64 491.90 46.65 o 13 2 1 1.21 17.96 38.18 o 14 2 1 55.58 31.48 46.75 o 15 2 1 5.35 0.00 58.92 o -14 3 1 31.69 30.75 47.62 o -13 3 1 299.02 276.65 48.43 o -12 3 1 83.70 72.72 30.76 o -11 3 1 5.10 14.50 26.28 o -10 3 1 151.22 162.59 21.76 o -9 3 1 24.78 46.06 16.35 o -8 3 1 820.82 742.48 26.84 o -7 3 1 314.13 328.00 19.54 o -6 3 1 0.08 38.13 14.08 o -5 3 1 5173.64 5225.29 68.33 o -4 3 1 306.52 330.90 18.54 o -3 3 1 1561.59 1657.31 35.62 o -2 3 1 1452.53 1435.68 37.12 o -1 3 1 432.54 458.62 22.34 o 1 3 1 6722.55 7451.53 130.41 o 2 3 1 9531.05 9380.34 137.51 o 3 3 1 36.61 32.77 12.38 o 4 3 1 526.77 503.64 17.24 o 5 3 1 241.10 232.23 14.65 o 6 3 1 59.97 51.90 13.07 o 7 3 1 54.09 96.28 15.31 o 8 3 1 1287.49 1430.87 54.44 o 9 3 1 459.79 455.74 32.53 o 10 3 1 77.03 103.34 21.43 o 11 3 1 298.59 305.06 30.77 o 12 3 1 11.22 14.73 30.92 o 13 3 1 12.83 23.63 39.50 o 14 3 1 28.74 14.15 47.03 o -14 4 1 65.57 71.07 45.41 o -13 4 1 12.38 0.00 36.14 o -12 4 1 15.47 37.08 33.34 o -11 4 1 63.14 78.06 24.10 o -10 4 1 99.86 122.75 22.82 o -9 4 1 0.16 10.34 18.54 o -8 4 1 14.52 13.85 16.20 o -7 4 1 71.39 96.77 16.54 o -6 4 1 4327.81 4057.67 57.39 o -5 4 1 0.48 0.00 13.92 o -4 4 1 0.01 5.26 14.52 o -3 4 1 47.10 93.31 15.65 o -1 4 1 855.73 909.46 38.75 o 1 4 1 343.31 310.76 42.70 o 2 4 1 776.05 837.03 32.53 o 3 4 1 902.11 982.87 30.13 o 4 4 1 4878.22 4864.49 67.14 o 5 4 1 4.49 8.05 12.82 o 6 4 1 92.57 112.03 16.34 o 7 4 1 326.54 341.61 20.28 o 8 4 1 248.67 288.03 21.49 o 9 4 1 1218.43 1322.89 39.85 o 10 4 1 240.47 301.67 27.68 o 11 4 1 107.14 89.86 24.16 o 12 4 1 2.22 14.18 31.10 o 13 4 1 22.76 27.31 35.35 o 14 4 1 14.74 30.92 52.19 o -13 5 1 110.20 106.60 39.86 o -12 5 1 3.59 0.00 30.81 o -11 5 1 17.51 14.92 25.49 o -10 5 1 227.05 240.87 28.72 o -9 5 1 266.29 271.54 25.94 o -8 5 1 199.87 224.42 23.14 o -7 5 1 1571.50 1535.11 38.52 o -6 5 1 160.17 138.57 15.64 o -5 5 1 104.17 100.74 18.48 o -4 5 1 2624.85 2851.64 61.61 o -3 5 1 557.93 723.47 31.82 o -1 5 1 826.01 877.19 70.04 o 0 5 1 159.07 159.80 39.74 o 1 5 1 1133.19 1120.37 131.98 o 2 5 1 72.34 55.12 18.56 o 3 5 1 304.27 279.47 19.13 o 4 5 1 21.74 28.85 14.77 o 5 5 1 50.30 28.97 13.75 o 6 5 1 252.02 265.46 19.95 o 7 5 1 179.16 198.44 19.92 o 8 5 1 11.76 17.17 18.51 o 9 5 1 208.82 206.06 24.05 o 10 5 1 151.65 171.86 26.96 o 11 5 1 0.29 0.00 26.75 o 12 5 1 5.72 0.00 31.41 o 13 5 1 24.30 16.78 50.47 o -13 6 1 12.09 33.63 54.08 o -12 6 1 3.06 0.00 30.23 o -11 6 1 0.03 0.00 27.39 o -10 6 1 249.78 238.78 30.02 o -9 6 1 67.87 62.84 24.42 o -8 6 1 40.95 26.84 21.65 o -7 6 1 462.27 485.06 29.19 o -6 6 1 1484.27 1648.10 48.49 o -5 6 1 7.11 9.19 17.59 o -4 6 1 1050.83 980.67 33.75 o -3 6 1 60.71 54.63 21.89 o -2 6 1 328.75 334.16 29.68 o -1 6 1 467.30 340.94 53.97 o 0 6 1 574.98 558.48 31.35 o 1 6 1 1261.13 1567.84 126.73 o 2 6 1 5.14 0.00 21.21 o 3 6 1 2412.23 2333.84 53.74 o 4 6 1 1317.31 1459.76 41.20 o 5 6 1 0.58 1.50 16.87 o 6 6 1 689.77 631.32 32.47 o 7 6 1 9.21 29.60 19.77 o 8 6 1 36.81 26.94 22.23 o 9 6 1 40.67 29.66 24.33 o 10 6 1 22.44 26.50 26.96 o 11 6 1 127.44 132.71 32.04 o 12 6 1 101.90 121.98 41.69 o 13 6 1 34.97 15.43 55.65 o -12 7 1 17.00 13.28 57.15 o -11 7 1 0.60 0.00 41.20 o -10 7 1 2.81 14.52 32.02 o -9 7 1 204.57 229.74 32.68 o -8 7 1 1.78 23.71 27.13 o -7 7 1 319.97 294.68 28.11 o -6 7 1 35.77 15.60 21.21 o -5 7 1 220.64 243.07 25.08 o -4 7 1 59.13 39.96 21.77 o -3 7 1 38.14 22.51 24.12 o -2 7 1 336.75 436.99 37.60 o -1 7 1 393.81 428.18 34.93 o 0 7 1 1018.53 1118.79 46.47 o 1 7 1 221.44 277.17 34.27 o 2 7 1 151.48 146.56 22.28 o 3 7 1 188.56 211.48 25.75 o 4 7 1 17.14 13.22 18.56 o 5 7 1 0.01 3.14 19.43 o 6 7 1 1766.21 1768.97 67.76 o 7 7 1 149.28 142.71 26.17 o 8 7 1 3.01 0.00 25.53 o 9 7 1 163.84 161.67 29.70 o 10 7 1 118.05 128.01 49.77 o 11 7 1 0.81 54.35 57.73 o 12 7 1 20.96 23.09 59.32 o -11 8 1 0.03 0.00 60.75 o -10 8 1 1.54 11.27 48.52 o -9 8 1 272.52 247.79 46.14 o -8 8 1 0.52 0.00 34.00 o -7 8 1 40.89 49.94 34.38 o -6 8 1 33.24 39.83 28.28 o -5 8 1 112.96 97.10 26.43 o -4 8 1 18.92 30.03 20.73 o -3 8 1 65.96 55.65 22.67 o -2 8 1 592.51 587.51 34.28 o -1 8 1 75.91 77.42 23.15 o 0 8 1 479.18 490.02 34.70 o 1 8 1 4.04 17.34 22.44 o 2 8 1 234.54 208.25 27.58 o 3 8 1 358.47 364.71 31.20 o 4 8 1 26.87 34.88 29.94 o 5 8 1 2.63 28.35 31.35 o 6 8 1 192.72 197.36 37.04 o 7 8 1 13.95 0.00 33.79 o 8 8 1 48.91 22.12 49.68 o 9 8 1 23.83 0.00 50.47 o 10 8 1 6.59 0.00 50.62 o 11 8 1 0.33 0.00 60.20 o -9 9 1 2.81 0.00 61.70 o -8 9 1 6.04 11.56 57.00 o -7 9 1 0.37 0.00 39.25 o -6 9 1 5.20 0.00 36.47 o -5 9 1 82.00 60.39 36.07 o -4 9 1 10.31 9.87 36.22 o -3 9 1 73.97 60.74 56.24 o -2 9 1 7.39 46.30 44.16 o -1 9 1 0.03 2.89 38.98 o 0 9 1 745.42 815.13 89.24 o 1 9 1 621.42 612.60 62.23 o 2 9 1 407.55 425.04 48.57 o 3 9 1 100.33 81.36 37.29 o 4 9 1 86.07 96.47 36.40 o 5 9 1 33.42 12.56 38.19 o 6 9 1 4.74 0.00 44.92 o 7 9 1 310.52 358.58 59.45 o 8 9 1 45.92 10.62 59.45 o 9 9 1 95.75 108.00 62.14 o -7 10 1 1.98 42.74 83.99 o -6 10 1 74.62 86.24 101.24 o -5 10 1 65.09 40.16 59.89 o -4 10 1 104.76 109.20 56.67 o -3 10 1 13.01 8.98 54.23 o -2 10 1 342.33 288.61 59.21 o -1 10 1 190.80 217.83 60.10 o 0 10 1 0.72 0.00 46.58 o 1 10 1 35.13 19.18 50.09 o 2 10 1 515.85 583.91 67.29 o 3 10 1 0.03 0.00 51.30 o 4 10 1 0.15 0.00 80.24 o 5 10 1 17.26 25.50 89.99 o 6 10 1 1.01 0.00 125.98 o 7 10 1 2.29 58.49 102.74 o -4 11 1 0.27 35.99 107.98 o -3 11 1 9.37 14.54 69.01 o -2 11 1 2.36 0.00 103.49 o -1 11 1 3.06 0.00 62.57 o 0 11 1 6.56 0.00 59.95 o 1 11 1 2.76 0.00 62.82 o 2 11 1 34.52 0.00 101.24 o 3 11 1 71.44 173.98 122.98 o 4 11 1 12.58 11.25 178.47 o -15 0 2 0.79 0.00 68.24 o -14 0 2 49.53 53.24 60.74 o -13 0 2 477.87 513.68 73.49 o -11 0 2 73.03 140.98 49.49 o -10 0 2 64.64 41.99 34.50 o -9 0 2 2405.52 2344.17 89.99 o -8 0 2 864.28 882.54 34.58 o -7 0 2 71.00 91.24 16.90 o -6 0 2 8713.75 8695.23 229.47 o -5 0 2 2180.96 2241.86 41.95 o -4 0 2 1162.74 1156.51 21.85 o -3 0 2 119747.25 124221.91 1631.31 o -2 0 2 11436.31 13298.53 205.21 o -1 0 2 0.99 2.65 3.95 o 1 0 2 16725.56 18465.37 380.20 o 2 0 2 1259.65 1264.32 23.84 o 3 0 2 18004.66 18913.29 271.18 o 4 0 2 89.92 128.52 13.51 o 5 0 2 77.06 95.03 14.15 o 6 0 2 2030.41 1954.51 64.49 o 7 0 2 4715.10 4983.84 95.54 o 8 0 2 197.94 323.46 29.19 o 9 0 2 70.13 63.74 34.50 o 10 0 2 300.68 280.46 41.99 o 11 0 2 529.38 512.18 55.49 o 12 0 2 361.56 322.45 53.99 o 13 0 2 12.23 18.00 47.99 o 14 0 2 124.38 132.73 64.49 o 15 0 2 104.33 60.74 88.49 o -15 1 2 16.42 0.00 51.14 o -14 1 2 0.18 0.00 43.15 o -13 1 2 133.37 168.89 40.50 o -12 1 2 0.22 0.00 26.37 o -11 1 2 25.99 45.61 31.39 o -10 1 2 1995.18 1995.73 64.88 o -9 1 2 238.57 260.12 20.01 o -8 1 2 144.79 141.59 16.09 o -7 1 2 315.91 397.71 15.99 o -6 1 2 75.14 97.54 10.14 o -5 1 2 1482.87 1472.45 26.83 o -4 1 2 1487.22 1366.93 24.10 o -3 1 2 33856.39 34978.02 374.35 o -2 1 2 110.02 179.28 10.53 o -1 1 2 3511.58 3703.68 59.11 o 0 1 2 3346.74 3738.94 65.20 o 1 1 2 527.88 494.72 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175.92 37.60 o -5 4 29 323.25 313.29 34.80 o -4 4 29 92.18 94.20 23.89 o -3 4 29 301.62 319.66 24.40 o -2 4 29 1233.48 1216.73 36.29 o -1 4 29 7.97 30.09 13.41 o 0 4 29 3.57 6.97 18.02 o 1 4 29 33.89 26.98 18.04 o 2 4 29 46.56 52.46 20.73 o 3 4 29 0.14 0.07 21.07 o 4 4 29 0.55 15.92 22.35 o 5 4 29 109.97 157.74 28.18 o 6 4 29 228.25 210.50 28.96 o 7 4 29 88.41 88.55 27.79 o 8 4 29 0.90 0.00 36.06 o 9 4 29 60.25 29.33 41.48 o 10 4 29 9.69 2.12 49.25 o 11 4 29 27.59 6.59 54.23 o -11 5 29 20.64 24.98 53.80 o -10 5 29 7.40 0.00 41.01 o -9 5 29 7.37 22.38 44.46 o -8 5 29 87.35 52.13 37.24 o -7 5 29 153.66 200.67 47.72 o -6 5 29 1245.78 1147.96 61.16 o -5 5 29 54.45 47.34 33.49 o -4 5 29 146.67 212.30 29.58 o -3 5 29 51.31 55.07 25.35 o -2 5 29 825.76 888.39 40.97 o -1 5 29 1020.47 902.95 47.31 o 0 5 29 734.63 799.41 62.78 o 1 5 29 120.70 116.06 25.27 o 2 5 29 136.87 134.28 25.40 o 3 5 29 74.71 86.45 26.05 o 4 5 29 1.05 8.66 23.61 o 5 5 29 613.93 622.14 38.14 o 6 5 29 92.98 121.59 31.38 o 7 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