#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2013293.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2013293_Fobs loop_ _publ_author_name 'Domaga\/la, Ma\/lgorzata' 'Linden, Anthony' 'Olszak, Tomasz A.' 'Mlosto\'n, Grzegorz' 'Heimgartner, Heinz' _publ_section_title ; 1,3-Thiazolidine derivatives from regioselective [2+3]-cycloadditions of azomethine ylides with thioketones ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first o250 _journal_page_last o253 _journal_volume 59 _journal_year 2003 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.240 _cell_angle_gamma 90.000 _cell_length_a 15.6658 _cell_length_b 18.1538 _cell_length_c 17.2513 _exptl_crystal_F_000 2071.60 _reflns_d_resolution_high 0.7706 _[local]_cod_data_source_file gg1163VIsup2.hkl _[local]_cod_data_source_block VI #BEGIN Tags that were not found in dictionaries: _shelx_title ' MG225/03/MEOH (HG0305)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 312.83 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 55134.72 57940.79 1404.59 o 6 0 0 994.56 919.02 28.08 o 8 0 0 1290.27 1329.98 38.29 o 10 0 0 3.26 40.78 15.29 o 12 0 0 980.41 874.93 48.47 o 14 0 0 1152.57 1267.78 79.08 o 16 0 0 220.48 262.56 50.98 o 18 0 0 86.84 109.60 45.88 o 20 0 0 79.25 45.88 56.07 o 2 1 0 598.74 541.76 10.22 o 3 1 0 56609.55 58049.03 1384.87 o 4 1 0 1464.18 1444.99 25.58 o 5 1 0 596.20 607.29 12.76 o 6 1 0 354.26 283.07 10.20 o 7 1 0 3596.38 3483.39 51.23 o 8 1 0 81.26 96.86 10.20 o 9 1 0 188.22 188.65 12.75 o 10 1 0 263.06 260.04 15.30 o 11 1 0 1229.76 1283.43 40.82 o 12 1 0 72.31 58.62 15.29 o 13 1 0 0.76 20.39 15.29 o 14 1 0 9.66 0.00 15.29 o 15 1 0 151.20 158.04 20.39 o 16 1 0 766.66 872.10 58.65 o 17 1 0 200.06 180.98 33.14 o 18 1 0 0.19 2.55 28.04 o 19 1 0 12.77 58.62 33.13 o 20 1 0 395.72 474.17 101.97 o 1 2 0 54.05 53.54 2.55 o 2 2 0 60715.03 62061.84 1847.75 o 3 2 0 3734.90 3368.12 48.93 o 4 2 0 303.62 334.11 7.65 o 5 2 0 397.12 428.50 10.20 o 6 2 0 626.43 619.95 15.31 o 7 2 0 2797.08 2821.83 43.49 o 8 2 0 109.14 99.41 10.20 o 9 2 0 32.80 10.20 10.20 o 10 2 0 244.52 206.50 15.30 o 11 2 0 3747.54 3866.52 99.73 o 12 2 0 1686.53 1748.31 53.60 o 13 2 0 5716.94 6128.31 176.63 o 14 2 0 64.68 71.37 15.29 o 15 2 0 20.60 17.84 17.84 o 16 2 0 114.12 89.21 25.49 o 17 2 0 130.59 86.66 28.04 o 18 2 0 30.15 17.84 25.49 o 19 2 0 476.30 489.49 96.88 o 20 2 0 129.80 180.97 53.53 o 1 3 0 13308.50 12203.53 213.07 o 2 3 0 999.96 881.89 15.34 o 3 3 0 9441.13 8627.33 122.50 o 4 3 0 2624.11 2439.24 35.87 o 5 3 0 6048.88 5793.82 82.40 o 6 3 0 656.17 604.64 15.31 o 7 3 0 4254.80 4302.97 61.51 o 8 3 0 692.91 691.27 17.86 o 9 3 0 0.12 2.55 10.20 o 10 3 0 351.77 321.25 15.30 o 11 3 0 3226.18 3440.30 86.90 o 12 3 0 4890.62 5135.61 153.53 o 13 3 0 1340.88 1339.45 48.48 o 14 3 0 305.50 323.76 22.94 o 15 3 0 539.22 502.29 35.70 o 16 3 0 113.00 124.90 28.04 o 17 3 0 0.02 -28.04 28.04 o 18 3 0 62.04 79.01 33.13 o 19 3 0 47.24 17.84 30.59 o 20 3 0 44.93 66.27 40.78 o 0 4 0 97861.36 112429.38 5039.16 o 1 4 0 96.09 132.57 5.10 o 2 4 0 1582.20 1588.79 25.58 o 3 4 0 1458.51 1398.44 23.01 o 4 4 0 31.59 43.33 5.10 o 5 4 0 1057.46 1008.45 17.87 o 6 4 0 296.25 288.13 10.20 o 7 4 0 633.28 635.14 17.86 o 8 4 0 8807.08 9281.04 131.26 o 9 4 0 548.32 561.04 20.40 o 10 4 0 822.18 818.78 28.06 o 11 4 0 3206.68 3207.49 79.23 o 12 4 0 280.56 252.38 17.85 o 13 4 0 2781.49 3016.32 97.05 o 14 4 0 17.75 -17.84 17.84 o 15 4 0 666.85 637.47 45.90 o 16 4 0 259.30 193.74 38.24 o 17 4 0 61.39 147.83 40.78 o 18 4 0 37.12 71.37 38.23 o 19 4 0 17.34 25.49 40.78 o 20 4 0 42.26 68.82 45.88 o 1 5 0 3398.29 3232.47 53.92 o 2 5 0 2088.53 1906.83 30.71 o 3 5 0 29.01 53.53 5.10 o 4 5 0 866.18 883.12 17.87 o 5 5 0 20.14 2.55 5.10 o 6 5 0 1463.11 1440.26 25.54 o 7 5 0 1993.58 2082.13 35.77 o 8 5 0 2506.91 2601.62 43.45 o 9 5 0 228.37 203.95 12.75 o 10 5 0 31.85 40.78 10.20 o 11 5 0 633.14 650.28 25.50 o 12 5 0 356.52 390.07 22.95 o 13 5 0 2114.12 2180.01 94.45 o 14 5 0 220.82 180.99 22.94 o 15 5 0 692.00 652.78 51.00 o 16 5 0 609.56 639.98 73.94 o 17 5 0 372.99 443.58 84.13 o 18 5 0 4.54 17.84 35.68 o 19 5 0 15.03 7.65 38.23 o 0 6 0 30811.58 30028.14 1022.56 o 1 6 0 4636.39 4418.27 74.54 o 2 6 0 4937.73 4866.01 77.12 o 3 6 0 5424.27 5504.44 79.70 o 4 6 0 187.24 152.97 7.65 o 5 6 0 492.19 517.74 12.75 o 6 6 0 34.49 22.94 7.65 o 7 6 0 272.21 318.69 12.75 o 8 6 0 3943.07 4099.62 94.69 o 9 6 0 4.25 5.10 10.20 o 10 6 0 117.08 150.39 15.29 o 11 6 0 671.34 701.29 30.60 o 12 6 0 158.09 127.45 15.29 o 13 6 0 36.57 25.49 15.29 o 14 6 0 510.23 474.23 30.60 o 15 6 0 941.02 948.71 68.86 o 16 6 0 30.63 40.78 28.04 o 17 6 0 14.89 28.04 30.59 o 18 6 0 603.35 668.00 114.73 o 19 6 0 287.85 367.08 94.32 o 1 7 0 12085.24 12156.12 231.12 o 2 7 0 3.40 12.74 5.10 o 3 7 0 3943.93 4475.25 64.08 o 4 7 0 1503.55 1297.37 22.98 o 5 7 0 12552.70 12337.58 160.46 o 6 7 0 682.64 691.25 15.30 o 7 7 0 1713.86 1772.04 30.64 o 8 7 0 0.95 -2.55 10.20 o 9 7 0 2259.95 2334.35 58.74 o 10 7 0 0.15 12.74 12.74 o 11 7 0 2512.24 2484.89 79.17 o 12 7 0 420.32 418.13 25.50 o 13 7 0 42.09 30.59 12.74 o 14 7 0 4.22 20.39 20.39 o 15 7 0 166.30 158.04 28.04 o 16 7 0 13.99 -2.55 28.04 o 17 7 0 121.94 56.08 35.69 o 18 7 0 95.41 89.21 43.33 o 19 7 0 46.34 101.95 45.88 o 0 8 0 17762.56 17935.88 472.68 o 1 8 0 13.26 30.59 5.10 o 2 8 0 1619.48 1864.65 33.21 o 3 8 0 737.09 775.56 15.31 o 4 8 0 3551.53 3655.35 51.20 o 5 8 0 122.10 130.00 10.20 o 6 8 0 1081.32 1125.30 20.41 o 7 8 0 550.39 489.63 15.30 o 8 8 0 1322.78 1334.64 33.17 o 9 8 0 115.57 132.55 12.75 o 10 8 0 867.83 869.74 33.16 o 11 8 0 303.14 305.92 20.39 o 12 8 0 28.42 40.78 15.29 o 13 8 0 0.67 10.20 17.84 o 14 8 0 203.63 160.59 25.49 o 15 8 0 128.83 79.02 25.49 o 16 8 0 11.49 -5.10 30.59 o 17 8 0 230.60 272.75 58.63 o 18 8 0 105.19 45.88 45.88 o 19 8 0 159.90 163.13 58.63 o 1 9 0 2110.10 2149.11 38.33 o 2 9 0 9.70 22.94 5.10 o 3 9 0 679.77 660.65 15.30 o 4 9 0 275.17 254.95 10.20 o 5 9 0 5498.99 5996.16 87.16 o 6 9 0 1447.67 1623.35 38.29 o 7 9 0 48.69 56.08 10.20 o 8 9 0 381.08 374.79 15.30 o 9 9 0 4469.38 4853.01 122.80 o 10 9 0 761.82 744.68 30.60 o 11 9 0 48.57 40.78 12.74 o 12 9 0 156.00 122.35 17.84 o 13 9 0 758.34 706.36 45.90 o 14 9 0 54.34 50.98 20.39 o 15 9 0 131.45 109.61 33.14 o 16 9 0 47.92 73.92 35.68 o 17 9 0 36.42 56.07 38.23 o 18 9 0 75.40 101.95 45.88 o 0 10 0 2335.70 2057.16 63.89 o 1 10 0 1609.08 1478.39 28.09 o 2 10 0 3194.97 3102.51 63.94 o 3 10 0 1434.01 1595.41 28.08 o 4 10 0 764.76 897.87 25.51 o 5 10 0 652.52 645.25 20.40 o 6 10 0 285.11 321.23 12.75 o 7 10 0 640.95 622.25 20.40 o 8 10 0 147.66 158.04 12.75 o 9 10 0 1592.93 1538.85 45.94 o 10 10 0 414.98 379.88 20.40 o 11 10 0 0.06 -2.55 12.74 o 12 10 0 40.80 38.23 15.29 o 13 10 0 16.80 -17.84 17.84 o 14 10 0 0.68 -22.94 22.94 o 15 10 0 0.02 -12.74 22.94 o 16 10 0 62.24 73.92 35.68 o 17 10 0 73.53 107.05 40.78 o 18 10 0 30.03 35.68 43.33 o 1 11 0 821.71 880.06 30.61 o 2 11 0 2814.15 2671.01 79.24 o 3 11 0 9.85 7.65 5.10 o 4 11 0 3798.22 3849.76 86.97 o 5 11 0 358.97 336.55 12.75 o 6 11 0 2.15 2.55 7.65 o 7 11 0 10.93 10.20 7.65 o 8 11 0 290.43 237.09 12.75 o 9 11 0 453.50 464.03 20.40 o 10 11 0 7.89 15.29 12.74 o 11 11 0 0.03 7.65 15.29 o 12 11 0 0.90 25.49 17.84 o 13 11 0 5.21 -7.65 17.84 o 14 11 0 21.64 17.84 25.49 o 15 11 0 0.54 -20.39 28.04 o 16 11 0 116.50 63.72 33.14 o 17 11 0 2.29 -20.39 35.68 o 0 12 0 386.45 336.56 28.05 o 1 12 0 764.20 655.50 28.06 o 2 12 0 318.25 331.44 15.30 o 3 12 0 177.39 209.03 15.29 o 4 12 0 1001.25 1015.31 30.61 o 5 12 0 350.46 323.79 12.75 o 6 12 0 10.07 5.10 7.65 o 7 12 0 133.13 130.00 12.75 o 8 12 0 1165.61 1142.86 38.27 o 9 12 0 183.94 170.79 15.29 o 10 12 0 36.81 58.62 12.74 o 11 12 0 2.25 -12.74 12.74 o 12 12 0 1400.49 1500.02 99.49 o 13 12 0 25.57 61.17 20.39 o 14 12 0 42.34 61.17 25.49 o 15 12 0 54.62 91.76 33.13 o 16 12 0 192.53 198.82 61.18 o 17 12 0 33.35 63.72 48.43 o 1 13 0 207.65 183.54 17.84 o 2 13 0 17.83 33.13 10.20 o 3 13 0 489.58 441.12 22.95 o 4 13 0 208.38 178.44 10.20 o 5 13 0 62.37 66.27 10.20 o 6 13 0 114.73 104.51 10.20 o 7 13 0 63.63 79.02 12.74 o 8 13 0 21.18 10.20 10.20 o 9 13 0 642.41 558.43 28.05 o 10 13 0 0.03 17.84 12.74 o 11 13 0 24.75 43.33 15.29 o 12 13 0 6.77 10.20 17.84 o 13 13 0 521.24 555.80 66.29 o 14 13 0 11.70 28.04 30.59 o 15 13 0 194.17 206.47 56.08 o 16 13 0 180.45 101.96 35.69 o 0 14 0 384.31 374.78 40.79 o 1 14 0 533.89 446.23 28.05 o 2 14 0 714.35 650.31 43.35 o 3 14 0 63.55 56.08 10.20 o 4 14 0 139.35 175.88 25.49 o 5 14 0 7.54 10.20 7.65 o 6 14 0 173.75 135.10 12.75 o 7 14 0 2.83 -10.20 10.20 o 8 14 0 2600.13 2775.52 109.80 o 9 14 0 538.71 512.49 33.15 o 10 14 0 552.39 555.83 35.70 o 11 14 0 0.50 0.00 15.29 o 12 14 0 29.59 56.07 20.39 o 13 14 0 0.01 12.74 22.94 o 14 14 0 93.96 12.74 33.14 o 15 14 0 10.69 12.74 35.68 o 16 14 0 41.66 84.11 43.33 o 1 15 0 12.57 -5.10 17.84 o 2 15 0 1574.05 1681.65 71.45 o 3 15 0 530.29 563.50 30.60 o 4 15 0 83.85 127.45 17.84 o 5 15 0 858.66 918.12 48.46 o 6 15 0 11.15 0.00 12.74 o 7 15 0 204.99 188.63 17.84 o 8 15 0 286.75 277.87 22.94 o 9 15 0 1221.97 1349.36 76.52 o 10 15 0 0.74 -5.10 12.74 o 11 15 0 5.07 0.00 17.84 o 12 15 0 226.31 226.87 35.69 o 13 15 0 189.18 196.28 45.88 o 14 15 0 30.20 68.82 38.23 o 15 15 0 358.85 461.41 122.36 o 0 16 0 166.45 186.08 35.69 o 1 16 0 852.75 754.90 48.46 o 2 16 0 210.05 196.28 25.49 o 3 16 0 29.94 30.59 20.39 o 4 16 0 193.20 196.28 17.84 o 5 16 0 983.05 1022.74 58.66 o 6 16 0 0.43 15.29 15.29 o 7 16 0 100.67 142.74 17.84 o 8 16 0 357.97 412.99 30.59 o 9 16 0 153.51 168.23 22.94 o 10 16 0 4.51 17.84 15.29 o 11 16 0 23.12 17.84 20.39 o 12 16 0 1121.68 1124.72 132.62 o 13 16 0 3.50 2.55 30.59 o 14 16 0 69.66 86.66 45.88 o 1 17 0 91.28 35.68 20.39 o 2 17 0 246.73 216.68 28.04 o 3 17 0 0.01 -7.65 22.94 o 4 17 0 168.19 180.98 17.84 o 5 17 0 0.27 15.29 12.74 o 6 17 0 284.11 300.81 30.59 o 7 17 0 79.61 71.37 20.39 o 8 17 0 12.24 12.74 12.74 o 9 17 0 2.88 2.55 15.29 o 10 17 0 12.77 22.94 17.84 o 11 17 0 0.04 -20.39 20.39 o 12 17 0 6.62 66.27 30.59 o 13 17 0 449.08 522.62 130.02 o 14 17 0 7.84 30.59 43.33 o 0 18 0 3.30 -20.39 33.13 o 1 18 0 4652.96 5343.15 352.80 o 2 18 0 168.71 114.71 25.49 o 3 18 0 12.65 12.74 20.39 o 4 18 0 874.41 810.96 79.06 o 5 18 0 389.98 387.51 45.89 o 6 18 0 78.59 66.27 17.84 o 7 18 0 42.53 38.23 17.84 o 8 18 0 165.50 178.43 30.59 o 9 18 0 66.08 50.98 25.49 o 10 18 0 352.64 392.59 63.73 o 11 18 0 32.45 28.04 28.04 o 12 18 0 36.78 28.04 35.68 o 13 18 0 202.61 209.02 71.37 o 1 19 0 163.26 183.53 33.14 o 2 19 0 103.34 104.51 28.04 o 3 19 0 113.02 114.70 30.59 o 4 19 0 55.49 68.82 30.59 o 5 19 0 291.20 351.79 38.24 o 6 19 0 382.55 415.54 58.63 o 7 19 0 175.90 188.63 30.59 o 8 19 0 251.05 219.22 45.88 o 9 19 0 39.20 28.04 28.04 o 10 19 0 60.11 73.92 38.23 o 11 19 0 33.90 15.29 40.78 o 12 19 0 283.68 336.49 94.32 o 0 20 0 65.37 30.59 40.78 o 1 20 0 1706.50 2127.84 275.55 o 2 20 0 174.14 117.25 33.14 o 3 20 0 0.55 17.84 25.49 o 4 20 0 15.73 -7.65 33.13 o 5 20 0 23.38 -20.39 30.59 o 6 20 0 21.80 33.13 17.84 o 7 20 0 95.69 124.90 35.68 o 8 20 0 5.80 15.29 30.59 o 9 20 0 48.05 81.56 33.13 o 10 20 0 63.30 140.19 50.98 o 1 21 0 2.99 58.62 35.68 o 2 21 0 3.52 -28.04 33.13 o 3 21 0 60.47 58.62 43.33 o 4 21 0 608.48 650.16 114.73 o 5 21 0 154.22 130.00 45.88 o 6 21 0 205.83 260.00 68.82 o 7 21 0 138.24 50.98 56.08 o 8 21 0 31.36 38.23 35.68 o 9 21 0 56.54 101.95 48.43 o 0 22 0 125.52 132.54 71.37 o 1 22 0 305.80 290.61 73.93 o 2 22 0 16.19 76.46 45.88 o 3 22 0 28.73 40.78 43.33 o 4 22 0 223.57 224.32 63.73 o 5 22 0 51.32 61.17 43.33 o 6 22 0 79.18 68.82 61.17 o 7 22 0 114.96 84.11 58.62 o 1 23 0 1.74 30.59 81.56 o 2 23 0 346.00 275.32 117.26 o 3 23 0 13.46 28.04 84.11 o 4 23 0 158.09 86.66 94.31 o -19 0 1 168.02 201.37 76.47 o -17 0 1 104.03 91.76 43.33 o -15 0 1 14.43 20.39 22.94 o -13 0 1 12.97 20.39 17.84 o -11 0 1 1.21 5.10 12.74 o -9 0 1 5642.97 5510.58 117.96 o -7 0 1 16306.92 16115.98 330.86 o -5 0 1 24528.59 24597.94 543.60 o -3 0 1 3278.38 2978.38 72.08 o 3 0 1 41447.25 41287.09 1007.28 o 5 0 1 3700.66 3613.71 84.70 o 7 0 1 3892.28 3928.05 84.56 o 9 0 1 363.99 382.46 22.95 o 11 0 1 13.86 58.62 17.84 o 13 0 1 1003.69 1178.43 61.22 o 15 0 1 287.46 308.46 38.24 o 17 0 1 514.39 530.31 81.59 o 19 0 1 142.60 130.00 56.08 o -20 1 1 16.00 -45.88 45.88 o -19 1 1 125.93 183.52 56.08 o -18 1 1 102.92 124.90 35.68 o -17 1 1 334.69 277.87 38.24 o -16 1 1 350.24 331.41 30.59 o -15 1 1 57.08 43.33 17.84 o -14 1 1 548.05 530.35 30.60 o -13 1 1 492.74 451.30 25.50 o -12 1 1 5325.20 5685.59 163.83 o -11 1 1 297.37 288.09 17.85 o -10 1 1 352.83 336.55 17.85 o -9 1 1 34.32 79.01 10.20 o -8 1 1 3210.45 3282.65 48.61 o -7 1 1 3202.60 3169.11 48.64 o -6 1 1 382.13 379.99 12.75 o -5 1 1 2315.77 2216.76 35.84 o -4 1 1 6656.55 6595.28 106.08 o -3 1 1 304.82 331.64 7.65 o -2 1 1 11548.84 10148.53 178.61 o 1 1 1 1170.69 0.00 25664.87 o 2 1 1 2467.58 2213.75 36.04 o 3 1 1 11846.55 11061.78 176.63 o 4 1 1 6918.59 6710.28 103.55 o 5 1 1 261.42 290.70 10.20 o 6 1 1 45.29 53.53 7.65 o 7 1 1 1660.25 1688.53 30.65 o 8 1 1 61.12 66.27 10.20 o 9 1 1 1976.59 1974.37 35.76 o 10 1 1 18.81 40.78 10.20 o 11 1 1 1504.19 1472.60 43.39 o 12 1 1 31.32 38.23 12.74 o 13 1 1 3686.91 3936.16 117.57 o 14 1 1 203.79 175.89 20.39 o 15 1 1 93.26 71.37 20.39 o 16 1 1 393.20 384.96 38.24 o 17 1 1 9.05 -15.29 30.59 o 18 1 1 56.25 84.11 33.13 o 19 1 1 39.01 38.23 30.59 o 20 1 1 48.38 53.53 35.68 o -20 2 1 450.23 537.92 117.27 o -19 2 1 42.97 45.88 40.78 o -18 2 1 1.79 33.13 33.13 o -17 2 1 0.94 30.59 30.59 o -16 2 1 3.30 15.29 17.84 o -15 2 1 4.24 0.00 17.84 o -14 2 1 1063.99 1058.54 48.46 o -13 2 1 0.18 -10.20 15.29 o -12 2 1 883.80 964.12 35.71 o -11 2 1 161.23 163.14 15.29 o -10 2 1 60.59 76.47 12.74 o -9 2 1 139.34 155.50 12.75 o -8 2 1 12.47 40.78 7.65 o -7 2 1 9048.17 9130.98 134.13 o -6 2 1 398.39 402.95 12.75 o -5 2 1 1378.07 1254.53 23.00 o -4 2 1 688.43 704.50 12.76 o -3 2 1 3540.17 3205.79 46.31 o -2 2 1 13283.56 11776.39 181.05 o -1 2 1 262.87 229.65 5.10 o 0 2 1 2222.38 1865.33 41.22 o 1 2 1 71.27 56.09 2.55 o 2 2 1 6.11 7.65 2.55 o 3 2 1 893.23 901.86 15.33 o 4 2 1 16646.42 15774.70 224.30 o 5 2 1 14.14 28.04 7.65 o 6 2 1 2128.05 2107.00 33.24 o 7 2 1 428.25 446.29 12.75 o 8 2 1 639.41 533.09 15.30 o 9 2 1 445.16 433.49 15.30 o 10 2 1 5372.18 5175.10 122.97 o 11 2 1 987.87 1007.64 30.61 o 12 2 1 72.42 66.27 15.29 o 13 2 1 1280.08 1293.48 45.92 o 14 2 1 39.91 7.65 15.29 o 15 2 1 33.08 28.04 17.84 o 16 2 1 5.27 0.00 22.94 o 17 2 1 65.91 61.17 25.49 o 18 2 1 203.05 206.47 43.33 o 19 2 1 3.02 -30.59 30.59 o 20 2 1 109.86 81.56 43.33 o -20 3 1 87.08 96.86 53.53 o -19 3 1 40.68 0.00 38.23 o -18 3 1 86.39 86.66 40.78 o -17 3 1 11.38 -22.94 28.04 o -16 3 1 877.45 780.35 73.95 o -15 3 1 726.97 637.50 43.35 o -14 3 1 8.48 48.43 17.84 o -13 3 1 1125.42 1119.85 43.37 o -12 3 1 5399.97 5595.88 156.15 o -11 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