#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/32/2013278.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013278_Fobs loop_ _publ_author_name 'Harvey, Miguel' 'Baggio, Sergio' 'Russi, Silvia' 'Baggio, Ricardo' _publ_section_title ; Two new dimeric cadmium(II) and zinc(II) sulfate complexes with 2,4,6-tris(2-pyridyl)-1,3,5-triazine and 2,2:6',2''-terpyridine ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m171 _journal_page_last m174 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 103.356 _cell_angle_beta 98.785 _cell_angle_gamma 110.451 _cell_length_a 8.8699 _cell_length_b 10.6402 _cell_length_c 12.6853 _exptl_crystal_F_000 576.00 _reflns_d_resolution_high 0.8108 _[local]_cod_data_source_file ga1011Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' Cd(SO4)Tpt in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 340.76 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 11692.46 12789.96 182.99 o 2 0 0 2174.36 2234.74 113.04 o 3 0 0 1006.00 1027.52 62.85 o 4 0 0 3043.88 3012.67 185.43 o 5 0 0 1270.11 1330.45 155.01 o 6 0 0 479.84 512.55 135.69 o 7 0 0 15.70 53.52 101.04 o 8 0 0 91.35 95.49 135.02 o 9 0 0 102.54 119.49 115.36 o -10 1 0 92.41 67.24 140.66 o -9 1 0 43.46 35.75 135.24 o -8 1 0 9.34 -31.98 106.60 o -7 1 0 32.77 49.97 93.49 o -6 1 0 1924.52 1980.46 199.87 o -5 1 0 1811.01 1634.25 166.33 o -4 1 0 2741.06 2683.55 174.55 o -3 1 0 487.95 475.02 86.83 o -2 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