#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/32/2013279.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013279_Fobs loop_ _publ_author_name 'Harvey, Miguel' 'Baggio, Sergio' 'Russi, Silvia' 'Baggio, Ricardo' _publ_section_title ; Two new dimeric cadmium(II) and zinc(II) sulfate complexes with 2,4,6-tris(2-pyridyl)-1,3,5-triazine and 2,2:6',2''-terpyridine ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first m171 _journal_page_last m174 _journal_volume 59 _journal_year 2003 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 110.343 _cell_angle_beta 116.590 _cell_angle_gamma 98.831 _cell_length_a 9.7002 _cell_length_b 9.7550 _cell_length_c 10.3240 _exptl_crystal_F_000 420.00 _reflns_d_resolution_high 0.8107 _[local]_cod_data_source_file ga1011IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' Zn(SO4)Tpy in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 207.97 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 68.36 50.64 3.32 o 2 0 0 1982.02 1848.68 45.75 o 3 0 0 3735.97 3780.97 46.27 o 4 0 0 2616.80 2633.04 44.91 o 5 0 0 70.12 74.92 10.06 o 6 0 0 1537.96 1507.67 42.77 o 7 0 0 446.58 470.56 26.89 o 8 0 0 11.18 16.34 12.41 o 9 0 0 30.61 25.91 20.58 o -10 1 0 1.19 7.17 16.17 o -9 1 0 246.84 273.65 43.74 o -8 1 0 60.11 35.29 19.85 o -7 1 0 1220.45 1214.82 40.23 o -6 1 0 708.54 646.43 27.01 o -5 1 0 30.72 19.82 6.92 o -4 1 0 368.91 320.89 15.07 o -3 1 0 5.85 5.98 3.64 o -2 1 0 3673.17 3856.72 63.97 o -1 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